On hold Date: 10/10/19

52K Pleated bottles

Leak Test Report By: YB

26 bags of 3.5oz Pleated Pouches were made during the last weekend of September, they were sampled by QC as per
Procedure, multiple samples found to have dents on the lip on top of the neck, which was suspected to cause a leak.

So, Challenging the product Quality we initiated a Test Procedure for Selected samples of the worst Lip defect, as shown
in below processes.
1. Leak test with air. Filled the pouches with 20 and 60 PSI air. Submerged them in water for at least 20 seconds to observe
any air bubbles indicating a leak. No leak found.

Pleated Bottle 3.5oz Pleated Bottle 3.5oz

Lot # Testing w/ Air 20 Lot # Testing w/ Air 60
Bag# Total pcs Bag# Total pcs
used psi used psi
9276 9 2 No leak 9276 10 10 No leak
9276 10 2 No leak 9276 11 10 No leak
9276 11 2 No leak 9276 12 10 No leak
9276 12 2 No leak 9276 16 10 No leak
9276 13 2 No leak 9276 19 10 No leak
9276 14 2 No leak 9276 20 10 No leak
9276 15 2 No leak 9276 22 10 No leak
9276 16 2 No leak 9276 23 10 No leak
9276 17 2 No leak 9276 24 10 No leak
9276 18 2 No leak 9277 1 10 No leak
9276 19 2 No leak 9277 8 10 No leak
Total pcs 22 Total pcs 110

2. Picture of the defects. (scratches on the lip / scratch on the side / and inside the neck.)

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 On hold Date: 10/10/19
52K Pleated bottles
Leak Test Report By: YB

3. Three damaged pouches were assembled on the lab crimper and vacuumed; waiting 24h to identify if vacuum will be lost.

Lot# 9276 Bag: 16

Date: 10/9/2019 Time 4:15pm Date: 10/10/2019 Time: 3:22pm

4. Testing pressure inside the can

Lot # used Testing Pressure

Bag # Range
Friday Monday
8.62 8.55 0.07
9 8.76 8.63 0.13
8.74 8.63 0.11
8.76 8.65 0.11
11 8.77 8.63 0.14
8.79 8.65 0.14
8.79 8.68 0.11
12 8.80 8.67 0.13
8.79 8.65 0.14
9276 8.72 8.59 0.13
13 8.77 8.62 0.15
8.83 8.68 0.15
8.71 8.57 0.14
15 8.80 8.69 0.11
8.79 8.63 0.16
8.79 8.65 0.14
17 8.77 8.64 0.13
8.79 8.66 0.13
8.79 8.64 0.15
18
8.88 8.74 0.14

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 On hold Date: 10/10/19
52K Pleated bottles
Leak Test Report By: YB

8.78 8.65 0.13

8.80 8.65 0.15
19 8.79 8.65 0.14
8.80 8.67 0.13
Avg 8.78 8.64 0.13
Max 8.88 8.74 0.16
Min 8.62 8.55 0.07
Range 0.26 0.19 0.09

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 On hold Date: 10/10/19
52K Pleated bottles
Leak Test Report By: YB

Drop test outside can: PASS

Picture after drop test.

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 On hold Date: 10/10/19
52K Pleated bottles
Leak Test Report By: YB

5. Testing on the oven temperature at 49°C

Oven on Oven on Oven on

Lot # used 10/11/2019 at 10/14/2019 at 10/21/2019
Bag # 11:30am 09:30am
Pcs Leaks Y/ N Leaks Y/ N Leaks Y/ N
10 1 No No No
9276 14 1 No No No
14 1 No No No
15 1 No No No

6. nformation of the production bags.

Lot# Bag# Start Time End time Op Group

9 2:45pm 3:35pm Dennis C
10 3:35pm 4:45pm Dennis C
11 4:45pm 5:55pm Dennis C
12 5:55pm 6:50pm Dennis C
13 6:50pm 7:45pm Oswaldo D
14 7:45pm 8:35pm Oswaldo D
15 8:35pm 9:30pm Oswaldo D
16 9:30pm 10:25pm Oswaldo D
9276 17 10:25pm 11:15am Oswaldo D
18 11:15am 12:10am Oswaldo D
19 12:10am 1:05am Oswaldo D
20 1:05am 2:00am Oswaldo D
21 2:00am 2:55am Oswaldo D
22 2:55am 3:45am Oswaldo D
23 3:45am 4:40am Oswaldo D
24 4:40am 5:50am Oswaldo D
25 5:50am 6:30am Oswaldo D

Lot# Bag# Start Time End time Op Group

9277 1 6:30am 7:15am Dennis A

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 On hold Date: 10/10/19
52K Pleated bottles
Leak Test Report By: YB

2 7:15am 8:15am Dennis A

3 8:15am 9:08am Dennis A
4 9:08am 10:01am Dennis A
5 10:01am 10:55am Dennis A
6 10:55am 12:31pm Dennis A
7 12:31pm 1:25pm Dennis A
8 1:25pm 2:25pm Dennis A
9 2:25pm 3:30pm Hung Do A

7. Conclusion

After testing the pouches that had scratches and marks on the neck and lip, we did not find any that leaked with air or

water.

Moreover, we don’t know and not able to test the effect of irradiation on our product, Therefor, we recommend the release

of the product, but to a less risky customer.

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