O Cial Methods of Analysis: 22nd Edition (2023) : Search in This Book

O icial Methods of Analysis of AOAC INTERNATIONAL (22)
Dr. George W Latimer, Jr. (ed.)
https://doi.org/10.1093/9780197610145.001.0001
Published: 2023 Online ISBN: 9780197610145 Print ISBN: 9780197610138
Search in this book
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FRONT MATTER
O cial Methods of Analysis: 22nd Edition (2023)

https://doi.org/10.1093/9780197610145.002.001 Pages xi–xvi
Published: January 2023
Collection: O icial Methods of Analysis of AOAC INTERNATIONAL
New in the 22nd Edition

® ®
SMPRs AOAC SMPR 2017.021 Quantitation of Wheat, Rye, and Barley Gluten in Oats
Revised March 2019 to provide better nal calculations (wet chemical analysis vs Dumas nitrogen content
method) used to determine gluten content for wheat, rye, and barley used for spiking samples
®
AOAC SMPR 2018.012 Quantitation of Peanut by ELISA-Based Methods
Revised March 2019 to correct “1 ppm peanut protein” to “2 ppm peanut protein” in Annex
®
NEW! AOAC SMPR 2019.001 Detection of Aspergillus in Cannabis and Cannabis Products
®
NEW! AOAC SMPR 2019.002 Identi cation and Quantitation of Selected Residual Solvents in Dried
Cannabis Materials
®
NEW! AOAC SMPR 2019.003 Quantitation of Cannabinoids in Plant Materials of Hemp (Low THC Varieties
Cannabis spp.)
®
NEW! AOAC SMPR 2019.004 Quantitation of Furan and Alkyl Furans in Selected Matrices
®
NEW! AOAC SMPR 2020.001 Determination of Heavy Metals in a Variety of Cannabis and Cannabis-Derived
Products
®
NEW! AOAC SMPR 2020.002 Detection of Salmonella species in Cannabis and Cannabis Products
®
NEW! AOAC SMPR 2020.003 Determination of 2’-Fucosyllactose (2’FL) in Infant and Adult/Pediatric
Nutritional Formula
®
NEW! AOAC SMPR 2020.004 Determination of Lacto-N-Neotetraose (LNnT) in Infant and Adult/Pediatric
Nutritional Formula
®
NEW! AOAC SMPR 2020.005 Determination of Bovine Lactoferrin in Infant and Adult/Pediatric Nutritional
Formula
®
NEW! AOAC SMPR 2020.006 Nontargeted Testing of Ingredients for Food Authenticity/Fraud Evaluation of
Honey
®
Extra Virgin Olive Oil
®
Pasteurized Whole Liquid Bovine Milk

®
NEW! AOAC SMPR 2020.009 Targeted Testing of Barley and Malt Extract, Beet Sugar Syrup, Corn and Cane
Sugar Syrup, C-4 Plant Sugar, and High-Fructose Corn Sugar for Adulteration of Floral and Acacia Honey
®
NEW! AOAC SMPR 2020.010 Targeted Testing of Other Vegetable Oils and Low-Quality Olive Oils as
Adulterants for Evaluation of Extra Virgin Olive Oil (EVOO)
®
NEW! AOAC SMPR 2020.011 Targeted Testing of Formaline/Formaldahyde, Starch, and Soy Protein as
Adulterants for Evaluation of Liquid Raw Bovine Milk
®
NEW! AOAC SMPR 2020.012 Detection of Shiga Toxin-Producing Escherichia coli in Cannabis and Cannabis
Products
®
NEW! AOAC SMPR 2020.013 Mycotoxin Screening Technique in Cannabis Plant Material and Cannabis
Derivatives
®
NEW! AOAC SMPR 2020.014 Characterization and Quantitation of Neutral Components from Glycerol
Esters of Wood Rosin (GEWR)
®
NEW! AOAC SMPR 2020.015 Characterization and Quantitation of Monoesters from Glycerol Esters of
Wood Rosin (GEWR)
®
NEW! AOAC SMPR 2020.016 Characterization and Quantitation of Component Fractions from Glycerol
®
p. xii NEW! AOAC SMPR 2020.017 Characterization and Quantitation of Residual Resin Acids from Glycerol
®
NEW! AOAC SMPR 2021.001 Determination of Chlorate and Perchlorate in Baby Foods, Infant/Adult
Formulas, and Their Ingredients
®
NEW! AOAC SMPR 2021.002 Determination of Vitamin C (L-Ascorbic Acid) in All Forms of Infant Formula,
Follow-Up Formula, Baby Foods, Adult/Pediatric Formula, Complementary Food Supplements, Nutritional
Supplements for Pregnant Women and Nursing Mothers, and Sports Nutrition Food
®
NEW! AOAC SMPR 2021.003 Determination of 3’-Sialyllactose (3’-SL) in Infant and Adult/Pediatric
Nutritional Formula
®
NEW! AOAC SMPR 2021.004 Determination of 3-Fucosyllactose (3-FL) in Infant and Adult/Pediatric
Nutritional Formula
®
NEW! AOAC SMPR 2021.005 Determination of 6’-Sialyllactose (6’-SL) in Infant and Adult/Pediatric
Nutritional Formula
®
NEW! AOAC SMPR 2021.006 Determination of Difucosyllactose (DFL) in Infant and Adult/Pediatric
Nutritional Formula
®
NEW! AOAC SMPR 2021.007 Determination of Lacto-N-Tetraose (LNT) in Infant and Adult/Pediatric
Nutritional Formula
®
NEW! AOAC SMPR 2021.008 Glyphosate, Its Metabolites, and Trimesium in Fruits and Vegetables, Cereals,
Food of Animal Origin, Pet food and Baby Food
®
NEW! AOAC SMPR 2021.009 Viable Yeast and Mold Count Enumeration in Cannabis and Cannabis Products
Chapter 4 NEW! 2018.07 (4.7.08) Fructan (Inulin, FOS, Levan, and Branched Fructan) in Animal Food

(Animal Feed, Pet Food, and Ingredients)
Chapter 9 2016.04 (9.2.43) Arsenic Speciation in Fruit Juice Final Action 2019
Chapter 17 2015.13 (17.2.12) Enumeration of Aerobic Bacteria in Food
D(11): Deleted “Average the counts between the replicate plates” for clarity
NEW! 2018.02 (17.2.13) Enumeration of Yeast and Mold in Select Foods
NEW! 2019.02 (17.2.14) Enumeration of Total Aerobic Count in Select Foods
NEW! 2018.05 (17.3.11) Enumeration of Enterobacteriaceae in Select Foods and Environmental Surfaces
Final Action 2021
NEW! 2018.13 (17.4.11) Enumeration of Escherichia coli and Coliform in a Broad Range of Foods and Select
Environmental Surfaces
Final Action 2021
NEW! 2019.03 (17.4.12) Escherichia coli O157:H7 in Select Foods
NEW! 2020.06 (17.4.13) Enterohemorrhagic E. coli in Select Foods
993.06 (17.5.04) Staphylococcal Enterotoxins in Selected Foods
Repealed 2019: Method uses 3M TECRA products that have been discontinued
989.14 (17.9.13) Salmonella in Foods
998.09 (17.9.24) Salmonella in Foods
2016.01 (17.9.41) Salmonella spp. in Select Foods and Environmental Surfaces
Final Action 2019
2017.09 (17.9.42) Con rmation and Identi cation of Salmonella species, Cronobacter species,
Campylobacter species, and Other Gram-Negative Organisms
Final Action 2020

Minor modi cation 2020
Included Revised First Action J. AOAC Int. reference
p. xiii 2018.01 (17.9.44) Cronobacter species in Select Foods and Environmental Surfaces
Final Action 2021
Included J. AOAC Int. reference
NEW! 2019.01 (17.9.45) Cronobacter species in Select Foods and Environmental Samples

NEW! 2020.02 (17.9.46) Salmonella species in a Broad Range of Foods and Select Environmental Samples
NEW! 2020.03 (17.9.47) Salmonella species in Select Foods
NEW! 2021.02 (17.9.48) Detection of Salmonella species in Broad Range of Foods and Selected
Environmental Surfaces
995.22 (17.10.06) Listeria in Foods
2002.09 (17.10.06A) Listeria in Foods
2016.07 (17.10.18) Listeria species in Select Foods and Environmental Surfaces
Final Action 2019
2016.08 (17.10.19) Listeria monocytogenes in a Variety of Foods and Select Environmental Surfaces
Final Action 2019
2017.10 (17.10.20) Con rmation and Identi cation of Listeria monocytogenes, Listeria species, and Other
Gram-Positive Organisms
Final Action 2020
Minor modi cation 2020
NEW! 2019.10 (17.10.21) Listeria species in a Variety of Foods and Select Environmental Samples
NEW! 2019.11 (17.10.22) Listeria monocytogenes in a Variety of Foods and Select Environmental Samples
Chapter 22 NEW! 2018.10 (22.1.12) Cannabinoids in Cannabis sativa Dried Flowers and Oils
NEW! 2018.11 (22.1.13) Quantitation of Cannabinoids in Cannabis Dried Plant Materials, Concentrates, and
Oils
Revised First Action 2020: Modi ed for extension to hemp and to include procedure for sample dry-weight
determination
Chapter 23 2013.07 (23.1.21) Determination and Identi cation of Nicarbazin in Chicken Tissues
Final Action 2021: Method applicability changed from “con rmation” to “identi cation” and
representative chromatogram was added, among other changes
NEW! 2020.04 (23.1.22) Screening of 154 Veterinary Drug Residues in Animal Source Foods
Chapter 29 2017.15 (29.1.30) Bisphenol A (BPA) in Commercially Packaged Ready-to-Consume

Carbonated and Noncarbonated Water and Nonalcoholic Beverages
NEW! 2019.07 (29.1.31) Free Bisphenol A (BPA) in Commercially Packaged, Ready-to-Consume,
Carbonated/Noncarbonated Water and Nonalcoholic Beverages
Chapter 30 NEW! 2019.04 (30.1.38) Ethanol in Kombucha Tea Products

NEW! 2019.08 (30.1.39) Ethanol Concentration in Kombucha Beverages
Chapter 31 NEW! 2020.05 (31.5.17) Flavanol and Procyanidin (by Degree of Polymerization 1–7) of Cocoa-
Based Products
Chapter 32 2012.01 (32.1.44) Gliadin as a Measure of Gluten in Food
Modi cation to include matrix extension
2015.05 (32.2.11) Partially Hydrolyzed Gluten in Fermented Cereal-Based Products
Final Action 2018: Revised applicability statement to include “and may not measure or detect all fermented
and/or hydrolyzed forms of gluten”
NEW! 2017.17 (32.2.13) Detection and Quantitation of Selected Food Allergens
NEW! 2018.15 (32.2.14) Gluten from Wheat, Rye, and Barley in Oats and Oat Products
Chapter 33 NEW! 2020.01 (33.2.69) Lactose in Low-Lactose and Lactose-Free Milk, Milk Products, and
Products Containing Dairy Ingredients
p. xiv NEW! 2020.08 (33.2.70) Lactose Concentration in Low-Lactose and Lactose-Free Milk, Milk Products, and
Products Containing Dairy Ingredients
Final Action 2021
NEW! 2020.09 (33.2.71) Lactose in Free or Low-Lactose Dairy Products
Chapter 35 2014.08 (35.1.46) Polycyclic Aromatic Hydrocarbons (PAHs) in Seafood
Final Action 2018
Chapter 44 NEW! 2018.16 (44.1.31) Sugar Pro le in Food, Dietary Supplements, Pet Food, and Animal
Feeds
Chapter 45 2017.16 (45.4.18) Total Dietary Fiber in Foods Final Action 2020
Chapter 50 2011.06 (50.1.29) Total Folate in Infant Formula and Adult Nutritionals
Final Action 2018
Codex Type II 2019
Included J. AOAC Int. Final Action reference

2011.14 (50.1.37) Minerals and Trace Elements in Milk and Milk Products, Infant Formula, and Adult
Nutritionals
Final Action 2018 (for infant formula and adult nutritionals only; matrix extension to infant formula)
2015.09 (50.2.08) trans and Total (cis+trans) Vitamin K1 in Infant, Pediatric, and Adult Nutritionals
Final Action 2018
Codex Type II, AOAC-ISO Method 2019
Included Final Action J. AOAC Int. reference

2015.14 (50.2.09) Simultaneous Determination of Total Vitamins B1, B2, B3, and B6 in Infant Formula and
Related Nutritionals
Final Action 2019
AOAC-ISO Method
Included Revised First Action J. AOAC Int. reference
2015.10 (50.6.05) Free and Total Choline and Carnitine in Infant Formula and Adult/Pediatric Nutritional
Formula
Final Action 2019
AOAC-ISO Method
2015.06 (50.10.01) Minerals and Trace Elements in Milk, Milk Products, Infant Formula, and Adult/Pediatric
Nutritional Formula
Codex Type II, AOAC-ISO/IDF Method 2019
2016.03 (50.11.03) Chloride in Milk, Milk Powder, Whey Powder, Infant Formula, and Adult Nutritionals
Codex Type II, AOAC-ISO/IDF Method
Included Final Action J. AOAC Int. reference
2016.14 (50.13.02) Fructans in Infant Formula and Adult Nutritionals
Final Action 2020
AOAC-ISO/IDF Method
2016.13 (50.14.01) Lutein, β-Carotene, and Lycopene in Infant Formula and Adult Nutritionals
Final Action 2019 (for β-carotene and lycopene only)
AOAC-ISO Method
2017.03 (50.15.01) Total Tryptophan in Infant Formula and Adult/Pediatric Nutritional Formula
Final Action 2019
NEW! 2018.06 (50.15.02) Total Amino Acids in Infant Formulas and Adult Nutritionals
NEW! 2019.09 (50.15.03) Total Proteinogenic Amino Acids and Taurine in Infant Formula and
Adult/Pediatric Formula
NEW! 2018.03 (50.16.01) 2- and 3-MCPD, 2- and 3-MCPD Esters, and Glycidyl Esters (GE) in Infant and
Adult/Pediatric Nutritional Formula
NEW! 2018.12 (50.16.02) 2-Monochloropropanediol (2-MCPD), 3-Monochloropropanediol (3-MCPD), and

Glycidol in Infant and Adult/Pediatric Nutritional Formula
p. xv NEW! 2021.01 (50.17.01) β-Galactooligosaccharides in Infant Formula and Adult Nutritionals
Chapter 51 NEW! 2018.14 (51.13.02) Quantitation of Aloe Vera Polysaccharides NEW! 2018.04 (51.21.01)

Select Nonvolatile Ginger Constituents in Dietary Ingredients and Finished Dosage Forms
NEW! 2019.05 (51.22.01) A-Type Proanthocyanidins in Cranberry‐Based Foods and Dietary Supplements
NEW! 2019.06 (51.22.02) Soluble Proanthocyanidins in Cranberry Foods and Dietary Supplements
Appendix P NEW! Guidance for Soil Collection, Characterization, and Application for Biothreat Agent Detection
Methods and Site Evaluations
Appendix Q NEW! Recommendations for Developing Molecular Assays for Microbial Pathogen Detection Using
Modern In Silico Approaches
Appendix R NEW! Guidelines for Verifying and Documenting the Relationships Between Microbial Cultures
If you have any questions of a technical nature or suggestions for editorial changes, please e-mail us at
p. xvi editoma@aoac.org.
Latest updates to OMA Online
May 2023
AOAC SMPR® 2022.001 Quantitation of Cannabinoids in Beverages
AOAC SMPR® 2022.002 Determination of Folate in Dietary Supplements
AOAC SMPR® 2022.003 Determination of Biological Spices and Botanicals and Relevant (Common)
Biological Adulterants
AOAC SMPR® 2022.004 Determination of Fatty Acids Which Are Esteri ed at SN-2 Position (Beta) of
Triacylglycerol Molecules in Infant and Adult/Pediatric Nutritional Formula
AOAC SMPR® 2022.005 A1- and A2-Type Beta-Casein in Infant Formulas and Adult Nutritionals
AOAC SMPR® 2022.006 Acrylamide Acrylamide in Potato Products, Baby Food, Bread, Other Cereal and
Bakery Products, Cocoa Products, Co ee, Tea, Herbs and Spices (Including Their Mixtures), Dry Pet Food,
and Nuts
Appendix L “AOAC Recommended Guidelines for Stakeholder Panel on Infant Formula and Adult
Nutritionals (SPIFAN) Single-Laboratory Validation”
June 2023
997.02 Yeast and Mold Counts in Foods and Dried Cannabis Flower (Revised First Action for Cannabis
Flower, THC >0.3%, Only)
2009.03 Salmonella in Foods and Environmental Surfaces (Revised 2021: Minor modi cation to Rotor-Gene
Q software)
2014.05 Enumeration of Yeast and Mold in Foods, Selected Surfaces, and Dried Cannabis Flower (Revised
First Action for Cannabis Flower, THC > 0.3%, and Selected Surfaces Only)
2015.13 Enumeration of Aerobic Bacteria in Food and on Selected Surfaces (Revised First Action for Selected
Surfaces Only)

2017.07 Ethanol in Food by Enzytec™ Liquid Ethanol (Final Action)
2018.06 Total Amino Acids in Infant Formula and Adult Nutritionals (Final Action)
2019.01 Cronobacter species in Select Foods and Environmental Samples (Final Action and Minor
Modi cation)
2019.03 E. coli O157:H7 in Select Foods (Final Action and Minor Modi cation)
2019.10 Listeria Species in a Variety of Foods and Select Environmental Samples (Final Action and Minor
Modi cation)
2019.11 Listeria monocytogenes in a Variety of Foods and Select Environmental Samples (Final Action and
Minor Modi cation)
2020.02 Salmonella Species in a Broad Range of Foods and Select Environmental Samples (Minor
Modi cation)
2020.05 Cocoa Flavanols and Procyanidins [by Degree of Polymerization (DP) 1–7] in Cocoa-Based Products
(Final Action)
2020.06 Enterohemorrhagic E. coli in Select Foods (Minor modi cation)
2020.07 Available Carbohydrates in Cereal and Cereal Products, Dairy Products, Vegetables, Fruit, and Food
Products and Animal Feeds (Final Action)
2020.08 Lactose Concentration in Low-Lactose and Lactose-Free Milk, Milk Products, and Products
Containing Dairy Ingredients (Final Action)
2020.09 Lactose in Lactose-Free or Low-Lactose Dairy Products (Final Action)
2021.03 Heavy Metals in a Variety of Cannabis and Cannabis-Derived Products (First Action)
2021.04 Measurement of Water Activity in the Presence of High Volatile Concentrations (First Action)
2021.05 Listeria monocytogenes in a Broad Range of Foods and Selected Environmental Surfaces (First
Action)
2021.06 Listeria species in a Broad Range of Foods and Selected Environmental Surfaces (First Action)
2021.07 Analysis of Bovine Lactoferrin in Infant Formula and Adult Nutritional Products (First Action)
2021.08 Cronobacter species in Infant Formulas, Infant Cereals, Ingredients, and Environmental Samples
(First Action)
2022.01 Insoluble, Soluble, and Total Dietary Fiber in Foods and Food Ingredients (First Action)
2022.02 Analysis of Six Human Milk Oligosaccharides (HMOs) in Infant Formula and Adult Nutritionals
(First Action)
NOVEMBER 2023
®
AOAC SMPR 2023.001 Pesticides in Cannabis-Containing Beverages
AOAC SMPR® 2023.002 Pyrrolizidine Alkaloids in Teas, Herbal Infusions, Dried Herbs, Seed Spices, Honey,
and Botanical Dietary Supplements and Ingredients

AOAC SMPR® 2023.003 Per- and Poly uoroalkyl Substances (PFAS) in Produce, Beverages, Dairy Products,
Eggs, Seafood, Meat Products, and Feed
2005.04 Escherichia coli O157:H7 in Selected Foods
2009.03 Salmonella in Foods and Environmental Surfaces
2018.16 Sugar Pro le in Food, Dietary Supplements, Pet Food, and Animal Feeds (Final Action 2023)
2022.03 Taurine in Infant Formulas and Adult Nutritionals (First Action)
2022.04 2′-Fucosyllactose (2′-FL), 3-Fucosyllactose (3-FL), 6′-Sialyllactose(6′-SL), 3′-Sialyllactose (3′-

SL), Lacto-N-Tetraose (LNT), and Lacto-N-neoTetraose (LNnT) in Infant Formula and Adult Nutritionals
(First Action)
Appendix G: Procedures and Guidelines for the Use of AOAC Voluntary Consensus Standards to Evaluate
Characteristics of a Method of Analysis
Appendix T: Standard Requirements for Nucleotide Sequences Used in Biothreat Agent Detection,
Identi cation, and Quanti cation: Veri ed Next-Generation Sequences (VNGS)
January 2024
AOAC SMPR® 2023.004 Selected Residual Solvents in Color Additives from Crop-Based Sources
AOAC SMPR® 2023.005 Heavy Metals in Cannabis-Containing Beverages
AOAC SMPR® 2023.006 Vanillin, Ethyl Vanillin, Methyl Vanillin, and Coumarin in Infant Formulas and
Their Ingredients
2017.01 Escherichia coli O157:H7 in Selected Foods

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O icial Methods of Analysis of AOAC INTERNATIONAL (22)

Dr. George W Latimer, Jr. (ed.)

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Downloaded from https://academic.oup.com/aoac-publications/book/45491/chapter/392327022 by guest on 22 March 2024