LAMPIRAN

Lampiran 1 Standar kekeruhan ion sulfat (SO42-)

Kekeruhan
Volume Konsentrasi Kekeruhan
Larutan terkoreksi
(mL) (ppm) (NTU)
(NTU)
Blanko 0.00 0.00 16.00 0.00
Standar 1 0.25 8.70 21.57 5.57
Standar 2 0.50 17.4 44.20 28.20
Standar 3 0.75 26.1 59.50 43.50
Standar 4 1.00 34.8 130.33 114.33
Standar 5 1.25 43.5 158.00 142.00
Standar 6 1.50 52.2 165.67 149.67
Contoh perhitungan :
1. Kekeruhan terkoreksi = kekeruhan standar - kekeruhan blanko
= 21.57 NTU – 16.00 NTU
= 5.57 NTU

2. [SO42-] = [K2SO4] x BM K2SO4 x 1000

= 0.01 M x 174 g/mol x 1000
= 1740 ppm

Volume standar ×konsentrasi sulfat

3. [standar 1] =
Volume total
0.25 mL × 1740 ppm
=
50 mL

= 8.70 ppm

180.00
y = 3.3169x - 17.532
160.00 R² = 0.933
Kekeruhan terkoreksi (NTU)

140.00
120.00
100.00
80.00
60.00
40.00
20.00
0.00
-20.00 0.0 10.0 20.0 30.0 40.0 50.0 60.0

-40.00
Konsentrasi (ppm)

Lampiran 2 Kurva deret standar SO42-

Lampiran 3 Data pengukuran kadar sulfat dengan turbidimetri
[SO42-]
Kekeruhan terkoreksi [SO42-]
Larutan Kekeruhan (NTU) sebenarnya
(NTU) (ppm)
(ppm)

Sampel 1 114 98 34.82 1741

Sampel 2 114 98 34.82 1741
Sampel 3 115 99 35.12 1756
Rerata 1746
SD 8.660
Ketelitian (%) 99.50
Contoh perhitungan (sampel 1) :
1. Kekeruhan terkoreksi = kekeruhan sampel 1 – kekeruhan blanko
= 114 NTU – 16 NTU
= 98 NTU

2. Konsentrasi SO42- dalam sampel :

y = 3.3169x – 17.532
98 = 3.3169[SO42-] – 17.532
98 + 17.532 = 3.3169[SO42-]
[SO42-] = 34.82 ppm

3. [SO42-]sebenarnya = [SO42-]sampel 1 × FP
= 34.82 ppm × 50
= 1741 ppm
4. Rerata [SO42-]
∑ni=1 xi (1741 + 1741 + 1756)
Rerata = = = 1746 NTU
n 3
5. Standar deviasi
∑n
i=1(xi −xrerata )
2 (1741−1746)2 +(1741−1746)2 +(1756−1746)2
SD = √ =√
n−1 3−1
= 8.660
6. Ketelitian
SD 8.660
Ketelitian = |1 − rerata| × 100% = |1 − | × 100% = 99.50 %
1746