Gas Chromatography/Mass Spectrometry - GC/MS:

.

.
) ( GLC
(
GSC ) .
.

.

( Mobile phase & flow control ) :

) ( Carrier gas
04 ) ( Psi
04 044 / .
) ( needle- valve ( mass flow
) controller
.
.
.
.
( Sample injection system ) :

.

.
( flash vaporization ) .

 ) ( gas- syringe
.

:

. (
) Stainless steel . 4040
40,0 .


.
( capillary columns ) .
(
) stream splitter ) ( overloading

.

( Solid Support ) :

.
Firebrick , Calcined diatomaceous earth .

 Celite,Chromosorb,Stermachol

) ( Si-OH

) ( Catalize ) ( decomposition
) ( rearrangment .

hexamethyldisilazone .
) ( silanized glass
) ( PTFE .

.

:
.
.
) ( bleed .

. (
) Silicone oil ( greases ) .

( ( Carbowaxes .....


Apiezon L greaze or Silicone oil DC 200 .


.
.
.

 .

. ( 16-30% )
. %04-0 %0
(
) overloading .



.

( Detector ) :

.
:
.
.
.

) ( thermal conductivity ) ( density
) ( flame ionization ( electrolytic
) conductivity ) (x-ray ionization
. .


) ( electron capture .

 :






.