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(Issued 1 Dec.

1973) C 38

CRD-C 38-73

METHOD OF TEST FOR


TEMPERATURE RISE IN CONCRETE

1. Scope 2.1.4.1 An electronic recording po-


tentiometer accurate to ±0.3 F
1.1 This method covers a proce- (±0.2 C),
dure for determining the temperature 2.1.4.2 a precision resistance
rise in concrete under adiabatic con- bridge, the least dial division of which
ditions primarily due to heat liberated is 0.0001 ohm,
on hydration of cement. 2.1.4.3 an electronic null indicator,
2.1.4.4 ten precision resistance
2. Apparatus thermometers, and
2.1.4.5 five iron-constantan
2.1 The apparatus used shall con- thermocouples.
sist of: 2.1.5 Jacket.- A sheet metal jacket
2.1.1 Cabinet.- An insulated cabi- (Fig. 2) to hold insulation material
net with heating elements and fans. around the specimen container. The
2.1.2 Room.- A controlled temper- jacket shall be 34 in. (864 mm) in di-
ature room capable of maintaining any ameter and 36 in. (914 mm) high; its
selected temperature within the range bottom shall be covered on the inside
of 35 to 135 F (2 to 58 C), and also of with polystyrene i n s u l a t i o n 2 i n .
automatic variation to maintain a con- (51 mm) thick.
stant difference of 0 to 10 F (0 to 6 C) 2.1.6 Specimen Container.- A sheet
between the room temperature and the metal specimen container, 30 in.
temperature in the insulated cabinet, (762 mm) in diameter and 30 in.
which is situated within the room. (762 mm) high, with a 1/2-in. (13-mm)-
2.1.3 Control Apparatus.- The flange at the top. A strap (1/8 by
temperature control apparatus (Fig. 1) 1 in.) (3.2 by 25 mm) shall extend
shall consist of the following: diametrically across the inside of the
2.1.3.1 An electronic indicating po- container at the top. The strap shall
tentiometer accurate to ±0.3 F (0.2 C) have five 1/2-in.- (13-mm-) diameter
to control the temperature of the holes, one at the midpoint and two on
room, and either side at 2 and 12 in. (50 and
2.1.3.2 a d-c amplifier, a magnetic 305 mm) from the midpoint.
amplifier, and an electronic recording 2.1.7 Specimen Container Cover.-
potentiometer with an 11-in. (279-mm) A specimen container cover of sheet
scale having a range of -0.4 to +0.4 F metal with holes corresponding to the
(-0.2 to +0.2 C), with least division holes in the strap (subpara 2.1.6).
of 0.004 F (0.002 C). These three Airtight packing glands shall be
instruments act in combination and brazed or soldered in place on the
are actuated by unbalance in a resis- container cover over the five holes.
tance bridge, one leg of which repre- The packing glands shall be of a size
sents concrete specimen temperature suitable for tightening on the shafts
and another of which represents cabi- of the resistance thermometers which
n e t t e m p e r a t u r e . They shall be will pass through the holes (para 3).
capable of maintaining cabinet air
temperature the same as specimen 3. Test Procedure
temperature or slightly higher or
lower than specimen temperature as 3.1 Calibration.- The ten resis-
may be necessary for the adjustments tance thermometers, which shall be
described in Paragraph 3.10. Accu- permanently wired to a terminal strip
racy of control shall be ±0.004 F within the cabinet, shall be calibrated,
(±0.002 C). by clipping the leads, to read to
2.1.4 Recording Apparatus.- The ±0.005 F (±0.003 C) at three constant
temperature measuring and recording temperatures covering the expected
apparatus (Fig. 1) shall consist of the range of the adiabatic temperature-
following: rise test. F o r t h i s p u r p o s e t h e

1
(Issued 1 Dec. 1973)

2 TEST FOR TEMPERATURE RISE IN CONCRETE (C 38-73)

Fig. 1. Temperature control and measuring equipment


for two adiabatic calorimeters

thermometers shall be taped together


and tested in a vacuum flask located
within the cabinet. During the cali-
bration, air currents shall be excluded
from the vacuum flask by use of pack-
ing material at the top. When the cal-
ibration of all thermometers is within
±0.005 F (±0.003 C) of the average,
each thermometer’s remaining de-
viation from the average shall be used
as a correction for that thermometer.
3.2 Positioning of Thermometers.-
The resistance thermometers shall be
positioned as follows: one suspended
in the air of the cabinet, two on oppo-
site sides inside the jacket, two on op-
posite sides outside the specimen con-
tainer, and five (Fig. 2) inside the
specimen container. The five ther-
Fig. 2. P r e p a r i n g m a s s c o n c r e t e mometers placed in the specimen con-
specimen for temperature-rise tainer shall be threaded through the
test; jacket and positioning of holes in the cover, passed through the
thermometers in specimen holes in the strap across the top of
are shown the container, and held in place during
(Issued 1 Dec. 1973) C 38

TEST FOR TEMPERATURE RISE IN CONCRETE (C 38-73) 3

placement of concrete by wooden 3.7 Sealing Specimen.- Immediately


straps near the top. Except for the after the concrete has been placed
air thermometer, all the thermom- (subpara 3.5 above) and vibrated, the
eters shall be positioned in a straight cover shall be soldered in place and
line passing diametrically through the the packing glands tightened; it is es-
midplane of the specimen container. sential that the specimen container,
3.3 Insulation.- The jacket shall be cover, and packing glands be vapor-
placed on a warehouse dolly in such a tight. One thermocouple shall be
position that it will be in the approxi- taped against the metal cover near the
mate center of the cabinet when the center, two suspended in air within the
dolly is rolled into the cabinet. The cabinet, and two suspended in air in
specimen container shall be placed the controlled temperature room; of
inside the jacket, the annular space these, one at each location shall be
filled with expanded vermiculite in- connected to the electronic recording
s u l a t i o n ( A S T M D e s i g n a t i o n : C 516, potentiometer and one at each air lo-
Type 2), a n d t h e w h o l e a s s e m b l y a l - cation shall be connected to the elec-
lowed to remain overnight in the cal- tronic indicating potentiometer used
orimeter room, which shall be main- to control room air temperature.
tained at approximately the expected 3.8 Final Insulation.- Expanded
casting temperature. vermiculite insulation shall be placed
3.4 Room Temperature Adjust- on top of the specimen container to a
ment.- The next day the approximate depth of about 3 in. (76 mm). The total
casting temperature shall be deter- amount of vermiculite used on the
mined as soon as possible, and the sides (Sec. 3.3) and top shall be 120 ±
room temperature shall be adjusted 20 lb (54 ± 9 kg). T h e t e s t a s s e m b l y
to agree closely with the casting tem- shall be rolled into the cabinet, and
perature. Room temperature will the door closed. The temperature of
later be adjusted and controlled as the room shall then be lowered to and
prescribed in Subparagraph 3.8 below. thereafter controlled at a tempera-
The door of the cabinet shall remain ture about 10 F (6 C) below cabinet
open during casting of the specimen. temperature.
3.5 Specimen.- The specimen shall 3.9 Temperature Recording.- The
b e m a d e f r o m a s i n g l e 1 1 . 9 f t3 ( 0 . 3 m3 ) temperatures indicated by the ten pre-
batch of concrete, made in accordance cision thermometers, as measured by
with the applicable provisions of CRD- means of the precision bridge, shall
C’s 10 and 49, shall be placed and vi- be recorded as soon as the thermom-
brated in three layers in the specimen eters are covered, again after 1 hr
container to form a cylindrical spec- and after 2 hr, and thence daily (dur-
imen 30 in. (762 mm) in diameter ing workdays) for 28 days. The air
and approximately 29 in. (737 mm) in thermometer and the central concrete
height. thermometer are normally connected
3.6 Temperature Balancing.- When to the automatic cabinet air tempera-
the precision thermometers are cov- ture control, forming two legs of the
ered with concrete during the place- resistance bridge network, Paragraph
ment of the specimen, the difference 2.1.3.2. They may, however, be
between concrete temperature and be switched to the precision bridge for
room temperature shall be noted and their temperatures to be read.
reduced promptly by manual control 3.10 Temperature Control Adjust-
of room temperature so that the dif- ment.- The temperature of the con-
ference shall be no more than ±0.4 F crete for the record and for control
(±0.2 C), the total range of the control adjustment purposes shall be the av-
potentiometer, which operates in an erage of four temperatures, two of
indicating, rather than a control, ca- which are the temperatures of the
pacity during this step of the proce- thermometers that are 2 in. (51 mm)
dure. This type of control is possible, distant from the center of the speci-
and necessary, only during the time men and two of which are the tem-
the door of the cabinet is open. peratures of the thermometers that
(Issued 1 Dec. 1973)

4 TEST FOR TEMPERATURE RISE IN CONCRETE (C 38-73)

are 12 in. (305 mm) distant from the difference kept. The accumulated dif-
center. The controls shall be ad- ference at the end of the test should
justed to initiate compensation for not be more than ±0.02 F (±0.01 C).
any difference between the concrete 3.11 Correction for Heat Loss.-
temperature so obtained and the tem- The temperature rise at any time
perature of the air as represented shall be increased by 4.0 percent to
by the average temperature of the two account for the heat loss to the insu-
thermometers that are located inside lation (Note).
the metal jacket. The adjustment is
accomplished either by moving the Note.- This correction is based on approximate cal-
pointer of the recording potentiome- culations involving heat capacities and the ratio of in-
side area to total area of the container.
ter, Paragraph 2.1.3.2, or by varying
resistors that are placed for this pur-
pose in series with the air and con- 4. Report
crete resistance thermometers. The
difference noted on the casting day 4.1 The report shall contain rel-
may be ignored; but beginning the first evant data on aggregates and mix-
day after casting, adjustments shall ture proportions, and a table and
be made as necessary on each work- plot of the corrected temperature-
day, and a cumulative record of the rise data.

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