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TABLE OF CONTENT................................................................................................i
LIST of TABLE...........................................................................................................ii
LIST OF FIGURES....................................................................................................ii
CHAPTER 1..................................................................................................................1
INTRODUCTION.......................................................................................................1
1.1 Background.....................................................................................................1
1.2 Objective..........................................................................................................2
1.3 Operational Definition......................................................................................2
CHAPTER 2..................................................................................................................3
Literature review........................................................................................................3
2.1 Theory A..........................................................................................................3
2.2 Previous Studies.............................................................................................4
CHAPTER 3..................................................................................................................5
Methodology..............................................................................................................5
3.1 Research Design.............................................................................................5
3.2 Data Analysis...................................................................................................5
3.3 Conclusion.......................................................................................................5
Reference..................................................................................................................6
LIST of TABLE
LIST OF FIGURES
Figure 2.1......................................................................................................................3
INTRODUCTION
1.1 Background
Vibrational spectroscopy is one of the use full tools to study small molecules in life
sciences and to characterise unknown chemical compounds.
vibrational spectroscopy is used as a diagnostic tool for the identification of bacteria,
cancerous cells and metabolites in living cells.
The success of vibrational spectroscopy in life sciences is certainly due, largely, to
technical developments leading, for instance, to the commercial availability of lasers
for Raman spectroscopy and rapid-scan interferometric detection systems for Fourier
transform infrared (IR) spectroscopy. In this way, the sensitivity of vibrational
spectroscopy increased considerably, allowing experiments that were hitherto
unimaginable to be carried out.
The enormous success of the union between vibrational spectroscopy and the life
sciences prompted many researchers from very different disciplines to adopt various
IR and Raman spectroscopic techniques for the study of biological systems, thereby
constituting a highly interdisciplinary research area at the interface between physics,
chemistry, and biology.
In all these respects, vibrational spectroscopy offers a variety of advantages.
Firstly, vibrational spectroscopy can contribute to the elucidation of details in the
molecular structures and intermolecular interactions that go far beyond the resolution
of even highly resolved crystal structures. Secondly, unlike NMR spectroscopy,
vibrational spectroscopy is in principle not restricted by the size of the sample and
thus can afford valuable information for small biomolecules in addition to complex
biological systems. Thirdly, vibrational spectroscopic methods are applicable
regardless of the state of the biomolecule, i.e., they can be used to study
1
1.2 Objective
CHAPTER 1
Literature review
2.1 Theory A
2.1.1 Theory AA
Figure 2.1
In this study, a design of experiment (DoE) method was utilised to identify the effect
of air plasma spray (APS) parameters on several
main properties of titanium dioxide (TiO2) coatings. Titanium dioxide (titania)
feedstocks with sizes ranging from 10 mmto 45 mm were sprayed onto the mild steel
substrates with different plasma spraying parameters. A 24 full factorial design was
used to investigate the effects of four varying principal parameters at two levels,
namely, the plasma power (20 and 40KW), the powder feed rate (6 and 22 g/min),
the scanning speed (0.2 and 0.5 m/s), and the number of cycles (10 and 20), on four
important properties of coatings; microhardness, thickness/cycle, deposition
efficiency (DE), and porosity. The results showed that one the most important factor
5
in affecting all responses was the plasma power. It strongly affected the hardness
and the porosity which had a primary effect on the thickness/cycle and the DE
values. In contrast, the interaction of the powder feed rate and the scanning speed
had a negative effects on both thickness/ cycle and DE. The number of cycles has
no profound effect on the considered responses; it can only be used as a factor to
achieve different coating thicknesses. To conclude, a plasma power of 30 kW with a
low level of powder feed rate of 6 g/min and 0.5 m/s of scanning speed is most
preferable to optimise TiO2 coating deposition on mild steels. &(Forghani et al.,
2013)
CHAPTER 2
Methodology
3.3 Conclusion
Reference
Forghani, S. M., Ghazali, M. J., Muchtar, a., Daud, a. R., Yusoff, N. H. N., & Azhari,
C. H. (2013). Effects of plasma spray parameters on TiO2-coated mild steel
using design of experiment (DoE) approach. Ceramics International, 39(3),
31213127. doi:10.1016/j.ceramint.2012.09.092
Yusoff, N. H. N., Ghazali, M. J., Isa, M. C., Daud, a. R., & Muchtar, a. (2013). Effects
of powder size and metallic bonding layer on corrosion behaviour of plasmasprayed Al2O3-13% TiO2 coated mild steel in fresh tropical seawater. Ceramics
International, 39(3), 25272533. doi:10.1016/j.ceramint.2012.09.012