(Reaffirmed 0) ,aqaq qqq lS 16481 : 2016

lndian Standard

qqG aTrenkd +trffi

-ftFc
fr sw+rT + frq fr*F* veq
ird -tdtrrfu

Textiles Synthetic Micro-Fibres for

-
Use in Cement Based Matrix
Specification
-

ICS 59 060 20i91.100.40

o Bts 2016

!]TIdTq qT{EF 4{I

BI]REAI] OF TNDIAN STANDARDS
q=d, taa. t ,t-Tt, 7't ETr :r c- ,uL,-
I!I]ANAK BHAVAN 9 BAHADUR SHAH ZAFAR N4ARG
FVn DFtII 1t 0002
N
,/tuu b s oro i !!rI4!1!!!!l!!!E t!
Technical Textiles for Build Tech SectionaL
Co nittee TXD 34

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 lS 1618 ri 1016

Lndian Slandurcl
rN
SYNTHETIC MICRO-FIBREIIoi!]lsE
TEXTILES
' -
"" Cit-""r-eesso MATRI*
- 'PECIFICATI.N
1 scopE tr'
H"::,ij"li"T;,'jil:Jtl',i L1[ii;;ii3"llixlii
thE ,,andar,l p"e,cnbe' ph)s:c
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:#il;.,;;,;"*^',"" *ii;ll,:iilii*:l*:"1;ili::,i'"i',',,'""ii.::::
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2 REFERENCES NoTE-1hc.,tu vato r Llirn e,eL srlLbe{rlcularedassir'n
sior'
the,,x-drrd(.'s'.J:n A'i'cx \ 'o'l'i ;'-^"'"''
p'ov
' (nLc .'\I' " ; ll-.],'."" r. r0 ribrc Disp(r\ion uucl'rs and d*r"'b"rron o'
"';.; i;",; :.,," 'e',,a",0' clrre '''E.orprbr:a Jr -
oL.tJ,c or 'o e: 'r:fo'rr\
,. ' :.';;,"t*-;.
l[".|1,,*.',,j,...,..:."'"
"i.:,""' ".
^]l l]::,:1,:: :;d',": ,;:",.","y,,
rhLoasrcn'triFtrrseJ.:l
cenn.u]ed^m,,'\.J.''Ir '
d':ono iDes 'rr(''rB
.';,;: ;; :";""""'"""' 1l'"".,".'"-L* ,es""'
,i,i'."",r.a:rcencoL,)r,ed ":":..l t"l.,:: .l',",..",r."r,.;, ,u'esrj.v,.,br(i '"eLr''t
rccen s.iu L' !' "
r''osL "
uoss,ui|lry olrolrlr'ng lhc l;a -d , re,flr J rLr d .pe. ',or

j rERNIrNol.oGY ':" ...r,1 ';il;";i;;'J'rtlr dispersed randomrv odented

lo. n(p, po.. ol ' ')u'dardL" 'or'o{'rgn'll'iLroo strensth

shrllaplly. [kx rnl srcngth-- The.flexurai
'....- ,,,'il'' 3.12

,.,nu*,,""**n'"*"-1"s -,r;it,"t,l"''"
bv r bbrng afd rrrc"uLr J:i:l:r;*i::;n,:-i:r'[|:d,::l:,li'
!esist being worn owrv
':'.,, (1)
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- .ar.
o
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rtd":','' 'i'',."". .,"
.'- ,.,,,,*'," .bovc
* . ,,.r
'empc*,turc
- rhe
vr.e' i,
Do ,,,e
oLre. ,h, r.
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a.,,,,,-ed,.,r :.J'.".;::, ,;1,',,....i.',a'dd,rdb"."e|r'll-n'
rr"lo,. i"g; , ,r\,ng'o I 'od i\ r' p'oD- '' , ,' ,,, t.,,,r. t. -no" i ,\(;1, " -""c
"ia erc, lrixed wirh !(meir
"".r "". tht NbbeD'orvtsco-
3.1Asgregaie_ snnd, sravcl. '*",'crlled
to forn concrete.
""iin.,Jn*r,.
elastic state'
equrvxlcnt energy consurned to
3.4 Aspect Rntio Tlre raiio ol lenglh to l.l.l lmlr(t Rcshtancc -The
-
offibre. i,,.,".i'" 'p'"r'*' of blows or the nlLmber in a
diameler

3.scompressivcs,re g,h-':".T:::tHrli::,""l
wh'n fl]c klii:i*:'*l?;::'I::eaerescribedleverof
.niaxial iompressr"e stl!ss reach(d
The.Latio of a solution\
fails completelv. 3.15 Intrinsic vhcosity -

i.6 co -
cre,e:\r
' \"1 c or Po rralc cc n:r
:;:ilcT:; l:i :;ii;j'; ;. ",: ":l;:i:"',:l ::[:l; ;
."4,."'o'''r"'r'''' v la' t'rLcr\rr'*'''i i.,'i,r".t...i" *"*,
rcac! and harden'

,.,,.,,"*,,.,"**.-S"1.:::i:t:1,:::T:l li:illlli::r;i',ji;:i,:,.H,:llli:::Ti:i"'
corcrci.ni$reJret'rer"-"'"pll"'l::;;i;\ in lensrle \rrr .,;^;;,.i,i.,'",l.,,,cIo,,qJrdorcr
c

.4,.1,*t '"*t - t*""se

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(01'-cl '
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ir erlrerseo rn NLpr' lli;.;'.;, s,;"" nrr'o 48 1nd'tsc rrr\ "r'
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led ";"'.iil;:;.,;.',,.
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'
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r'!rr
products casl al a site remotc I""t,-"r,_.".,
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3.19 Precast-CoDcrete
.l'i.-',. rdr, De -" Ji'P'r'e'r n 'h'
tom the fi!41 instalhtion' '::;;,.;; "J'iLo'.. ,a .,a e n,inr'f:n':o(r'al
1 ,n sl,ritrL!!c cnJ lcml(rxlure Crnckir'g - ,,
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r,t''' 's
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:'".i1;;";'; d..'o crlge'r'o 't "','ler 4 l.I'lhe r.Pr ''!''t' rior l'" llL''P
\ lt \DcLrii( ':r.'\rr\
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lor eath Lor

_ t '" frorrr thc p"ll nto suppher
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dl\ i'1'd b-v NOTES
l.2l Tcnrcil{ - ! The lP drrl n,luo rre ro' rc')!LeLl
; nrn.;." r' ' 'r''
"
1.:{ l..n.ilc:rrn,rh * L ('' r l. .
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Alk'lis
r "r ' lc:'' '0u'rc-' "''rr':'
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,],- :',;,^"";.;. "',r''|( dLv'Ir''Ir'c'"r
\' """' Annex D'
prescribed in
r)il'rrirrr'rlcll"t'l'ri'nnlrh' lir"''
,.:'"ir,..,
ls
4.5 Resistrnce lo Acids
n' ' rncir
o0
exfressc,i d lercenuge
('rlr(rt\ - l '' " \ nrh-uc .'u'e' J'a'r rP'drn I lM'r,e.'edpcrc' n'e' od
1]fi \\',rrt \b'otl'li\(
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,,,',.: ..;': ".'et' prescribed in ADnex E'
'.o, ,,,r,,'.-:J
rLit
,;D(1i1roI r,lrlJlLer ' 5n(i1l''l 4.6 Resistruce to Agcing
"'1.,-;
.1 R liQ tit R ti i\1ll \T S
rnc,c..pcc,,cn,t,l"' io agerng l,l":"ll'lar ";'llil
"L" r-, c--'lr\vhen strbjected
I

eJe' ibed'r' ls -u'u rPan 8i

.1.1Tll).s ol S:nthctic librts L]scd in SecortdrrY ,.1,'"ii'bi," t'"'"'" o ,, cn'irc
Rtirlotctnrcnt ol Cortcrttc 1i,,ii",.,^ -' .1," m,"''e'|'I oi'hei' srn

requlrclDenrr tbr slrergth

.1.1.1 lhis staldard mrnrlv corers
2
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6 SAMPLING ( ctause 1 .l)
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 IS 16{81 : lll t6

ANNEX A
(Clause 2)

LIST OF REFDRRDD INDIAN STANDARDS

-as,vr. Iitle /s Mo' Title

le sile 1959 Methods of sanpiitrg and analvsis of
235: 1989 Texriie fibres - 1199:
conqete
characteristics ofirdividual lLbres
-
Meihodsfordeterniination(frsr2336(P3riI):Metlrodsoflestforaggregatesfor
Part I Particle size aDd
rertstotl) 196i corcrete:
383 : 1970 ipecin"atlo" ro' coarse ana ft'" shape

ft*'t *u'*f ***t f"' 63 9 : 197 I

5 Method for co dilioring of texiiles
"ig..e"* Method lor detemiDation of wooi
6919 : 1973
corcrete (s€.ond /"!isroll)
fibre dia eter bf anflow nlethod
456:2000 i"i" "ip*"i"" for plair and ?016(PaIts)r Methods of test for coated and fl eared
rei,,roLc.a co'cLet" iloffrr' re"sio')
1975 fabics: Part 8 Accelerated ageirg
460 (Pn 2) : Specification for iest sieves: larl i
];;;-'- i'".i","'"a pL"" ril''a 7e03:2011 rextiies-rapauhs nmde flomhigh
misian) "u 'i"*' densitv lolvethvlene woven fabic
of Specificstion (&lr/d re'isr"')
516 | 1959 Methods of test tbr strength
concrete 9l0l l9T9 .. C-orn
.
rete adrn iltu res
- SpecificalioD

iJen'rl(r'ior ofre'rrr' tttr't"'\t-o'l

oo7 i98l \4erhods lor
Metlruds ofJesr lor mdl-llade staple
1r''-t'9
1070: 1992
*isian)
l'ibers

Rcagent
(wjth snpplement) 7':'' ^. rOOl+

gradewaler- Specific .,,".. i131i. *,: [1lffS',::ffXlj't'il:if,.11

grade specification (/ia' /e"sio'1)
lfii;.trcrisian) ,
-',ll'' .',]!:, -
:. "
';,.'t ".
/ru.i
ittil
"'i':'
::,1 l
':ltt:-
AN\!]\ I}
(C/rrrrse 4.1.1)

T\1,[soIs\'\lHl]IICI_lBltllstlsrDl\slco\D'\ltYlluh-rollcL]lll\lolr(loN(]]rtl['
B-2.2 Do specify synthelic fibres Ior'
B-1 CENI]R.\I
r) reduchs concrete crackirg due to plastic
There are two different phvsicaL fibre forms: i concrcte andllaslers;
slriDkase
rnorro',-.rror fib.es'r rrrr.ifhnrcr'r fi"re'fl d fiL'rrl 'I
no,e' nrodJccd ,'onr ttpe. \4o'r "\'' r'e r' lihk b, ,Lt'r. r err'i'1e ^"e me"l a"
'ppi?..rrg or
,",rrc:.iors ".e ar r\" lot .lose' 0'0u perc'rr 'o *codar\ - rci foIc'r"r: P c 'rl)
re: ,.or

o'jper.- , o, 'ott,re Je,er.J-rs 'rpo ""e I peolfihrP

.",,"r.urc " oc^ ,'q "lic ' colsidereo
r.iri;. t"u"L. tlt""r,.ngrn orthe concrete is coDsidered in,poftanii
uraffected. aDd clack control characteristics
xre c) red{cing concrcte permeabilily due io better
contrcl over oPening of cmcks;
$rasior of
B-2 IN,TPOR'IANT INFORX{AIION IOR USE OI' d) enlixnc g impact and resistance

SYNTI1ETIC IItBRtrS
e) fibrc application rcquiriDg notrnetallic orno'1
B'2.1 Svn.nert. liDL \ 'fi' " ri ' erl rrr!e
c-t1 \igr corosive secondary reillorce enti
.,'.*1. c. ro-,, e .. )o,.1' 1ce. b'' do ror' n .Lnejrie r.rr\ Ce ' 'n r''d lor rro '''r''
-r..rmre" -r.. i_r-c ' or"r' c ^l !r
r . ' bP Ll '"
:" rebound loss in shotcrete Gpraved coDcrete)
I''".,,r ..',on ll'e de.'le ' -o \e r B" l
qu
and B-2.2 caD hel! lo decide their nse
for I partic lar
g) rpllicaiioDs requiriDg
lS 16481 :2016
cliemicaLs
reinforcement which resists rlkalis' ntorcenreirtor it"
reohcLn: sn rlct!rJl steel Le
eDd chLorides
ncfo,ridrrcc dtrr ng se tre lrtc
B-2.3 Thc use of svnlhelic
fibres slionld be avoided
ernalcing compressivc, rensile or
flexlLral

slrengih ol corcretc; and

,r !or..oll:rs 'acr,'t; iri I'a'de''cd 'oric-cre ot creef
, rl) elimiDatug ot reducing cutiing
rcsulL,rrg';orne\rennl*rror'5a1dlo"g'c"'

ANTI,X C
(Clausc4l'I)
YIRGIN POLYTS'I]EIt IIBR!]
ACIO CoN1'[NT OT'TTIE
\IIITTIOD oI TES'I' FOIt ISOP}tTTIALIC

.-r Pnr\crrr.' .'-" "r't

:lilll::,1',:',i'::ii:.i':i lili:ii:;J*lI;
1.,!.' "S'
',',",',"'.1.(r'r'
:i."ii .'i ' :,:."': : '

Jl
r' L' -' l 'e i'r
..d.' i . t .' ,( ''rr.'.
r
,..''^., ...r'' _'r'lr "' I ' "''"' t -{ l C'r' t'l'runr:rru:rrl'h {''l:\'
"' er".,L (
;.,,.. '".'f,.' ,.
fre r' L' i JrrJ
'r 'r'r
i,",.,r,ii,,"n,'a,.1,,.,',,,: Jf c-l.: 6,,tpi,xrl coln.,n.60 nr l.rg1h ud l's:l nnn
\ I l\:l l' '' ' \' ' l I
c-2 l'o ll \ lt \l L\\ lolt\lt l n)l : nrl xrLl l0 l'
ri rcrltu LrUlliLU LDe'rr C_11 Disl)e scttc or l'iptlte
C-2.1 1rr.rs! ol sPilLrie 'o| 500 nrj
i" ,"",*n,-" ".."lr\L''.',.r """'"'''''' "- ".] lll c'd 'r vortrruc(ric tirrsk l00 Nr'
r'fer lJiltl f' Lro!'
,',r,"t ," ,,1. ' ""1 C_] 5 l'c'tkc'
nLr 'Lir rr' nscd
a-2..: ll\(lrorif n tr =!r rr J rf\r

."',i,;,, .,,,, , L.r" L ' L erJ5' 1 ' tll:::l: c,r.8 r*ring,cnt!r, 1o nrri.,tin r.r.p'rrlrrrc !r
,,,,,,,.,1 ll. -
.",-"' " '1""'*"1 : .l,1. (LrrlLl:f:l c'l.e.\rrG'|rde DiNrthrr rioptrrrrrit
(DNrr)
. L,rtrLL.Lu Lrr rrursrrr'-Jr llJl
rir c^n Lill ,rist utri.rrls ilr 'ul Gride tlenzll'\tcohol
ii i'ti .""*-"-'- iL) c-'110

r'l ll \l{('r'rd(( hlorolurrrr

c-J full \l'l \l \\lFl\'r't(tl\llo\\L
l{EALl ll lssu[s c-'11]Allcrrdel$l)r{}lll litorte
tik. srlel\,goq!1.s. rfLon. rgi'itl c-].13^lrGrrdcDirDcth!lsuLltrrrte
c-l.l I,rof.rt,t,F-\
hand gloves rc be rsed O\ OII SI'AN D:\RD
C-5 PR I I'r\ Il;\'I I
handled with care'
C-3.2 Classware is to be sot-u1'lo\s
l-ear. cr,eor< to le o twhilc handlmg ol
c-:.: "a'ried
gascylinde. C-5.1 StockDibenz!lStrbtrrxlc(ltrlcrtrrlStindrrd)
bandled with care'
C-3,4 Glasswarc is to be ,,,'" ,,:'_\l
I ' ',. I
olc'rlo'olonr c'"r'e' l" "on "'''
Lr':r.ron D'
a-l-5 I 0r ""
,,.; o , w., i('cu., d '
;;:"':...'-J,,. '/
 rS 16181 :2016

of 2 percent slandard IPA solulion' lf value of 2 0

tihate .liqesr li for 2
'l;i:r:::;.;;: ;.k.;i;.." h Allow
. "'I".:l
rr to cool up ru room
(,ci.,.r) -1.,ng,'.n".rt"'"p9p)rii'1,'1, ;;;;;;;;:;ll',lti:::";ll"';:1.,':Jl.iil:':
,:",".,.J;;.;.,|;;",.,.0r,:a.or,n\aru"r,ererL1
3";:lt,;'JITJ-'| :'" ::l' :lil"i'l: ii:l;l ffi;rl ll:rf
,t " :|i :'1",;;,i.: i;
2ml=xxxxxms. ,"r oibenzyL rt.ohol Add 3 drops of

c-5.2 stock Dimethyl Isopthrlate

(DMI) soluiion ".,[ "aJ, Drgc 't the solltron for t h' Allow it
't*t""L**"
rare.. 2 + 0.0i g ordimethtl""{1"'"'"
!?*ll-li;1 'i,,,':,"';;
ffi*T:::i'Jll:*1Tfl&':,',:':i:,11;t':::ii
^:;:llm#ll;:,ii:"ikl*l
* ."r,ui* p.+** ,, c-s 1 and sh,ke vigolousrv
'":Y'; i"''' r '"'p'"'urion 'n'o e's (hrol ''oe!rh'
,e,nic.r,, , r .h(r nl ,k. t '
r
rl ol' rne ' ' "i
" ' "'
,"..i,'s rt,. fa5l( by ,soplopvl alcolrol.This c-8 cHRoMArocR{pH sETTINGS
trillbe converted to dibenzyl isolthalale (DBL) I
"rl"i"i,,
Iliectoltemperaturc ri00'c
il''l#;;fi;;;i;:.i.ir=xxixx*g
c-s.3 strtr{tard sorutior ror Respo,sc Fictor ::::::,:'J::JJJ"" , ii:':
(
T?\e 1rn, or colf"on piepdled ir -5
1''''J 't r''l- 1.* ,,",
so.,rr,o., urcpd..l r' -5 J Add l0'n'
( ol'L"o'oro'n u,.
N:Lrogen . 20 f. rg
C-5.4 T\yo Perc€nt StaD.laril IPA Stock Soluiion Hydrogeiii : 30 r i0 lr]L/min
. j00 20 r 'l 'r 'r'
w. o. or, rccr.. rcry 0.100 0.005 g o rurc D\"11 A r
:;"i:.;;;;.,";;".rast.ron'>.L'otbc'4rrhe A,LenJ.,,on -4
l"or-ol -n,l J.ots or '"orropvl ti a ''e' 'elu\ R^.!r I
.ol-Lro| oI' nr(Jsen'rndoi'Jrero r00Pb\ r'olropll
clcohol. c]lcL.,.c .crur' D\41 'or'-er ''r'ioI
bv C-9 CALcI LAIIO\
"".-ia.,,*',.p.,,i.}andlabe|'l|enA|,,ll'.d'ruJl
*c.en llr,.in c"r,.oc. l.s\ver3'.rdr..1gi'rr'i"t'or 'i R.(ron.-l-.rorrPl-'
or iEa 1,1
"' -nl
C-5.5 Two Percent Sl.rndard IPA Solutionrlqi'r''
whcrc
cC r"i""i"' .' . .. ), : aLer oi dLb€nzvl slbtuJ(e (DBs) (Illemal
,.ke).0 n, tPA .Loct so'.. ,or '
rno.'Jd 2 | l-r rc-"al .'Jnd"otsolr'L'orr'
s.1ud,.d \re, C"5.lr:io..hr''he" hJd l0
rnr or x. s(':.r.olDBsi'r,olJ,rJn.'nrr9:
chlorulor',r. inre o Lle to bc hbe'lcd '
l0r"'r' ,r^ - are"or DBI t..r o? dsoluriorr'and
IPA.Inject I plinGC rr, = rerghrotOBl fi srrn(lJrJ solutioD, inrr1g.
.." CA I.-IBRATIO \ FOR PERFOR\IA\CL
!rl"i,i:i",i,iii^."rnsrAND\RDCHrps lffjili:t"l"':Xl:riil,lso;
c-7 AN ALyrrcAL tRocEDt RL .i.""iil:ii' -;.m;*,"
tlJr:Lr 'or '+f r " rl'o- rr.ior rrr',s''a -td
l.l.rl F, u ''.'d 'd
l-\L I irrlcr i rtr
L.eC_i.t'.rd'arc'r'"cr'es1on5e
 IS 16481 : 2016

ANNEX D
(Clat'rse 4'4)
OF FIBRES TO ALKALIS
I DETtrRMINAT]ON O[ RtrSISlANCE

D-1 MATERTAL. I00g ;:1";f'1"*:,': i:u',xi'|i i'1}:1":",,iTiilii

D-1.1 Sanpleof svnthetic fibesweislirrgabout humiditv.

D-1.2 solution of calciun hvdrcxide

oflH 12 to Ll o': s r'n't out tt'" urcakrng stren gth of rle 30
individnal
i.". i'o,o .r. reJ \p.c'rnen ac'ord rg 'o lS lts
D-2
TpRocEDURE i,r" l,"i.i'6rL*n",Li. ,"e,dge brexhrs
strergth for
nnd out the breakirs
'Lt il;;;;***
eacLr weighhg abo srDnrlv
D-2.1 Prepare 2 specnnens of fibre

D-2.2 Prepare a -olu'ior olcdlcrfl' n\dIo( de olpH :;;;". :;;., ;.,

frol! 12 to 13. N^TF _ F.r test,nq r,h,es or ter grh less rl1 l0 mDr,

,":,-:;:;," " be ne' o t '-'','' r''

;;;;;;,1,;;.;;,.""r,,,ou,,p/D-2.2,:',sL*
,,",""."a *p1of 12 to ll atrd
ternperuture
D-2.6 calculate lire percetrtage breakhg
streogth
"""i",ri,
otS0r"oc.o crrhe'olJrio'oonel\'rrdnr''narn
I rer reo., .nllo*l
rne Lcrrue'rlure a J0 2 'or )8 Jr) ' Keep 're

'"..ii'. i.-; *" ' 'r' 'rel ' -' uh & rn I )pecett
.r'''ldd'd tc, 'peci,.)e. or{'r';
,,,"",rr""",:- z"CrenrpeLrrrre. u"" Br,a(:uq\rrp..q.,. n.ergrh 'Avcritsel
' 00
a..o,,ror,J npre. - b e,tcns
Le,,,rJe l.ru,id,q -_. .;.;i;;i;;;",.""nt cor,r otsnc.rrncn
e'tge)
liom the ailiirue . ,.1t ( sh ensth A\
-
D-2.4 Reuove the test specimeu
! ,,'i;r."'r
'i,, - f,i:
.:: _: '
- ,:l,l:l
.lil ,,.-ir'
q|rNEx
t::)lolause 4 5)
!
' ''r:)
nuroq"fi lVnrrog$-li'slsrANc[oFFIBRtrsroAC,DS
\' -:'- soLution afier 28 days, wash,
drv and coDdition it
E-1 MAIERIALS i","ro ll i,,2't
and r.5+ 2 percent reLatil'e
"' oL' g
' ,.nt'e o. ' ' nLI\ lk ib e' ''e'' lrr' 00
f-l.l 3 r
lu.r.orr

tr-1.2 soluiion ofhvdrochioic rcid

ofpH 4 to 5 E-2 5 Fi d out the breakitrg stre gth of
tlte 30
to
ial"iar"L lt*t ft"* 't* tesi speciLner accordirg
breakhs
E-2 PROCEDURE i.iri!-i,* N*O. caLculate ihe avemge
D_z.lprepare2speci,nensofnbre eachweighnrgarrout
20 c ;l:li*_,:ffir:.,t"ni,:.lxl?l;J':.?.:xlli:
the J\ (rage treaklrg
i"*" "''.t ' tn'" tcu Lrte
F-2.2 ll o n'dIofforr' 1''dorp'r4 ';:.;.";
ep,. e ? ro,'rrro'r ""-'*"i i;. r.LIo !recrne'i'
lo 5. Norr.. _ Fo, rL$!r! L,u,!s ol engrl Less
llr 10 Dnr,
rnu,1"^:i", ,''\"'mr'" or'
r.-2.1,(ccnorre rpe..r,enrJreir'pe!'m"'r' "':
r,czd'2 :r ln rerass ;;;;;'*;' -'ib" '*""esdrg
rsnsile $renerh
i;i;:;;;ft;il';;"L,rtioLr
..r
.:;,j,:;, .;:r,,,:, ,, pH or ,, ,o d,.c rerrcrd,ure
L.,r.ocrcur..,cr,.eper.,.,a..b.e,\,nEs,,e.,ELh
.tt0 ro..co\er.'.e oliro'r,'rorerl Jr_'r'r'nrarr reL,i.eo a" ,o'.o\':
rU 2'C lo' 28 J") Kee'r lL'e
*",.r.r.",-,. al '
,",',"i,'.i"'"-.1,.,"'p"*re'rr(l:r'-t' rrres',drrd Tc'ner"c'bre''-nB
t no o' 2rlc-r' s,'e'r' l 'A\er'ge) . .r00
,",,""r."1.m, 20. rernpcturfle
B,er^rrs.,(-q.,.. -
t not * n1'e' :i;i;;;:;f...ar con'rorpe""nen ot i"rr!
'.",..ie ',,',rd,D ^.o' e]rgth A\ ernge)
slrecillen fron the alkdh
(
srL

E'-Z.O Ifor *" ,t *u

"
 IS 16481 :2016

ANNEX F
(Clause 4'7)
TO ULTRA VTOLtrT LIGHT
D]]TERMINATION OI'RITSISTANCE OF FIBRIS

I F-l TESTSPECIMENS iliil+IJJl,:::li:i:""""liiy,LJ::t::i::lilili

' .e .esL sie.rr1er,e lor '-rs,,e '. g'r h 'rl bP dken .nJ b",..
er e.'fied , F-2.
fon ihe sJ.ple as qPelrfied rtr ls l15'
[-3.3 DeLennire the avemge iensl]e strength of at ieast
for
r-z resr collrTloNs a0 nrdividMl fibres for each speciuer sepaEtelv
*"'" """"""'
r-2.r rrr" test sLaLL be carried oui w.h nuo*Scetr, '"[Jit'.ii"Jfii[}:Tn:]i"".:; '1"
UV-B lamp (re€ lS 790i)'
F-2.2 rhe duation of the rest shau be r44
! (hat ,s b l;:,,r,?il:l[rTj::::rx '|ete"tion of onstualtensire
davr.
h
[-2..] l'e ": cv. le .nrll be d l' rr u0 tor ' r'l' I'v Reientron.furr-qrn1l lensile,psceir= 100

,,.'",,", ,r'. "-'i',g df'P' 4 n ' '0 ' io' \1i'i

d = average tensiie strc $h before UV exPosure
be
F-2.4lradiation level tbroughout the test shall as obtiired jn I-3.1, and
rna taired a10.61+ 0.03 wmr' I = t"* .r,=ngth afler UV e&osrle
- iq nhri,ned m"F_l.l
"riii,g"
F-l IEST PROCEDURII ,| nor", .-
[-3.1 Deiem1ire the oigiraL average tensiLe stengt[,")
(wit\ lmlp
r 161y *** of fluole{eor hrtrps
is rri|he'\r s-r' ".^ "]r,v
e1
otcr lea.. 10indi\rdul frb-e" rorercn spec't 'ar Pi.u'
.erlSll5be'olee\po'ljre 'i'"'r' '"'' tr{r'to ''ed 'e\'o'tre,'e'e! u''a'e o'r'
:i"' '''od xi 'r'rc
"i'"j rrE" pc'mP'i"\"G":oo
F-3.:L\po,erhes,re,:neu.rlreflrcle,' rouluai:oler ,;'; (o'r''
e\poreo ru i oo' nr
"." or'"' 'i'
l'ghr,'orrearloru.o|J"r'-.r01''orere ne_ri(cyde..'trnu'

,,
'
-.:lt
,
:'ir-,
t+':
,\i ,,'1
. iili' rri;r"

'\-J trl'
ANNEX G
(CLause 4'8)
CAPACITY
DtrTERX{INATION OF WATtrR ABSORPTIVE
die test
G-2.3 D ish, for contanring lre n'ire gauze !vi!h
G-l PRINCIPLE piece attachcd. of sufiicient volLrDe to aliow a ivater

Thc water absorplive c.pacity is a rnea lre

of the depth ol 20 nnD
a tesi piece afte' specified
cover'
^-"untotwateLricrawitir dft iiage' lor praciical G-2.4 Suitable \Yeighing Glass, lvrlh
r;*". a,a
"rl,r',"esion
,""." .. .,, A-..,,g.
""rtical
I ne .uirc st1 r'' | ' is G-2.5 Brlance, capable of delelmhirg mass
to an
''
,..p... *. ,' er \ol'lr'c ''q I n..'e '"cd' accuEcy of0.01 g.
".0..,.f.,
r wLr-ch cr'c ar Jr\c5s.
-" ofe'xr r"L" '' lo' 'rdv
G-2.6 StoP Wrtch
G-2.? Rergent Crrde Watcr. scs IS 1070
G.2 APPARATUS
OT
G-2.1 Nire Gauze Test Pioce Suppoli' ol at leas! G.3 PREPARATION AND CONDITTONING
iro,lzo -r". n,"trt frame The grlizc shlrll be TEST SPtrCIMtrNS
'ritr.
,r*a" t". i"i'r""
" i€st sieve of2 mm no nral
" "*t
(Pat 2)l'
C-l.l l?p..re l.\i lP r."ccr'c.r '' '"eacl''l"1"
-Lre' or "/c
mesh size lree IS 460 irilol I u i4o' ,q 'r ""ce ol
on the grMe' 100 + l mDr: 100 i I mlr1'
G-2.2 Clips, to hold the tesl piece
 IS 16481 : 2016
at corner'
slrcjr cj s - ""rdbrd G-,1.6 ReNovc all clips except one
c_1 2 cold'L'or' ' 'c 'c " "' rn'.''L I
;;",".,.,... - ',J' G{.7 Hang freery andaenicallv to drair
lor 120 + s

.v .". 4 I :a Jir -e t ' ' 's ol\a' gauze without

'.,,,".;,,'',0 'c.o G-4.8 Take the test specinen off the
$":s\''e
i NOTF- Thc rvater shall trc lctt long
wi(h dre conditi.nins alnosphcre
cnou8h 10 cquilihrute
1,".. L. . ." "
sts
' ;'' '' "
'e, ''o
\',,th (o\er Jnd wersh ir
rr :o rne

wiih lhe remaining f'ru

G.4 PROCEDURE G-4.9 RePeat G_4.1 to C_4 8
c-4.1 C!-\ or' .he 'e'' rI lL" ' ''rJ'ru rLr '6p' fl-
n'-l :'i ..P",",.''''d'5 )ry'''' tc tt" NOTE Usc conditroDcd \'lcr lor c!'h tcst
- 'rcsll
hunidily.
w(rsr
'.;"'.3 rt- ^ranccr' ' '9c-2s'xirr "'"e
-";;r2
c-4 :"-1 '"' G-5 trXPRESSION OFTtrSTRESULTS

ll G-s.l ( a. rl: r.'l ( u".cr' b'J'TLi\e'apr'iL| MC''

weighitr;slasq wrrlr cover lI" G-2 r pcrce',.. of .'rch r(' n" r l' l ' lnr'1''rld'
'Pcc
G-4.3 p,.-cc I * ol rr'e'.ti.,e" Lre
--.,)"'' c-,:.,'..' ''"" '; '" 1''g-3"'"'''r*'ltp' WAC =t\:litrco
(s?e G-2.2).
c' 'Pet.rinen sl,e'-
C-4-4 ll',e rl,e.'rr,/e uill'lhe a rac"cd
,"*"-r',"" , :-o ,'^ *t"" ,n. ,'0,'" o': ,r,e.r,y red sreci nen. i,, ,. ald
d]sh {r€e G-2.31.nJ slrft rltt stof
watch
",(r?' ' ill;
(,''l ., - ".sio
i^;:::j.;;,.;;; iiq'-'i,.oJe 'o oidrrppirts; "l [iiJl:;::;:';;',i,J::'.,:i'J"*-*'
a:r bLbbles
*itcr 0bsorPrrvecapacitvor
G-4.s After 60 +I s, r€nio* **" n"
"'""1';;11.) i,"';HlX1'lJli,".,lj"l"
""
'n"
resr.peci,rcn 'il
suppo,L,,id
, .",5'.'"
, ::
,....'..
''--' ,..1.v
!i.'
..
""ilP
,.lto\ ,{r,

:,';; ,ANNEX H
a, L?abie l. S/ No' '
lir r.1

"i'iirsnn'riiirrol or sPECIFIC GRA\'IrY

1'l r'''e' 41
H-I laie a .pec:'n . o. ucigl"r " aoor ' Specific graviiy offibre = - -;-
,.,,1,"'",0r"'nolr' d'r Lirir'"'r rrdl'b"-'"i'r'
curarc'o
,.",",:-. ,,r. -r." ,." .ordl trr'oc u l"
H-4 l o. .rr'gJ o. cro.s_"lio ' "oe" c'l'r 'alc
l
(he fibre by the foonxlr'
speciflc gravrry ot
l'I-2 Let I be the near fibre length' i' cm' conect to
;";;;.,;,;r ;,.." d. re'cn,,,neo b 'r' I o'cd''c SpP..,,c . ayl. '' - o.ql 'rt '/
i..",it.a ll r':.r'-uaauerhern drr'' re dr'rr'rr 'd
erer' .frhc trbre ,^srnb0 .d/2 i
in
*,.." . "" a"t,l 'xlplace' ' s de ''n
"'.'",
rs 6919. qide of the equilateral trianglc of cross

H-.1 fo .r'.''ld. . o''_'cJ'ion

lo e c''cJ r" r' r
spe! 1fi( !Lil!rLy ur tlre fibre
bv tlrc tbL n J
 _t

lS 16181 : 1016

ANNEX J
llbble 1, Sl No. (vi) ard (tii)l
DtrTERMINATION OF IItrI-TINC AND GLASS TRANSTTION TI]MPIIR{TURIS

J-l GENERdL Frt d.es, to uniform cotrtroued

^) hc i,,! rcoolrnolrovide
iold.,.e.ruren Id eie,-x!r
'l h, ,e. roe.l oJ.oier" de,pr. r o :o , ol n elrir)g ard
srass traDsition ,enleratures .r poiy.'t..
io, n-^'vere:o.1.ne s by d ;-' i.,l s J.r;ng
",J :,ir:ffi?:::i,1;TiJ:,1"'J;::i11il:E
;",";,,;;" "
calo rner c rDs.) lr i. alp .rble o foly, e .
granular forniorto ary fabricated shape liom whicn il
b) Tenrytutule J'trsor' to provide qPecimcf
rerrrperaruret'anaccuia(yolt001'c'
is possible to cut appropriate specimerx. rhe nomal
op"'utl,tg t"n p".oiur" ..,ge is from the cryogenic c) Dilferential r"Jor' to dcLect heal flow
r"glo, t. eo6'c. Ceriai; equiEnenr allows rhe diffcrence between tire spe'inen aDd
ter;lerature mnge to be extended. reference equivalenl to I 1lrw

NorE Thn ilenrorr doer not pn.po.ltd iddre$,Llorrhe d) Medns of sustdi tLg d tett chatubet
saiily.orcons, associnrd wnh iu *" ,, t*p"*,oll,1 exrllo"re'l, ofpuqe gasl at apu€e flow rate
",," s.rity uDd
olrbe user orlhn ixrdhd ro esEblish rppniprixr. of t0 lo 50 + 5 rnl/rnin
..r .. {.od..jr r...,p^
use '!r.i1!I .o "o'v
NoTE-T\ptr5llv qo+n<tuer ltr( I rolen soro'heliml
limnalons friol Lo
ht .''-P orc ls1 i n.'..
o'v pL':'
J-t l,RI)(',I'LL 1-. remmDetrdpd drd is sseDil:L lor oPoration at sub-aDbienl
',

'llre fun'!i.l is
iPri nrxtc.ial
The test h. ed.r
ir heared {rioltd at II.onhoLled
or coolcd .onhoLled l'nrtenl0res'
Lar. undrr n spe.iicd ]rurse gas ar a .on(rolled ilow .!l.l 'peftnute onnallet, .apable of executirg
m€ xnd contii trousLr nlolr ilornrg \ nh plogram by otcrrung t|. ininr.c
'en seLected teDperatxre limits at a rale of
material ard a tcn lraterial due to cnelgv chaDges nr chaige ol0.5"C to 2o'C/nin corstanl to
the Da(eial. .\ rnrsition is rlrarke.l by !bsorftlon or

correspordnrg endolhe ric or exotller.mic pe 'i:,ll.r

''"' n.. rr,1r Derice,
", . irrb e of
Dp,, capable ol rccoin]1lg
"eco,J..1g aLld
J..o
basei e shjjt tu the heat g or cooli4griuive. ti'..-.,, J-.].1..1
,.\j"
J-3.1.3 Recotelins
..
displuyn,g a"y fraciion ofthe heat flow sigMl (DsC
NorES ,)'
curve) includnrg re signal noise as a luncrioD of
-.
lD..^'.'...ir r ,!o .ooj,S.r.'... e ,.tl-efi..1
resurrs rh.*fb( deprLtu,e rr.n ao' ditiotrs \pecin.Ll ror a t4.t.4 saftnarc, for inlegrating x.exs urder
e,dorrrennic varrevs or exotrre'.ic Peaks' or both
:!',:ilJ"':'"':::i,"l,i:iili::l..DoNi,o a,,i.r,,,. rnN,iotr
rtrrrcnrur.. piricuL:ry irti impurily tctrds $ roir solid J4-1.5 Cantdillo-t, pans. cNcibles and so lorth that
solrtrions or b be tuiscible n thd .lt ph.r. ,r rnerr to rhe recimen and reference rnalerials and
Iu ccrti ii r'diaLLoi lo$cs at icrn'c ttr'sLri!lcrLlrntr'100'c r"rr,.irr" u*.rL JtsrrJpe,Ld i,regrity lo
hivc beer kDoslr to raiect the ac.um.y olEsulrs rt ri,nc "rr.nuL.
4 Sitrce panicle sizE Lras af et.|ed rpotr delecred rx nion contanr the specimen aDd rcIerelce il) accorrl r.ewilh
tonpor,ltricr, thc spcciDrcns to bc coi,pa.cd shall bc the specific requireDrents ofllis nrethod.
apftuY,drxr.ly ire same Padicle size.
s tr cases ttil specimeN rcrcl *ilh air dur r 1! rhe (cnrpcmxtre J-3.1.6 Cooling capabllity to hasteD cool dolvt fi'otrl
cycrc, prolGior shaLl b. nmdc ior runnrg thc rci undcr elevatedtemp€ralues. to lrovide consiant coolilg lates
imfr sas blatrkctto avoid rDy iico,Ea rusremct si .e oI0.5.C 10" C / rr ro obianr I e peitrble crystallization
'o ,j,1.,,.,,",
', ', tempeLrlure ro ac lieve s!b!nlbie rt operaiion or to
used ro Jistugtrish benYcetr Jegmdariof aid lrnsirLo .
(Simeve,!snnllquuniaerorspeci)n.l,:Ented resetrtill suslain aD isothermal sub-aDbjenl teDrpcmture oL

. ,i,", *. t .,ioeen.ors xL EpEsonLatile. conbinatiol drereol

7lr""*.
.po...'.r 'r""i,*"
r'.. o'.o.ro,\ n.cn\"
J-3 2'41"" (anableoiweiglinqro+l0pg'
shon ncdnrg rhe nnrcrirl {h*n."ro.*.r", ."ii.
pesortrel orlo the xPp.L!trrs
J-4 TESTSPECIMENS
J-3 APPAR4TUS
J-4.1 Powdcrcd or Grarular spccimens
J'3.r DitfereDtial scrnning colorimeter (Dsc) {void ,g, f rhe pre r nird ) ihermat cycle as
sr LLrd
J4.l.rDSC-fettCho ber Il consists of(hc followirg: o tllned in J-6.1.3 is not lct lbrLred. Gdnd golslnilar

I1
 IS 16481 :2016
."
"':i.lii::*::l:"lfi ::':.':T:::::::'::."::1** ,,", .," ,.,-,-",
,ec,mique s for size reducii*
':':
lLt':;;:;::;.';:::;ll"i-iiil.lliJl:i':'" -r:i;.,;:,,'"',r';l -.r:; r:":
I I-1.2MoldedotPeuetedspccimens';i,l'i"'ili"'li;llil""i;i'Pre{nonnrdrep'!slnnury
::,,": .."",".".*.i,hJ,1,;c,ot"c.i'7urbr!:-c J-o.r.4pJrd,ne,e,npe''n""'o'''''11r'e'J-br'3\
li.ll i,,:j'ru;:;:u*I::"":"1:,::1 J-..' s..o,,,,,'
::':"":li[.;',;,,i';:
l:;j;;,:illl:;;l;r;"',i"1'" ;1ii1i,":lt'it ::"fl"t'l'l,llll,',:""'"'"'""'
f,r rhe : " , , rhe
"DecinLen,ne des red u':s'rr ..'n
_1
ror 'i''i1'
;":i;,,1,,;i; "". J-6.r.orroro,heLe'r'ren''"
ard
lii'*".ip'';a," g at a rate or i 0'c/min
J-6.1.7 Rcpeat the h",rt
record the heating clrNe'
J-4.3 lilm or Sheet Spccimcns
rlr rl''rr''e' J-6.r.8Mea'u,eLhcncr'rr:'entlliL!!.r$on'l'e'cu'rc
;.,.,,,".,".-", :1' ""'- oun'r iil'i;l't':"'"'
r'e r'u'e 'oc,,'"s
',",,rup,rl,veJ-4.2r
rLL,*..u.,','c,-,or. ,.1,helDecrr'-r ^*r 'ao'' lf
Ji,\..ir,',e(:,c..1,' r(rnen'p-'' "'11
.'1"'"i'^;'"0'er'"er,'rrc'ndr''el'nspc'I
r
rrje'r: ' J-r't J-r'r 'erpe
'u'e'
;-;.;..",", 'h0re or r"r'n r' '' ' n' lbc
^.--^. ,^h.n cor-u. ,'rg rcr.rce t-o t '' .t-0.2 Cli'rTr rsili"rrlcmPcrxlure
i,i,rJ*,iJ"" n*' '" 'n"'n'a '" ..r-s.z.trL,ai,riie"gu,.l,allbeusedduringtestirgThe tt'e os L's"a ir
t'e tLe ""'r"
r-s cALTBIG.*lo\ r,ilJ ':l:.ii;:;;;'-t,Lt
".'
,-,.r r''**"" *"' t" usea au'rns ",,::ji}:. , (necineD mass appropriate for thc
car'b'dio4i:i':;''
"t' 1e.r.pe..,,..c (:enrl ,,';nts ' d r0,o l0 ,'s
:._"a. r,,," .*". r\e
J_s.2(a.iL,a,e,l,c D\(. l;",,i:;::'
',.i,,*',,," .0'c,,. ],"..,,, , ,". ',,.,."v
\\ergr 'PPcrn" '
ro

:'rr"C n l0rp
J-51r," 1rcLr'DSC'rJ'florL_'':'1 "''gl 'c"i'vi''
.*"i'o"cr''i"' .a:-,). ;,. J-6.2.rPerrorn'drecord::f:'Ui'J"',li;li*i,l"i:
pi,sr"-e,,'",,:1,::l: :,1I,",:""Tljl ,n. , .,'"'
J.s.4so
iJ.l,';;i;k;li:J',1i:.'1,i..
frti::":tl'it"llil.l,llillilTiliiiiii:,*,i.* l::;";.;,,.,;.,'.""*"u,',ernrr'rlo')
sjrrcr'i''ron r rrrr\
" *,u'uri
r''re ,e e,rpe,l ure ,or
li;;::l;;:;:,;i"i"
' .,-b.2.4 Hord
"-;.1' coor ro 'L le1'' ooc betow the
J-o PRocEDuRL J-6 2 5 Qtrc' '
Lr tetnPerrlUre of inleresL
'f\thon
J-6.1 llcliirgTcmpcr"lu iLie iemperatLLrc
rrh
fol 5
J-6.2.6 llold
J-r,.r.r,''.r'''*s"' nor'*l:11'1" " ".Ii,,,11
be tLre 'Mc J' LD\! " g'r" "f '0"' I "il-d']':" J

aer ed' ri(r"r''

shJll r.6 u.?Repe"r''e"'" ercs
flo\\'nLe ot tlle lis iiJ,'.,,,,:.., ," "i'
caLiblalior (10'Chn11)'

r-6.r.2 J". " .*l "1..:t:";'l'"l,!xl.,ii

1,.
,i.,,cri,lro be .. "ed' ln '::' '"':' ',: '.t,:::"';
w' E" ,r.
,""r. toutt,tto'y' Aloid overlonoLIg'
"
cpecir.re,rorrr'trc'":r'vot "ul.. .. ", *..",.."
**.;+l1ut*t*:q*irt
E,--'fi.n iTN .nJ Tg !esnecttv('j'r "'"
""ll- l::',',...rne.rn,u'er'ru'cdure t-t' r't'd
i
- i:l* ";l;r;ll;;,".,, rro,''he 'econd 'e" '. ''D
*:i*, (rae G-6.17)'
elrsure flat =-ir*::''1,*i*'
Pan bottotns'
o'.'
J-o.z.q Mef .ne r, c' rrdrcr
Jnd :1
j:'.LE
:TiJr:l:
ieJexrra!urJ""
,-".,., t.,1,'" " "" l:" 1';;:1"i, ]'?1"1i'"1 n iar,o,rt t"'np"t''tut"
.1.i,, :.i';:' ' " "
",1 ::li"li: iili,'x"*:':
l2
 IS 16181 :2016

ANNEX K
lTable l, SI No. (ttiii)l
DETORMINATION OF INTRINSIC VISCOSITY

K.l C]jNERAL K.4 REAGENTS

I This netllod covers detennnradoD

of poly
of tdnsicviscosity
erhyLeDe tere!hthalate (lET), poly
K-4.1 Phenol/1, 1, 2, 2_tth-ac hloroethvletre Solution,
60/40 (m/ ) mixxue. Prolecled to mailtain this level'
hexamethylcnediafiine (PA) ard po ]y pro pvletre (ll) Chtor id i n d A(eto n€, AR Gr,t.te,
K-4.2 M th \ lc e
so.r.b,e a, u. 0 per.e1 corr' er'rm. orr,', rJz0 l, at'
e n e

LsrIs\orvelr'
poenol 1.,.2.2-ie,ra-lrlo.oer ,) le.,e so .,.ro.,. 8s o(.' 'rr
(m/,r) foNic acid solution aDd decalm solutiorN' K-4.3 ChromicAcid, cieaning solution.
respectivel, by mexns ofa glass caliLlary visconeter'
Hi;hly crystailiDe forms of PET or PA that are ]rot K-5 HEALTU AI{D SAFtrTY PRECAII I'IoNS
so-uble . tie.e ,o ve.,r nri,, ,rre. a'e r.o . overeC ' ' L-5.1 nre u'.en.. lo dL o..,.ror o PFl,lA.-.llP
procedure
this
arc toxic and rcquire care in handling lD dddition lo
usirg alood torade'luale venlilalion inlaDdlinglhese
K-2 pRtNClpLE
c'.r,i ..Jo.r..or. so.,"5(rr. rs\.1ilr
|,r
The l l]lstr vV.(U.LL}
lrtrjlsic iscosiry is detennlrred by ea$ g the
2
flolv tiNe ola soLutiotr ofLnown polyDler concertranon l(-5 Usc
saleiv precauho ts siver Lrr the Material
saicry DarqsheeB (MSDS) ior merhyLene drloide,
;;d the l.tow time of the pLrresolvenruncapiltcrl . .c d .lsol .ror..
.,..r.0 .1,p..r,,,. Tre.r r.r-,.
a-clo.re c.,ro ,
" 'o

K.3 APP,\IL\'I'US

K-l.l C.rnrr0n ;:'

tjbbcld e'tl?c llt \'isc0nrelcr PcrceLrt !r
ucriint or morr of ircrt nlrt.rirl sncl rs tilxnnnn
LrNL' !L
.".di.o)riJc or sL,rss fib.r, d.rcrlirrc th. dnannrl oI i!..1
K-3.2 \iiscometcr Holder .'.; .]iiiit".i
-:.,:,rhiterial *;,""t,
accurateLy L,y a rnelhod srdtable for the irert

K-1..1LlccrricTimcnsrLhara(cu.a.,oru.r J ' :
marerial DreseDr

K-'4coft"u,re,nperx,ureBi,. o,,oaber, I;i;:,i:["li:;::il::'i:il"iiilfl';;]lffi:

J0 0'01'('' l'r nidrt) rn 1r' oic,
r'd'Lion 'r dr) r'r' ''arnple
K-3 5 Knrenntic viscositv Th..eirnometii,:feiuse at '
ror about 2 h ai 65 :r 5'c or nlil a cotrslant mass

10"C. of+ 0.1 perccnl is reached.

inristrnt coilerr
l(-3.6 TenPcratu rt Controtlrblc M agnetic S tirring NorE
- L]\c r nri1.bLe
'tLhdd
ro detennino

Itot Pl:rtc K-6.1lfrhe slmlle is difficult to dissolve, rcduce the

l(-3.' rFF-Fr oroc:rrbo, r'1.,:ric'cur (d

Brrs and r Masnctic Bnr RetdeYcr
srirrirs ;'";',"j]':."..,:'r'lill' i ili|l :l;:';:; ;':
oper.rion by usilidry icc o;tiquid nitrosen. CIn]d a
ml js ne!cslarv
K-3.8 Volumetric Flnshs and StoPPcrs, 50 15-20 g sample lr is likeLv tbat drvnrg
calachy. after Lhe dry ice glrndhg step'

K-3.9 Annlyticxl Bnlalc€, wirh an accuracv of K-7 PROCEDURI

0'000 I g'
K-7 1 AccLrratelv weigh between 0'2'17 5 aDd

K-3.10 Borosilicnte Funnels 0'252 5 g('1rccuratcto 0 000 2 g) ofsampLenlto

'clexn
K.3.lrstrn,,cssstee,Fi,(erscreeniDs,32sNeshor iiil,iSl"Lillffllllii,*;"llli:i":ljl'fl"i*ilil;
lLner :urrplcn"essr'1 to giv' thc sl)'cfiellimourLofPEl'
PA oiPP
K-3.12 Aspirator
K-7 2 PlaG a TF E fluorocnrbon plastic-coat'd sljlTing
K-3.13 Wiley Miu Grirder, with 20 mesh staiDLess
bar iDto the flask atrd add approxrrnatctv 25 ml of
steel screen.
solvcDt. Prcparc one flxsk wjtlout any samPle!rcscn1'
K"3.14 Drying OYen Clrp tlre flrsks'

t:
 lS 16481 : 2016
l '( or I past fie caiibraiion nrarlG
bml r" '' d
l'-7.1 P,-'c ,'.e nd"i '
ii..*,,.".,i"..",.,"
'r "cc'
1.'bJe'ID r'dr'' oI J" l\-7.9 R nu$ rrednurq''d,'rer''"ur'rcn'
rord rh.
R r'o\eaa (' ,. *,r.",, r,.,..g. 'r.' ic{1 " e"' 'lrc ' 'e'
;i.:,il";"1:,;, ""h,c-,.r; "'.
il;;:;.;,".i ;:; .oried rt I PA '' Pt r ' '.i'e :' ;';'.;"i"o, ;"r. h "cenrare'Jojn1a
.r"-'"ol
" co tael"l) ex e rurhe 'rrI'"rr! 'c
"' ,, .".,,.".",t .o'' ''r'ri'f i!r'9" ol o I '.ar"
"i'*'* rne 'dr'Dre bl "".'
1 r'r."'.Si,;. V".<"
e're so \cn llo! "'n'
I i", ," ;o
; ""1;;;.,.;'..
le ;r\'pe' rir's
'" '""'" ' rr" ''rhc 'r'npre r':rs d''s'r\e
'o
".,.'..
., .t,. ',,''. "-""' !' 'rc fo$ rji"e of 'hc ' 'L'rh n
11",i".,i ,;'r,' * t 'p;o'iu- r 'o aopt'"' n'c
(o''"d' r"co 'l 'ne M'\
K-7.4 \ l.er' .'.e I ' r'.' lorc 'o'1L'',rerv'' J K-7 10 D lrlb ln' ncr' rremenrl q
n, ro' dle 'rrd ' ' 'h'' ru :";;.;';;;,; he n drcn oo !':::"" ''
,"r"" ^- " "
'^l:;,;",;;,.,"t.,i,,",',o.,,',e,roc,)''|r' : r J' rc ur L !
",". runEe rn leirpelJrure does not exceeo
;;:;. ;;,".,,.s,e,:( rc.:e\c .nu,-.r,rP re n' rl'e
K-7.11 $ b",, Lca ' I errc''l' are 'or"olcred' "
,lli'*ii, *' r. i,, s rhe $':h ' 'r\'n' r0'rr-r' k '1.:;,;.; .;;; ,\e Lr \ rnd "rr) P"J'rr'
"-r, '";' n"sL' odd addr':on'rl 'ohe''' r' r
,,, .i'.."'".*,,i'
i":', t. -' s0 rr' r1'rk P' 'ce rr'c I sk'
.:il;.;;:; ia i'.o re'r'r''a'eI "(L\ d',.o'"
il'". '". jo: ucr{
"u*
l;,,;.;"'"; ';,",,-.brrr0 'nre{L'
I,1",',* n"r' '; ", ror I rr' 'o r""c ' rr. '"''1 K-8 CALCULAIION
l'"",.,,,,.. ,:,'. "r""puc ed {r ' h ro "''. h '"r
:; i1,', ;;:".' ,J, , ,. :^ L' ,d , -r," "1
, K-8.1 DeterNine the inher€nt viscositv as lolLows:

;'.;;,.;j j..' taJ o' u" j'' \e

in "
nrt
''"'
Lrlrrt :l+ (/ nx1.)
ir.l d te'et ut) ro rhe
,; 1-9;=---
whe|9t-",r
- .i , ,tere,r'riscos't) d' 10"' dnd a po\rrel aL

'.T.' '-",..,,,"'r" ' oi o's g a roinen':ors ol

inhercft \'iscosiiy are dl/g);
= relative visoosiry (,/h);
= a\,emge solution flow time' iD s;
= average solvert flo$ time' iD si and
= polyme. solutioD conceitlation' in
g/d1
C

K-8.2 {,'.,.ld c I e,,'rr' r"i( \ r''oc'v n rrol a'''pLe

;;*.', ..'*, rre 'e'|drrv'\ '( o'rr) bv rhe Brr"nevei
"
l=0.2s(n. 1+3lnI)/C
K-9 REPORT
Report the Iollowing hlolmstiorr
Samplc identification and
desciption;

b)
?crcent ol inet Lnaterial;
") aDd te'nperat'rrc;
d) Salnple dissolution tlme
e) Avelage solvenl flow tinrei
ri-?.d
''; .", *-;,, .. h--.- ' ',"' r''"r 0 A!crage solLrrion flow tine:

,i'.r,'."1
-:",, , .,\b , , j''
c) Average viscometel bath temperature;
nnle,eni viscosilv (three significant
places);
:,
,,- '. ' i ..1
11)

: l: :. .:"
l.';;'',:
,",;
.i ". . r,." , ::r "iL ' "11
j) lntiirlsicris.osit)'

l:1
 IS r6:lUr :2016

ANNEX L
lTdble 2, SL No. (i)l
DtrTtrIiMT\ATION OF trQUTVALENT FIBRE DIANIE:I'ER

L-r trtRIiL \\'t tll CtiicuLtR CROSS_

sIclto\ o.t,-,.ed"e.r r,- Co 11.rl.e. Lr, be.
' I oJ. filre Ie,.jro.-.,n,t rrrdoI t,e.,.e.d..
r--l.l |o.llbres $.lll]. diuner.r lis\ thi,, ! I niD. the
mass ofnidivldual 1ib.e by divrdirg rhc mass of s!np ie
m{$r.d usilg ot,li.rLnii.tuscure.
diarncro slull b. by t|e lohl rLrDrber offibres iD it. Measue tte tensth
ill x irdrri ilbr.i diinrerer sh.| b. Dreasure(t xnd or 5u 4D,es J.c,.,eJ. ,rio .,,. L..r- i,e...e J,;.
Ihen nrern fibre dixmerer sh3| b. cxtcflire(l 'ergrh. , he d\e )ge - ,d .tre a\e..s.
L-1.2 !., lib,es sirI x di!rner.r grerlrrrhar 0.l rrr. 'cPvelor-o 'c". ,,.. . ,, , .i t.. nbre s,,.,r Le
",
deteLrnirled 10 an accuracy of 0.001 g and 0.01 trm.
thc dii,I.l.r olrh. libr. shrtt be rr.JsLtr.d nirh r rcspectively. The equivalenr fibre djaDrerer shalt be
nicro, cr.rrort)re.isioDot000l j n j0 mdi\,trtual ,o rpl'-dfiorlr,e.r.,....u.. eoc,.top(d ..rgl ..,r,
,r.
fibres airLrclor shall be sured rnd rtr.n e.u iible the follolvirg foflnula witl lhe DomjDal densitv olthe
dixnreler null bc calcutrted. fibre, p, nr g/cDrr:
L.2 [IBItE \IITH TIiId\C U I.,\R/IRTII'GUI-AR
cRoss-slct to\
L-2.1 liken sxrrl)leolill)Less..t!t:rngr jljur j 3lu(l

l\'lJ f,un r|e equivrlcfL fib.e di nreLcr ined by the procedures describe.l in L-2.1, detennine tlre aspecr

Mean fibr€ tengfi, in nlln

E.lui!aleDr iibre dirmerer, ir nrn
Length ol thc synlhclic fibre stralt bc detemined by tte nrcthod given
in IS t0014 (parr l).
IS 16481 : 2016

ANNEX N
(Table3,Note3)
PRtrPAR.{TION OF RtrFERINCE CEMtrNT BAStrD MATRIX'TO BI UStrD IORtrVA1'I]ATINC
SYNTIItrTIC l'IBRES FOR RtrlNIORCEMENT IN CtrMtrl\"T BASED CONSTRUCT]oNS

N-1 GENtrRAL iDdextogethernotnore than 30 percent The aggregates

shall be from had rocl6. such as basah or gra te
The comtosition and characteristics of refereDce
cementb;sed matrix for construction used to evaluate N-3 1 2 Fi'e aggregate shall be tho sand coDforming
irr" p".r.""un"" of synthetic fibres nder standard to Zone II as def red in IS :83' wirh a dDinurr
laboratory coDdiliorls. of: percent of tle material passhg through the 75
OI' REFNREN'I'
N-2 REQUIREMENTS
NlATRlx l'OR N-3.1.3 The aggre€ate grading, measured accordiog to
CENIENT BASED IS 2186 (Part I) shall conform to IS 3S3
CONSTRUCTTON
N-1.2 Nlixing \Yritr
\--2.1 Fls\urxl Slr.ngtl'
\vrler lbr nriii|8 in tun'Lerc iod-rbr ntrins sh ll
'lhe t.lcrcncc concrcles slrall be dcsigred to |reet
' conl-omr io u]' requircnrcnh ol ts 456 (s"{r 5)
,."r.,,n"i il"**, **sn. as aefincrl ir ras c '1
N-].ll Cen)cDt
'Ilble 4 Pirrdtcters ol Rtlerencc Ccm.nt ll,sed
OrdiDxry lor(lrLri 5:] grade niDg
[{r1ri\ lo, Construct n 'cucrrt '!nl_o
n' lS lll('9 ilrilll'c rLscd
lcl'rlr? \'2'Ll
.::' \{nitr'l \i"'i'''"' \l'\"' in \_ll"l \rlI'rr\ l'rr "'
No. \Itrki\ FlNtr;l txriN D Cr drr $'rt' cpla(l.c./eror(.,.''rolds... /er. d \ ne .:. dldn I '\ I re
| , '||,,,' ., tr'' .' ArlasLLcLzerorsuDerrlasucrzer,a\lhemicaladmixtxre.
ql0l may le r$d.
l( o.0J'n.) r" "o L oi '
...d to
co.rrlr'r.B
i\rr'r a',l3rtgxrt Letrr' rr'"i'' ,'rtotnplv"'g n-lS
:l:
":lll"ln"me
i,-i - i -:,' ' uo.kab i,. llatr
r,,ll.in'6rl(ability lld r .o '' i'ed rrs.e.lerc
n.\L-e is
adrnixture
::..iitlt and <losage mus be meniioned with all the resLlts'

i) Re{lnrcmefh 43+l):l 2A N-3.5 Fib'es

The fibre uscd aDd iis type, that is monofilamen,

N-2.2 DosNge ol rribrcs hultifi lanenrfi briUated shall be reporied.
Tests usnrg Llfcrence.cnrcntbascd rnr!i\ rrc nscd tur N-4 SPtrCTIIEN PREPAR{'I'ION
pcrror.I
'r
.e o. l,u- b) rJ nD..rirr" rle D.'operlres
onLan'.rl urrr, r\e relercr ,e.n,r,irlo$',i.1 fibres c Tlre refererce cenrent based matrix shall trc prepared
,.]de.l with those of the sarDe releleDce cerncDt based
natdx \\,ithout the addition of fibres. Dose of fibi:s a) Prcpare a matix baLch, the volune ofwhich
slull !c 0.06 lercent by voLume of tlre ccDrcrt based o i0 o a0 i" .er o 'c nrix'r
" ,r,, be L

N-2.3 \Yorkrbility b) Pour all d1r rggregatcs into dre mixer, add
.al'.1 1.1,. .lis: .r'n.l_ r( lo. r..rr.
The workability of the rcference ce ent brsed matix,
c) While continunigthe mixtug, add dre cement
wiitroxl fibres, shall be 100*20nN TheDuhixshaLlbe
a d lhe olher half of the batch lvatet durilg
fiee liom bleeding or segregdion. Workatrilitv shaLl be Di ne ofmixirrg.
the Dexr
measutd at 20 * 5 min fro the cnd olDrixing process.
d) After adding the adnrixnuc (ilapplicable) nlix
N.3 MATtrRIALS TO Btr USED FOR CEN1ENT i'oramilrimun2mnr
BASED MATRIX e) The fibres slall be addcd at thc rPProl riate
stage ir
accordance with the manufachutr's
N-3,1 Aggreg.ttes insl ctions. Cenerally, fibres caD be added
N-3.1.1Coa$e aggrcgat€s shallbe crushed stone! wltll aftcr the agg.egatcs bave been added to the
waler alsorptioD less than 2 Percent by rnass' Tle mixer. The Drixing tnne after adding all ihe
coarse aggegate sli:rli have elong:rlio! aDd flakrness
;r tsreJi-.r. ., 1 i \ Lo.( rn''11 ini
"'
I6
 lS 16481 :2016

0 Forthe l11atdx with fibres, care slull be lake! relortirg the average flexurai strenglh.
to enst}Ie thai the fibres are evenly dislributed
throughout ihe mix. N-6 REPoRT
TLe following irfonnation shaLl be rccorded lor the
N-S STRENGTII EVALUA.r.roN reference coDcrete:
N-5.1 Compressive sn ength shrll be detennined uslns Jl orrgin Jnd pa icre n2e drqrriburio! ofco se
t50nmxl50mmxl5onnncubesatrheageof2Sdays, mrl fire aggreeates, and brand and rype of
lor bolh the concrcte ixes without aDd fibres.
with ,r"a;
the "",r"nt -i-ua,ii^rr,r",
N-5 2 If rhe reduction i! conpressivc sh'ength of b) Mix co posirion nrcludtug dry aggregales and
tnanix with fibres is lbiuld to be nrore than 5 percent admixhres, m Lg/mr, and details of mixjng
tMntLatofihemahixwithoutfibres,thercferencemal x procedure;
shall be checked lor cohesiveress, ail entlamment and c) Fibre rype and propeties descdbed accord g
voids, and ilrc reference mix may be corected, if to this siardald tuorm/guidei
nec€ssary Nomally, statislically significanr rcduction d) Worl€biliry aDd conpressive shengd! ofthc
in corpressive streDgth, indicates inappropriate mix Dlain and fibre cement based matri\
proponlon,a reeds revislon ofthe assresate 8raditrg. O i*" -a rLne oi rasting rfd lesting of
I\-s.SSirrri.nrri(.50',r, l<0',r' )50n]n.io' sle'r'ci('
even lougci) spechens, made fi o a relerence natrix 0 DD'ing shrirLrage as ler lS I199;ard
without incorpomting fibres willbe tested for flexural s) FlextLial,strength to the nearest 0.05 MPa
strelgrh atier z8 dayiunderthird-poht loading (at one (aygi4!e or specimem) ror fie plain cenent
rl,.rd spJr t or o r50 mIr cpJ '! oer iS \.u. lor ' od.ed I d'rir
'. .
.-].',. ,,1:.1

:.,
.......,
,ltit.
. ,,.ii'
']. ':::..
:.]

.,.').,
.,1

i.'''.j'

L7
IS 16481 : 2016

ANNEX P
(ForetvorQ
COI{I{ITTEE COMPOSITION
TechdcaL Texriles for BuiLd Tech Sectional ComDriftee, TXD 14

Orya iatia
Indhtr lnstitutc olTcchnology. Ncw Ddhi Prcr B. BH^nr.rL^RrLr (Crdr,x,,
E.l. Dupont Indi. lrivaie Lrd. Gr€aoD
si rL ArN! ALrMh (rr,a/t,t )

Flcbl, Ne$ DeLhi

Stskr suNsH K\NN^N (,lr,d,el
Reliance hrdlsrics Ltd. Nerv Delti
SHU R^nv c^uu (,,11/e/adrP)

All India Fht Tape MartrIacxtre soci.iion, Ne{ DcLli

SHr S^N,^Y llrN llr.,,r/e)
Bckaert lndlsths PLivare Lrd, Pone
Nrv(r N^uY \ (tre,,,re)
SHR]

Du.lo.n! \aa.c'iah z .o re.n'olo$ f'oro .on D s' " l( vs A' L1'\'

' ',r
(orn.i'.N$ D.ll'' r"J'K 'tu "a?'me'
BJ, ,e- .o-oroil'oi .o r e, !., Dc.'.i ' e '^' l:Lu '

centnl Buirdns Research ltoo,kcc

ln$ituie, s*,s:'-n n*,
cenr*l Road Reseallh ,n$itute, New Delhi i"ii"
,"t"'
'3;t"',,,,"-,
,clFc, ..r t'ts.'.c..1 'c,.rnt (!n"c. .1nr I c-", Coh ' s'
'1'' t \ Ru"'Xu! r',ll''-'1
Dcllor ... l-s lji., . . 'a l'" J,b..d :_ sj I \ ^\. 5 ! {n
, , ,,' , 5,\ ""' ,ta,,r
"/
DsC C 0,0, N.w D- ni .. M \ Soo '
.;?) 'o'
.rd.0 tr ca. Te"" cs o.i. r.
'e \4-obai " s,D+{ \... ,5^.,
I ! i+-t',t.
lr$, & Tr.b.o tro. .,Jeq D-,i .'- '.
Nin" .on.n1c s\, c n rlr t.r.nco. V;L'b! ) r r. . I G
'l jrli SM K^usBrL P^RtrG (,4rernar.)
officc orrcxtile co,ni,ission* M!;iGi sHr Ar^Y PANDr'
soRr lvl. BAL!.ir^vY l,a/rc,d/z)
Oicnhl InliNtructuro Lnnncd,
lEC Udveciry of Technolosy, Cha.digarh
Dr P K. Gurh (,lrs,,,re)
Ilastindin Foundalion, Mumbri SrLR SURLNDER CrrouDrrARY
SHr LK SNGL lrr.rlrrtl
R.ini ltrduslries Privare L1d, Mumbri
Shxpoo!i PalLarji & Co Lnntcd, NePUr
s IIFMAT_I ConiAr, losr l,lr!/trd/z)

Syndretic & At SiLk MiLh R.scrrch A$ourrior' Mlnbri S rr RAvi Puus8 Sr\.H
Sr R hEVNm SuNlsE (,.{re,',rz)

Textile CoMrittee. New Delhi

S n' \r SA$L._a {,.1/rsr,,/.)

ILr pesonti crpaciry (Jd O/./ J,.h Nasn. fii 1ll4 RDul

SHir PuDHA(AI Rrr, Scientnr 'E and Head (TXD)

lRepEsrrirg Dnedor Ocrerrl (rr ol.,o)l

Scicnrht C (TxD), BIs

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