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Point of View

Air Entrainment
and Delaminations
How air entrainment contributes to distress of
concrete slabs subjected to a hard-trowel finish

BY DAVID R. LANKARD

R ecently, the construction industry has given


considerable attention to distress of concrete slab
surfaces—namely, blistering and delamination. Both of
Based on my experience, as well as that of other
petrographers,1 I suggest that most slab delaminations
involve air-entrained concrete. The apparent influence
these phenomena involve the separation of a thin layer of of air entrainment on delaminations in hard-trowel-
concrete from the slab surface. The separation plane is finished concrete slabs is the motivating issue for the
most often parallel to, and 3 to 10 mm (0.1 to 0.4 in.) present article. Observations made during petrographic
below, the slab surface, although the plane may be as examinations of air-entrained concrete support a
much as 30 mm (1.2 in.) below. hypothesis that the physical forces caused by troweling
In the analyses of slab delaminations to date, most can be responsible for creating delaminations. The forces
view air entrainment as one of many variables that can arise from the trowel acting on a material (concrete) of
affect the entrapment of bleed water. If the entrapment variable, and decreasing, (with depth in the slab) stiffness.
of bleed water is the principal source of delaminations In this scenario, the effect of entrained air voids on the
in hard-trowel-finished concrete slabs, however, it is stiffness gradient through the slab thickness helps
reasonable to expect that distress would occur with equal to explain the role of air entrainment in delaminations. In
frequency in nonair-entrained and air-entrained slabs. cases of delaminations in hard-trowel-finished, air-
In fact, it can be claimed that there should be more entrained concrete slabs, bleed water entrapment is
cases of delaminations that occur in nonair-entrained frequently not involved. These issues are explored in
concrete slabs because this type of concrete is used the remainder of this article, using examples of nonair-
more often in interior slab construction. As experience entrained and air-entrained concrete slabs that have
has shown, the opposite is true—that a greater percentage exhibited blistering and delamination distress.
of air-entrained concrete slabs delaminate.
PETROGRAPHIC EXAMINATIONS
This point of view article is presented for reader interest by the The opinions expressed here represent interpretations
editors. However, the opinions expressed are not necessarily those of observations made during petrographic examinations
of the American Concrete Institute. Reader comment is invited. of 30 cases of blistering and delamination in hard-
trowel-finished slabs; most of which used air-entrained

Concrete international / NOVEMBER 2004 21


CRUSTING, BLISTERING, elevations in the slab, and on the bleeding rate
AND DELAMINATION and bleeding capacity of the concrete. These
Current knowledge and understanding of variables include:5,9,10,13
crusting, blistering, and delamination can be ■ Ambient conditions (wind speed, temperature,
summarized as follows:1-13 relative humidity);
1. Crusting and blistering are not nearly as common ■ Radiant heat from sunlight;
as delamination. ■ Cold sub-base;
2. No distinction is usually made regarding the ■ Moisture loss or retention by the sub-base;
frequency of occurrence of crusting and ■ Slab thickness;
blistering as influenced by the presence or absence ■ Types of finishing tools;
of air entrainment. ■ Concrete water content;
3. Delamination problems most commonly occur with ■ Concrete air entrainment;
interior floor slabs, but also occur in parking ■ Cement content of the concrete; and
structure deck slabs and other types of slabs when ■ The use of supplementary cementing materials.
a hard trowel finish has been used. 7. Despite the fact that the majority of interior floor
4. A prevailing opinion is that conditions for slabs are constructed with nonair-entrained
delaminations to form are created when the slab concrete, delamination problems are most common in
surface is sealed by the initiation of the trowel air-entrained concrete slabs.3,4 Evidence supporting
finishing operation prior to the cessation of a major involvement of entrained air in the problem
bleeding. This leads to the entrapment of bleed is compelling enough that several consensus
water, creating a plane of weakness along which a documents published by ACI warn of the increased
separation subsequently occurs. risk of delaminations when air entrainment is used
5. It is thought that delaminations are most likely to for hard-trowel-finished slabs.6,7
form from bleed water entrapment when the top of 8. Although it is recognized that air entrainment can
the slab hardens or stiffens faster than the reduce the bleeding rate in concrete, and thus affect
underlying concrete—a condition referred to as bleed water entrapment, the disproportionate
“top-down stiffening.”13 influence of air entrainment on the delamination
6. Premature finishing is frequently cited as a cause of problem has not been clearly elucidated.
bleed water entrapment. It is also acknowledged 9. Either through omission, or by inference in the
that, what otherwise might simply be blamed on literature, lightweight aggregate concretes are
premature finishing, often involves contributions considered to be less vulnerable than normalweight
from other design, construction, environmental, and concretes to the delamination problem. This issue
material variables that influence top-down stiffening needs to be re-examined as field experience has
in a slab. This influence is exerted through the demonstrated that air entrainment also increases
effect that these variables have on the rate of the risk of delaminations in lightweight-aggregate
setting or stiffening of the concrete at different concretes that are hard-trowel finished.

concrete. Concrete samples provided for examination microscopic examination. This procedure is used to
are cores and sawed pieces taken from the slabs. ensure preservation of the features of the as-received
Samples were taken from areas of the slabs where samples during the various sample preparation
spalling of the delaminated concrete had occurred, procedures. The air content of many of the concretes
as well as areas where the slab-wearing surface was was measured using the ASTM C 457 procedure (Modified
still intact. Point Count Method).15
The guidelines of ASTM C 85614 were followed in The water-cementitious material ratios (w/cm) of the
sample preparation and examination. Examples discussed concretes were estimated based on observations of color,
here represent observations made using reflected light texture, hardness, appearance of fracture surfaces,
microscopy examinations on saw-cut/lapped surfaces, porosity, and relative abundance of unhydrated cement
delamination surfaces, and intentionally created fracture grains of the cement paste phase. Because there is no
surfaces. Lapped examination surfaces are sections taken standard procedure for this subjective estimate, an
perpendicular to the plane of the slab surface. In some assessment of concrete-to-concrete variability in w/cm is
cases, an epoxy layer was placed on the wearing difficult. Many of the features and characteristics of the
surface of the sample prior to preparing the sample for cement paste used to estimate the w/cm are influenced

22 NOVEMBER 2004 / Concrete international


by variables such as curing procedure, the duration of
the curing period, and cement hydration rate. More Epoxy
confidence can be placed in estimates of variability in
w/cm for a given concrete sample. DSL
In the projects reviewed for the present study, the
w/cm ranged from 0.35 to 0.55, with most in the range S
of 0.40 to 0.50. The total air content for the air-
entrained concretes ranged from 3.8 to 9.4%, with APC
most between 4.5 and 7.5%. The total cementitious
content of the concretes ranged from 500 to 700 lb/yd3
(300 to 415 kg/m3). About half of the concretes contained
fly ash.
In all of the photographs and photomicrographs 1 mm
shown in this article, the wearing surface is toward
the top of the page. These examples provide a clear Fig. 1: Section view (10x) perpendicular to the plane of the
picture of the effect of the hard-troweling operation wearing surface in a nonair-entrained concrete slab that
on the microstructure of the concretes; particularly blistered during troweling. The densified surface layer (DSL) is
2 mm (0.1 in.) thick. The blister separation (s) is 0.6 mm (0.02 in.)
in the concrete in the top 1 in. (25 mm) thickness of thick. Concrete underlying the blister separation has
the slab. microstructural features of the bulk, as-placed concrete (APC)

BLISTERING to the initiation or cessation of bleeding was the only


When a hard-trowel finish is applied to any concrete way delaminations formed, it is expected that the
slab, a thin layer of the wearing surface is compacted and delamination plane would always be located at, or very
densified. Energy going into the slab surface in the form near, this boundary. In the cases involving air-entrained
of frictional heat and pressure significantly reduces the concrete slabs examined here, the delamination typically
local w/cm and virtually eliminates any entrapped or does not occur at this boundary. In these slabs, the
entrained air present prior to troweling. delamination plane is often well below the DSL in
This compacted, densified surface layer (DSL) is concretes that have the same w/cm, but a lower air
easily identified in section views by its darker color, content and different microstructural features relative to
which is due to its lower w/cm relative to the underlying the APC. I offer an explanation of this phenomenon by
concrete. An example is Fig. 1, which shows a blister examining the effect that air entrainment has on the
separation in a nonair-entrained concrete slab (2.6% air). mechanical response of the concrete to troweling near
Here the DSL is 2 mm (0.1 in.) thick with a w/cm estimated the slab surface.
at less than 0.30. The DSL is principally a mortar that,
due to its low w/cm, has a lower permeability than the HARD-TROWELING
underlying, as-placed concrete (APC), which has a w/cm AIR-ENTRAINED CONCRETE
of 0.48. In Fig. 1, the DSL was formed prior to the When concrete is air entrained, there are further
cessation of bleeding and the slab surface blistered consequences of hard troweling beyond the creation of a
during troweling. The blistered separation (about 0.6 mm DSL. The “top-down” stiffening phenomenon, also
[0.02 in.] thick) is located at the boundary between referred to as differential stiffening,12,13 appears to be
the DSL and the APC. Separation resulted from the involved. For purposes of illustration, it is convenient
subsidence of the concrete immediately under the DSL to envision the DSL as a thin, hard, stiff steel plate
as bleeding was interrupted. At this site, the bleed overlying a more-plastic, less-stiff concrete, which is in
water that originally filled the separation cavity was the process of hardening. As troweling proceeds, the
reabsorbed by the underlying concrete without concrete under the plate is compressed and physically
significantly affecting its w/cm. There is a very thin distorted by the lateral shear forces acting on the plate
layer of laitance on the top surface of the APC following by the trowel. The greater the difference in stiffness
blistering, but the separation itself had already taken between the plate and the underlying concrete, the
place, and no further mixing of the bleed water with the greater the probability of movement and disruption in
concrete occurred. the underlying concrete that is directly in contact with
When crusting or blistering occurs in nonair-entrained the plate. The entrained air voids (in this scenario)
and air-entrained concrete slabs, the plane of separation cause a significant reduction in the stiffness and yield
typically is located at the boundary between the DSL stress of the cementitious phase of the concrete
and the underlying APC. If sealing of a slab surface prior compared to the same concrete without air entrainment.

Concrete international / NOVEMBER 2004 23


TABLE 1:
CHARACTERIZATION OF DISTINCTIVE CONCRETE LAYERS CREATED WHEN AIR-ENTRAINED CONCRETE RECEIVES A HARD-TROWEL FINISH
Layer Abbreviation used
identification Characteristics relative to the as-placed concrete for the layer
■ Forms the immediate wearing-surface layer;
■ Significantly higher cement paste content;
■ Virtual absence of entrapped and entrained air voids;
Densified
■ Significantly lower w/cm; DSL
surface layer
■ The typical thickness of this layer is 1 to 4 mm (0.1 to 0.2 in.), but can be
as thick as 8 mm (0.3 in.); and
■ Overlies the DT.
■ Comparable cement paste content;
■ Significantly reduced entrained-air-void content;
■ Similar w/cm;
■ Contains distinctive microstructural features including irregularly shaped
Distorted layer voids, tears within the cementitious phase, and cement paste-aggregate DT
bond disruptions;
■ The typical thickness of this layer is 1 to 10 mm (0.1 to 0.4 in.), but it can
be as thick as 22 mm (1 in.); and
■ Overlies the APC.
■ The term used to identify the concrete at and near the slab-wearing
surface that is compressed, manipulated, and distorted by the action of
Trowel-affected the trowel, representing the combined thickness of the DSL and the
TAZ
zone DT; and
■ The typical thickness is 2 to 14 mm (0.1 to 0.5 in.), but can be as thick as
30 mm (1.2 in.).
■ Has the cement paste content of the APC;
■ Has the total air-void content of the APC;
As-placed ■ Has the air-void size distribution of the APC;
APC
concrete ■ Air-void shape is spherical;
■ Has the w/cm of the APC; and
■ Forms the remaining thickness of the concrete slab under the TAZ.

This is the same effect that entrained air has on


increasing the slump in concrete. During troweling,
the concrete layer immediately under the plate is
subject to greater movement and manipulation of the
air-entrained paste.
As troweling proceeds, the “distorted” concrete
immediately under the plate experiences a reduction in
entrained air content, but no reduction in w/cm relative
to the APC. The presence of hard, stiff aggregate
particles in the initially air-entrained paste creates
more opportunities for physical disruptions to occur
within the cementitious phase and at cement paste-
aggregate boundaries.
In concretes examined from service, a number of
Fig. 2: Schematic diagram showing the different layers formed microstructural features are preserved in the near-
in and near the wearing surface of an air-entrained concrete surface hardened concrete that attest to the distortion
slab that has received a hard-trowel finish. A characterization
of the features and microstructure of these layers is given in and manipulation effects of troweling described
Table 1 previously. In addition to actual delaminations, these

24 NOVEMBER 2004 / Concrete international


features include: 1) relatively large, irregularly (3a)
shaped voids within the cementitious phase of the DSL
concrete; 2) short, discontinuous separations or tears
within the cementitious phase; 3) a partial disruption
of the bond between aggregate particles and the
DT
adjacent cementitious phase; and 4) voids adjacent to
aggregate particles.
The distinctive layers resulting from a hard-trowel APC
finish of an air-entrained concrete slab are illustrated
schematically in Fig. 2. They include: 1) the DSL, which in
the cases considered here, ranges from as thin as 1 mm
(0.04 in.) to as thick as 8 mm (0.3 in.) overlying; 2) the
“distorted” layer (DT) which ranges from 1 to 22 mm
(0.04 to 1 in.) thick and overlies; 3) concrete that retains
the same w/cm and air content of the APC.
Taken together, the combined thickness of the DSL
and the DT will be referred to as the trowel-affected
zone (TAZ), which can range in thickness from 2 to 30 mm
(0.1 to 1 in.).
Relative to the APC, the DSL shows: 1) a significantly
lower w/cm; 2) a significantly higher cement paste (3b)
content; and 3) virtually no entrapped or entrained
air voids.
Relative to the APC, the DT shows: 1) a similar w/cm; DT
2) a reduced entrained air void content; 3) a different
air-void size distribution; and 4) the presence of one or
more of the microstructural features described previously,
which are attributed to the manipulation of this layer
prior to its hardening.
As implied, the APC contains the w/cm, the entrained-
air-void content, and the air-void size distribution of the APC
concrete as placed.
Table 1 summarizes all of the features described here
and illustrated in Fig. 2. Figure 3 through 8 show examples
of the microstructural features present in the TAZ of Fig. 3: Delamination in an air-entrained, lightweight aggregate
trowel-finished, air-entrained concrete slabs. These concrete slab; (a) The densified surface layer (DSL) is 4 to 6 mm
(0.2 to 0.3 in.) thick in this core sample; (b) A delamination is
features can be present in slabs that show few or no present 13 to 19 mm (0.5 to 0.8 in.) below the wearing surface at
delaminations. When delaminations do occur, the the boundary between the distorted layer (DT) and the as-placed
delamination plane is typically at or near the boundary concrete (APC)
between the DT and the underlying APC. This boundary
represents an abrupt transition between concrete The DSL, which is 4 to 6 mm (0.2 to 0.3 in.) thick in this
having a low to very low entrained air void content, and case, can be seen in Fig. 3(a) as the dark wearing surface
concrete that has the elevated entrained air void layer. If this DSL had been formed prior to cessation of
content of the APC. By virtue of this difference in air bleeding, trapping the bleed water, it is expected that the
entrainment, this boundary also defines the separation delamination would occur 4 to 6 mm (0.2 to 0.3 in.) below
between cementitious phases that differ significantly in the wearing surface. In fact, the delamination is 13 to
yield stress. 19 mm (0.5 to 0.8 in.) below the wearing surface, at the
boundary between the DT, which is 8 to 14 mm (0.3 to 0.5 in.)
DELAMINATIONS thick, and the APC.
Figure 3(a) and 3(b) show two views of delamination When troweling began, the entrained air content was
in a lightweight aggregate concrete slab in which probably uniform throughout the slab. After troweling, as
delaminations were detected after the slab had been in indicated by the petrographic examination, the air
service for 20 months. The estimated w/cm of the content in the DSL is virtually zero, and the air content
concrete is 0.40 and the measured air content is 9.8%. in the DT is significantly reduced relative to the APC.

Concrete international / NOVEMBER 2004 25


DSL
LENTICULAR VOIDS
DT
LENTICULAR VOIDS

DT APC

1 mm

APC Fig. 5: Section view (10x) perpendicular to the plane of the


wearing surface in an air-entrained (6.5%), lightweight aggregate
concrete slab showing an incipient delamination (arrows) 14 mm
(0.5 in.) below the wearing surface. An irregularly shaped void
having a sinusoidal upper surface forms part of the delamination,
which is at the boundary between the distorted layer and the
as-placed concrete

IRREGULARLY SHAPED VOIDS


1 mm At the initiation of slab troweling, the entrained air
content is probably more or less uniform throughout
Fig. 4: Section view (10x) perpendicular to the plane of the the slab. Troweling virtually eliminates the entrained
wearing surface in an air-entrained (6.0%), normalweight air voids in the DSL and significantly reduces the
concrete slab in which delaminations were detected 9 months entrained-air-void content in the DT. It is reasonable
after the slab was placed in service. The densified surface layer
is 2 mm (0.1 in.) thick, the distorted layer (DT) is 5 mm (0.2 in.) to conclude that some of the entrained air voids in the
thick, and the thickness of the TAZ is 7 mm (0.3 in.). The DT are joined or coalesced during the physical
delamination plane (marked with arrows) is at the boundary manipulation of the concrete to form the irregularly
between the DT and the as-placed concrete. A lenticular void is
present in the cementitious phase 4.5 mm (0.2 in.) below the shaped voids observed here. When viewed in two
wearing surface dimensions on a lapped section, these voids typically
exceed 0.5 mm (0.02 in.) in size. Many of these voids
As shown in Fig. 3(b), the delamination occurs at the are elongated or lenticular in shape with the long axis
boundary between the DT and the APC. The delamination typically, but not always, oriented parallel to the
passes around fine and coarse aggregate particles. The plane of the slab surface. Frequently they show a
w/cm is the same on both sides of the delamination. sinusoidal upper surface suggesting that they represent
Figure 4 shows an example of an incipient delamination two or more air voids joined together. Figure 4 and 5
in an air-entrained, normalweight concrete. The w/cm show examples of this lenticular void type. In the
of the APC is estimated at 0.40, and the air content is normalweight concrete shown in Fig. 4, the void is a
6.0%. The concrete sample examined here is a 4-in.- little over 1 mm long and is contained within the
diameter (100 mm) core. Delamination distress was first cementitious phase about 2 mm (0.1 in.) above the
observed in this slab 9 months after the concrete was delamination plane.
placed. In the core shown in Fig. 4, the DSL is 2 mm Figure 5 is a section view of a 2-3/4-in.-diameter (70 mm)
(0.1 in.) thick, the DT is 5 mm (0.2 in.) thick, and the core of lightweight aggregate concrete with a w/cm
TAZ is 7 mm (0.3 in.) thick. The delamination plane estimated at 0.45 and an air content of 6.5%. This slab
occurs at the boundary between the DT and the was in service for 3 months before delaminations were
underlying APC. The w/cm is the same on both sides of detected. In the example shown in Fig. 5, a lenticular void
the delamination. forms part of an incipient delamination at the boundary
In both the normalweight- and lightweight-aggregate between the DT and the APC.
concretes that show delamination distress, the delamination Another type of irregularly shaped void that is
plane typically is right at or very near the boundary commonly seen in the DT is a single void that, when
between the DT and the APC. This boundary represents viewed in two dimensions on a lapped surface, shows
an abrupt transition in entrained-air-void content. an irregular shape rather than the circular cross section

26 NOVEMBER 2004 / Concrete international


(6a)

A
B
DSL

DT C
1 mm

Fig. 7: Section view (10x) perpendicular to the plane of the


wearing surface in a core taken from an air-entrained (6.2%),
(6b) DSL lightweight-aggregate concrete slab showing cement paste/
aggregate bond disruptions in coarse aggregate particles in the
densified surface layer (A, B), and in the DT (C)

entrapped or entrained air voids. In the case of one


type of lenticular void, the final shape can be explained
as the result of the action of the trowel breaching the
DT web of cement paste between adjacent air voids.
In other cases, the irregular shape of single voids can
be explained as a compression and distortion of
entrapped or entrained air voids captured by the
DT 1 mm action of the trowel within relatively stiff, but still
plastic, cement paste; and
Fig. 6: Four-inch diameter core (6(a)) taken from an air-entrained ■ When premature sealing of a slab is involved, water
(6.4%), normalweight concrete slab that showed delaminations voids can and do form directly under the DSL. In air-
after 9 months in service. The densified surface layer is 2 mm
(0.1 in.) thick, and the DT is 18 mm (0.7 in.) thick. The maximum entrained concrete slabs that have delaminated, the
thickness of the TAZ is 25 mm (1 in.). Thin tears in the irregularly shaped voids are present at various levels
cementitious phase that pass around cement paste/aggregate in the DT, often well below the DSL.
boundaries in the DT are shown in the enlarged section view
(6(b)). The tears are parallel to the plane of the wearing surface
at five different levels TEARS
A commonly observed microstructural feature in
normally seen with entrained air voids. These voids, the DT is short (typically less than 25 mm [1 in.] when
which range from less than 0.1 mm (0.004 in.) to well measured in two dimensions on a lapped surface)
over 1 mm (0.04 in.), are judged to represent entrained tears within the cementitious phase. For the formation
or entrapped air voids that have been compressed and of one type of lenticular void (Fig. 4 and 5) in the DT, it
distorted by troweling. Numerous examples of these was suggested that the cement paste lying between
voids can be seen in Fig. 3 to 5. adjacent air voids had been literally pulled apart by
The question arises as to whether some or all of these the troweling forces, creating a tear that united the
voids are water voids. A number of factors that suggest air voids.
that they are not water voids include: Figure 6(a) and (b) show a second type of tear in a
■ By definition, water voids form on the underside of normalweight concrete slab that had a w/cm of 0.50
aggregate particles or reinforcement during bleeding. and an air content of 6.4%. Delaminations in this slab
The voids considered here are present within the were detected within 9 months of placement as small
cementitious phase and are not in contact with wearing-surface spalls and as shallow spalling along
aggregate particles. The w/cm is similar in the joints. Thin tears in the cementitious phase in the DT
cementitious phase surrounding these voids; pass around cement paste-aggregate boundaries and
■ The shape of these voids, which are present typically also pass through distorted air voids. The maximum
in the DT, strongly suggests that they were originally depth of the TAZ in cores examined from this slab is

Concrete international / NOVEMBER 2004 27


25 mm (1 in.). In the example shown in Fig. 6(b), there are along the boundary between the cementitious phase
tears parallel to the plane of the wearing surface at five and an aggregate particle. An example is shown in
different levels in the DT. These tears are located in the Fig. 7, which is a section view (10x) of a 2-3/4-in.-
same vertical plane in the slab. Considering that bleeding diameter (70 mm) core taken from a lightweight
is actually a solid particle sedimentation phenomenon, it aggregate, air-entrained (7.2%) concrete slab that
does not seem likely that these tears could be attributed delaminated 3 months after being placed into service.
to bleed water entrapment. In addition, the tears are Here, there is a separation along the top surface of a
below the bottom of the DSL, and the w/cm is the same coarse-aggregate particle (C) that is partly embedded
on both sides of the tears. in the DSL and partly in the DT. Clearly, this is not a
The tears described here are similar to features water void as the “material” under the void is not
observed in precast concrete elements when forms are cement paste. There is also a slight bond disruption in
removed at an early age while the concrete is still in a the two smaller coarse-aggregate particles overlying the
plastic state. In these instances, the tears have been larger one (A, B)—both of which are completely
referred to as “plastic microfractures.” embedded in the DSL. In one of these particles (A), the
Thin, short tears such as the ones described in this separation is along the top surface; on the other (B), the
article are common features seen in the DT of hard-trowel bottom surface.
finished, air-entrained concrete slabs. As these tears In other cases examined here, cement paste-
increase in size regarding the amount of area that they aggregate bond disruptions form with about equal
cover, they become incipient delaminations. frequency along the top, bottom, and sides of
aggregate particles.
CEMENT PASTE-AGGREGATE Figure 8 is a section view (10x) of a 3-3/4-in.-
BOND DISRUPTIONS diameter (95 mm) core taken from a normalweight,
Another common microstructural feature observed air-entrained (3.8%) concrete slab that blistered during
in the DT, and occasionally in the DSL, is a separation troweling. The maximum depth of the TAZ in the slab

REDUCING DELAMINATIONS IN before the building is under roof at a time when


AIR-ENTRAINED CONCRETES freezing events are likely. Air entrainment may be
Two situations must be considered here. One deals specified in this case to guard against freezing-and-
with those instances where air-entrained concrete is thawing damage. A second situation is the use of air
inadvertently delivered to a job site. The other is when entrainment to improve the workability and finishing
air entrainment has been specified, and a hard-trowel characteristics of lightweight-aggregate concrete, or
finish is still desired. In both cases, greater effort must to reduce its density. A third situation is the use of a
be made to educate owners, concrete specifiers, trowel finish on concrete that will definitely be
concrete suppliers, and concrete contractors of the exposed to freezing events, and where a subsequent
risk of delaminations when any air-entrained concrete surface treatment requires a smoother finish than can
(normalweight or lightweight) is hard-trowel finished. otherwise be obtained.
It is surprising how many are still unaware of the If it is proposed to use air entrainment on a slab
problem. In practice, two steps can be taken to avoid that will receive a hard-trowel finish, all of the
or minimize the risk. principals involved in the project should be made
With regard to inadvertent air on the job, the aware of the possible consequences of this action,
obvious answer is to measure air content on all with consideration given to a protocol for a resolution
concrete delivered for interior floor slab construction. of problems if they do arise.
This measurement is easily made using relatively The following steps are recommended to reduce the
inexpensive equipment, following well-defined risk of delamination when a hard-trowel finish on an
test procedures.16 Because fresh concrete unit air-entrained concrete is desired:
weight varies with air content, this property, too, can ■ Minimize the amount of air entrainment;
be used in a quick and inexpensive test to flag ■ Place the concrete at as low a slump as possible;
potential problems. ■ Delay the trowel finishing operation as long as
And what of those situations in which a hard- possible;
trowel finish has been specified for air-entrained ■ Consider actions that can be taken to minimize the
concrete? There are at least three situations where magnitude of the stiffness differential in the slab; and
this can occur. An interior floor slab may be placed ■ Minimize the intensity and duration of troweling.

28 NOVEMBER 2004 / Concrete international


at this coring site is 30 mm (1.2 in.). The view shown
in Figure 8 represents a depth of 8 to 18 mm (0.3 to
0.7 in.) below the plane of the wearing surface, well
within the DT.
Two gravel coarse aggregate particles separated by
a 3-mm-thick (0.1 in.) cementitious phase are shown.
One aggregate particle shows a bond disruption along
its top surface (A), while the overlying aggregate particle
(B) shows a bond disruption along its bottom surface.
If bleeding had caused this latter separation, it is
expected that there would be no separation along the
top surface of the underlying aggregate particle (A).
Also arguing against the involvement of bleeding is the
presence of fine aggregate particles, not cement paste,
under the elongated voids in contact with aggregate
particle B.
In other instances of paste-aggregate bond disruptions,
the separation surfaces are rough and jagged,
suggesting that the boundary was literally torn apart. Fig. 8: Section view (10x) perpendicular to the plane of the
In yet others, a common geometry of the separation wearing surface in a core taken from an air-entrained (3.8%),
normalweight concrete slab showing cement paste/
surface and the aggregate particle surface leave little aggregate bond disruptions on the top (A) and bottom (B)
doubt that the aggregate particle was once in contact surfaces of coarse aggregate particles. The densified surface
with this paste. layer is 3 mm (0.1 in.) thick, and the DT has a maximum
thickness of 27 mm (1 in.). These bond disruptions occur in the
The features described previously attest to a physical DT at a depth of 8 to 18 mm (0.3 to 0.7 in.) below the plane of the
movement of stiff aggregate particles within a plastic wearing surface
cementitious phase that has a lowered yield stress due
to the presence of entrained air voids at the start of ■ Irregularly shaped voids within the cementitious
troweling. The troweling manipulation results in a phase, which often are lenticular or elongated
disruption of the cement paste-aggregate bond that in shape;
occurs with about equal frequency along the top, ■ Thin, short tears within the cementitious
bottom, or sides of the aggregate particle. phase; and
■ Cement paste-aggregate bond disruptions that
AIR INFLUENCES DELAMINATIONS occur with about equal frequency along the top,
Microstructural and other features of hard-trowel bottom, and sides of aggregate particles.
finished concrete slabs that have delaminated, or show Evidence is presented to support the conclusion
incipient delaminations, support the conclusion that that these microstructural features are not water
physical forces from the hard-troweling operation are voids, and are not caused by interrupting the
frequently involved in the creation of delaminations. bleeding process.
This interpretation appears to explain the disproportionate 4. The extent of damage that occurs in hard-trowel-
influence of air entrainment in slabs that delaminate. finished, air-entrained concrete slabs depends, in
Other significant observations and conclusions addition to the contribution of the entrained air
derived from this study include: voids, on a number of other design, construction,
1. Most of the concrete slabs that exhibit delamination environmental, and material variables that have been
distress (as opposed to crusting and blistering) were identified in previous studies. Because of the many
air-entrained. variables involved, delamination is seen as a
2. The disproportionate influence of air entrainment on complex phenomenon; not one that is easily
slabs that delaminate is attributed to a lowering of the anticipated or controlled.
yield stress of the cementitious phase of the concrete, 5. In worst-case situations, tears in the cementitious
creating a greater ease of distortion and manipulation phase can cover areas of 1 ft 2 (90,000 mm 2) or
of the concrete during trowling. more, creating an opportunity for full delamination
3. Microstructural features that are present near the and subsequent spalling of the wearing surface.
surface of hard-trowel-finished, air-entrained Full delamination is most likely to occur when
concretes that support this distortion and manipulation project conditions result in a very abrupt change
hypothesis include: in stiffness in the concrete that is affected by the

Concrete international / NOVEMBER 2004 29


trowel-generated forces. Often, delamination Air-Entrained Concrete Floors,” Concrete Construction, Feb. 1999,
planes are located at or near the boundary pp. 35-37.
representing an abrupt transition from a region of 4. Bimel, C., “Is Delamination Really a Mystery?” Concrete
very low air entrainment to one of a higher level of International, V. 20, No. 1, Jan. 1998, pp. 20-34.
air entrainment. 5. Suprenant, B. A., and Malisch, W. R., “Diagnosing Slab
6. It has been observed that not all air-entrained concrete Delaminations,” Concrete Construction, Jan. 1998, pp. 29-34.
slabs that receive a hard-trowel finish experience 6. “Guide for Concrete Floor and Slab Construction (ACI 302.1R-96),”
delaminations. The results of the present study American Concrete Institute, Farmington Hills, MI, 67 pp.
suggest that in these slabs, the microstructural 7. “Specifications for Structural Concrete (ACI 301-99),”
features in the concrete resulting from the trowel- American Concrete Institute, Farmington Hills, MI, 49 pp.
generated forces have not advanced to the point of 8. “Problem: Finishing Too Early,” Concrete Construction,
connectedness that large enough areas are affected to Sept. 2001, p. 66.
create a delamination problem. 9. Suprenant, B. A., and Malisch, W. R., “Diagnosing Slab
If the interpretation proposed here is valid, it is Delaminations,” Concrete Construction, Feb. 1998, pp. 169-175.
judged likely that all air-entrained concrete slabs that 10. Suprenant, B. A., and Malisch, W. R., “Sealing Effects of
receive a hard-trowel finish will show some of these Finishing Tools,” Concrete Construction, Sept. 1999, pp. 38-43.
microstructural features. 11. “What, Why, and How?: Delamination of Troweled Concrete
7. In two of the projects reviewed in the present study, Surfaces,” National Ready Mixed Concrete Association Document
the petrographic examination was initially prompted CIP 20, 1992, pp. 1-2.
by a concern other than delamination. The initial 12. Suprenant, B. A., and Malisch, W. R., “Troubleshooting
petrographic examination in one of these cases Crusted Concrete,” Concrete Construction, Apr. 1997, pp. 375-378.
provided evidence of all of the microstructural 13. Suprenant, B. A., and Malisch, W. R., “Diagnosing Slab
features discussed here, short of full delamination. Delaminations,” Concrete Construction, Mar. 1998, pp. 277-283.
A chain drag survey was recommended, which 14. ASTM C 856-03, “The Standard Practice for Petrographic
subsequently revealed a number of delaminated Examination of Hardened Concrete,” Annual Book of ASTM
areas, although most were under 1 ft 2 (90,000 mm 2) Standards, Section Four, “Construction,” V. 04.02, Concrete
in extent. The circumstances of this particular and Aggregates, 2003, 16 pp.
example provide clues as to what can be done to 15. ASTM C 457-03, “The Standard Test Method for Microscopical
reduce the risk of delaminations in air-entrained Determination of Parameters of the Air-Void System in Hardened
concrete slabs that must be given a hard-trowel finish. Concrete,” Annual Book of ASTM Standards, Section Four,
In this case, the slab was slated to receive a membrane, “Construction,” V. 04.02, Concrete and Aggregates, 2003, 14 pp.
and the project documents called for a reduced 16. ASTM C 231-03, “The Standard Test Method for Air Content of
intensity and duration of troweling. In examining a Freshly Mixed Concrete by the Pressure Method,” Annual Book of
number of cores from this project, it was observed ASTM Standards, Section Four, “Construction,” V. 04.02, Concrete
that the thinner the TAZ, the fewer the occurrences and Aggregates, 2003, 8 pp.
of the microstructural features associated with the
delamination distress. Received and reviewed under Institute publication policies.
8. The projects reviewed here confirm an increased risk
of delaminations when air entrainment is used in either
normalweight or lightweight aggregate concretes that
receive a hard-trowel finish.

Acknowledgments David R. Lankard, FACI, has operated


Thanks are given to Nick J. Scaglione of Concrete Research & Lankard Materials Laboratory, Inc.,
Testing, Columbus, OH, for helpful discussions and for permission Columbus, OH, since 1978, which
to use several of the photomicrographs that appear here. provides petrographic, research, and
development services to producers and
References users of portland cement concrete and
1. Moulzolf, G. M., “Reader Response: Delamination Causes,” refractory concrete. He has served on a
Concrete Construction, Jan. 2003, p. 14. number of ACI committees and is past
2. Anon., “Hard-Trowel Finish on Air-Entrained Concrete,” Chair of ACI Committee 547, Refractory
American Society of Concrete Contractors, Position Statement No. 1, Concrete. Lankard received the 1973 ACI Wason Medal for Most
Concrete Construction, Mar. 2003, p. 66. Meritorious Paper and he is also a Fellow of the American
3. Suprenant, B. A., and Malisch, W. R., “Beware of Troweling Ceramic Society.

30 NOVEMBER 2004 / Concrete international

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