ST.

JOSEPH’S INDIAN COMPOSITE PU COLLEGE

DEPARTMENT OF CHEMISTRY
CHEMISTRY SCHEME OF VALUATION – FINAL PRACTICAL EXAMS, 2024
TOTAL MARKS: 30 MARKS MAX. TIME: 2 HOURS
Report 30min before the commencement of the exam near the lab with record & hall ticket
SALT ANALYSIS: 10 marks
“ANY ONE SALT FROM THE FOLLOWING – Al2(SO4)3, BaCl2, CaCO3, NH4Br, MnSO4, Sr(NO3)”
PRELIMINARY TEST - 1 MARK
IDENTIFICATION OF ACID RADICAL – 4 MARKS
Identification of acid radical group - 1 mark
Identification of acid radical - 1 mark
Confirmatory test for acid radicals - 2 mark
IDENTIFICATION OF BASIC RADICAL – 4 MARKS
Identification of basic radical group - 1 mark
Identification of basic radical - 1 mark
Confirmatory test for basic radicals - 2 marks
SYSTEMATIC PROCEDURE ALONG WITH THE ABSENCE OF GROUPS - 1 MARK

TITRATION: 10 marks – Estimation of KMnO4 using std. FAS solution

PERFORMING TITRATION - 3 MARKS
TABULAR COLUMN WITH THREE TRIALS - 4 MARKS
CALCULATION - 3 MARKS (CALCULATE USING THE CONCORDANT TITRE VALUE)
- Formula - 1 mark
- Substitution - 1 mark
- Molarity answer with units - 1 mark

RECORD: 6 marks
VIVA: 4 marks
QUESTIONS TO BE BASED ON THE FOLLOWING TESTS (refer record)
Alcohol - Lucas test, ceric ammonium nitrate test (experiment, observation & inference)
Phenols - neutral ferric chloride test, phthalein fusion test (experiment, observation & inference)
Aldehydes and ketones - 2,4-DNPH test, Tollen’s test (experiment, observation & inference)
Carboxylic acid – Litmus test, sodium bicarbonate test, esterification (experiment, observation &
inference)
Amines - carbylamine test, diazotization test. (experiment, observation & inference)