Measure

what is measurable
and make measurable
that which is not.
Galileo Galilei (1564-1642)

Service Manual
MCP 100
MCP 150
Modular Circular Polarimeter
 Service Manual
MCP 100
MCP 150
Modular Circular Polarimeter
Anton Paar GmbH assumes no liability for technical or printing errors or omissions in
this document.

Nor is any liability assumed for damages resulting from information contained in the
document.

Anton Paar GmbH reserves the right to content changes. This also extends to
changes to delivery volumes or any features of delivered parts.

All rights reserved (including translation). This document, or any part of it, may not
be reproduced, changed, copied, or distributed by means of electronic systems in
any form (print, photocopy, microfilm or any other process) without prior written
permission by Anton Paar GmbH.

Trademarks, registered trademarks, trade names, etc. may be used in this manual
without being marked as such. They are the property of their respective owner.

Published by Anton Paar OptoTec GmbH, Germany

Printed by Anton Paar GmbH, Graz, Austria
Copyright © 2015 Anton Paar GmbH, Graz, Austria

Address of the instrument producer:

Anton Paar OptoTec GmbH
Albert-Einstein-Str. 5
30926 Seelze-Letter / Germany – Europe
Tel: +49 (0) 511 400950
Fax: +49 (0) 511 4009534
E-Mail: info.optotec@anton-paar.com
Web: www.anton-paar.com

Date: November 22, 2018

Document number D02IB012EN-D

Contents

1 About the Service Manual .............................................................................................................. 5

2 Safety Instructions .......................................................................................................................... 7
3 The Measuring Principle ................................................................................................................ 9
3.1 Definition of Optical Rotation (Biot’s Formula) ........................................................................ 9
3.2 Optical Rotation Measurement ............................................................................................... 9
4 MCP 100 / MCP 150 - An Overview ............................................................................................. 11
4.1 Features and Benefits ........................................................................................................... 11
5 Functional Components ............................................................................................................... 12
5.1 View of the Front .................................................................................................................. 12
5.2 Interfaces on the Left Side .................................................................................................... 12
5.3 Rear View ............................................................................................................................. 13
5.4 View into the Cell Compartment ........................................................................................... 13
6 Opening the Instrument ............................................................................................................... 14
6.1 Required Tools ...................................................................................................................... 14
7 Overview ........................................................................................................................................ 17
8 Connecting Ports .......................................................................................................................... 19
9 Checking the Air Inlet / Air Outlet ................................................................................................ 21
10 Checking for Contamination Inside the Instrument .................................................................. 22
11 Checking / Replacing the Fan ...................................................................................................... 23
12 Checking / Replacing the Device Feet ........................................................................................ 25
13 Checking / Replacing the Drying Cartridge ................................................................................ 26
14 Cleaning ......................................................................................................................................... 27
14.1 Cleaning and Drying Sample Cells ....................................................................................... 27
14.2 Cleaning the Sample Cell Compartment .............................................................................. 28
14.3 Cleaning the Protection Glasses .......................................................................................... 29
14.4 Cleaning the Instrument Housing and Touchscreen ............................................................. 30
15 Checking and Adjusting the Instrument ..................................................................................... 31
15.1 Definitions ............................................................................................................................. 31
15.2 Checks .................................................................................................................................. 31
15.2.1 Check Settings ...................................................................................................... 31
15.2.2 Performing a Check ............................................................................................... 32
15.2.3 Viewing, Printing or Exporting Check Results ....................................................... 33
15.3 Adjustments .......................................................................................................................... 33
15.3.1 Performing an Adjustment ..................................................................................... 33
15.3.2 Viewing, Printing or Exporting Adjustment Results ................................................ 34
15.3.3 Restoring the Factory Adjustment ......................................................................... 34
16 Replacing the Buffer Battery ....................................................................................................... 35
16.1 Required Parts and Tools ..................................................................................................... 35
17 Replacing the Display / Foil Cable .............................................................................................. 36
17.1 Required Parts and Tools ..................................................................................................... 36
18 Replacing the Toradex Board ...................................................................................................... 38
19 Replacing the IO-Board / ePC Board ........................................................................................... 40
20 Temperature validation of sample cells and quartz control plates .......................................... 43
20.1 Temperature validation needle .............................................................................................. 43
20.2 Validation process sample cells ............................................................................................ 44
20.3 Validation process quartz control plates ............................................................................... 45
21 Service Utilities ............................................................................................................................. 47
21.1 Updating the Firmware ......................................................................................................... 47
21.2 System Information ............................................................................................................... 47
21.3 Backup of Instrument Settings .............................................................................................. 48
21.4 Restore the Instrument Settings ........................................................................................... 48
21.5 Live Raw Data ...................................................................................................................... 49
22 Spare Part list ............................................................................................................................... 51
1 About the Service Manual

1 About the Service Manual

This service manual informs you about repair work and maintenance procedures
on the instrument. Make sure that the service manual is easily accessible to all
personnel involved with servicing the instrument. Pay special attention to the
safety instructions and warnings in the manual and on the instrument.

Conventions for safety messages

The following conventions for safety messages are used in this instruction
manual:

DANGER
Danger indicates a hazardous situation which, if not avoided, will result in
death or serious injury.

WARNING
Warning indicates a hazardous situation which, if not avoided, could result in
death or serious injury.

CAUTION
Caution indicates a hazardous situation which, if not avoided, could result in
minor or moderate injury.

Hot surface
This symbol calls attention to the fact that the respective surface can get
very hot. Do not touch this surface without adequate protective measures.

High voltage
This symbol calls attention to the risk of high voltage. Do not proceed until
the indicated conditions for averting this threat are fully understood and met.

NOTICE Notice indicates a situation which, if not avoided, could result in damage to
property.

TIP Tip gives extra information about the situation at hand.

Typographical conventions

5 D02IB012EN-D
 The following typographical conventions are used in this instruction manual:

Convention Description
<key> The names of keys and buttons are
written inside angle brackets.
"Menu Level 1 > Menu Level 2" Menu paths are written in bold, inside
straight quotation marks. The menu
levels are connected using a closing
angle bracket.

D02IB012EN-D 6
2 Safety Instructions

2 Safety Instructions
• Read the instruction manual before using the instrument.

• Follow all hints and instructions contained in this instruction manual to

ensure the correct use and safe functioning of the instrument.

• Make sure that this instruction manual is easily accessible to all personnel
involved with the instrument.

Liability

• This manual does not claim to address all safety issues associated with the
use of the instrument. It is your responsibility to establish health and safety
practices and determine the applicability of regulatory limitations.

• Anton Paar only warrants the proper functioning of its instruments if no

modifications have been made to the mechanics, electronics, firmware and
instrument software.

• Only use MCP 100 / MCP 150 for the purpose described in this instruction
manual. Anton Paar is not liable for damages caused by incorrect use of
MCP 100 / MCP 150.

• The results delivered by MCP 100 / MCP 150 not only depend on the correct
functioning of the instrument, but also on various other factors. We therefore
recommend you have the results checked (e.g. plausibility tested) by skilled
personnel before consequential actions are taken based on the results.

Installation and Use

• The installation and operation of the instrument has to be done according to

the instructions in the instrument manual, otherwise the accuracy and the
safety is endangered.

• MCP 100 / MCP 150 is not an explosion-proof instrument and therefore

must not be operated in areas with risk of explosion.

• The installation procedure should only be carried out by authorized

personnel who is familiar with the installation instructions.

• Do not use any accessories or wearing parts other than those supplied or
approved by Anton Paar

• Make sure all operators are trained to use the instrument safely and correctly
before starting any applicable operations

• In case of damage or malfunction, do not continue operating MCP 100 /

MCP 150. Do not operate the instrument under conditions which could result
in damage to goods and/or injuries and loss of life.

Moving the instrument

• Before you move or lift the MCP 100 / MCP 150 make sure that all hoses and
the sample cell are empty.

7 D02IB012EN-D
 Handling of chemicals

• Observe all safety regulations regarding the handling of the samples,

cleaning, rinsing and waste liquids (e.g. use and disposal of lead-clarified
samples).

• Check the chemical resistance of all materials which come into contact with
the sample or cleaning liquid before starting the measurement.

• Make sure that different liquids (samples and cleaning liquids) that come into
contact with each other are chemically compatible. They should not react
exothermically or produce any solid particles that might stick to the inner wall
of the sample cell.

• Prior to starting a measurement or cleaning procedure, make sure that all

parts that come into contact with fluids, especially the measuring cell, hoses
and waste container, are properly connected and in good condition.

Precautions for highly inflammable samples and cleaning agents

• Only store the minimum required amount of sample, cleaning agents and
other inflammable materials near the MCP 100 / MCP 150.

• Do not spill sample/cleaning agents or leave their containers uncovered.

Immediately remove spilled sample/cleaning agents.

• Make sure that the setup location is sufficiently ventilated. Ensure the
sufficient supervision of MCP 100 / MCP 150 during operation.

Service and repairs

• Service and repair procedures may only be carried out by authorized

personnel or by Anton Paar GmbH.

• Prior to sending the instrument to your representative or Anton Paar GmbH

for repair or service, make sure that all liquids and solvents are completely
drained out of the instrument.
An instrument must not be returned if contaminated by radioactive materials,
infectious agents or other harmful substances that cause health hazards.

Returns

• To initiate a service request please visit the "Service/Support" section of the

Anton Paar homepage (www.anton-paar.com). For repairs send the cleaned
MCP unit together with the RMA to your Anton Paar representative. Only
return the instrument with the completed "Safety Declaration", also available
in the "Service/Support" section of the Anton Paar homepage.

Disposal

• Concerning the disposal of MCP 100 / MCP 150, observe the legal
requirements in your country.

D02IB012EN-D 8
3 The Measuring Principle

3 The Measuring Principle

3.1 Definition of Optical Rotation (Biot’s Formula)

The optical rotation α is the basic measurement of a polarimeter. Optical rotation

is defined in angular degrees. It can be calculated with the specific rotation α Tλ
multiplied by optical pathway l [dm] multiplied by the concentration c [g/100 ml]:

α Tλ ⋅ l ⋅ c
α = --------------------------
-
100
T
The specific rotation α  λ depends on the temperature T and the wavelength λ.
Standard temperature is typically 20 °C. Literature sometimes states 25 °C. For
historical reasons, only a few wavelengths are in use. The standard wavelength
is 589 nm, which is the yellow emission wavelength of the element sodium.

3.2 Optical Rotation Measurement

Fig. 3 - 1 Principle of the optical rotation measurement

To measure optical rotation, a Light Emitting Diode (LED) produces a beam of

ordinary light. This light first passes through a polarizer (polarization filter) in
order to obtain a defined orientation of the plane of polarization. The polarized
light then passes through the sample cell. If the sample is optically active, the
plane of polarization becomes rotated.

The light with the rotated plane of polarization passes through an analyzer, which
is a second polarization filter. Now the MCP 100 / MCP 150 rotates the first
polarizer, until the photo receiver measures a transmission minimum. If the
sample is optically inactive, polarizer and analyzer are now oriented
perpendicular to another.

If the sample is optically active, the MCP 100 / MCP 150 rotates the polarizer until
the plane of polarization behind the sample cell is perpendicular to the
polarization plane of the analyzer again. The resulting degree of rotation is a

9 D02IB012EN-D
 direct measure of the optical rotation of the sample. The correct wavelength for
the measurement is precisely selected by an interference filter positioned in the
beam in front of the photo receiver.

D02IB012EN-D 10
4 MCP 100 / MCP 150 - An Overview

4 MCP 100 / MCP 150 - An Overview

The MCP 100 / MCP 150 is a Modular Circular Polarimeter and concentration
meter that was developed to combine high accuracy with ease of operation and
a robust design.

4.1 Features and Benefits

Convenient

• With its compact design, MCP 100 / MCP 150 requires next to no space and
fits into any laboratory.

• The instrument is easy to operate – simply switch it on, measure your

sample and get correct results within seconds.

• An internal data memory ensures that no data is lost. The measured data
can be automatically exported to a connected printer or to a server, via
Ethernet.

Reliable

• MCP 100 / MCP 150 complies with all national and international
pharmacopoeias, so you can be sure of a solution that is fit for the future.

• Defined user hierarchies ensure that only authorized personnel operates the
instrument.

• The Audit Trail function clearly and irrevocably documents every instrument
interaction as required by e.g. 21 CFR Part 11, GLP or GMP.

• Automatic Peltier temperature control entirely eliminates the risk of

measurement errors due to inaccurate sample temperature.

Safe

• MCP 100 / MCP 150 can be automatically adjusted and calibrated with
Toolmaster quartz control plates. The instrument guides you safely and
easily through the required process.

• With MCP 100 / MCP 150 there are no data input errors. MCP 100 / MCP
150 provides seamless documentation and full traceability.

• The MCP 100 / MCP 150 is equipped with a Peltier module providing a fast
and precise automatic temperature control of the sample cell.

11 D02IB012EN-D
 5 Functional Components

5.1 View of the Front

Fig. 5 - 1 View of the front side of MCP 100 / MCP 150

1 ... LCD color touchscreen

2 ... Sample cell compartment

5.2 Interfaces on the Left Side

Fig. 5 - 2 Three USB ports on the left side

1 ... USB ports for memory, mouse, keyboard, bar code reader or printer.

D02IB012EN-D 12
5 Functional Components

5.3 Rear View

2 3 4 5 6

7 8 9

Fig. 5 - 3 MCP 100 / MCP 150 rear view

1 ... Drying Cartridge

2 ... CAN out interface
3 ... CAN in interface
4 ... USB service interface
5 ... Power inlet
6 ... Power switch
7 ... Ventilation grill
8 ... Ethernet interface
9 ... RS-232 interface

5.4 View into the Cell Compartment

1 2 3

Fig. 5 - 4 MCP 100 / MCP 150 cell compartment

1 ... Temperature-controlled sample cell holder

2 ... Wireless interface for Toolmaster sample cells
3 ... Cell compartment window

13 D02IB012EN-D
 6 Opening the Instrument

6.1 Required Tools

• Torx screwdriver TX10

WARNING
Before opening the housing disconnect the instrument from the mains.

1. Switch off the instrument and unplug it from the mains.

WARNING
After switching the instrument off, it takes approx. 30 seconds for the
instrument to be free of voltage.

2. Untighten the screws marked in red with the Torx screwdriver TX 10.

Fig. 6 - 1 Remove the screws marked in red

D02IB012EN-D 14
6 Opening the Instrument

Fig. 6 - 2 There is one screw at the back panel

3. Remove the USB protection plugs before moving the housing

Fig. 6 - 3 Position of protection plugs

4. Lift the MCP 100 / MCP 150 housing.

Fig. 6 - 4 MCP with open housing. Take care of the foil cable.

15 D02IB012EN-D
 5. Disconnect the display foil cable and the security rope.

Fig. 6 - 5 Display foil cable and security rope

Fig. 6 - 6 MCP with removed housing

D02IB012EN-D 16
7 Overview

7 Overview

4 1

5 2

8
3

Fig. 7 - 1 Front View

10 17 16

11 12 13 14 15

Fig. 7 - 2 Rear View

17 D02IB012EN-D
 1 Instrument Housing
2 Measuring Chamber
3 Sensor Module
4 Display with Touch
5 Cable PWR E-PC Board
6 Foil Cable 10pol
7 IO-Board MCP 100
8 E-PC Board MCP 100
9 Cable Fan MCP 100
10 Drying Cartridge
11 Ethernet Interface
12 CAN in
13 RS232 Interface
14 Power in DC 24V 120W
15 Power Switch
16 USB Interface
17 CAN out

D02IB012EN-D 18
8 Connecting Ports

8 Connecting Ports

7 6 5 4 3 2 1

IO-BOARD

10 8 9 8

11

12

Reset ARM

Reset PC

13
uC Reset

E-PC BOARD
14

15

SENSOR MODULE

16 17

19 D02IB012EN-D
 No.
1 CABLE PWR E-PC BOARD
2 ePC Board Connection between IO-Board
MCP100 and E-PC Board
MCP100
3 CAN OUT CAN Bus out
4 CAN IN CAN Bus in
5 USB SERVICE Serial USB type B
6 POWER IN DC 24V 120W Power input
7 Power switch
8 Mainboard foil connector SENSOR
MODULE E-PC BOARD
9 Ethernet interface
10 RS232 RS232 Interface
11 DEBUG USB Debug port
12 Battery
13 TORADEX BOARD
14 USB INTERFACE MOUSE / FLASH DRIVES
15 DISP Connector for DISPLAY WITH
TOUCH
16 DEBUG Debug port
17 FAN_PWM Fan connector

D02IB012EN-D 20
9 Checking the Air Inlet / Air Outlet

9 Checking the Air Inlet / Air Outlet

To check the air inlet take a look below the device ground plate. There you find
slots for air admittance. These slots need to be open and free of dust.

The air outlet is on the back of the instrument. This is where the fan is located.
Check the fan by listening to the noise it makes. A noisy fan can be a sign that it
is about to malfunction. Also check that the fan is not blocked and free of dust.

Fig. 9 - 1 Air inlet below the ground-plate

Fig. 9 - 2 Air outlet on the backplate

21 D02IB012EN-D
 10 Checking for Contamination Inside the
Instrument

CAUTION
Unplug the instrument from the mains before opening.

After opening the device housing (Chapter 6) you can check for contamination
inside the instrument. Dust on semiconductors may cause excessive heat and
lead to instrument malfunction. Use compressed air to remove the dust. The
compressed air has to be free of oil. Check for loose materials like screws which
can damage the electronics.

D02IB012EN-D 22
11 Checking / Replacing the Fan

11 Checking / Replacing the Fan

The fan is important for the temperature control of the measuring chamber.
Without cooling the peltier elements inside cannot reach the required
temperature. Check whether there is dust on the fan or if it is damaged. A
damaged fan can be detected by the sound it makes. A noisy fan should be
replaced before it malfunctions. Remove dust or other objects which may block
the fan.

Fig. 11 - 1 Remove the 3 screws of the fan housing (red) and the 4 fan screws
(green).

Fig. 11 - 2 Then remove the 2 screws on the sensor board

23 D02IB012EN-D
 Fig. 11 - 3 Remove the fan housing and unplug the cable of the fan. Take care
not to damage the grey thermal foil, it insulates the sensor board
against the ground plate.

CAUTION
Do not damage the thermal foil!
A damaged thermal foil has to be replaced.

Fig. 11 - 4 Take care not to bend the cable after reassembling.

D02IB012EN-D 24
12 Checking / Replacing the Device Feet

12 Checking / Replacing the Device Feet

The device feet can wear out after some years. It is important that the instrument
stands very stable, without wobbling.

Fig. 12 - 1 Unscrew the device foot

25 D02IB012EN-D
 13 Checking / Replacing the Drying
Cartridge
A drying cartridge in the rear of the instrument protects the optical system from
moisture. The cartridge is equipped with a humidity indicator behind the window
in the center. This allows you to check the status of the cartridge without the need
to remove it.

When the desiccant in the cartridge saturates with moisture, the indicator
changes its color from blue to pale pink. If the blue color disappears, the cartridge
should be replaced. To evaluate the status of the cartridge, you can compare it
with the replacement delivered with your instrument:

dry replace saturated

Fig. 13 - 2 Humidity indicator of drying cartridge

If it is necessary to replace the cartridge, use the transparent, protective sleeve

as a screwdriver. Unscrew the used cartridge counterclockwise. Remove
residues around the threaded hole of the housing. Then check the gasket of the
fresh cartridge and screw it into the hole.

NOTICE • Don’t exchange the cartridge unless it needs exchanging.

• Leaving the optical system open for a prolonged time might result in
damage to the instrument.

D02IB012EN-D 26
14 Cleaning

14 Cleaning
To assure a constant and high accuracy of your measurements, establish a
regular and effective cleaning routine and store the instrument under the
recommended conditions.

WARNING
Before applying any cleaning liquid onto your instrument or before filling any
sample or cleaning liquid into your sample cell make sure that:
• All safety instructions concerning the use of chemicals and the use of
inflammable chemicals are met (see Chapter 2).
• The fire point of the liquid in use is higher than 97 °C (25 °C above the
maximum temperature of the Peltier module which is 72 °C).
• No source of ignition exists close to the instrument.
• Sufficient ventilation is guaranteed.
• All wetted parts are resistant.

14.1 Cleaning and Drying Sample Cells

Cleaning frequency

Clean and dry the measuring cell at least after each working day or working shift.
Cleaning more frequently can become necessary when:

• you perform adjustments

• you measure a sample that is not miscible with the previous sample (e.g.,
water after a petrochemical sample)

• you want to measure using a minimum sample amount

• you measure a sample that could chemically react with the previous sample

• the cell windows are dirty

Cleaning liquids

For cleaning and drying, employ two cleaning liquids:

• Cleaning liquid 1 dissolves and removes sample residues in the measuring

cell. It has to be a good solvent for all sample components.

• Cleaning liquid 2 removes cleaning liquid 1 and is easily evaporated by a

stream of dry air in order to accelerate drying of the cell. Cleaning liquid 2
has to be a good solvent for cleaning liquid 1.

Recommended for aqueous samples: Water (cleaning liquid 1) and ethanol

(cleaning liquid 2).

Recommended for chemical samples: Ethanol (cleaning liquid 1) and acetone

(cleaning liquid 2).

27 D02IB012EN-D
 If you are not sure if a cleaning liquid is suitable for your sample, perform a
preliminary test in a test tube to see if any phase separation, precipitate or
opalescence can be observed.

To perform a cleaning and drying procedure

1. Rinse the sample cell with cleaning liquid 1 (minimum 50 mL). If your sample
is viscous or contains particles, use a cleaning brush.

2. Empty the sample cell.

3. Rinse the sample cell with cleaning liquid 2 (minimum 20 mL).

4. Empty the sample cell.

5. Dry the sample cell with compressed air.

6. Check if the windows are clean.

To clean the sample cell windows

1. Remove the screw caps.

2. Remove the rubber washers.

3. Remove the windows (and exchange them if necessary).

4. Clean the windows by using cleaning liquid 1 first and then cleaning liquid 2.

5. Clean the sample cell using a brush.

6. Reassemble the sample cell.

TIP The rubber washers have no gasket function! The windows are in direct
contact to the sample cell in order to guarantee the proper optical length, e.g.
100.0 mm. The rubber washer’s only function is to equally distribute the
contact pressure from the screw cap to the window.

14.2 Cleaning the Sample Cell Compartment

Cleaning frequency

How often the device should be cleaned depends on the usage and the
environment. To ensure that the inserted sample cell or quartz control plate is in
close contact with the Peltier element, take care that the surface is clean and free
of any residues.

D02IB012EN-D 28
14 Cleaning

Cleaning liquids

Cleaning of the sample cell compartment is only necessary when:

• Sample is spilled

• The sample hose slips off the hose connector of a filled cell

• The liquid is crystallizing in the sample cell compartment

To clean the sample cell compartment use cleaning liquid 1 and cleaning liquid 2
(see Chapter 14.1).

TIP • Don’t contaminate the protection glasses.

• Cover the instrument if it is not in use for a prolonged time to avoid
accumulation of dust in the sample cell compartment.

14.3 Cleaning the Protection Glasses

Contaminants on the protection glasses like dust, skin oils or sample residues
scatter the light and can therefore impair the measuring result. The path of the
measuring beam has to be kept clean. Dust and loose contaminants should be
blown off first, before you use other cleaning methods. Air from a can with inert
dusting gas or a bulb blower are recommended.

NOTICE To protect the glasses:

• never clean windows if not contaminated
• never use dry or abrasive wipes
• never use abrasive cleaning agents
• never use strong mechanical action

If blowing of the surfaces of the glasses is not sufficient, it has to be cleaned with
a wipe. Acceptable wipes are cotton swabs or lens cleaning tissues. Never use a
dry wipe. Moisten it moderately with a solvent, preferably isopropyl alcohol or
acetone of optical grade. Clean from the center of the glass to the outside in a
spiral movement.

Fig. 14 - 3 Clean the protection glasses from the center in a spiral

movement outwards.

29 D02IB012EN-D
 14.4 Cleaning the Instrument Housing and
Touchscreen

To clean the instrument housing or the touch screen, use a soft tissue that can be
moistened with an ethanol water mix or warm water, if necessary with some mild
cleaning agent added (pH < 10).

NOTICE To protect the surface of your Instrument never use:

• highly nonpolar solvents (e.g. toluene, hexane, solvent naphta)
• strong acids or bases (e.g. nitric acid, sulfuric acid, hydrochloric acid,
caustic soda)
• strong mechanical action (steel brush).

D02IB012EN-D 30
15 Checking and Adjusting the Instrument

15 Checking and Adjusting the

Instrument

15.1 Definitions

Checking

Checking the correct state of operation of an instrument by measuring a sample

of exactly known measurement properties and comparing the result with the
expected values.

Adjusting

Enabling correct measurements in the future by measuring a reference standard

of exactly known measurement properties and adjusting the instrument’s
constants in a way that the correct results are found by the instrument.

Calibrating

Calibrations are checking procedures which are carried out using certified
standards. By comparing the measured result with the standard reference value,
you can evaluate the quality of your measurements.

15.2 Checks

15.2.1 Check Settings

Two different types of checks can be performed:

• A quartz check requires a Toolmaster quartz plate, which functions as a

certified optical rotation reference standard.

• A custom check requires a substance with known measurement properties

as a reference standard. The custom check is performed with a Toolmaster
sample cell.

To edit the quartz check settings

1. Tap the check symbol to open the checks window.

2. Tap the gears symbol to open the check settings list.

3. Enter the following settings:

• Temperature: 20 °C/68 °F, 25 °C/77 °F or without temperature control.

• Reminder and the number of days to remind after.
• Define if the check is GxP relevant.

4. Tap <OK>.

31 D02IB012EN-D
 To edit the custom check settings

1. Tap the check symbol to open the checks window.

2. Tap the gears symbol to open the check settings list.

3. Enter the following settings:

• Quantity of check: Optical rotation, specific rotation or concentration.

• Temperature: 20 °C/68 °F or 25 °C/77 °F or without temperature control.
• Reference value of the standard.
• Check tolerance, defined by entering an allowed deviation.
• Reminder and the number of days to remind after.
TIP It is recommended to perform checks always with temperature control.

4. Tap <OK>.

15.2.2 Performing a Check

1. Tap the check symbol to open the checks window.

2. Tap the symbol to execute the check.

3. Follow the instructions on the screen.

4. After the check is finished, tap <Export> if you want to print or export the
check results.

Fig. 15 - 1 Successful quartz check

TIP If a check failed, it is recommended to perform a quartz adjustment.

D02IB012EN-D 32
15 Checking and Adjusting the Instrument

15.2.3 Viewing, Printing or Exporting Check Results

1. Tap <Menu> and select "Data Memory > Check Data" to open the check
data list.

2. Tap on an item to see more detailed information.

3. Tap <Edit>.

4. Tap <Print> or <Export All> to perform a printout on paper or to a PDF file or

to export the data as an MS Excel or text file.

5. Follow the instructions on the screen.

15.3 Adjustments

A high-precision polarimeter like the MCP 100 / MCP 150 requires an adequately
precise calibration. Checking the accuracy is performed with a Toolmaster quartz
control plate and may result in a reading that differs substantially from the
temperature-corrected optical rotation value of the quartz standard. In such case
calibration is required.

15.3.1 Performing an Adjustment

1. Remove the quartz plate or the sample cell from the instrument.

2. Tap <Menu> and select "Adjustments > Quartz Adjustment".

3. Choose the temperature to adjust at: <20 °C/68 °F> or <25 °C/77 °F>. Or
choose <-- °C/°F> for an adjustment without temperature control. Tap
<Next>.

TIP It is recommended to always perform adjustments with temperature control.

4. Insert a quartz after the instrument has set its zero point.

5. When the instrument finished measuring the quartz you can check the
results and the recommendation on the screen. Select one of the options,
<Reject> or <Accept>.

33 D02IB012EN-D
 Fig. 15 - 2 Successful quartz adjustment

15.3.2 Viewing, Printing or Exporting Adjustment Results

1. Tap <Menu> and select "Data Memory > Adjustment Data" to open the
adjustment data list.

2. Tap on an item to see more detailed information.

3. Tap <Edit>.

4. Tap <Print> or <Export All> to perform a printout on paper or to a PDF file or

to export the data as an MS Excel or text file.

5. Follow the instructions on the screen.

15.3.3 Restoring the Factory Adjustment

You can restore the factory adjustment for the optical rotation measurement.

1. Tap <Menu> and select "Adjustments > Reset to Factory Adjustment".

2. Tap <Yes>.

D02IB012EN-D 34
16 Replacing the Buffer Battery

16 Replacing the Buffer Battery

16.1 Required Parts and Tools

• Flat-blade screwdriver

• Buffer battery, item number 61693

Fig. 16 - 1 Push the buffer battery carefully forward using a flat-blade

screwdriver.

WARNING
Disconnect the instrument from mains before working on it.

35 D02IB012EN-D
 17 Replacing the Display / Foil Cable

17.1 Required Parts and Tools

• Torx screwdriver TX10

• MCP 100 Display with touch, item number 134987

WARNING
Disconnect the instrument from mains before working on it.

Open the instrument (Chapter 6). Release the connector bar to get the foil cable
out and unscrew the security rope (Fig. 6 - 5)

Fig. 17 - 2 Untighten the four screws marked red.

Fig. 17 - 3 Check the display sealing for damages.

D02IB012EN-D 36
17 Replacing the Display / Foil Cable

Fig. 17 - 4 Open the foil connector of the display by turning the black bar
towards the cable.

Fig. 17 - 5 Remove the foil cable

Assemble the Display vice versa.

37 D02IB012EN-D
 18 Replacing the Toradex Board

WARNING
Disconnect the instrument from mains before working on it.

Open the instrument (Chapter 6).

Fig. 18 - 1 Push the 2 levers of the socket to the outside to remove the Toradex
board.

Fig. 18 - 2 Before inserting the Toradex board align the position of the gap with
the socket.

D02IB012EN-D 38
18 Replacing the Toradex Board

Fig. 18 - 3 Insert the board deep into the socket and then push it down.

39 D02IB012EN-D
 19 Replacing the IO-Board / ePC Board

WARNING
Disconnect the instrument from mains before working on it.

Open the instrument (Chapter 6).

Fig. 19 - 1 Disconnect the foil cable and the power cable

Fig. 19 - 2 Remove 7 screws at the ground plate ...

D02IB012EN-D 40
19 Replacing the IO-Board / ePC Board

Fig. 19 - 3 ... and the 2 spacer bolts of the RS232 port at the rear panel.

Fig. 19 - 4 Move the ePC Board together with the IO-Board carefully to the front
of the instrument.

Fig. 19 - 5 Remove the 2 screws on the IO-Board and lift the board up. Take
care about the connector between IO-Board and ePC Board (green).

41 D02IB012EN-D
 Fig. 19 - 6 IO-Board and ePC Board separated, the green marks are showing
the connection between the 2 boards.

Assemble the boards vice versa. Use the holes of the IO-Board and the spacer
bolts of the ePC Board to center the connection between the boards.

D02IB012EN-D 42
20 Temperature validation of sample cells and quartz control plates

20 Temperature validation of sample cells

and quartz control plates
For the validation of the temperature measurement of a Toolmaster sample cell,
the following accessories are required.

20.1 Temperature validation needle

Item Description Cat. No.

Temperature For 50mm sample cell 108253
validation needle
For 100mm sample cell 108252

MKT 50 Millikelvin thermometer 26878

Temperature Temperature sensor, 0- 74557

sensor 100°C, accuracy 1mK

43 D02IB012EN-D
 20.2 Validation process sample cells

For the temperature validation of sample cells, the temperature validation needle
corresponding to the path length of the sample cell must be used.

After unscrewing one screw cap of the sample cell, the needle must be screwed
in the same way into the cell. Then a MKT / CKT temperature sensor needs to be
stuck into the needle as deep as possible. Due to the design / size of the needle
the MKT / CKT sensor is measuring the temperature nearly in the same position
as the built in temperature sensor of the sample cell.

Now the sample cell must be filled with water and must be placed into the
automatic Peltier temperature control. Select the temperature inside the
polarimeter software and correlate the displayed ° C value with the measured
temperature of the MKT / CKT.

If the temperature measurement is within the specifications, the validation

passed. In case that the validation measurement failed, please contact the Anton
Paar OptoTec service for further information.

MKT / CKT sensor

inside val. needle
Validation Cable
needle MKT

Fig. 20 - 1 Sample cell with validation needle and MKT / CKT sensor

D02IB012EN-D 44
20 Temperature validation of sample cells and quartz control plates

20.3 Validation process quartz control plates

Item Description Cat. No.

Allen Key 2mm Allen key 26878

MKT 50 Millikelvin thermometer 26878

Temperature Temperature sensor, 0- 74557

sensor 100°C, accuracy 1mK

At one end of the quartz control plate is a 2mm Allen screw located. Remove this
screw and the protection pipe of the MKT / CKT sensor. Use a small amount of
thermal grease at the tip of the sensor, place the sensor into the quartz control
plate and push it inside until the end Fig. 20 - 2

Due to the design / size of the needle the MKT / CKT sensor is measuring the
temperature nearly in the same position as the built in temperature sensor of the
quartz control plate.

Now the quartz control plate must be placed into the automatic Peltier
temperature control. Select the temperature inside the polarimeter software and
correlate the displayed °C value with the measured temperature of the MKT /
CKT.

If the temperature measurement is within the specifications, the validation

passed. In case that the validation measurement failed, please contact the Anton
Paar OptoTec service for further information.

45 D02IB012EN-D
 MKT / CKT sensor Cable MKT

Fig. 20 - 2 Quartz control plate with MKT /CKT temperature sensor

Hole for MKT / CKT

temperature sensor

Fig. 20 - 3 Location of 2mm Allen screw

D02IB012EN-D 46
21 Service Utilities

21 Service Utilities
In this chapter, you can find information about service software features as
performing a firmware upgrade, getting details about the system and viewing the
live raw data as well as information about how to check the status of the drying
cartridge.

21.1 Updating the Firmware

To update the instrument software, you need administrator rights.

To update the instrument software

1. Load the latest software (file name extension ".aup") onto your USB memory
device.

2. Insert the memory device into a USB port on the left side of your instrument.

3. Tap <Menu> and select "Service > Update > System Update".

4. Select the "storage location" (USB memory device) and the "file name" of the
new firmware (file name extension ".aup").

5. Tap <OK>.

6. Follow the instructions on the screen.

21.2 System Information

In this menu, you find information about the configuration of the hardware and the
firmware. The instrument type, serial number and firmware versions are shown in
a table.

In this menu, you can also save an instrument log file to a USB memory device.
This file contains the last operating steps and may help during trouble shooting.

To view system information

1. Tap <Menu> and select "Service > System Information" to open the
configuration overview table.

2. Use the vertical scrollbar to scroll through the table.

To save the instrument log file

1. Tap <Menu> and select "Service > System Information" to open the
configuration overview table.

2. Insert a USB memory device into a USB interface and tap <Save Logfile>.

47 D02IB012EN-D
 3. Accept the generated file name or enter a new one and tap <OK>.

The instrument log file is now saved to the main directory of the USB
memory device.

21.3 Backup of Instrument Settings

You can use this utility for:

• Saving the current instrument status in case that settings are changed
accidentally.

• Saving the current settings for safety reasons before performing a firmware
upgrade.

• Copying the instrument settings to one or more other MCP 100 / MCP 150.

A backup file contains the following instrument settings and instrument

information:

• Global settings in the control panel (regional settings, keyboard settings,

network settings)

• Users

• System settings (instrument settings, audit trail settings, printout settings)

• Adjustment data

To make a backup of the instrument settings

1. Tap <Menu> and select "Service > Backup" to open the "Backup" dialog.

2. Select the "storage location" (USB memory device) and enter a "file name"
or accept the automatic file name.

3. Tap <OK>.

The backup file is stored into the root directory of your USB flash drive.

21.4 Restore the Instrument Settings

NOTICE When restoring the instrument settings, make sure that the backup file
corresponds with the instrument type.

1. Tap <Menu> and select "Service > Restore" to open the "Restore" dialog.

2. Select the "storage location" (USB memory device) and the "file name". The
backup file must be stored in the root directory of your USB flash drive.

3. Tap <OK > to restore the settings.

D02IB012EN-D 48
21.5 Live Raw Data

In this menu, you get a live view of sensor signals including raw data.

1. Tap <Menu> and select "Service > Live Raw Data".

D02IB012EN-D 50
 Spare Part List
MCP 100 / MCP 150

1 Spare Part list

Symbol Article Description Mat. No.
5.7" DISPLAY WITH TOUCH 134987

SEALING DISPLAY MCP 100/150 143927

FOIL CABLE DISPLAY 91502

E-PC BOARD MCP 100, PRECONFIGURED 146630

E-PC BOARD MCP 150, PRECONFIGURED 162092

IO-BOARD MCP 100/150 132614

CABLE PWR E-PC BOARD 134805

TORADEX BOARD, PRECONFIGURED MCP100 146634

TORADEX BOARD, PRECONFIGURED MCP150 162093

FAN MCP 100/150 143733

BUFFER BATTERY 61693

6 D02IE030EN-D
 1 Spare Part list

Symbol Article Description Mat. No.

INLINE SCREW FOR FAN M5X15 143941

SENSOR MODULE MCP100 143918

SENSOR MODULE MCP150 161927

THERMAL FOIL, FAN COVER 143944

FOIL CABLE 10POL 50MM 132812

DEVICE FOOT 96946

DRYING CARTRIDGE 96950

POWER SUPPLY 99780

D02IE030EN-D 7
 Appendix A: Technical Data
Table A.1: General Technical Data of MCP 100/150

Dimensions (L x W x H) 370 mm x 320 mm x 130 mm

Weight 8.6 kg (19 lbs) incl. power supply
Mains voltage From 100 VAC to 240 VAC, 50/60 Hz
Power consumption Typical 70 VA, max. 120 VA
Power inlet According to IEC/EN 60320-1/C14,
protection class I
AC adapter output DC 24 V, max. 5 A
Housing material
Front, top and side cover Styrene/Butadiene
Back, bottom Stainless Steel
Environmental conditions Indoor use only
(EN 61010)
Ambient temperature From 15 °C to 35 °C
(from 59 °F to 95 °F)
Air humidity From 20% to 80% relative humidity,
non-condensing
Pollution degree 2
Over-voltage category II
Light source LED, average lifetime of 100 000 h
Wavelength 589 nm
Touchscreen display 145 mm (5.7"), 640 x 480 pixel
Memory • 2500 measuring values
Interfaces • 3 x USB 2.0
• 1 x USB Type B for service
• 1 x Ethernet (100 Mbit)
• 1 x RS-232
• 1 x CAN out
• 1 x CAN in

NOTICE • Only connect devices to the interfaces that comply with PELV (protective
extra-low voltage) according to EN 61140 or with SELV (safety extra-low
voltage) according to EN 60950.
• Connect only Anton Paar equipment or equipment with a maximum power
consumption of 250 mA to the CAN interface.
• Only connect USB devices with a maximum current load of 250 mA to the
USB ports.

53 D02IB012EN-D
 Measuring Performance

Table A.2: Measuring Performance of MCP 100/150

MCP 100 MCP 150

Measuring range ±89.9 °OR (Optical Rotation)
Resolution 0.001 °OR
Accuracy ±0.01 °OR ±0.004 °OR
Repeatability ±0.01 °OR ±0.004 °OR
Sample cell volume From 200 μL to10 mL
Optical cell length From 2.5 mm to 100 mm
Peltier temperature 20 °C, 25 °C From 15 °C to 35 °C *
control and disabled and disabled
Temperature accuracy ±0.2 °C ±0.1 °C
Optical wavelength 589 nm
Transmission,
Up to 2.0 OD
optical density

* At standard laboratory conditions (ambient temperature of 23 °C)

Wetted Parts

The following parts are in contact with samples and cleaning liquids during normal
operation.

Table A.3: Wetted parts of sample cells

Sample cell parts Material

Sample cell Stainless steel or Ni-Alloy
Sample cell windows Borosilicate glass
Luer adpater Ethylene tetrafluoroethylene (ETFE)

The following parts of the instrument can come in contact with samples and
cleaning liquids if the sample/liquid is spilled or if the sample cell is leaking.

D02IB012EN-D 54
 Table A.4: Wetted parts of MCP 100/150
MCP 100/150 parts
Toolmaster base station
Gasket of Toolmaster base station
Sample cell holder
Sample cell holder windows
Window gaskets
Sample cell compartment mid-frame
Gasket between sample cell holder
and mid-frame
Sample cell compartment top-frame
Gasket between mid-frame and top-
frame
55
Material
Polychlorotrifluoroethene (PCTFE)
Perfluoroelastomer (FFKM)
Aluminum anodized
Borosilicate glass
Perfluoroelastomer (FFKM)
Polyoxymethylene black (POM)
Fluoroelastomer (FKM)
Aluminum anodized
Fluoroelastomer (FKM)
D02IB012EN-D