S3 PTLs-MTS data

S3 coated PTLs-MTS testing data

1st batch shipment
Coating methodology Observed
PTL ICR-ASR
S.No (Deposition temperature & Stack Id complete Status as on Remarks
sample ID (mΩ.cm2) short (h)
duration)
Assembled. Passed the cross-leak test at 350psi, cross-leak
1 S3 PTL22 pH adjustment (pH-2), 80 °C, 1hr 240 616 - 22-09-2023
observed at 400psi
2 S3 PTL 23 pH adjustment (pH-1.5), 80 °C, 1hr 20 611 - 22-09-2023 Assembled. Passed the cross-leak test at 400psi
3 S3 PTL 24 pH adjustment (pH-2), 60 °C, 1hr 290 610 - 22-09-2023 Passed the cross-leak test at 400psi. Running at 31A @1.9V

4 S3 PTL25 pH adjustment (pH-2), 80 °C, 2hr 110 614 - 22-09-2023 Assembled. Passed the cross-leak test at 400psi. Under activation

Not taken Mismatch in Active area, Unable to hold the back pressure, cross
5 S3 PTL26 Sintering (pH-1.5), 80 °C, 1hr 255 - for MTS 22-09-2023 leaked at 50psi, MEA is bulged due to this. Need to re-send on
testing coating the same recipe
Passed the cross-leak test at 400psi. observed low performance
running at 5A @2V , ECSA results is good. MPPs burnt due to less
6 S3 PTL27 Sintering (pH-2), 80 °C, 1hr 170 612 - 22-09-2023
contact. Reassembly with new MPPs ensuring sufficient contact in
assembly.

Running with low current, less activation. Initiated re-assembly to

7 S3 PTL28 Sintering (pH-3), 80 °C, 1hr 2451 609 - 22-09-2023
cross-verify the contact of MTS components.

Acknowledgements: YCH &CKB team- Vani, Arun Kumar, Pavithra, Sneha……

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 S3 coated PTLs-MTS testing data
2nd batch shipment
Coating methodology Observed
PTL ICR-ASR
S.No (Deposition temperature & Stack Id complete Status as on Remarks
sample ID (mΩ.cm2) short (h)
duration)

8 S3 PTL29 SLS addition (pH-2), 80 °C, 1hr 311 - 22-09-2023

9 S3 PTL 30 SLS addition (pH-3), 80 °C, 1hr 977 - 22-09-2023

Shipped the PTLs from YCH to CKB on 22-09-2023
10 S3 PTL 31 pH adjustment (pH-3), 80 °C, 1hr 499 - 22-09-2023

11 Bare PTL - 155 - 22-09-2023

Acknowledgements: YCH &CKB team- Vani, Arun Kumar, Pavithra, Sneha……

www.ohmium.com | confidential 3
 S3 coated PTLs-MTS testing data
3rd batch shipment
Coating methodology ICR-ASR Observed
PTL
S.No Stack Id complete Status as on Remarks
sample ID (Deposition temperature & duration) (mΩ.cm2) short (h)

12 S3 PTL32 pH adjustment (pH-2), 80 °C, 2hr - 21-09-2023

13 S3 PTL 33 pH adjustment (pH-3), 80 °C, 2hr - 21-09-2023

Electroreduction to be done
14 S3 PTL 34 pH adjustment (pH-1.5), 80 °C, 2hr - 21-09-2023

15 S3 PTL 35 pH adjustment (pH-2), 80 °C, 2hr - 21-09-2023

16 S3 PTL36 SLS addition, Sintering (pH-1.5), 80 °C, 1hr - 21-09-2023

17 S3 PTL 37 SLS addition, Sintering (pH-2), 80 °C, 1hr - 21-09-2023

Ready to be shipped for ICR & MTS testing
18 S3 PTL 38 SLS addition, Sintering (pH-3), 80 °C, 1hr - 21-09-2023
pH adjustment (pH-1.5), 80 °C, 1hr
19 S3 PTL 39 - 21-09-2023
(Repetition of PTL23)
Sintering (pH-1.5), 80 °C, 1hr
20 S3 PTL 40 - 21-09-2023 Electrodeposition & reduction to be started
(Repetition of PTL26)

Acknowledgements: YCH &CKB team- Vani, Arun Kumar, Pavithra, Sneha……

www.ohmium.com | confidential 4
 S3 coated PTLs-MTS testing data
3rd batch shipment
Coating methodology ICR-ASR Observed
PTL
S.No Stack Id complete Status as on Remarks
sample ID (Deposition temperature & duration) (mΩ.cm2) short (h)

12 S3 PTL32 pH adjustment (pH-2), 80 °C, 2hr - 21-09-2023

13 S3 PTL 33 pH adjustment (pH-3), 80 °C, 2hr - 21-09-2023

14 S3 PTL 34 pH adjustment (pH-1.5), 80 °C, 2hr - 21-09-2023

15 S3 PTL 35 pH adjustment (pH-2), 80 °C, 2hr - 21-09-2023

16 S3 PTL36 SLS addition, Sintering (pH-1.5), 80 °C, 1hr

17 S3 PTL 37 SLS addition, Sintering (pH-2), 80 °C, 1hr

18 S3 PTL 38 SLS addition, Sintering (pH-3), 80 °C, 1hr

pH adjustment (pH-1.5), 80 °C, 1hr

19 S3 PTL 39
(Repetition of PTL23)
Sintering (pH-1.5), 80 °C, 1hr
20 S3 PTL 40
(Repetition of PTL26)

Acknowledgements: YCH &CKB team- Vani, Arun Kumar, Pavithra, Sneha……

www.ohmium.com | confidential 5