DATA PENGAMATAN

Dapar Fosfat pH 7.4 (F1)

NaOH 0.2N + kH2Po4 0.2 M up to 200 ml aq

39.1ml 50ml 100ml

20ml 25ml

NaOH

0.2N = g/ 40 x 1000/20 x 1

= 0.16g in 20ml

kH2Po4

0.2M = g/150 x 1000/25

=0.75g in 25ml

Larutan baku

1ppm = 1mg/ L

500ppm = 50mg/100ml

5ppm = 1ml

500ppm(x) =10ppm(100ml)

X=2ml (from 500ppm up to 100ml)

1. 2ppm
10ppm(x) = 2ppm(20ml)
X= 4ml
2. 4ppm
10ppm(x)=4ppm(20ml)
X=8ml

3. 6ppm
10ppm (x)= 6ppm(20ml)
X= 12ml
4. 8ppm
10ppm(x)=8ppm(20ml)
X= 16ml

5. 10ppm
X=20ml

X 1 2 3

2ppm 0.626 0.0622 0.0633 0.0627

4ppm 0.115 0.1148 0.1123 0.1142

6ppm 0.1596 0.1613 0.1600 0.1603

8ppm 0.2209 0.2226 0.2232 0.2222

10ppm 0.2995 0.2992 0.3017 0.3001

Find
y=ax+b
r = 0.9943
a = -2.94 x 10-3
b = 0.02914
 Kurva kalibrasi Asam Salisilat
0.35

0.3

0.25

0.2

0.15

0.1

0.05

0
2 ppm 4 ppm 6 ppm 8 ppm 10ppm