LAMPIRAN Perhitungan Resin Urea Formaldehid

LAMPIRAN II
PERHITUNGAN
BM Formaldehid
30 gr/ml
BM Urea
60,06 gr/ml
BM Amoniak
17,031 gr./ml
Densitas Amoniak
0,86 kg/ml
A.
Perhitungan Jumlah Formaldehid
Massa larutan formaldehid

m
= v
= 1,10185 gr/ml 100ml
= 110,185 gram
Massa formaldehid
= % massa larutan formaldehid

= 40% 110,185 gram
= 44,074 gram
Mol formaldehid
=
massa formaldehid
BM formaldehid
mol
44,074 gram
30 gr /mol
mol
= 1,469 mol
B.
Penentuan Jumlah Urea
mol
U
F
= 1,2
Mol urea
Mol urea
mol formaldehid
1,2
1,469 mol
1,2
= 1,224 mol
Massa urea
Massa urea
Massa urea
= mol urea BM urea

= 1,224 mol 60,06 gr/mol
Massa urea = 73,51 gram

Massa katalis NH3
Massa katalis NH3 = 5% X
Massa katalis NH3 = 0,05x
Massa buffering agent
Massa buffering agent = 5% 5%

Massa buffering agent = 0,05 0,05
Massa buffering agent = 0, 0025
Massa total
Massa total = massa formaldehid + massa urea + massa NH3 + massa Na2CO3
Massa total = 44,074 gr +73,51 gr + 0,05 gr + 0,0025x
x-1
= 117,637
0,9x
= 117,637
x
= 130,707 gram
Massa katalis NH3 yang ditambahkan
Massa katalis = 5% massa total
Massa katalis = 0,05 130,707 gr
Massa katalis = 6,535 gram
NH3 yang digunakan 25%
massa katalis yang ditambahkan
Massa NH3 =
25
Massa NH3
6,535 gram
25
Massa NH3 = 26, 14 gram

Volume NH3
massa NH 3 yang digunakan
Volume NH3 =
25
Volume NH3 =
26, 14 gram
25
Volume NH3 = 30,395 ml
Massa Na2CO3
Massa Na2CO3 = 5% massa total katalis

Massa Na CO = 0,05 6,535 gr
2
Massa Na2CO3 = 0,327 gram

C.
1.
Analisa Sampel 0
Analisa Densitas
Picnometer kosong
= 12,185 gram
Picnometer + air
= 17,559 gram
(Picnometer + air) - Picnometer kosong
= 17,559 gram - 12,185 gram

= 5,374 gram
Picnometer + sampel 0
= 17,926 gram
(Picnometer + sampel 0) - Picnometer kosong
= 17,926 gram - 12,185 gram

= 5,741 gram
Sampel 0
2.
massa sampel 0
massa air
5,741 gram
5,374 gram
1,0683 gram
Analisa Viskositas
K (air)
= 0,25 sekon
t sampel 0
= 0,24 sekon
Sg sampel 0
densitas sampel
densitas air
1,0683 gram
0,99
= 1,079
sampel 0
= k sg sampel t
= 0,25 1,079 0,24
= 0,065
3.
4.
Analisa pH
nilai pH = 10 yang menandakan larutan bersifat basa
Analisa Kadar Formaldehid Bebas
Gr CH 2 O
3 x ml HCl x HCl
=
ml sampe 0
ml larutan
Gr CH 2 O
40 ml
Gr CH2O
m HCl = ml titrasi
= 18,3 ml
3 x 0,6 ml x 0,5 N
10 ml
=
=
0,09 40
3,6 gram
ml titrasi blanko
17,7 ml
= 0,6 ml
D.
1.
Analisa Sampel 1
Analisa Densitas
Picnometer kosong
= 12,185 gram
Picnometer + air
= 17,559 gram
= 17,559 gram - 12,185 gram

= 5,374 gram
= 18,329 gram
= 18,329 gram - 12,185 gram

= 6,144 gram
Sampel 1
2.
massa sampel 1
massa air
6,144 gram
5,374 gram
1,1432 gram
Analisa Viskositas
K (air)
= 0,25 sekon
t sampel 1
= 0,22 sekon
Sg sampel 1
densitas sampel
densitas air
1,1432 gram
0,99
=1,155
sampel 1
= k sg sampel t
= 0,25 1,155 0,22
= 0,0635
3.
4.
Analisa pH
Gr CH 2 O
3 x ml HCl x HCl
=
ml sampe1
ml larutan
Gr CH 2 O
40 ml
Gr CH2O
m HCl = ml titrasi
= 18 ml
3 x 0,5 ml x 0,5 N
10 ml
=
=
0,075 40
3 gram
ml titrasi blanko
17,5 ml
= 0,5 ml
E.
1.
Analisa Sampel 2
Analisa Densitas
Picnometer kosong
= 12,185 gram
Picnometer + air
= 17,559 gram
= 17,559 gram - 12,185 gram

= 5,374 gram
= 18,367 gram
= 18,367 gram - 12,185 gram

= 6,182 gram
Sampel 2
massa sampel 2
massa air
6,182 gram
5,374 gram
=
=
2.
1,150 gram
Analisa Viskositas
K (air)
= 0,25 sekon
t sampel 2
= 0,33 sekon
Sg sampel 2
densitas sampel
densitas air
1,1432 gram
0,99
=1,155
sampel 2
= k sg sampel t
= 0,25 1,150 0,22
=0,096
3.
4.
Analisa pH
Gr CH 2 O
3 x ml HCl x HCl
=
ml sampe2
ml larutan
Gr CH 2 O
40 ml
Gr CH2O
m HCl = ml titrasi
= 18 ml
3 x 0,4 ml x 0,5 N
10 ml
0,06 40
2,4 gram
ml titrasi blanko
17,6 ml
= 0,4 ml
F.
1.
Analisa Sampel 3
Analisa Densitas
Picnometer kosong
= 12,185 gram
Picnometer + air
= 17,559 gram
= 17,559 gram - 12,185 gram

= 5,374 gram
= 18,370 gram
= 18,370 gram - 12,185 gram

= 6,185 gram
Sampel 3
massa sampel 3
massa air
6,185 gram
5,374 gram
=
2.
1,151 gram
Analisa Viskositas
K (air)
= 0,25 sekon
t sampel 3
= 0,34 sekon
Sg sampel 3
densitas sampel
densitas air
1,151 gram
0,99
= 1,163
sampel 3
= k sg sampel t
= 0,25 1,163 0,34
= 0,098
3.
4.
Analisa pH
Gr CH 2 O
3 x ml HCl x HCl
ml sampe 3
ml larutan =
Gr CH 2 O
40,5 ml
Gr CH2O
=
=
3 x 0,5 ml x 0,5 N
10 ml
3,038 40,5
m HCl = ml titrasi
= 19 ml
3,038 gram
ml titrasi blanko
18,5 ml
= 0,5 ml
G.
1.
Analisa Sampel 4
Analisa Densitas
Picnometer kosong
= 12,185 gram
Picnometer + air
= 17,559 gram
= 17,559 gram - 12,185 gram

= 5,374 gram
= 18,378 gram
= 18,378 gram - 12,185 gram

= 6,193 gram
Sampel 4
massa sampel 4
massa air
6,193 gram
5,374 gram
=
2.
1,152 gram
Analisa Viskositas
K (air)
= 0,25 sekon
t sampel 4
= 0,32 sekon
Sg sampel 4
densitas sampel
densitas air
1,152 gram
0,99
= 1,164
sampel 4
= k x sg sampel x t
= 0,25 x 1,164 x 0,32
= 0,093
3.
Analisa pH
4.

Gr CH 2 O
3 x ml HCl x HCl
=
ml sampe 4
ml larutan
Gr CH 2 O
40,5 ml
Gr CH2O
m HCl = ml titrasi
= 18 ml
3 x 0,3 ml x 0,5 N
10 ml
=
=
=
0,045 x 40,5
1,823 gram
ml titrasi blanko
17,7 ml
= 0,3 ml
H.
1.
Analisa Sampel 5
Analisa Densitas
Picnometer kosong
= 12,185 gram
Picnometer + air
= 17,559 gram
= 17,559 gram - 12,185 gram

= 5,374 gram
= 18,383 gram
= 18,383 gram - 12,185 gram

= 6,198 gram
Sampel 5
massa sampel 5
massa air
6,198 gram
5,374 gram
=
2.
1,153 gram
Analisa Viskositas
K (air)
= 0,25 sekon
t sampel 5
= 0,32 sekon
Sg sampel 5
densitas sampel
densitas air
1,153 gram
0,99
= 1,165
sampel 5
= k sg sampel t
= 0,25 1,165 0,32
= 0,093
3.
4.
Analisa pH
Gr CH 2 O
3 x ml HCl x HCl
=
ml sampe 5
ml larutan
Gr CH 2 O
41ml
Gr CH2O
m HCl = ml titrasi
= 18 ml
3 x 0,3 ml x 0,5 N
10 ml
=
=
=
0,045 x 41
1,845 gram
ml titrasi blanko
17,7 ml
= 0,3 ml
I.
1.
Analisa Sampel 6
Analisa Densitas
Picnometer kosong
= 12,185 gram
Picnometer + air
= 17,559 gram
= 17,559 gram - 12,185 gram

= 5,374 gram
= 18,391 gram
= 18,391 gram - 12,185 gram

= 6,206 gram
Sampel 6
massa sampel 6
massa air
6,206 gram
5,374 gram
=
2.
1,155 gram
Analisa Viskositas
K (air)
= 0,25 sekon
t sampel 6
= 0,36 sekon
Sg sampel 6
densitas sampel
densitas air
1,155 gram
0,99
= 1,166
sampel 6
= k sg sampel t
= 0,25 1,166 0,33
= 1,105
3.
4.
Analisa pH
Gr CH 2 O
3 x ml HCl x HCl
=
ml sampe 6
ml larutan
Gr CH 2 O
40,5 ml
Gr CH2O
m HCl = ml titrasi
= 18 ml
3 x 0,2 ml x 0,5 N
10 ml
0,045 40,5
1,823 gram
ml titrasi blanko
17,8 ml
= 0,2 ml
J.
1.
Analisa Sampel 7
Analisa Densitas
Picnometer kosong
= 12,185 gram
Picnometer + air
= 17,559 gram
= 17,559 gram - 12,185 gram

= 5,374 gram
= 18,398 gram
= 18,398 gram - 12,185 gram

= 6,213 gram
Sampel 7
massa sampel 7
massa air
6,213 gram
5,374 gram
=
2.
1,156 gram
Analisa Viskositas
K (air)
= 0,25 sekon
t sampel 7
= 0,36 sekon
Sg sampel 7
densitas sampel
densitas air
1,156 gram
0,99
= 1,168
sampel 7
= k sg sampel t
= 0,25 1,168 0,36
= 1,105
3.
4.
Analisa pH
Gr CH 2 O
3 x ml HCl x HCl
=
ml sampe 6
ml larutan
Gr CH 2 O
40 ml
Gr CH2O
m HCl = ml titrasi
= 18 ml
= 0,2 ml
3 x 0,2 ml x 0,5 N
10 ml
=
=
0,03 x 40
1,2 gram
ml titrasi blanko
17,8 ml

LAMPIRAN Perhitungan Resin Urea Formaldehid

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LAMPIRAN Perhitungan Resin Urea Formaldehid

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LAMPIRAN II

Perhitungan Jumlah Formaldehid

Massa larutan formaldehid

= 1,10185 gr/ml 100ml

= % massa larutan formaldehid

Penentuan Jumlah Urea

= mol urea BM urea

Massa urea = 73,51 gram

Massa buffering agent = 5% 5%

Massa NH3 = 26, 14 gram

Volume NH3 = 30,395 ml

Massa Na2CO3 = 5% massa total katalis

Massa Na2CO3 = 0,327 gram

(Picnometer + air) - Picnometer kosong

= 17,559 gram - 12,185 gram

(Picnometer + sampel 0) - Picnometer kosong

= 17,926 gram - 12,185 gram

(Picnometer + air) - Picnometer kosong

= 17,559 gram - 12,185 gram

(Picnometer + sampel 1) - Picnometer kosong

= 18,329 gram - 12,185 gram

(Picnometer + air) - Picnometer kosong

= 17,559 gram - 12,185 gram

(Picnometer + sampel 2) - Picnometer kosong

= 18,367 gram - 12,185 gram

(Picnometer + air) - Picnometer kosong

= 17,559 gram - 12,185 gram

(Picnometer + sampel 3) - Picnometer kosong

= 18,370 gram - 12,185 gram

(Picnometer + air) - Picnometer kosong

= 17,559 gram - 12,185 gram

(Picnometer + sampel 4) - Picnometer kosong

= 18,378 gram - 12,185 gram

nilai pH = 8 yang menandakan larutan bersifat basa

(Picnometer + air) - Picnometer kosong

= 17,559 gram - 12,185 gram

(Picnometer + sampel 5) - Picnometer kosong

= 18,383 gram - 12,185 gram

(Picnometer + air) - Picnometer kosong

= 17,559 gram - 12,185 gram

(Picnometer + sampel 6) - Picnometer kosong

= 18,391 gram - 12,185 gram

(Picnometer + air) - Picnometer kosong

= 17,559 gram - 12,185 gram

(Picnometer + sampel 7) - Picnometer kosong

= 18,398 gram - 12,185 gram

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