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    This document describes procedures for iodometric and permanganometric titrations. It contains calculations for standardizing a sodium thiosulfate solution using potassium dichromate and determining the copper content in two samples using iodometry. It also includes the standardization of a potassium manganate solution with sodium oxalate and calculations to determine the iron content in three samples using permanganometry. The percentages of error for the determinations are reported.

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    This document describes procedures for iodometric and permanganometric titrations. It contains calculations for standardizing a sodium thiosulfate solution using potassium dichromate and determining the copper content in two samples using iodometry. It also includes the standardization of a potassium manganate solution with sodium oxalate and calculations to determine the iron content in three samples using permanganometry. The percentages of error for the determinations are reported.

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    5 views4 pages

    4) Lampiran A

    Uploaded by

    nadiadwiayu22
    This document describes procedures for iodometric and permanganometric titrations. It contains calculations for standardizing a sodium thiosulfate solution using potassium dichromate and determining the copper content in two samples using iodometry. It also includes the standardization of a potassium manganate solution with sodium oxalate and calculations to determine the iron content in three samples using permanganometry. The percentages of error for the determinations are reported.

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    of 4

    IODO-IODIMETRI PERMANGANOMETRI

    LEMBAR PERHITUNGAN IODO-IODIMETRI

    1. Standarisasi Na2S2O3 dengan K2Cr2O7 0,01N


    N Na2S2O3

    10 0,01
    12

    = 0,0083 N
    2+

    2. Kadar Cu dalam sampel


    a.

    Sampel I
    Kadar asli

    = 838,6 ppm

    Percobaan 1
    Ppm 1

    = 3,5 x 0,0083 x 63,5 x

    1000
    10

    = 184,46ppm
    Persen error

    = 78,00%

    Percobaan 2
    Ppm 2

    = 3,2 x 0,0083 x 63,5 x

    1000
    10

    = 168,65ppm
    Persen error

    = 79,8%

    Percobaan 3
    Ppm 3

    = 3,3 x 0,0083 x 63,5 x

    1000
    10

    = 173,92ppm
    Persen error

    b.

    = 79,2%

    Sampel II
    Kadar asli

    = 716,8 ppm

    Percobaan 1
    Ppm 1

    = 3,1 x 0,0083 x 63,5 x

    1000
    10

    = 163,38ppm
    Persen error

    = 77,00%

    Percobaan 2

    LABORATORIUM DASAR TEKNIK KIMIA I

    A-1

    IODO-IODIMETRI PERMANGANOMETRI
    Ppm 2

    = 3,1 x 0,0083 x 63,5 x

    1000
    10

    = 163,38ppm
    Persen error

    = 77,00%

    Percobaan 3
    Ppm 3

    = 3,0 x 0,0083 x 63,5 x

    1000
    10

    = 158,11ppm
    Persen error

    = 78%

    LABORATORIUM DASAR TEKNIK KIMIA I

    A-2

    IODO-IODIMETRI PERMANGANOMETRI
    LEMBAR PERHITUNGAN PERMANGANOMETRI

    1. Standarisasi KMnO4 dengan Na2C2O4 0,01N


    N KMnO4

    10 0,01
    0,7

    = 0,115 N
    2. Kadar Fe dalam sampel

    Sampel I
    Mg zat

    = 8,4 x 0,115 x 56
    = 54,09 mg

    BE zat

    56
    1

    =1
    Kadar

    54,09
    238

    100%

    = 22,7 %
    Persen Error

    = 12,7%

    Sampel II
    Mg zat

    = 5,6 x 0,115 x 56
    = 37,99 mg

    BE zat

    56
    1

    =1
    Kadar

    37,99
    165

    100%

    = 23,02 %
    Persen Error

    = 14,2%

    Sampel III
    Mg zat

    = 7,6 x 0,115 x 56
    = 48,94 mg

    BE zat

    56
    1

    LABORATORIUM DASAR TEKNIK KIMIA I

    A-3

    IODO-IODIMETRI PERMANGANOMETRI
    =1
    Kadar

    48,94
    220

    100%

    = 22,24 %
    Persen Error

    = 10,42%

    LABORATORIUM DASAR TEKNIK KIMIA I

    A-4

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