Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Sample Summary
Weston Solutions, Inc.
Job No:

JB12842

RFP# 234
Sample
Number

Collected
Date
Time By

Matrix
Received Code Type

Client
Sample ID

JB12842-1

08/02/12 15:57

08/03/12 SO

Oil

P001-AQ001-0000-001

JB12842-1A 08/02/12 15:57

08/03/12 AQ

Surface Water

P001-AQ001-0000-001

JB12842-2

08/02/12 16:03

08/03/12 AQ

Surface Water

P001-AQ002-0000-001

JB12842-3

08/02/12 16:06

08/03/12 SO

Oil

P001-AQ003-0000-001

JB12842-3A 08/02/12 16:06

08/03/12 AQ

Surface Water

P001-AQ003-0000-001

JB12842-4

08/02/12 16:25

08/03/12 AQ

Surface Water

P001-AQ004-0000-001

JB12842-5

08/02/12 16:35

08/03/12 AQ

Surface Water

P001-AQ005-0000-001

JB12842-6

08/02/12 16:40

08/03/12 AQ

Surface Water

P001-AQ006-0000-001

JB12842-7

08/02/12 17:00

08/03/12 AQ

Surface Water

P001-AQ007-0000-001

JB12842-8

08/02/12 16:00

08/03/12 SO

Soil

P001-SS001-0002-001

JB12842-9

08/02/12 16:05

08/03/12 SO

Soil

P001-SS002-0002-001

JB12842-10

08/02/12 16:08

08/03/12 SO

Soil

P001-SS003-0002-001

JB12842-11

08/02/12 16:45

08/03/12 SO

Soil

P001-SS004-0002-001

Soil samples reported on a dry weight basis unless otherwise indicated on result page.

Draft: 1 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-AQ001-0000-001
JB12842-1
SO - Oil
SW846 8082A SW846 3580A
RFP# 234

File ID
5G3386.D

DF
1

Analyzed
08/03/12

Initial Weight
0.50 g

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
HQ

Prep Date
08/03/12

Prep Batch
OP58754

Analytical Batch
G5G82

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

1000
1000
1000
1000
1000
1000
1000
1000
1000

260
600
510
320
300
470
330
290
320

ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

98%
77%
124%
88%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
22-141%
22-141%
18-163%
18-163%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 2 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-AQ001-0000-001
JB12842-1A
AQ - Surface Water
SW846 8082A SW846 3510C
RFP# 234

File ID
XX122339.D

DF
1

Analyzed
08/03/12

Initial Volume
200 ml

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
AZ

Prep Date
08/03/12

Prep Batch
OP58746

Analytical Batch
GXX4433

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5

0.64
1.4
1.9
0.43
0.73
0.71
1.0
0.65
0.30

ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

68%
49%
28%
10%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
27-144%
27-144%
10-139%
10-139%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 3 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Page 1 of 1

P001-AQ002-0000-001
JB12842-2
AQ - Surface Water
SW846 8082A SW846 3510C
RFP# 234

Run #1
Run #2 a

File ID
XX122340.D
5G3417.D

DF
1
1

Analyzed
08/03/12
08/04/12

Run #1
Run #2

Initial Volume
945 ml
100 ml

Final Volume
10.0 ml
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
AZ
HQ

Prep Date
08/03/12
08/04/12

Prep Batch
OP58746
OP58522

Analytical Batch
GXX4433
G5G83

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53

0.14
0.29
0.41
0.091
0.15
0.15
0.22
0.14
0.063

ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

Limits

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

69%
76%
4% b
3% b

87%
77%
30%
29%

27-144%
27-144%
10-139%
10-139%

(a) Confirmation run.

(b) Outside control limits due to matrix interference.

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 4 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-AQ003-0000-001
JB12842-3
SO - Oil
SW846 8082A SW846 3580A
RFP# 234

File ID
5G3387.D

DF
1

Analyzed
08/03/12

Initial Weight
0.50 g

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
HQ

Prep Date
08/03/12

Prep Batch
OP58754

Analytical Batch
G5G82

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

1000
1000
1000
1000
1000
1000
1000
1000
1000

260
600
510
320
300
470
330
290
320

ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

96%
72%
151%
86%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
22-141%
22-141%
18-163%
18-163%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 5 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-AQ003-0000-001
JB12842-3A
AQ - Surface Water
SW846 8082A SW846 3510C
RFP# 234

File ID
XX122341.D

DF
1

Analyzed
08/03/12

Initial Volume
200 ml

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
AZ

Prep Date
08/03/12

Prep Batch
OP58746

Analytical Batch
GXX4433

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5

0.64
1.4
1.9
0.43
0.73
0.71
1.0
0.65
0.30

ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

136%
71%
13%
14%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
27-144%
27-144%
10-139%
10-139%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 6 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-AQ004-0000-001
JB12842-4
AQ - Surface Water
SW846 8082A SW846 3510C
RFP# 234

File ID
XX122342.D

DF
1

Analyzed
08/03/12

Initial Volume
940 ml

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
AZ

Prep Date
08/03/12

Prep Batch
OP58746

Analytical Batch
GXX4433

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53

0.14
0.29
0.41
0.091
0.15
0.15
0.22
0.14
0.064

ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

87%
94%
33%
35%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
27-144%
27-144%
10-139%
10-139%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 7 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Page 1 of 1

P001-AQ005-0000-001
JB12842-5
AQ - Surface Water
SW846 8082A SW846 3510C
RFP# 234

Run #1
Run #2 a

File ID
XX122343.D
5G3418.D

DF
1
1

Analyzed
08/03/12
08/04/12

Run #1
Run #2

Initial Volume
945 ml
100 ml

Final Volume
10.0 ml
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
AZ
HQ

Prep Date
08/03/12
08/04/12

Prep Batch
OP58746
OP58522

Analytical Batch
GXX4433
G5G83

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53

0.14
0.29
0.41
0.091
0.15
0.15
0.22
0.14
0.063

ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

Limits

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

144%
68%
5% b
2% b

96%
83%
26%
25%

27-144%
27-144%
10-139%
10-139%

(a) Confirmation run.

(b) Outside control limits due to matrix interference.

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 8 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Page 1 of 1

P001-AQ006-0000-001
JB12842-6
AQ - Surface Water
SW846 8082A SW846 3510C
RFP# 234

Run #1
Run #2 a

File ID
XX122344.D
5G3419.D

DF
1
1

Analyzed
08/03/12
08/04/12

Run #1
Run #2

Initial Volume
930 ml
100 ml

Final Volume
10.0 ml
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
AZ
HQ

Prep Date
08/03/12
08/04/12

Prep Batch
OP58746
OP58522

Analytical Batch
GXX4433
G5G83

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

0.54
0.54
0.54
0.54
0.54
0.54
0.54
0.54
0.54

0.14
0.29
0.41
0.092
0.16
0.15
0.22
0.14
0.065

ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

Limits

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

45%
85%
8% b
8% b

113%
93%
48%
47%

27-144%
27-144%
10-139%
10-139%

(a) Confirmation run.

(b) Outside control limits due to matrix interference.

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 9 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-AQ007-0000-001
JB12842-7
AQ - Surface Water
SW846 8082A SW846 3510C
RFP# 234

File ID
XX122345.D

DF
1

Analyzed
08/03/12

Initial Volume
1000 ml

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: n/a

By
AZ

Prep Date
08/03/12

Prep Batch
OP58746

Analytical Batch
GXX4433

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50

0.13
0.27
0.39
0.086
0.15
0.14
0.21
0.13
0.060

ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

75%
81%
36%
38%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
27-144%
27-144%
10-139%
10-139%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 10 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-SS001-0002-001
JB12842-8
SO - Soil
SW846 8082A SW846 3546
RFP# 234

File ID
5G3390.D

DF
1

Analyzed
08/03/12

Initial Weight
15.0 g

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: 88.4

By
HQ

Prep Date
08/03/12

Prep Batch
OP58748

Analytical Batch
G5G82

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

38
38
38
38
38
38
38
38
38

9.8
23
19
12
11
18
12
11
12

ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

92%
61%
813% a
1083% a

Limits
22-141%
22-141%
18-163%
18-163%

(a) Outside control limits due to matrix interference.

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 11 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-SS002-0002-001
JB12842-9
SO - Soil
SW846 8082A SW846 3546
RFP# 234

File ID
5G3396.D

DF
1

Analyzed
08/04/12

Initial Weight
16.4 g

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: 71.9

By
HQ

Prep Date
08/03/12

Prep Batch
OP58748

Analytical Batch
G5G82

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

42
42
42
42
42
42
42
42
42

11
26
21
13
13
20
14
12
13

ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

79%
75%
96%
93%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
22-141%
22-141%
18-163%
18-163%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 12 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-SS003-0002-001
JB12842-10
SO - Soil
SW846 8082A SW846 3546
RFP# 234

File ID
5G3397.D

DF
1

Analyzed
08/04/12

Initial Weight
16.4 g

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: 79.2

By
HQ

Prep Date
08/03/12

Prep Batch
OP58748

Analytical Batch
G5G82

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
131
ND
ND

38
38
38
38
38
38
38
38
38

10
23
19
12
12
18
13
11
12

ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

85%
67%
86%
80%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
22-141%
22-141%
18-163%
18-163%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 13 of 14

Accutest LabLink@17:54 04-Aug-2012 Preliminary Data

Report of Analysis
Client Sample ID:
Lab Sample ID:
Matrix:
Method:
Project:

Run #1
Run #2

Run #1
Run #2

Page 1 of 1

P001-SS004-0002-001
JB12842-11
SO - Soil
SW846 8082A SW846 3546
RFP# 234

File ID
5G3398.D

DF
1

Analyzed
08/04/12

Initial Weight
15.1 g

Final Volume
10.0 ml

Date Sampled: 08/02/12

Date Received: 08/03/12
Percent Solids: 51.0

By
HQ

Prep Date
08/03/12

Prep Batch
OP58748

Analytical Batch
G5G82

PCB List
CAS No.

Compound

Result

RL

MDL

Units

12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
11100-14-4
37324-23-5

Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1268
Aroclor 1262

ND
ND
ND
ND
ND
ND
ND
ND
ND

65
65
65
65
65
65
65
65
65

17
39
33
21
20
30
21
19
21

ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg

CAS No.

Surrogate Recoveries

Run# 1

Run# 2

877-09-8
877-09-8
2051-24-3
2051-24-3

Tetrachloro-m-xylene
Tetrachloro-m-xylene
Decachlorobiphenyl
Decachlorobiphenyl

78%
88%
79%
83%

ND = Not detected
MDL - Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range

Limits
22-141%
22-141%
18-163%
18-163%

J = Indicates an estimated value

B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound

Draft: 14 of 14