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  • Project: WWW Tannery, 41000451: 5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463

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    Kate McIntosh
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    The document is a laboratory report from TriMatrix Laboratories analyzing soil samples from the WWW Tannery site for hexavalent chromium content. Sample results ranged from 390 to 6600 micrograms per kilogram of soil. One result was qualified due to issues with the quality control batch. The report provides the analytical methods used and details of the samples analyzed.

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    1203091 MDEQ

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    The document is a laboratory report from TriMatrix Laboratories analyzing soil samples from the WWW Tannery site for hexavalent chromium content. Sample results ranged from 390 to 6600 micrograms per kilogram of soil. One result was qualified due to issues with the quality control batch. The report provides the analytical methods used and details of the samples analyzed.

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    Attribution Non-Commercial (BY-NC)
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    17 views15 pages

    Project: WWW Tannery, 41000451: 5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463

    Uploaded by

    Kate McIntosh
    The document is a laboratory report from TriMatrix Laboratories analyzing soil samples from the WWW Tannery site for hexavalent chromium content. Sample results ranged from 390 to 6600 micrograms per kilogram of soil. One result was qualified due to issues with the quality control batch. The report provides the analytical methods used and details of the samples analyzed.

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    Attribution Non-Commercial (BY-NC)
    Download as PDF, TXT or read online from Scribd
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    of 15

    March 21, 2012

    MDEQ Attn: Mr. Joseph Walczak 525 W. Allegan St., 4th Floor North Lansing, MI 48909

    Project: WWW Tannery, 41000451 Dear Mr. Joseph Walczak, Enclosed is a copy of the laboratory report for the following work order(s) received by TriMatrix Laboratories: Work Order 1203091 Received 03/06/2012 Description Laboratory Services

    This report relates only to the sample(s) as received. Test results are in compliance with the requirements of the National Environmental Laboratory Accreditation Program (NELAP) and/or one of the following certification programs: ACLASS DoD-ELAP/ISO17025 (#ADE-1542); Arkansas DEP (#10-046-0); Florida DEP (#E87622-24); Georgia EPD (#E87622-24); Illinois DEP (#002841); Kansas DPH (#E-10302); Kentucky DEP (#0021); Louisiana DEP (#03068); Michigan DPH (#0034); Minnesota DPH (#367345); New York ELAP (#44950); North Carolina DNRE (#659); Texas CEQ (#T104704495-11-1); Virginia DCLS (#1239); Wisconsin DNR (#999472650); USDA Soil Import Permit (#P330-09-00163). Any qualification or narration of results, including sample acceptance requirements and test exceptions to the above referenced programs, is presented in the Statement of Data Qualifications section of this report. Estimates of analytical uncertainties and certification documents for the test results contained within this report are available upon request. If you have any questions or require further information, please do not hesitate to contact me. Sincerely,

    Lisa M. Harvey Project Chemist

    Page 1 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 11:15 J.Walczak 03/06/12 17:15

    Client Sample ID: SD1/0-12 1203091-01 Lab Sample ID: Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 47 4200 U RL 0.1 4200 MDL 0.1 380 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:11 HLB 1203179

    Page 2 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 11:15 J.Walczak 03/06/12 17:15

    Client Sample ID: SD1/12-24 Lab Sample ID: 1203091-02 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 77 2600 U RL 0.1 2600 MDL 0.1 230 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:12 HLB 1203179

    Page 3 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 12:00 J.Walczak 03/06/12 17:15

    Client Sample ID: SD2/0-9 Lab Sample ID: 1203091-03 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 36 5600 U RL 0.1 5600 MDL 0.1 510 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:13 HLB 1203179

    Page 4 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 12:00 J.Walczak 03/06/12 17:15

    Client Sample ID: SD2/9-15 Lab Sample ID: 1203091-04 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 55 3700 U RL 0.1 3700 MDL 0.1 330 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:16 HLB 1203179

    Page 5 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 12:30 J.Walczak 03/06/12 17:15

    Client Sample ID: SD3/0-6 Lab Sample ID: 1203091-05 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 36 5500 U RL 0.1 5500 MDL 0.1 490 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:19 HLB 1203179

    Page 6 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 12:30 J.Walczak 03/06/12 17:15

    Client Sample ID: SD3/6-28 Lab Sample ID: 1203091-06 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids *Chromium, Hexavalent Analytical Result 37 5300 U RL 0.1 5300 MDL 0.1 480 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:20 HLB 1203179

    *See Statement of Data Qualifications Page 7 of 15


    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 14:30 J.Walczak 03/06/12 17:15

    Client Sample ID: SD4/0-14 Lab Sample ID: 1203091-07 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 47 390 J RL 0.1 4000 MDL 0.1 360 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:29 HLB 1203179

    Page 8 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 15:05 J.Walczak 03/06/12 17:15

    Client Sample ID: SD5/0-15 Lab Sample ID: 1203091-08 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 30 6600 U RL 0.1 6600 MDL 0.1 600 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:31 HLB 1203179

    Page 9 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 15:05 J.Walczak 03/06/12 17:15

    Client Sample ID: SD5/15-33 Lab Sample ID: 1203091-09 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 38 5200 U RL 0.1 5200 MDL 0.1 470 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:33 HLB 1203179

    Page 10 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    ANALYTICAL REPORT
    Client: Project: MDEQ WWW Tannery, 41000451 Work Order: Description: Sampled: Sampled By: Received: 1203091 Laboratory Services 03/06/12 15:35 J.Walczak 03/06/12 17:15

    Client Sample ID: SD6/0-12 Lab Sample ID: 1203091-10 Matrix: Soil

    Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Analyte Percent Solids Chromium, Hexavalent Analytical Result 59 3400 U RL 0.1 3400 MDL 0.1 300 Unit % ug/kg dry Dilution Factor Method 1 1
    USEPA-3550B USEPA-7196A

    Date Time Analyzed

    By

    QC Batch

    03/12/12 13:10 KCS 1203202 03/12/12 12:34 HLB 1203179

    Page 11 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    QUALITY CONTROL REPORT Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    QC Type Sample Conc. Spike Qty. Result Unit Spike % Rec. Control Limits RPD RPD Limits RL MDL

    Analyte:
    Method Blank

    Chromium, Hexavalent/USEPA-7196A
    Analyzed: 03/12/2012
    2000 U 40000 37000 1800000 1580000 <RLU <RLU <RLU 98300 2860000 1930 J 490000 U 5300 U ug/kg wet ug/kg wet ug/kg wet ug/kg dry ug/kg dry ug/kg dry 92 88 2 0 72-117 72-117 46-126 46-126 20 20 20 20 20

    QC Batch: 1203179 (3060A Alkaline Digestion)


    Laboratory Control Sample Laboratory Control Sample 1203091-06 [SD3/6-28] Matrix Spike Matrix Spike Duplicate

    By: HLB
    2000 2000 200000 4900 490000 5300 180 180 18000 440 44000 480

    Analyte:
    Method Blank

    Percent Solids/USEPA-3550B
    Analyzed: 03/12/2012
    0.1 U 77 78 % % 2 5

    QC Batch: 1203202 (General Inorganic Prep)

    By: KCS
    0.1 0.1 0.1 0.1

    1203091-02 [SD1/12-24] Duplicate

    Page 12 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    STATEMENT OF DATA QUALIFICATIONS Physical/Chemical Parameters by EPA/APHA/ASTM Methods


    Qualification: The post-digestion spike recovery for this sample was outside the control limit. Sample matrix interference is suspected and the reported result must be considered as estimated. Analysis: USEPA-7196A Sample/Analyte: 1203091-06 SD3/6-28 Chromium, Hexavalent

    Qualification: The MS and/or MSD recovery was outside the control limit. The non-spiked sample result is considered estimated. Analysis: USEPA-7196A Sample/Analyte: 1203091-06 SD3/6-28 Chromium, Hexavalent

    Page 13 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    Page 14 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

    Page 15 of 15
    This report shall not be reproduced, except in full, without written authorization of TriMatrix Laboratories, Inc. Individual sample results relate only to the sample tested.

    5560 Corporate Exchange Court SE Grand Rapids, MI 49512 616.975.4500 Fax 616.942.7463 www.trimatrixlabs.com

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