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Ve Rau Qua Xac Dinh Du Luong Thuoc Bao Ve Thuc Vat Phuong Phap Sac Ky Khi tcvn83192010903112
Ve Rau Qua Xac Dinh Du Luong Thuoc Bao Ve Thuc Vat Phuong Phap Sac Ky Khi tcvn83192010903112
- Dung dch chun lm vic 6: cc hot cht difenoconazole v permethrin c nng 0,025
g/ml, cc hot cht cyfluthrin, cypermethrin, fenvalerate, indoxacarb v iprodion c nng 0,02
g/ml, cc hot cht chlorothalonil, -cyhalothrin, -endosulfan, -endosulfan, fipronil v
propiconazole c nng 0,01 g/ml;
Cc dung dch chun lm vic c bo qun 4 oC v c thi hn s dng l 6 thng.
4.11. Kh ni t, c tinh khit khng nh hn 99,999 %.
4.12. Kh hydro, c tinh khit khng nh hn 99,999 %.
4.13. Khng kh nn dng cho thit b sc k kh.
5. Thit b, dng c
S dng cc thit b, dng c ca phng th nghim nh sau:
5.1. Bnh nh mc, dung tch 10 ml, 50 ml v 100 ml.
5.2. Pipet, dung tch 2 ml, 5 ml v 10 ml, chia vch n 0,1 ml.
5.3. Micropipet, dung tch t 50 l n 200 l v t 200 l n 1 000 l.
5.4. Cc ly tm, dung tch 250 ml.
5.5. ng ong, dung tch 50 ml.
5.6. ng nghim, dung tch 15 ml.
5.7. Xyranh, dung tch 10 l, c chia vch n 1 l.
5.8. Cn phn tch, c th cn chnh xc n 0,01 mg.
5.9. Cn k thut, c th cn chnh xc n 0,01 g.
5.10. Thit b ng ha Ultra-Turrax, tc khng nh hn 13 500 r/min.
5.11. Thit b thi kh nit.
5.12. My nghin mu.
5.13. My ly tm, tc khng nh hn 2 000 r/min, c ng ly tm dung tch 250 ml.
5.14. Thit b sc k kh 1, c trang b nh sau:
- Bung bm mu chia dng v khng chia dng;
- Detector quang k ngn la, knh lc phospho (FPD/P);
- Ct mao qun DB-5, c chiu di 30 m, ng knh 0,32 mm, chiu dy pha tnh 0,25 m, hoc
loi tng ng;
- My vi tnh.
5.15. Thit b sc k kh 2, c trang b nh sau:
- Bung bm mu chia dng v khng chia dng;
- Detector cng kt in t (ECD);
- Ct mao qun DB-5, c chiu di 30 m, ng knh 0,32 mm, chiu dy pha tnh 0,25 m, hoc
loi tng ng;
- My vi tnh.
6. Ly mu
Vic ly mu khng c quy nh trong tiu chun ny. Nn ly mu theo TCVN 5139:2008
(CAC/GL 33-1999) Phng php khuyn co ly mu xc nh d lng thuc bo v thc
vt ph hp vi cc gii hn d lng ti a (MRL).
240 oC;
Th tch bm mu:
Nhit ct tch:
Tc kh mang (N2):
2 ml/min;
220 oC;
Tc kh hydro (H2):
75 ml/min;
100 ml/min;
Tc nit b tr:
60 ml/min.
7.6.1. Thit b sc k kh 2
Nhit bung bm mu:
240 oC;
Th tch bm mu:
Nhit ct tch:
2 ml/min;
300 oC;
Tc nit b tr:
60 ml/min.
VE V1
P
V2 m 100
Trong :
Xo l nng tng thuc BVTV (4.7) trong mu th c xc nh theo 7.8, tnh bng microgam
trn mililit (g/ml);
VE l th tch phn mu th thu c (xem 7.3), tnh bng mililit (ml);
V1 l th tch dch chit thu c (xem 7.3), tnh bng mililt (ml);
V2 l th tch dch chit c ly ra thi kh (xem 7.3), tnh bng mililt (ml);
m l khi lng mu th, tnh bng gam (g);
P l tinh khit ca cht chun, tnh bng phn trm (%).
9. Hiu sut thu hi v gii hn xc nh
9.1. Hiu sut thu hi ca phng php: t 70 % n 110 %.
9.2. Gii hn nh lng ca phng php (LOQ)
- i vi acephate, chlorpyriphos, diazinon, dimethoate, fenitrothion, profenophos, methidathion,
iprodion, cyfluthrin, cypermethrin, fenvalerate, permethrin, difenoconazole, indoxacarb: 0,05
mg/kg;
- i vi chlorothalonil, -endosulfan, -endosulfan, fipronil, lambda cyhalothrin, propiconazole:
0,02 mg/kg.
10. Bo co th nghim
Bo co th nghim phi ghi r: