UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

Sample Elapsed KHCO3 Solid Rotor Fresh Temp Temp Temp

Number Time conc. in Feed Speed Solvent Stage 1 Stage 2 Stage 3
Notes
Solid NF NR TS T1
[% wt] [kg/hr] [rev/hr] [°C] [°C] [°C] [°C]

1 0:00:00 1.8 0.3750 5.3 25.0 55.2 54.8 54.6

2 0:00:15 1.8 0.3750 5.3 25.0 55.2 55.0 54.7
3 0:00:30 1.8 0.3750 5.3 25.0 55.2 55.0 54.6
4 0:00:45 1.8 0.3750 5.3 25.0 55.1 54.9 54.6
5 0:01:00 1.8 0.3750 5.3 25.0 55.0 54.8 54.6
6 0:01:15 1.8 0.3750 5.3 25.0 55.1 54.9 54.6
7 0:01:30 1.8 0.3750 5.3 25.0 55.1 54.9 54.5
8 0:01:45 1.8 0.3750 5.3 25.0 55.1 55.0 54.5
9 0:02:00 1.8 0.3750 5.3 25.0 55.0 55.0 54.7
10 0:02:15 1.8 0.3750 5.3 25.0 55.1 55.0 55.0
11 0:02:30 1.8 0.3750 5.3 25.0 55.1 55.1 55.1
12 0:02:45 1.8 0.3750 5.3 25.0 55.2 55.1 54.8
13 0:03:00 1.8 0.3750 5.3 25.0 55.3 55.1 55.5
14 0:03:15 1.8 0.3750 5.3 25.0 55.2 54.3 56.1
15 0:03:30 1.8 0.3750 5.3 25.0 55.2 54.3 56.1
16 0:03:45 1.8 0.3750 5.3 25.0 55.1 54.4 55.8
17 0:04:00 1.8 0.3750 5.3 25.0 55.2 54.5 55.7
18 0:04:15 1.8 0.3750 5.3 25.0 55.1 54.6 55.7
19 0:04:30 1.8 0.3750 5.3 25.0 55.0 54.8 55.7
20 0:04:45 1.8 0.3750 5.3 25.0 55.1 55.0 55.9
21 0:05:00 1.8 0.3750 5.3 25.0 55.0 55.0 56.0
22 0:05:15 1.8 0.3750 5.3 25.0 55.1 54.9 55.9
23 0:05:30 1.8 0.3750 5.3 25.0 55.1 54.8 55.7
24 0:05:45 1.8 0.3750 5.3 25.0 55.1 54.6 55.6
25 0:06:00 1.8 0.3750 5.3 25.0 55.0 54.7 55.6
26 0:06:15 1.8 0.3750 5.3 25.0 55.1 54.6 55.5
27 0:06:30 1.8 0.3750 5.3 25.0 55.1 54.6 55.4
28 0:06:45 1.8 0.3750 5.3 25.0 55.3 54.8 55.4
29 0:07:00 1.8 0.3750 5.3 25.0 55.2 54.9 55.3
30 0:07:15 1.8 0.3750 5.3 25.0 55.2 55.1 55.4
31 0:07:30 1.8 0.3750 5.3 25.0 55.3 55.1 55.3

Page 1
 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

32 0:07:45 1.8 0.3750 0.0 25.0 55.2 55.1 55.1

33 0:08:00 1.8 0.3750 0.0 25.0 54.2 54.8 54.7

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 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

Temp Cond Cond Cond Cond Stage 1 Stage 2 Stage 3 Stage 4 Pump Pump Pump
Stage 4 Stage 1 Stage 2 Stage 3 Stage 4 Conc1 Conc2 Conc3 Conc4 Stage 1 Stage 2 Stage 3
T4 C1 C2 C3 C4 N1 N2 N3
[°C] [mS] [mS] [mS] [mS] [% wt] [% wt] [% wt] [% wt] [litre/hr] [litre/hr] [litre/s]

48.2 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.7 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.1 0.0 0.0 0.0 0.1 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.0 0.0 0.0 0.0 0.1 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.5 0.0 0.0 0.0 0.3 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.8 0.0 0.0 0.0 0.8 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.0 0.0 0.0 0.0 0.5 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.7 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.1 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.6 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.7 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.7 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.4 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
47.1 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.7 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.6 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
46.2 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.9 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.4 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.2 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.1 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.3 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.2 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.2 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.4 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.4 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.6 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.6 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658

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 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

45.6 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658
45.7 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 10.2502 7.3762 9.4658

Page 4
 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

Final Miscella Final Miscella Final Miscella Final Miscella

M4 FLUJO
Volume Collected Time to Collect Flow Rate Flow Rate
densidad MASICO DE LA
V t Fm Fm
MISELA FINAL
[m³] [s] [litres/hr] [litres/hr]

0.1 35.0 10.2857 0.99960 10.2857 10.2816

0.1 35.0 10.2857 0.99960 10.2857 10.2816
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853
0.1 35.0 10.2857 0.99996 10.2857 10.2853

Page 5
 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

0.1 35.0 10.2857 0.99996 10.2857 10.2853

0.1 35.0 10.2857 0.99996 10.2857 10.2853

Page 6
 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

M1 flujo
M1 flujo masico
ML flujo MI FLUJO
Fresh Pump masico del Solid KHCO3 del
M4 FLUJO masico de MASICO DE
Solvent Stage 1 disolvente Feed conc. in disolvente
MASICO DE LA disolvente que NaHCO3 DE
TS N1 fresco que NF Solid fresco
MISELA FINAL se pierde en el ENTRADA AL
[°C] [litre/hr] ingresa al [kg/hr] [% wt] que
proceso PROCESO
sistema ingresa al
25.00000 10.25024 10.21626 10.28159 -0.06532 0.3750 1.8000 0.0068 10.21626
sistema
25.00000 10.25024 10.21626 10.28160 -0.06534 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626
25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626

Page 7
 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626

25.00000 10.25024 10.21626 10.28530 -0.06904 0.3750 1.8000 0.0068 10.21626

Page 8
 MI FLUJO UOP4 MkIIM1Solid/Liquid
flujo Extraction Unit - Run 1 Results
MASICO masico
DE del
MO NaHCO3 disolvent
SALIDA DE Cp e fresco
Stage 4 DE ENTRAD ? % DE capacida que Temp Fresh Q1 Pump Stage 2 Temp M2 FLUJO
Conc4 NaHCO3 A AL EXTRAC d ingresa Stage 1 Solvent NECESARIA ENERGIA Stage 2 Conc2 Stage 2 MASICO
DEL
DEL PROCES CION DE caorifica al T1 TS PARA LA N2 DISOLVENT
[% wt] PROCES O NaHCO3 del agua sistema [°C] [°C] 1ETAPA [litre/hr] [% wt] [°C] E FRESCO
0 O 0 0.00675 0 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 54.83398 7.544266
0 0 0.00675 0 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 54.98047 7.545218
0.005182 0.000529 0.00675 7.84361 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 55.0293 7.545536
0.007799 0.000797 0.00675 11.80326 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 54.93164 7.544901
0.018376 0.001877 0.00675 27.81197 4184 10.21626 54.98047 25 1281511 7.376221 0.0000 54.83398 7.544266
0.042757 0.004368 0.00675 64.71348 4184 10.21626 55.07813 25 1285685 7.376221 0.0000 54.88281 7.544583
0.026537 0.002711 0.00675 40.16462 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 54.93164 7.544901
0 0 0.00675 0 4184 10.21626 55.07813 25 1285685 7.376221 0.0000 55.0293 7.545536
0.002591 0.000265 0.00675 3.921421 4184 10.21626 55.0293 25 1283598 7.376221 0.0000 55.0293 7.545536
0 0 0.00675 0 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 55.0293 7.545536
0 0 0.00675 0 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 55.07813 7.545854
0 0 0.00675 0 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 55.12695 7.546173
0 0 0.00675 0 4184 10.21626 55.32227 25 1296121 7.376221 0.0000 55.07813 7.545854
0 0 0.00675 0 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 54.3457 7.541115
0 0 0.00675 0 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 54.29688 7.540802
0 0 0.00675 0 4184 10.21626 55.07813 25 1285685 7.376221 0.0000 54.39453 7.541429
0 0 0.00675 0 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 54.54102 7.542372
0 0 0.00675 0 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 54.63867 7.543002
0 0 0.00675 0 4184 10.21626 55.0293 25 1283598 7.376221 0.0000 54.78516 7.54395
0 0 0.00675 0 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 55.0293 7.545536
0 0 0.00675 0 4184 10.21626 55.0293 25 1283598 7.376221 0.0000 55.0293 7.545536
0 0 0.00675 0 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 54.93164 7.544901
0 0 0.00675 0 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 54.78516 7.54395
0 0 0.00675 0 4184 10.21626 55.07813 25 1285685 7.376221 0.0000 54.58984 7.542687
0 0 0.00675 0 4184 10.21626 54.98047 25 1281511 7.376221 0.0000 54.6875 7.543317
0 0 0.00675 0 4184 10.21626 55.12695 25 1287772 7.376221 0.0000 54.58984 7.542687
0 0 0.00675 0 4184 10.21626 55.07813 25 1285685 7.376221 0.0000 54.58984 7.542687
0 0 0.00675 0 4184 10.21626 55.27344 25 1294034 7.376221 0.0000 54.78516 7.54395
0 0 0.00675 0 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 54.88281 7.544583
0 0 0.00675 0 4184 10.21626 55.22461 25 1291946 7.376221 0.0000 55.07813 7.545854
0 0 0.00675 0 4184 10.21626 55.27344 25 1294034 7.376221 0.0000 55.12695 7.546173

Page 9
 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

0 0 0.00675 0 4184 10.21626 55.17578 25 1289859 7.376221 0.0000 55.07813 7.545854

0 0 0.00675 0 4184 10.21626 54.19922 25 1248116 7.376221 0.0000 54.83398 7.544266

Page 10
 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

Cp M3 FLUJO
capacida Temp Pump Stage 3 Temp MASICO
d Stage 4 Q2 ENERGIA Stage 3 Conc3 Stage 3 DEL
NECESARIA DISOLVNET
caorifica T4 PA LA 2 N3 E FRESCO
del agua [°C] ETAPA [litre/s] [% wt] [°C]
4184 48.24219 208071.4543 9.46582 0.0000 54.58984 9.6811091
4184 47.65625 231219.6724 9.46582 0.0000 54.6875 9.6819249
4184 47.11914 249727.7684 9.46582 0.0000 54.58984 9.6811091
4184 46.97266 251248.1344 9.46582 0.0000 54.63867 9.6815168
4184 46.5332 262015.9054 9.46582 0.0000 54.63867 9.6815168
4184 45.75195 288229.604 9.46582 0.0000 54.63867 9.6815168
4184 46.04492 280534.7268 9.46582 0.0000 54.54102 9.6807018
4184 46.67969 263601.5334 9.46582 0.0000 54.54102 9.6807018
4184 47.11914 249727.7684 9.46582 0.0000 54.73633 9.6823334
4184 47.55859 235854.0035 9.46582 0.0000 54.98047 9.6843826
4184 47.70508 232780.7627 9.46582 0.0000 55.07813 9.6852053
4184 47.70508 234332.2505 9.46582 0.0000 54.78516 9.6827424
4184 47.36328 243571.9239 9.46582 0.0000 55.46875 9.6885132
4184 47.11914 228012.6862 9.46582 0.0000 56.05469 9.6935266
4184 46.72852 238787.1491 9.46582 0.0000 56.05469 9.6935266
4184 46.63086 244969.7627 9.46582 0.0000 55.81055 9.6914301
4184 46.48438 254245.6879 9.46582 0.0000 55.66406 9.6901774
4184 46.5332 255807.9441 9.46582 0.0000 55.66406 9.6901774
4184 46.48438 262004.9095 9.46582 0.0000 55.71289 9.6905945
4184 46.19141 279016.8277 9.46582 0.0000 55.9082 9.6922674
4184 45.89844 288266.0043 9.46582 0.0000 55.95703 9.6926867
4184 45.41016 300572.9216 9.46582 0.0000 55.85938 9.6918485
4184 45.16602 303617.454 9.46582 0.0000 55.66406 9.6901774
4184 45.11719 298943.7763 9.46582 0.0000 55.61523 9.6897607
4184 45.26367 297427.7047 9.46582 0.0000 55.56641 9.6893444
4184 45.16602 297402.829 9.46582 0.0000 55.46875 9.6885132
4184 45.21484 295861.8817 9.46582 0.0000 55.41992 9.6880982
4184 45.36133 297452.6326 9.46582 0.0000 55.41992 9.6880982
4184 45.41016 299018.9475 9.46582 0.0000 55.32227 9.6872695
4184 45.55664 300610.9187 9.46582 0.0000 55.37109 9.6876836
4184 45.55664 302165.2704 9.46582 0.0000 55.27344 9.6868558

Page 11
 UOP4 MkII Solid/Liquid Extraction Unit - Run 1 Results

4184 45.60547 299069.3243 9.46582 0.0000 55.07813 9.6852053

4184 45.6543 289758.766 9.46582 0.0000 54.6875 9.6819249

Page 12