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ACCURATT Range of Solutions FOR EVERY HPI LABORATORY

About

ACCURATT is founded by Khalid Tafrasti to deliver high quality analytical solutions and dedicate to
customers in various industries.

The long sales (more then twenty years) and service experience in the Middle East, Africa and Europe and
the customers close relationship of the founder is the drive behind the start of a new concept in the region.

ACCURATT provides complete solutions and new technology to our customers:

25 years of experience in Applications, Service and training with the following GC, HPLC, GCMS platforms:

• JAS
• PAC (AC)
• Agilent Technologies
• Perkin Elmer
• Shimadzu
• SCION Instruments (Varian)
2
ACCURATT Partners

ACCURATT if the official Distributor of


JAS.de in the BENELUX and North-Africa.
JAS is a value-added reseller of Agilent
Technologies

ACCURATT if the official Distributor of ETECH,


physical properties supplier

ACCURATT if the official Distributor of Spectra


Analysis in the BENELUX and North-Africa.
Spectra Analysis is the provider of GC-FTIR.
Combining the power of FTIR with Gas
Chromatography and Liquid Chromatography

ACCURATT is a Partner of Separation


Systems for providing Calibration
standards, Reference Material and HPI
software (Expert)

ACCURATT is a partner of ARO Scientific


for certified reference material and for your
working standards
ACCURATT is a service Provider; what do we Provide?

• Service & Service Contracts


• Maintenance
• Preventive Maintenance
• Calibration and Verification
• Validation
We provide Training:

• Standardization Training
• Application Training
• Trouble Shooting
• Software
• Hardware
• Results verification and statistics
• Reporting
Provider of high-quality Calibration Standards, CRM’s for every Lab: Gas Chromatography Standards

Standardization Application
ASTM D2887 Diesel and Jet fuel SIMDIS Calibration and Reference Standards

ASTM D3606 Benzene Toluene Standards


ASTM D3710 (see also ASTM D7096) Naphtha, Gasoline Calibration and Reference Standards
ASTM D4815 Oxygenates Calibration Standards
ASTM D6729/D6730/D6733/D5134 DHA Calibration and Reference Standards, gravimetric evaluation blend

ASTM D5307 Internal Standard, calibration standard


ASTM D5580 - Aromatics Calibration standards
ASTM D5623 Sulfur Calibration standards and Internal standard
ASTM D5796 Benzene, Toluene, and Total Aromatics standards
ACCURATT recognises that our customers ASTM D6296 Olefin calibration standards with MTBE and ETBE
should be always provided with products and ASTM D6352/D7500 Distillates and Lube oils 100-725°C Calibration and Reference standards
services they can reply upon, trust and have ASTM D6379 Calibration standards Aromatics HPLC method
confidence to use on a daily basis. Our ASTM D6591 Calibration standards Aromatics HPLC method
commitment to quality and our accreditations ASTM D6584/EN14124 Free and Total Glycerol, mono-, di,- tri-glycerides in FAME standard
demonstrates that we have rigorous systems
ASTM D7011 Thiophene in Benzene Calibration standards
in place that allow us to provide customers
ASTM D7096 Naphtha, Gasoline Calibration and Reference Standards
with the highest quality products possible, ASTM D7213 VGO, Lube Oil SIMDIS Calibration and Reference Standards
which are accepted globally. ASTM D7169 Crude Oils and Residuals Calibration standards, Reference. Gravimetric blend
and response factor standard
ASTM D7423 Trace Oxygenates standard
ASTM D7754 Trace Oxygenates Standards
ASTM D7845 Chemical Species in Marine Fuel Oil

ASTM D7900 DHA FE, DHA Calibration and Reference Standards, gravimetric evaluation
blend

Internal standard
ASTM D8071 Calibration and reference Standard PIONA analysis by GC-VUV

EN 14103/EN16300 Ester and linolenic acid methyl ester

EN 14105 Free & total glycerol, mono-, di-, and triglyceride

Calibration and CRM’s


EN 14110 Methanol in Fame calibration and Reference Standards
Example PIONA Ce r tificate Analyze d by GC - MSD
Provider of high quality Calibration Standards, CRM’s: Physical Properties

# Standards and CRM’s


1 ACID NUMBER (AN) PACKS - TOTAL ACID NUMBER (TAN)
2 ACID NUMBER (AN) X3 PACKS - TOTAL ACID NUMBER (TAN)
3 BASE NUMBER (BN) - TOTAL BASE NUMBER (TBN)
4 BASE NUMBER (BN) X3 PACKS - TOTAL BASE NUMBER (TBN)
5 FLASH POINT SECONDARY WORKING STANDARD (SWS). Pensky-Martens Closed Cup PMCC
6 FLASH POINT SECONDARY WORKING STANDARD (SWS). Cleveland Open Cup COC
7 FLASH POINT CRM
8 DENSITY CRM
9 DISTILLATION CRM
10 CLOUD POINT CRM
11 COLD FILTER PLUGGING POINT (CFPP) CRM
12 FREEZING POINT CRM
13 SMOKE POINT CRM
14 POUR POINT CRM
15 SULFUR CRM, DIESEL (SYNTHETIC)
16 SULFUR CRM, DIESEL (SYNTHETIC) KITS
17 SULFUR CRM, HEAVY MINERAL OIL
18 SULFUR CRM, HEAVY MINERAL OIL KITS
19 COLOUR STANDARDS, ASTM COLOUR
20 COLOUR STANDARDS, GARDNER COLOUR
21 COLOUR STANDARDS, SAYBOLT COLOUR
22 COLOUR STANDARDS, LOVIBOND RYBN COLOUR STANDARD
23 COLOUR STANDARDS, PT-CO/HAZEN/APHA COLOUR STANDARD
24 COLOUR STANDARDS, AOCS-TINTOMETER COLOUR STANDARD

Example ce r tificate of a Cloud Point CR M


Smoke Point Flash Point testers Physical Distillation
EIE-SP-03 EIE-FP EIE-DI-01

• ASTM D1322, ISO 3014, GB 382 • Full range of Flash point testers
• One-Button start • ASTM D86, ASTM D850,
• One-Button start
• "M-Vision" technology adopted EN ISO 3405 ASTM D1078
• "M-Vision" technology adopted
• Automatic ignition system • Fully automated Atm.
• Automatic ignition system
• Automatic atmospheric pressure adjustment Distillation system
• Automatic atmospheric pressure adjustment
• Built-in printer • Touch screen and physical
start button

Standard 2 years warranty


Physical Distillation
EIE-DI-01 • The dual optical measurement system Range: 0 - 103%
Resolution: 0.01 ml Accuracy: ±0.1 ml

• Built-in 2 units of flame detectors, built-in fire extinguisher


(need external air source, pressure 700 ± 50 kPa)

• 1000 result data or expand storage capacity as needed.

• RJ45 Ethernet (optional WIFI), can connect to LIMS, LAN, Internet


• connect to an external printer by USB
EIE-FP170-03
EIE-FP92-3 EIE-FP93-03

• ASTM D92, ISO 2592, IP 36


• One-key start • ASTM D93, ISO 2719 • ASTM D56, IP 170, EN ISO 1373,DEF STAN 91-091
• M-Vision Technology to • One-Button Start. The tester can • Temperature range -30 - 80°C
detect flash point the use automatically perform the ignition, heating • Unknown sample pre-test function
of AI , stirring, detection, pressure correction at • Heating rate: 0.2 - 6°C /min continuously
flash point, printing, and cooling. adjustable
• The first non-contact stirring method. • Ignition Temperature interval: 0.1 - 3°C
• Build-in the atmospheric pressure sensor. continuously adjustable

Standard 2 years warranty


EIE-CT-101 EIE-170-008 EIE-170-012
EIE-TAV-01 EIE-RVP-3

• ASTM D3242, GB/T 12574 •ASTM D323, GB/T 8017 • Constant Low Temperature • Constant Low Temperature Water • Sample Preparation Bath is
• Automatic Total Acid Value •One-Button Start. The tester can Bath Bath supporting equipment
Tester automatically perform the oscillation, • Temperature Range: • Temperature Range: designed and used for the
• The cutting-edge "machine measuring, recording, and printing. 2°C - 10°C - 30°C - 50°C Abel Flash Point Analyzer.
vision" technology. •It adopts advanced wireless data • Display resolution: 0.1°C • Display resolution: 0.1°C
• Using a high-speed micro- transmission technology to minimize the • Temperature accuracy: • Temperature accuracy: ±0.1°C
industrial computer and influence of air leakage on the test. ±0.1°C
industrial-grade high-fidelity •3 Groups of detection units are • Sample cooling <10 min
high-speed cameras equipped

Viscosity
• ASTM D455
➢ Advanced software can simultaneously run two analyzers doing the analysis automatically in proper sequence
➢ Passivated and deactivated piping system prevents the adsorption of trace sample
➢ The capacity of working with different gas chromatography (please check with us)
➢ Inert gas blowing function, to ensure the purification of the injection system, to avoid the sample interference in the
pipeline
➢ All sampling functions indicated by "methods" for simple operation
➢ Processing sample bags of 3,6,10,12,14 or more if required

EIE-GAS-05 EIE-AHSD-01
EIE-GAS-01

H2S Analyzer
JAS (Joint Analytical Solutions) is a Value-added
reseller of Agilent Technology and provides total
solutions for the Oil and Gas industry

Accuratt is a Partner of
FULL RANGE OF APPLICATIONS

JAS provides a full range of Analyzers


for the Oil and Gas Industry based on
Agilent Technologies Platform

▪ GAS Analysis (Refinery Gas and Natural Gas)

▪ LPG Analysis

▪ Naphtha Analysis

▪ Mid-distillates Analysis

▪ Crude Oil and Residual Analysis

▪ Elemental Analysis

▪ Impurities Analysis

▪ Trace Analysis
How can we serve you ?

JAS Provides Unique


Solutions that will
make your daily tasks
easier:

Gas Bag Sampler (GBS)


Gas Injection Control Unit (GICU) Customized Multi Sample GC Preparative Fraction
Automatic Gas Sampler
Stream Analyzers Collector (EzPrep)
How can we serve you?

JAS Provides Unique


Solutions that others
don’t:

Swap

Swap and Go External Valve systems Customized systems GC Atomic Emmission Detector
How can we help?

1. Make your lab efficient: Cost effective, Space effective and increase the usage
time of your instruments

2. Let technology work for you and win time

3. Decrease your Calibration Gases and standards by using smart alternatives

4. Use alternative gases and make use of Gas Generators


1. How to make your lab efficient: Cost effective, Space effective and increase the usage
time of your instruments

• Combine more analyzers in one, the quality and technology permits it:

• Purchase cost of the multi-channel analyzer is less than two or three instruments
• Usage cost of 1 instrument is lower than 2 or 3 instruments: Power, Gas, Lab space
– (how much does your lab space cost?)
• Depreciation cost will decrease
• Less spare parts needed
1. Example Multi Channel Analyzers

• Four detectors including SCD


• Four different channels for 4
different analysis

1. Example Multi Channel Analyzers

• Five detectors including MSD


• Four different channels for 4
different analysis

Objections?!
Mach RGA: Refinery Gas Analysis

Permanent gases :H2, O2, N2, CH4, CO, CO2


Hydrocarbons :C1-C5, C6+ [extended analysis to C9]
Sulfur components :H2S
Optional: : Trace CO, CO2

 Standardization: ASTM D7388, UOP539, ASTM D1945, ASTM D1946


ASTM D2598*, ASTM D3588*, EN ISO 7941, IP 405, EN 15984, DIN 51666, GOST
31371
 Extended Mode: BTEX

 Add on: LSV or Vaporizer: ASTM D2163, EN27491, ISO 7941 & UOP373, ASTM
D2504, ASTM D2505
Natural Gas Analysis
The Gas Processors Association (GPA) creates industry standards around technology and procedures for processing
natural gas. These guidelines determine design, installation and maintenance of natural gas distribution, delivery
and measurement systems.

GPA2161: Analysis for Natural Gas and Similar Gaseous Mixtures by Gas Chromatography
GPA2286: Method for the Extended Analysis of Natural Gas and Similar Gaseous Mixtures by Temperature Program Gas
Chromatography
GPA2186: Method for the Extended Analysis of Hydrocarbon Liquid Mixtures Containing Nitrogen and Carbon Dioxide by
Temperature Programmed Gas Chromatography
GPA2172: Calculation of Gross Heating Value, Relative Density and Compressibility Factor for Natural Gas Mixtures from
Compositional Analysis

ISO: International Organization for Standardization

ISO 6974: Natural gas — Determination of composition with defined uncertainty by gas chromatography — Part 6: Determination
of hydrogen, helium, oxygen, nitrogen, carbon dioxide and C1 to C8 hydrocarbons using three capillary columns
ISO 6975: Natural gas — Extended analysis — Gas-chromatographic method
ISO6976: Natural gas — Calculation of calorific values, density, relative density and Wobbe index from composition
ISO13443: This International Standard specifies the standard reference conditions of temperature, pressure and humidity to be
used for measurements and calculations carried out on natural gases, natural-gas substitutes and similar fluids.
ISO13686: specifies the parameters required to describe finally processed and, where required, blended natural gas

ASTM D1945: Standard Test Method for Analysis of Natural Gas by Gas Chromatography
ASTM D1946: Standard Practice for Analysis of Reformed Gas by Gas Chromatography
Gas Bag Sampler (GBS)
Automatic Gas Sampler

The JAS GBS allows automated sampling of gases, stored in tedlar bags or gas
sampling balloons, as well as gas cylinders, e.g. calibration gas cylinders.
Sample transfer is carried out via a multi-position valve. Each gas sampling inlet
is equipped with an in-line filter to avoid multi-position valve blocking.
Connection to the GC can be made by means of 1/16” SS tube.
The GBS is controlled via a special JAS Control Software.

Available Models

• GBS-8
• GBS-10

Features

• Can handle bags/balloons of 2-3 bar


• Flow paths can be purged
• Includes pump for samples with atmospheric pressure
• Intuitive JAS Control Software
• Bags can be selected randomly
• Display shows current port position
• Minimum waiting time between runs (sample loops can be purged while run is still in progress)
• Existing GC methods do not need to be changed
• In one sequence pressurized samples and samples with atmospheric pressure can be processed
• For Agilent and third-party GCs (control via start-stop/remote cable)
Gas Injection Control Unit (GICU)

Reproducible results with low Relative Standard Deviations (RSD; measured in percent)
are two main aspects of modern gas analysis. Fundamental is the gas sample injection
at reproducible and controllable volumes, pressures and temperatures.

This is especially challenging in cases where one GC system is required to handle


samples coming from different sample containers and where the sample characteristics
may vary from injection to injection.

The JAS GICU Software

The JAS GICU Software is literally self-explaining. It can control a MPV for automation
of low-pressure sample containers. The program surface can be divided into five
sections:

1.Toolbar
2.Process indicator
3.Element area
4.Loaded sequence
5.Software revision The element area shows the main hardware components such as:
a. Gas cylinder / Tedlar bag / Bypass
b. Safety valve
c. Remote GC
d. Valve
e. Programmable sample loop pressure
f. Pump valves
g. Vacuum pump
JAS LPG Vaporizer
General specifications :
JAS LPG Vaporizer
• Vaporizer temperature: 55 – 155 °C
• Heated transfer line temperature: 70 °C
• Heated transfer line length: 1.5 m
• Max inlet pressure: 413 bar (6000 Psig)
• Max outlet pressure: 25 bar (360 Psig)
• Connectors: Swagelok quick connector
• Power supply: 110 V / 220 V
• Size: L x W x H (mm): 360 x 225 x 260
• Weight: 12 Kg
Save Cost and Space by using GasMix
and LiquidMix
Using GasMix Aiolos II you benefit of :
AIOLOS/NEPHOS
• Dedicated, user-friendly and intuitive software
• Less time consuming: programmed injection sequences is a great time-saver for
routine quality procedures
• Full automation: by synchronizing dilutions, injection, flushing timings with an
external analyzer
• Improved accuracy: multipoint MFC calibration curves for each used gas
• Rigorous metrology : full traceability, documentation, certification of the
concentration accuracy
• Compliance with ISO 6145-7

Using LiquidMix NEPHOS you benefit of :

• Create a calibration gas on demand from one or upto four gases, and one or two liquids
• A very wide range of concentrations from ppb to %
• The heated lines, up to the point of delivery, avoid recondensation of the vaporized
compounds
• A modular construction that allows you to evolve according to your growing needs
• A dedicated software performs all specific calculations and analyzer control
• Creation, storage, and implementation of complex sequences of mixtures and/or
dilutions
• Robust design, easy to use and fully automatic operation saves significant operator time
Calibration Wafers
ASTM D7807 SULFUR SIMDIS GC-SCD:
Sulfur Analysis
Sulfur in LPG: UOP791
• Sulfur in Naphtha/Gasoline and Gasoline: ASTM Sulfur in Natural Gas and LPG: ASTM D5504
D5623
• Thiophene in Benzene: ASTM D7011
• Sulfur SIMDIS: ASTM D7807
ASTM D7807 SULFUR SIMDIS GC-SCD:

Sulfur in Natural Gas + Natural Gas composition:


GC-PFPD ASTM D6228 and GPA2286

Trace COS in propylene: ASTM D5303


Sulphur compounds in natural gas and gaseous fuels: ASTM D6228
Sulphur compounds in natural gas: ISO 19739
Trace thiophene in refined benzene: ASTM D4735
Upgrade your Analyzer to a Multi-channel Analyzer

We provide upgrades for


any existing Analyzers or
unused GC‘s in your lab
JAS Valve upgrade kit
JAS Valve upgrade kit

Covers with Insulation

Actuators/Valves/tubing
Heated blocks and heaters Solenoids and connections Transfer lines and
connections
JAS Valve upgrade kit

Heated Transfer Line

External Valve Box to be connected to any GC


JAS GC-AED

ATOMIC EMISSION DETECTION


JAS is a champion in customized
solution for every application

JAS AED
The JAS AED III is the only commercially available
Atomic Emission Detector for gas chromatography.

The AED allows you to detect a great number of


specific elements within any volatized compound
(except helium, the carrier gas) at picogram level
sensitivity, with excellent selectivity.
Combined GC and
Spectroscopy
JAS AED detects elements in Gas and Liquids
JAS AED Sulfur analysis compared
to existing technology

FPD PFPD SCD AED


Minimum Detectability 10 pgS/sec 1 pgS/sec 0.5 pgS/sec 0.04 pgS/sec

HC Selectivity 104-105 104-105 104-105 105

Linear Response No No No Yes

Equimolar Response No No No Yes

Detection Range 103 103 103 104

Simultaneous Multi Element No No No Yes


Response
HC Response No No No Yes

Packed And Capillary Yes Yes Yes Yes


Columns
Easy to Operate and Yes Yes Yes Yes
Maintain
JAS GCxGC solutions
JAS Unique Inlets for all the applications

For isothermal vaporization of The JAS PTV inlet with a wide The perfect choice for high The optimum injector for
thermally stable components variety of potential uses temperature applications SimDis applications
in a hot injector
Because of it's special heating • S/SL and PTV modes •Splitless mode
•S/SL and Pulsed S/SL Modes device, temperature ramps up to • max. temperature: 500 °C •max. temperature: 450 °C
•max. temperature: 400 °C (for 8890 720 °C per minute with 1° • heating rate: 720 °C/min •heating rate: 720 °C/min
GCs) increments are possible. • low thermal mass allows rapid •low thermal mass allows rapid
•also available for Agilent 8860 GCs heating and cooling heating and cooling
•easily upgradable to UNIS 2100 PTV The PTV injector is controlled via • extended heater to avoid 'cold •sample injection without any
Agilent OpenLAB Software or GC spots' - even at an oven discrimination
keypad. temperature of -20 °C
LNI Swiss Gas Generators

Nitrogen 5.0 Hydrogen 5.0 Zero Air Combined Gas Generators:


Flow: 10 – 35 L/min Flow: 1.5 – 40 L/min Flow: 1.5 – 40 L/min N2, H2.
Thank you for your time

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