The document provides procedures for determining ash and acid-insoluble ash in materials. To determine ash, 3 g of a material is weighed and incinerated at no more than 450°C until carbon free, then weighed. To determine acid-insoluble ash, the material's ash is boiled with hydrochloric acid for 5 minutes, the insoluble matter is collected and ignited at 500°C, and the weight is calculated. Both procedures aim to precisely measure ash and acid-insoluble ash content in materials.
Original Description:
Determinacion de Ceniza y Ceniza Inoluble en Acido
Original Title
Determinacion de Ceniza y Ceniza Inoluble en Acido
The document provides procedures for determining ash and acid-insoluble ash in materials. To determine ash, 3 g of a material is weighed and incinerated at no more than 450°C until carbon free, then weighed. To determine acid-insoluble ash, the material's ash is boiled with hydrochloric acid for 5 minutes, the insoluble matter is collected and ignited at 500°C, and the weight is calculated. Both procedures aim to precisely measure ash and acid-insoluble ash content in materials.
The document provides procedures for determining ash and acid-insoluble ash in materials. To determine ash, 3 g of a material is weighed and incinerated at no more than 450°C until carbon free, then weighed. To determine acid-insoluble ash, the material's ash is boiled with hydrochloric acid for 5 minutes, the insoluble matter is collected and ignited at 500°C, and the weight is calculated. Both procedures aim to precisely measure ash and acid-insoluble ash content in materials.
The International Pharmacopoeia - Fifth Edition, 2015
4.1 Determination of ash and acid-insoluble ash
4.1 Determination of ash and acid-insoluble ash
Recommended procedures Determination of ash Place about 3 g of the ground material, accurately weighed, or the quantity specified in the monograph, in a suitable tared dish (for example, of silica or platinum), previously ignited, cooled and weighed. Incinerate the material by gradually increasing the heat, not exceeding 450 C, until free from carbon; cool, and weigh. If a carbon-free ash cannot be obtained in this way, exhaust the charred mass with hot water, collect the residue on an ashless filter-paper, incinerate the residue and filter-paper, add the filtrate, evaporate to dryness, and ignite at a temperature not exceeding 450 C. Calculate the content in mg of ash per g of airdried material. Determination of acid-insoluble ash Boil the ash for 5 minutes with 25 mL of hydrochloric acid (~70 g/l) TS; collect the insoluble matter in a sintered crucible, or on an ashless filter-paper, wash with hot water, and ignite at about 500 C to constant weight. Calculate the content in mg of acidinsoluble ash per g of air-dried material.
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