SHRI. DR. R. G.

RATHOD ARTS AND SCIENCE COLLEGE, MURTIZAPUR,

DIST. Akola

Certificate
 
This is to certify that the Seminar title
“Synthesis and characterization of nio nanoparticles by Green method ”
Has been successfully completed by
Bhushan R. Kharbadkar
under the guidance of
Prof. A. K. Raut
in recognition to the partial fulfillment for
M.Sc. Part-II, Semester IV (Chemistry)
Sant Gadge Baba Amravati University,
Amravati (2023-22).
 
 INTRODUCTION

Nanoparticles :

Nanoparticles are often crystalline and end up being referred to as nanocrystals. High surface area
is a critical factor in the performance of catalysis and structures such as electrodes, allowing
improvement in performance of such surface of a particle over that of those in the technologies as
fuel cells and batteries.

METHOD OF SYNTHESIS :

There are so many methods for the synthesis of nano particles here will be used Biological
methods or green methods. In recent years, a number of technique, including co-precipitation,
sol-gel processes, etc

BIOLOGICAL METHODS :

The green chemistry technique is used of moderately pollutant free chemical to synthesis of
nano materials and embrace the use of beings solvent such as water, natural extract
 EXPERIMENTAL METHODS

 
NiO nano-particles synthesis (synthesis of 0.05 M solution)

Chemicals: Ni (0.05M), NaOH, Distilled water, leaf extract of Kalanchoe pinnata, etc.
Apparatus: Magnetic stirrer, PH meter, beaker, glass rod, dropper etc.
Procedure: 1) 0.05 M Ni dissolved in distilled water in 100 ml std. flask.

2) Take 5 ml leaf extract which are diluted with distilled water

in 50 ml std. flask.
2) Take 5 ml leaf extract which are diluted with distilled water in 50 ml std. flask.

3) Take 50 ml leaf extract solution in beaker and add the dropwise 0.05 M Ni solution
(100 ml) with constant stirring.
4) After the addition of NaOH solution maintain the PH-10-12 using NaOH solution.

5)After the addition of NaOH solution is stirred for six hours.

 FLOW CHART

0.01M/0.05M Ni is diluted in 100 ml distilled water in std.

flask

5ml of leaf extract is dil. with 50 ml distilled water in std .

flask

Ni solution was mixed with leaf extract drop by drop

NaOH is added to maintain in ph 10-12

Product obtained NI is calcinated at 400

 Application

• Industries :

• 01.In food industry :

Nano particles are used to make packing material and containers to store food.

• Medicine :

• 01.Nano drugs:
Nano materials are used as drugs for the treatment of cancer and TB
• Electronics :
01.Quantum wires have electrical conductivity

• Biomaterials :

01.Nano materials are used as bone cement and bone plates in hospitals
  
Conclusion

Recently, a variety of microorganisms and plant extracts have been used to efficiently synthesize metal
nanoparticles for green synthesis. The physical and clinical effects of antimicrobial, antioxidative and non-
toxic nanoparticles obtained by green synthesis are becoming increasingly important. Future studies will
probably focus on obtaining nanoparticles with antimicrobial effects at its maximum level and toxicity at
minimum. Because of this reason, synthesizing metallic nanoparticles, -especially by non-toxic green
synthesis method-, which are used in many application fields such as cancer treatment, drug transport,
biosensor construction is of great importance today

 
 References
 

1) Chandra, Sulekh, Avdhesh Kumar, and Praveen Kumar Tomar. "Synthesis of Ni nanoparticles and their characterizations." Journal of
Saudi Chemical Society 18.5 (2014): 437-442.

2) Nadaroglu, Hayrunnisa, Azize ALAYLI GÜNGÖR, and İ. N. C. E. Selvi. "Synthesis of nanoparticles by green synthesis
method." International Journal of Innovative Research and Reviews 1.1 (2017): 6-9.

3) Gour, Aman, and Narendra Kumar Jain. "Advances in green synthesis of nanoparticles." Artificial cells, nanomedicine, and
biotechnology 47.1 (2019): 844-851.

4) Hussain, Imtiyaz, et al. "Green synthesis of nanoparticles and its potential application." Biotechnology letters 38 (2016): 545-560.

5) Parveen, Khadeeja, Viktoria Banse, and Lalita Ledwani. "Green synthesis of nanoparticles: Their advantages and disadvantages." AIP
conference proceedings. Vol. 1724. No. 1. AIP Publishing LLC, 2016.

6) Mubayi, Anamika, et al. "Evidence based green synthesis of nanoparticles." Advanced materials letters 3.6 (2012): 519-525.

7) Rafique, Muhammad, et al. "A review on green synthesis of silver nanoparticles and their applications." Artificial cells, nanomedicine,
and biotechnology 45.7 (2017): 1272-1291.

8) Shameli, Kamyar, et al. "Synthesis and characterization of polyethylene glycol mediated silver nanoparticles by the green
method." International journal of molecular sciences 13.6 (2012): 6639-6650.

9) Huang, Haizhen, and Xiurong Yang. "Synthesis of polysaccharide-stabilized gold and silver nanoparticles: a green method." Carbohydrate
research 339.15 (2004): 2627-2631.

10) Awwad, Akl M., and Nidà M. Salem. "Green synthesis of silver nanoparticles by Mulberry Leaves Extract." Nanoscience and
Thank You