Data File C:\CHEM32\1\DATA\S BENZOATE\THURS-2-G1 2011-11-03 15-15-11\051-0101.

D
Sample Name: sprite
This is a special file, named RPTHEAD.TXT, in the directory of a method
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Instrument 1 11/3/2011 3:31:56 PM Marcus Tin

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Data File C:\CHEM32\1\DATA\S BENZOATE\THURS-2-G1 2011-11-03 15-15-11\051-0101.D

Sample Name: sprite
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=====================================================================
Acq. Operator
: Marcus Tin
Seq. Line :
1
Acq. Instrument : Instrument 1
Location : Vial 51
Injection Date : 11/3/2011 3:15:25 PM
Inj :
1
Inj Volume : 20 l
Sequence File
: C:\Chem32\1\DATA\S BENZOATE\THURS-2-G1 2011-11-03 15-15-11\THURS-2-G1.S
Method
: C:\Chem32\1\DATA\S BENZOATE\THURS-2-G1 2011-11-03 15-15-11\SODIUM BENZOATE.M
Last changed
: 11/3/2011 11:37:15 AM by Marcus Tin
=====================================================================
Module
Type
Firmware rev.
Serial number
--------------------------------------|------|---------------|--------------1200 Binary Pump SL
G1312B A.06.10 [005]
DE63059161
1100/1200 Diode Array Detector SL
G1315C B.01.06 [0001] DE73457836
1200 Column Thermostat SL
G1316B A.06.10 [004]
DE60558946
1200 Autosampler SL
G1329B A.06.10 [006]
DE64155870
Software Revision: Rev. B.03.02 [341] Copyright Agilent Technologies
=====================================================================
Instrument Conditions
Column Temp. (left)
Column Temp. (right)
Pressure
Flow

:
:
:
:
:

At Start
40.0
40.0
91.3
0.800

Detector Lamp Burn Times: Current On-Time

DAD 1, UV Lamp
:
3.06
DAD 1, Visible Lamp
:
OFF

At Stop
40.0
40.0
92.0
0.800

C
C
bar
ml/min

Accumulated On-Time
933.9
h
193.8
h

Solvent Description
:
PMP1 , Solvent A
: H2O - 10mM acetate buffer
PMP1 , Solvent B
: MeOH =====================================================================
Run Logbook
=====================================================================
Method
Method started: line# 1 vial# 51 inj# 1
15:15:15 11/03/11
Method
Instrument running sample Vial 51
15:15:15 11/03/11
PUMP
1 Pressure = 91.3 bar
15:16:29 11/03/11
THM
1 Column temperature = 40.0 C
15:16:29 11/03/11
PUMP
1 Pressure = 92.0 bar
15:31:29 11/03/11
THM
1 Column temperature = 40.0 C
15:31:29 11/03/11
Method
Instrument run completed
15:31:45 11/03/11
Method
Saving Method SODIUM BENZOATE.M
15:31:47 11/03/11
Instrument 1 11/3/2011 3:31:56 PM Marcus Tin

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Data File C:\CHEM32\1\DATA\S BENZOATE\THURS-2-G1 2011-11-03 15-15-11\051-0101.D

Sample Name: sprite
CP Macro
Analyzing rawdata 051-0101.D
15:31:47 11/03/11
=====================================================================
4.778 - Sodium benzoate

DAD1 A, Sig=235,4 Ref=360,100 (051-0101.D)

mAU
80

70

60

50

30

1.542

40

2.725

10

1.816
2.054

20

0
2

10

12

14

=====================================================================
External Standard Report
=====================================================================
Sorted By
Calib. Data Modified
Multiplier
Dilution
Do not use Multiplier

:
Signal
:
Monday, October 31, 2011 2:31:36 PM
:
1.0000
:
1.0000
& Dilution Factor with ISTDs

Signal 1: DAD1 A, Sig=235,4 Ref=360,100

RetTime Type
Area
Amt/Area
Amount
Grp
Name
[min]
[mAU*s]
[mg/L]
-------|------|----------|----------|----------|--|-----------------4.778 BB
556.62683 1.37675e-2
7.66337
Sodium benzoate
Totals :

7.66337

=====================================================================

Instrument 1 11/3/2011 3:31:56 PM Marcus Tin

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min

Data File C:\CHEM32\1\DATA\S BENZOATE\THURS-2-G1 2011-11-03 15-15-11\051-0101.D

Sample Name: sprite
=====================================================================
Calibration Curves
=====================================================================
Area
Sodium benzoate at exp. RT: 4.866
DAD1 A, Sig=235,4 Ref=360,100
5
5000
Correlation:
0.99994
Residual Std. Dev.:
27.08418
4000
Formula: y = mx + b
4
3000
m:
76.60604
b:
-30.43343
2000
3
x:
Amount
2
1000
1
y: Area
Measured point: (7.663, 556.627)

0
0

50
Amount[mg/L]

=====================================================================
*** End of Report ***

Instrument 1 11/3/2011 3:31:56 PM Marcus Tin

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