KPT 3013 1

PREPARATION

OF SOLUBLE SALT
KPT 3013 2
Salt Preparation
Salt type
(Na
+
, K
+
, NH
4
)

salt type Except
(Na+, K+, NH4)

Soluble salts
Insoluble salts


Acid +Alkaline

Acid + Metallic oxide
Acid + metallic carbonate
Acid + Metal
KPT 3013 3
Acid + Alkali Salt
HCl + NaOH NaCl + H
2
O
KOH + HBr KBr + H2O
Neutralization reaction
acid + alkali react with each other
form salt & water
H
+
(acid) + OH
-
(alkali) H
2
O(water
Cl
-
(-ve of acid) + Na (+ve from alkali)
salt(NaCl)
KPT 3013 4
(HCl + NaOH) NaCl
Titration method
Evaporation/Heating
Cooling/crystallization
Filtration
Dry
KPT 3013 5
Add metallic
oxide/metal/carbonate oxide
Heating
Filtration
Zn + 2HCl ZnCl
2
+ H
2
Recrystallisation
KPT 3013 6
Heating Filtration Evaporation
Dry
Filtration
KPT 3013 7
Titration
Burette
HCl
Retort stand
25 ml

NaOH +
phenolphthalein
(2 drops)
Erlenmeyer
Flask
KPT 3013 8
Evaporation/Heating
Heat
Triport
Stand
Heat the salt
solution until
saturated~1/3
from initial volume
KPT 3013 9
Cooling/crystallization
Salt
Crystal
Crystallization
KPT 3013 10
Filtration
Salt crystal
Filter paper
Filter funnel
Filtered
solution
KPT 3013 11
Dry
Filter paper
Soluble salt
crystal


Dried by
filter paper

KPT 3013 12
Add metallic metal/metal/metallic
carbonate powder until saturated
Rode glass
30ml acid
Metallic metal
CuO/MgO/ZnO

Metal
Zn/Mg

Metallic carbonate
ZnCO
3
/

MgCO
3
/CuCO
3
KPT 3013 13
Heating
Rode glass
salt solution
Heat
KPT 3013 14
Evaporation
Rode glass
Salt solution
Heat
KPT 3013 15
Filtration
Saturated salt
crystal
Rode glass
Filter paper
Remainder: metallic
oxide/excess metal
Salt solution
KPT 3013 16
Filtration
Rode glass
Pure salt
crystal
salt solution
KPT 3013 17
Salt crystal characteristic
Flatted surface
Straight side
Shape edge
Uniform
geometry
Degree between
neighboring
surface is
constant

KPT 3013 18
KPT 3013 19
Heating
Impurities
salt solution
Heat
KPT 3013 20
Filtration
Rode glass
Impurities
salt solution
Remainder
Salt solution
KPT 3013 21
Evaporation
Heat
Rode glass
Salt
solution
KPT 3013 22
Filtration
Rode glass
Remainder
Salt solution
Impurities
salt solution
KPT 3013 23
Filtration
Rode glass
Pure salt
crystal
salt solution