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PETRONAS RAPID Project Nov 2012

Johor, Malaysia
350 KTA LLDPE PLANT Vol. : 4
Project n° 61070F
Process Design Package

VOLUME 4

CHAPTER 3

PROCESS INTERLOCK DESCRIPTION

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial
Services UK Limited, and the information and images it contains are strictly confidential and may not be altered or
amended, copied, used or disclosed without the express permission of INEOS Commercial Services UK Limited.
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Technologies RAPID L20 INE PRO DES 3200 0013


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SPECIFICATION

PROCESS INTERLOCK DESCRIPTION

PROCESS INTERLOCK DESCRIPTION

1 11-DEC-12 PDP update FMA A. CONIL A. CONIL


0 5-NOV-12 ISSUE FOR PDP A. CONIL A. CONIL A. CONIL
XA 28-SEP-12 PRELIMINARY ABA A. CONIL A. CONIL
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Document revisions.

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and the information and
images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the express permission of INEOS Commercial
Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 2 / 110

PROCESS INTERLOCK DESCRIPTION

CONTENTS
1. INTRODUCTION................................................................................................................................................................ 7
1.1 MISCELLANEOUS ................................................................................................................................................... 8
1.2 ABBREVIATIONS ..................................................................................................................................................... 8
1.3 REFERENCE DOCUMENTS .................................................................................................................................. 8
2. INTERLOCK TABLES .................................................................................................................................................... 10
2.1 SECTION 100 .......................................................................................................................................................... 10
I-1010-O: FLARE DRUM PUMPS ................................................................................................................................. 10
I-1012-O: FLARE KO DRUM OVERFILL ..................................................................................................................... 10
I-1013-O: BACK FLOW FROM OSBL TO FLARE ...................................................................................................... 10
I-1020-O: LP CONDENSATE RETURN PUMPS PROTECTION ............................................................................. 11
I-1508-O: POWDER RECEIVER DRUM EMPTYING ................................................................................................ 11
I-1601-O: POLYMER WATER EXPORT PUMP STOP / START BY LEVEL CONTROL ..................................... 11
I-1702-O: PHNP (HIGH PRIORITY HP NITROGEN) NITROGEN SUPPLY PRIORITY ...................................... 12
I-1730-S: BACKFLOW INTO PHNP NITROGEN FROM USERS ............................................................................ 12
I-1731-S: BACKFLOW INTO MN NITROGEN FROM MN AND LN USERS .......................................................... 12
I-1732-S: BACKFLOW INTO LP NITROGEN FROM MPN USERS ........................................................................ 13
I-1733-S: BACKFLOW INTO LP NITROGEN MAIN HEADER ................................................................................. 14
I-1744-S: BACKFLOW INTO HP NITROGEN FROM NITROGEN TREATERS .................................................... 14
I-1751-S: BACKFLOW INTO LP NITROGEN FROM LPN USERS ......................................................................... 14
2.2 SECTION 200 .......................................................................................................................................................... 16
I-2025-O: HIGH TEMPERATURE IN STEAM CONDENSATE HEADER FROM ETHYLENE REGENERATION
HEATER ............................................................................................................................................................................ 16
I-2302-S: ETHYLENE O2 AND CO REMOVAL TREATERS EXOTHERM ............................................................ 16
I-2303-S: LOW PRESSURE AT SUCTION OF ETHYLENE COMPRESSOR ....................................................... 18
I-2304-S: FPU ETHYLENE DEPRESSURISATION ................................................................................................... 18
I-2305-O: ETHYLENE RECYCLE COMPRESSOR AUTO-START ......................................................................... 19
I-2306-S: LOW TEMPERATURE IN ETHYLENE O2 AND CO TREATERS .......................................................... 19
I-2307-S: REGENERATION AIR TO FLARE............................................................................................................... 20
I-2308-O: ETHYLENE CO/O2 TREATERS EXOTHERM DUE TO EXCESS H2 INJECTION ............................ 20
I-2309-S: HC RELEASED TO ATM DURING ETHYLENE TREATERS REGENERATION ................................ 21
I-2310-O: ETHYLENE CO/O2 TREATERS EXOTHERM DUE TO EXCESS O2 INJECTION ............................ 21
I-2311-O: HIGH PRESSURE AT ETHYLENE COMPRESSOR ............................................................................... 22
I-2312-O: ETHYLENE FEED TO TREATERS HEATING CUT-OFF ....................................................................... 22
I-2314-O: BACKFLOW THROUGH ETHYLENE COMPRESSOR MINI FLOW LINE ........................................... 22
I-2323-S: BACKFLOW INTO REGENERATION INSTRUMENT AIR FROM ETHYLENE TREATERS ............. 23
I-2324-S: HC RELEASED TO ATM DURING COMONOMER OR PENTANE TREATERS REGENERATION 23
I-2327-S: LOW TEMPERATURE IN ETHYLENE ADSORBERS ............................................................................. 24
I-2328-O: BACKFLOW INTO H2 FROM CO/O2 ETHYLENE TREATER ............................................................... 24
I-2410-S: COMONOMER PREPARATION UNIT ISOLATION ................................................................................. 25
I-2411-O: COMONOMER PUMPS ................................................................................................................................ 25
I-2412-O: COMONOMER DRUM OVERFILLING ....................................................................................................... 26
I-2416-S: COMONOMERS SIMULTANEOUS FEED................................................................................................ 26
I-2417-O: COMONOMER INJECTION PUMPS .......................................................................................................... 27
I-2420-S: PENTANE PREPARATION UNIT ISOLATION.......................................................................................... 27

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


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PROCESS INTERLOCK DESCRIPTION

I-2421-O: PENTANE PUMPS ........................................................................................................................................ 28


I-2422-O: PENTANE STORAGE DRUM OVERFILLING........................................................................................... 29
I-2425-S: LRU OR TEAL BACKFLOW TO PENTANE ............................................................................................... 29
I-2426-O: PENTANE STORAGE DRUM AUTOMATIC REFILLING ........................................................................ 29
I-2439-S: LOW TEMPERATURE IN PENTANE TREATERS ................................................................................... 30
I-2458-S: LOW TEMPERATURE IN COMONOMER TREATERS ........................................................................... 30
I-2470-S: HYDROGEN TREATMENT UNIT ISOLATION .......................................................................................... 30
I-2471-S: LOW PRESSURE AT HYDROGEN COMPRESSOR A SUCTION ........................................................ 31
I-2474-O: HIGH PRESSURE AT HYDROGEN COMPRESSOR A DISCHARGE ................................................. 32
I-2475-O: BACKFLOW FROM HYDROGEN TREATING SYSTEM INTO H2 OSBL PREVENTION ................. 32
I-2481-S : LOW PRESSURE AT HYDROGEN COMPRESSOR B SUCTION ...................................................... 32
I-2484-O: HIGH PRESSURE ON HYDROGEN COMPRESSOR B DISCHARGE ................................................ 33
I-2734-S: BACKFLOW OF H2 INTO REGENERATION NITROGEN FROM H2 TREATERS ............................. 33
I-2735-S: BACKFLOW OF HYDROGEN INTO REGENERATION NITROGEN FROM ETHYLENE TREATERS
............................................................................................................................................................................................ 33
I-2752-S: REGENERATION NITROGEN HEATER OVERHEATING...................................................................... 34
I-2760-S: NITROGEN CO/O2 REMOVAL TREATERS EXOTHERM ...................................................................... 34
I-2761-O: NITROGEN CO/O2 REMOVAL TREATERS EXOTHERM DUE TO EXCESS OF H2 INJECTION . 35
I-2764-O: N2 CO/O2 REMOVAL TREATERS EXOTHERM DUE TO EXCESS OF O2 INJECTION ................. 35
I-2765-O: LPN NITROGEN SUPPLY PRIORITY ........................................................................................................ 36
2.3 SECTION 300 .......................................................................................................................................................... 37
I-3060-O: COMONOMER / CATALYST COMBINATION .......................................................................................... 37
I-3061-S: SIMULTANEOUS INJECTION OF ZIEGLER AND METALLOCENE .................................................... 38
I-3069-O: ZIEGLER CATALYST (SDX) STOCK LINES BACK FLOW .................................................................... 39
I-3070-S: ZIEGLER CATALYST (SDX) STORAGE HP/LP INTERFACE ............................................................... 39
I-3071-O: HP NITROGEN OPEN PATH TO CV (SDX) ............................................................................................. 39
I-3077-S: ZIEGLER CATALYST (SDX) STOCK LINES BACK FLOW FROM REACTOR ................................... 40
I-3078-O: ZIEGLER CATALYST CONVEYING LINE PLUGGING........................................................................... 40
I-3079-O: ZIEGLER CATALYST CONVEYING LINE PLUGGING........................................................................... 41
I-3080-O: METALLOCENE CATALYST CONVEYING LINE PLUGGING ............................................................. 41
I-3081-O: METALLOCENE CATALYST CONVEYING LINE PLUGGING .............................................................. 42
I-3082-O: METALLOCENE CATALYST CONVEYING LINE PLUGGING .............................................................. 42
I-3087-O: CATALYST STINGER ASSIST GAS .......................................................................................................... 43
I-3169-O: ZIEGLER CATALYST (NCT) STOCK LINES BACK FLOW .................................................................... 44
I-3170-S: ZIEGLER CATALYST (NCT) STORAGE HP/LP INTERFACE ............................................................... 44
I-3171-O: HP NITROGEN OPEN PATH TO CV (NCT) ............................................................................................. 44
I-3177-S: ZIEGLER CATALYST (NCT) STOCK LINES BACK FLOW FROM REACTOR ................................... 45
I-3269-O: METALLOCENE CATALYST STOCK LINES BACK FLOW ................................................................... 46
I-3270-S: METALLOCENE CATALYST STORAGE HP/LP INTERFACE ............................................................... 46
I-3271-O: HP NITROGEN OPEN PATH TO CV ......................................................................................................... 47
I-3277-S: METALLOCENE CATALYST STOCK LINES BACK FLOW FROM REACTOR .................................. 47
2.4 SECTION 400 .......................................................................................................................................................... 48
I-4001-S: BATTERY LIMIT ISOLATION FOR PEG PLANT ...................................................................................... 48
I-4009-S: MAIN LOOP SEPARATOR ISOLATION ..................................................................................................... 49
I-4011-S: BACK FLOW INTO ETHYLENE HEADER FROM GAS LOOP............................................................... 49
I-4013-O: BACK FLOW INTO COMONOMER FEEDING FROM MAIN LOOP SEPARATOR ............................ 49
I-4014-O: BACK FLOW INTO COMONOMER FEEDING FROM GAS LOOP (K400 DISCHARGE) ................. 50
I-4015-S: BACK FLOW INTO LIQUID ADDITIVE B1 UNLOADING STATION DRUMS ...................................... 50
I-4016-S: BACK FLOW INTO VRU MAIN SEPARATOR FROM GAS LOOP ........................................................ 50
I-4017-O: BACK FLOW INTO VRU COMPRESSOR SUCTION DRUM FROM GAS LOOP............................... 51
I-4018-S: REACTOR FEEDS EMERGENCY ISOLATION ........................................................................................ 51
I-4019-O: BACK FLOW INTO PURGE COLUMN FROM REACTOR VIA START-UP POWDER LINE ............ 53

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 4 / 110

PROCESS INTERLOCK DESCRIPTION

I-4020-S: TEAL SYSTEM ISOLATION ......................................................................................................................... 53


I-4021-S: MAXI KILL........................................................................................................................................................ 54
I-4022-S: BACK FLOW INTO LIQUID ADDITIVE S1 UNLOADING STATION DRUMS ...................................... 55
I-4023-S: BACK FLOW INTO VRU C8 COMPRESSOR SUCTION DRUM FROM GAS LOOP ......................... 55
I-4024-O: NITROGEN BACK-UP FOR MAIN LOOP COMPRESSOR PURGE GAS ........................................... 56
I-4025-S: BACK FLOW INTO H2 FEED FROM REACTOR ..................................................................................... 56
I-4029-O: OVERHEATING COOLING WATER LOOP PROTECTION ................................................................... 56
I-4031-S: BACK FLOW INTO H2 FROM METALLOCENE CATALYST INJECTION ........................................... 57
ST
I-4032-O: BACK FLOW INTO PENTANE FEED OR INTO 1 STAGE K.O. DRUM OF RECYCLE GAS
COMPRESSOR ............................................................................................................................................................... 57
DEGASSING VARIABLE TRIP SETTINGS ................................................................................................................. 58
I-4041-S: POOR DEGASSING: REACTOR LOW TEMPERATURE ....................................................................... 62
I-4042-S: STOP CATALYST FEEDERS: DEGASSING CAPACITY LIMIT ............................................................ 62
I-4071-S: HP LIQUID INJECTION PUMPS ................................................................................................................. 63
I-4072-S: BACK FLOW INTO NITROGEN / ETHYLENE FROM HP LIQUID INJECTION .................................. 64
I-4080-S: LIQUID CARRY OVER TO MAIN LOOP COMPRESSOR ...................................................................... 64
I-4410-S: TEAL TO NITROGEN BACKFLOW............................................................................................................. 65
I-4447-O: TEAL AND LIQUID ADDITIVES SIMULTANEOUS INJECTION ............................................................ 65
I-4538-O: TEAL PUMP OVERPRESSURE ................................................................................................................. 65
I-4554-O: STOP TEAL INJECTION WHEN NO ZIEGLER CATALYST INJECTION ............................................ 66
I-4555-S: BACK FLOW INTO TEAL FEED .................................................................................................................. 66
2.5 SECTION 600 .......................................................................................................................................................... 68
I-6204-S: OVERPRESSURISATION OF DEGASSER .............................................................................................. 68
I-6207-O: OVERFILLING OF DEGASSER .................................................................................................................. 69
I-6305-S: POOR DEGASSING IN DEGASSER: HIGH HIGH PRESSURE ............................................................ 69
I-6329-O: OVERFILLING OF PURGE COLUMN OR CONVEYING FILTER OR CONVEYING LINE
BLOCKAGE OR OVERFILLING OF START-UP POWDER SILO ........................................................................... 69
I-6330-S: POOR DEGASSING IN DEGASSER: HIGH STRIPPING GAS FLOW ................................................. 71
I-6331-O: DEGASSER OUTLET ROTARY VALVE DAMAGE ................................................................................. 71
I-6333-O: DEGASSER RECYCLING LINE BLOCKAGE ........................................................................................... 72
I-6334-O: POWDER BUILD-UP IN DEGASSER RECYCLE ROTARY VALVE ..................................................... 72
I-6338-S: STOP DEGASSER FILLING WHEN IN EMPTY MODE .......................................................................... 72
I-6339-S: STOP POWDER FEEDING FROM DEGASSER WHEN POOR DEGASSING IN DEGASSER: LOW
RESIDENCE TIME .......................................................................................................................................................... 73
I-6340-S: POOR DEGASSING IN DEGASSER: LOW STRIPPING GAS FLOW .................................................. 73
I-6341-S: HIGH HC CONTENT IN STRIPPING GAS TO DEGASSER ................................................................... 74
I-6342-S: HIGH DIFFERENTIAL TEMPERATURE BETWEEN REACTOR AND DEGASSER .......................... 75
I-6368-O: N2 OR PROCESS GAS BREAKTHROUGH ON DEGASSER SAMPLING SYSTEM ........................ 75
I-6369-S: DEGASSER POWDER SAMPLING SYSTEM OPERATOR ................................................................... 76
I-6408-S: DEGASSING VENT ROUTED TO ATM AND SNUFFING SYSTEM ..................................................... 76
I-6409-O: AIR INGRESS AT PURGE COLUMN OFFGAS FAN .............................................................................. 77
I-6435-S: STOP PURGE COLUMN FILLING WHEN IN EMPTY MODE ................................................................ 77
I-6441-O: POOR DEGASSING IN PURGE COLUMN: LOW LEVEL AT STARTUP ............................................. 77
I-6442-S: POOR DEGASSING IN PURGE COLUMN: LOW STRIPPING GAS FLOW ........................................ 78
I-6443-S: POOR DEGASSING IN PURGE COLUMN: LOW RESIDENCE TIME ................................................. 78
I-6444-S: STOP STEAM INJECTION INTO PURGE COLUMN WHEN INSUFFICIENT NITROGEN FLOW .. 79
I-6445-S: POOR DEGASSING IN PURGE COLUMN: HIGH STRIPPING FLOW OR HIGH PRESSURE ....... 80
I-6446-O: PURGE COLUMN OUTLET ROTARY VALVE DAMAGE ....................................................................... 80
I-6462-S: PELLET WATER TOO HIGH TEMPERATURE – ABSORBED HC DRIVING OFF PELLETS (ALL
GRADES) .......................................................................................................................................................................... 81
I-6656-S: AIR INGRESS AT CONVEYING GAS BLOWER (A) ................................................................................ 81
I-6657-S: AIR INGRESS AT CONVEYING GAS BLOWER (B) ................................................................................ 81

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
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PROCESS INTERLOCK DESCRIPTION

I-6664-O: START-UP CONVEYING LINE BLOCKAGE ............................................................................................ 81


I-6665-O: DEGASSER RECYCLE ROTARY VALVE AND START-UP POWDER ROTARY VALVE DAMAGE
............................................................................................................................................................................................ 82
I-6666-O: PURGE COLUMN RECYCLING LINE BLOCKAGE................................................................................. 82
I-6667-O: START-UP SILO RECYCLING LINE BLOCKAGE PREVENTION ........................................................ 83
I-6668-O: START-UP SILO OUTLET ROTARY VALVE DAMAGE PROTECTION .............................................. 83
I-6701-S: LIQUID CARRY OVER TO RECYCLE COMPRESSOR .......................................................................... 83
I-6702-S: RECYCLE GAS COMPRESSOR SUCTION KO DRUM HIGH LEVEL ................................................. 84
I-6717-S: AIR INGRESS TO RECYCLE COMPRESSOR ......................................................................................... 84
I-6750-O: POOR DEGASSING IN DEGASSER: NITROGEN BACKUP ................................................................. 85
I-6754-O: LOW TEMPERATURE IN PIPE WORK FROM VRU MAIN SEPARATOR .......................................... 85
I-6756-O: VRU RECYCLE PUMPS ............................................................................................................................... 85
I-6771-O: VRU WASHING PUMPS PROTECTION ................................................................................................... 86
I-6772-O: BACK FLOW INTO RECYCLE COMPRESSOR FROM GAS LOOP .................................................... 86
I-6776-O: RECYCLE GAS COMPRESSOR CONDENSATE PUMPS .................................................................... 86
I-6777-O: AUTOMATIC VRU GAS TO NITROGEN SUPPLY TO THE DEGASSER FILTER BACK FLUSH ... 87
I-6778-O: RECYCLE GAS COMPRESSOR CONDENSATE PUMPS .................................................................... 87
I-6801-S: LIQUID CARRY OVER TO C8 COMPRESSOR ....................................................................................... 88
I-6802-S: C8 GAS COMPRESSOR SUCTION KO DRUM HIGH LEVEL ............................................................... 88
I-6805-S: POOR DEGASSING IN C8 DEGASSER: HIGH HIGH PRESSURE ...................................................... 88
I-6807-O: OVERFILLING OF C8 DEGASSER OR C8 CONVEYING FILTER OR CONVEYING LINE
BLOCKAGE ...................................................................................................................................................................... 89
I-6817-S: AIR INGRESS TO C8 RECYCLE COMPRESSOR................................................................................... 89
I-6830-S: POOR DEGASSING IN C8 DEGASSER: HIGH STRIPPING GAS FLOW ........................................... 89
I-6831-O: C8 DEGASSER OUTLET ROTARY VALVE DAMAGE ........................................................................... 90
I-6833-O: C8 DEGASSER RECYCLING LINE BLOCKAGE ..................................................................................... 90
I-6834-O: POWDER BUILD-UP IN C8 DEGASSER RECYCLE ROTARY VALVE ............................................... 91
I-6838-S: STOP C8 DEGASSER FILLING WHEN IN EMPTY MODE .................................................................... 91
I-6839-S: STOP POWDER FEEDING FROM C8 DEGASSER WHEN POOR DEGASSING IN C8
DEGASSER: LOW RESIDENCE TIME ........................................................................................................................ 91
I-6840-S: POOR DEGASSING IN C8 DEGASSER: LOW STRIPPING GAS FLOW ............................................ 92
I-6841-S: HIGH HC CONTENT IN STRIPPING GAS TO C8 DEGASSER ............................................................ 93
I-6842-S: HIGH DIFFERENTIAL TEMPERATURE BETWEEN REACTOR AND C8 DEGASSER .................... 93
I-6850-S: ENSURE ROUTING TO C8 DEGASSER WHEN IN C8 OPERATION .................................................. 94
I-6852-S: STOP POWDER FEEDING FROM C8 DEGASSER WHEN POOR DEGASSING IN DEGASSER:
START C8 WITH EMPTIED C8 DEGASSER ............................................................................................................. 95
I-6854-O: LOW TEMPERATURE IN PIPE WORK FROM C8 VRU MAIN SEPARATOR .................................... 95
I-6856-O: C8 VRU RECYCLE PUMPS ........................................................................................................................ 96
I-6871-O: C8 VRU WASHING PUMPS PROTECTION ............................................................................................. 96
2.6 SECTION 700 .......................................................................................................................................................... 97
I-7101-S: LIQUID RECOVERY ROUTING TO LRU OR TO DC .............................................................................. 97
I-7104-O: RECOVERED LIQUID FROM LRU ROUTING TO HCD STORAGE DRUM OR TO PROCESS ..... 97
I-7105-S: LRU UNIT ISOLATION .................................................................................................................................. 97
I-7106-O: LRU COLUMN FEED PUMP PROTECTION ............................................................................................ 98
I-7107-O: LRU COLUMN HIGH LEVEL ....................................................................................................................... 99
I-7108-O: LRU COLUMN LOW LEVEL OR HIGH TEMPERATURE ....................................................................... 99
I-7109-S: AIR INGRESS IN LRU COLUMN................................................................................................................. 99
I-7110-O: CLEAN HC DRAIN DRUM HIGH LEVEL ................................................................................................. 100
I-7112-O: LRU RECYCLE DRAIN DRUM HIGH LEVEL ......................................................................................... 100
I-7113-O: BACKFLOW FROM MAIN LOOP SEPARATOR TO LRU ..................................................................... 100
I-7115-O: LRU RECYCLE FAN ................................................................................................................................... 101
2.7 SECTION 800 ........................................................................................................................................................ 102

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
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PROCESS INTERLOCK DESCRIPTION

ST
I-8249-O: 1 EXTRUDER FEED SCREW ................................................................................................................ 102
ND
I-8250-O: 2 EXTRUDER FEED SCREW ................................................................................................................ 102
I-8251-O: EXTRUDER STOPPED .............................................................................................................................. 103
I-8252-O: ADDITIVE ACCUMULATION WHEN POWDER FEED TO EXTRUDER IS STOPPED................... 103
I-8256-S: NITROGEN AND DUST EXPLOSURE FOR OPERATOR IN ADDITIVE FIBC UNLOADING
STATIONS ...................................................................................................................................................................... 104
I-8260-O: POLYMER VIBRATING SCREEN WASTE SKIP SYSTEM .................................................................. 106
I-8417-O: PELLET CONVEYING HOPPER OVERFILLING ................................................................................... 106
I-8418-O: EXTRUDER SHUTDOWN DUE TO PELLETISER PROBLEM ............................................................ 106
I-8419-O: EXTRUDER SHUTDOWN DUE TO PELLET DRYER/DEWATERING STOPPAGE ........................ 107
I-8420-O: PELLET DRYER/DEWATERING .............................................................................................................. 107
I-8470-S: PELLETIZER HOOD OPENING WHILE HOT WATER CIRCULATING .............................................. 108
I-8471-S: PELLET DRYER/DEWATERING DOORS OPENING WHILE HOT WATER DIRECTED TO PELLET
DRYER ............................................................................................................................................................................ 108
I-8801-O: PELLET CONVEYING LINE FROM FEED HOPPER BLOCKAGE ..................................................... 109
2.8 LIST OF PROCESS DATA SHEETS INCLUDING INEOS TECHNOLOGIES CONTROL SPECIFIC
REQUIREMENTS .............................................................................................................................................................. 110

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 7 / 110

PROCESS INTERLOCK DESCRIPTION

1. INTRODUCTION

This chapter provides the narrative description of the DCS and SIS interlocks, which protect
the INEOS Technologies licensed process.

The DCS interlocks are noted I-xxxx-O and SIS I-xxxx-S and are shown on the PID drawings
with a diamond symbol as per:

I I

xxxx xxxx

S O

SIS interlocks DCS interlocks

xxxx is the serial number.

The implementation of interlocks in the DCS and the SIS must follow the requirements
described in the Instrument and Process Control Philosophy chapters “DCS hardware
implementation”, “SIS hardware implementation” and ”Interlock functionality”.

This document (Process Interlock Description) is a simplified description of the way that each
piece of logic should work. As such, all of the details are not explicitly described.

To improve reading of the document, the instrument and equipment tags do not include the
prefix 3200.

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 8 / 110

PROCESS INTERLOCK DESCRIPTION

1.1 MISCELLANEOUS

 The trip settings are not listed in this document. Values are gathered in the instrument
datasheets or instrument lists.

 Trip on control valves: when an interlock is activated and trips a control valve, 2 types
of trip are required:

 For a DCS interlock trip, the action on the valve is made via the DCS analogue output
to the valve positioner. The relevant action is noted FMC or FMO meaning that the
relevant controller is forced into manual mode and the output is forced to close or open
position. It will be noted ―FMC FIC-xxxxxx‖ or ―FMO FIC-xxxxxx‖ in the interlock
description.

 For a SIS interlock trip, the action on the valve is made via a solenoid valve installed on
the control valve actuator and via the DCS analogue output to the valve positioner.
The relevant actions are noted ―Close FV-xxxxxx (SIS)‖ or ―Open FV-xxxxxx (SIS)‖ in
the interlock description.

 When a DCS or a SIS interlock trips an on/off valve, if there is a corresponding control
valve, the DCS should force the control valve to manual and either open or close the
control valve, as appropriate. This will ensure that the control valve and controller are
in the correct state when the on/off valve is reset.

1.2 ABBREVIATIONS

 FMC: Forced manual close

 FMO: Forced manual open

 DCS: Distributed control system

 SIS: Safety instrumented system

 2oo3: Two out of three (voting)

 1oo2: One out of two (voting)

 1oo3: One out of three (voting)

 DE: Detailed engineering contractor

1.3 REFERENCE DOCUMENTS

 Instrument and Process control philosophy

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

 Instrument list and instrument data sheets

 PID

 Complex control and calculations description

 Sequence description

 Equipment Process Data Sheets

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

2. INTERLOCK TABLES

2.1 SECTION 100

I-1010-O: FLARE DRUM PUMPS


Hazard: Prevent pumps running dry
Causes:
LT-10501 (LL) Flare KO drum PID:0104
Actions:
Stop P-105A Flare drum pump PID:0104
AND
Stop P-105B Flare drum pump PID:0104
Notes:  Auto-reset interlock
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-1012-O: FLARE KO DRUM OVERFILL


Hazard: Liquid into flare with damage of the flare system and resulting fire or explosion.
Causes:
LT-10501 (H) Flare KO drum PID:0104
Actions:
Start spare pump P-105A or P-105B Flare drum pumps PID:0104
(pulse command) (note 1)
Notes:  Note 1: Detailed engineering to develop the duty/spare pump start-up
logic

Minimum SIL level: 0

I-1013-O: BACK FLOW FROM OSBL TO FLARE


Hazard: Overfilling of flare KO drum leading to flare damage
Causes:
PDT-10503 (LL) HC slops to OSBL PID:0104
Actions:
Close XV-10503 HC slops to OSBL PID:0104

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PROCESS INTERLOCK DESCRIPTION

Notes:  Auto-reset
Minimum SIL level: 0

I-1020-O: LP CONDENSATE RETURN PUMPS PROTECTION


Hazard: Prevent pumps running dry. Pump damage.
Causes:
LT-10612 (LL) LP condensate flash drum PID:0101
Actions:
Stop P-109A LP condensate pump PID:0101
AND
Stop P-109B LP condensate pump PID:0101
Notes:  Auto-reset interlock
Minimum SIL level: No SIL requirement by INEOS Technologies

I-1508-O: POWDER RECEIVER DRUM EMPTYING


Hazard: Risk of flare connection to atmosphere when emptying powder receiver drum.
Risk of air ingress into flare when depressurising powder receiver drum. Explosion.Risk of
nitrogen released when emptying powder receiver drum. Asphixiation.
Causes:
XZV-10307 not closed Powder relief vent drum bottom PID:0107
OR
XZV-10308 not closed Powder receiver drum to PV PID:0107
OR
PT-10305 (H) Powder receiver drum PID:0107
Actions:

Close XZV- 10309 Powder receiver drum emptying line PID:0107


Notes:
Minimum SIL level: 0

I-1601-O: POLYMER WATER EXPORT PUMP STOP / START BY LEVEL CONTROL


Hazard: Level control of the polymer water pit

Causes:
LT-10103 (SL) Polymer water pit PID:0108
Actions:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PROCESS INTERLOCK DESCRIPTION

Stop P-161 Polymer water pit pump PID:0108


Causes:
LT-10103 (SH) Polymer water pit PID:0108
Actions:
Start P-161 Polymer water pit pump PID:0108
Notes:  Auto-reset interlock
 The level control is described as an interlock for convenience but can
be developed as a sequence during detailed engineering
Minimum SIL level: No SIL requirement by Licensor

I-1702-O: PHNP (HIGH PRIORITY HP NITROGEN) NITROGEN SUPPLY PRIORITY


Hazard: Cut nitrogen supply to low priority users in case of nitrogen pressure drop.

Causes:
PT-20513 (LL) Nitrogen header PID:0215
Actions:
FMC PIC-10581 Nitrogen to low priority users PID:0102
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-1730-S: BACKFLOW INTO PHNP NITROGEN FROM USERS


Hazard: Backflow of HC into nitrogen headers from downstream users. Main consequence is
contaminated nitrogen used to degas powder in purge column leading to poor degassing.
Explosion in downstream equipments.
Causes:
PZDT-10314 (LL) PHNP from nitrogen treaters PID:0103
Actions:
Close XZV-10311 PHNP from nitrogen treaters PID:0103
Notes:
Minimum SIL level: 1

I-1731-S: BACKFLOW INTO MN NITROGEN FROM MN AND LN USERS


Hazard: Backflow of HC into nitrogen headers from downstream users. Main consequence is
contaminated nitrogen used to degas powder in purge column leading to poor degassing.
Explosion in downstream equipments.
Causes:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

PZDT-10184 (LL) MN from nitrogen treaters PID:0102


Actions:
Close XZV-10185 MN from nitrogen treaters PID:0102
Notes:
Minimum SIL level: 1

I-1732-S: BACKFLOW INTO LP NITROGEN FROM MPN USERS


Hazard: Backflow of HC into nitrogen headers from dowstream nitrogen. Main consequence is
contaminated nitrogen used to degas powder in purge column leading to poor degassing.
Explosion in downstream equipments.
Causes:
PZDT-10080 (LL) MPN to users other than purge column PID:0102
Actions:
Close XZV-10080 MPN to users other than purge column PID:0102
Notes:
Minimum SIL level: 1

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PROCESS INTERLOCK DESCRIPTION

I-1733-S: BACKFLOW INTO LP NITROGEN MAIN HEADER


Hazard: Backflow of HC into nitrogen headers from dowstream nitrogen. Main consequence is
contaminated nitrogen used to degas powder in purge column leading to poor degassing.
Explosion in downstream equipments.
Causes:
PZDT-10089 (LL) LP nitrogen to users PID:0102
Actions:
Close XZV-10090 LP nitrogen to users PID:0102
Notes:
Minimum SIL level: 1. DE to review the SIL rating after identification of consequences on
backflow to OSBL

I-1744-S: BACKFLOW INTO HP NITROGEN FROM NITROGEN TREATERS


Hazard: Backflow of HC into nitrogen headers from downstream users. Main consequence is
contaminated nitrogen used to degas powder in purge column leading to poor degassing.
Explosion in downstream equipments.
Backflow to OSBL with unkown consequences to be assessed by DE.
Causes:
PZDT-10319 (LL) HP nitrogen from OSBL PID:0102
Actions:
Close XZV-10319 HP nitrogen from OSBL PID:0102
Notes:
Minimum SIL level: 1. DE to review the SIL rating after identification of consequences on
backflow to OSBL

I-1751-S: BACKFLOW INTO LP NITROGEN FROM LPN USERS


Hazard: Backflow of HC into nitrogen headers from dowstream nitrogen. Main consequence is
contaminated nitrogen used to degas powder in purge column leading to poor degassing.
Explosion in downstream equipments.
Causes:
PZDT-10095 (LL) LP nitrogen to users PID:0102
Actions:
Close XZV-10095 LP nitrogen to users PID:0102

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PROCESS INTERLOCK DESCRIPTION

Notes:
Minimum SIL level: 1

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

2.2 SECTION 200

I-2025-O: HIGH TEMPERATURE IN STEAM CONDENSATE HEADER FROM ETHYLENE


REGENERATION HEATER
Hazard: Condensate can exceed design temperature of steam condensate network.
Causes:
TT-20318 (HH) Steam condensate network PID:0212
Actions:
Close XV-20317 Steam condensate network to ATM PID:0212
AND
FMC LIC-20311 Regeneration Nitrogen steam heater PID:021
2
Notes:  The cause must be reset by the operator as the temperature is detected
in the condensate header downstream the isolation valve.
Minimum SIL level: 0

I-2302-S: ETHYLENE O2 AND CO REMOVAL TREATERS EXOTHERM


Hazard: Exotherm during H2 regeneration or Air regeneration or during normal operation leading to
catalyst bed destruction. Require depressurization of treaters for complete protection.
Exotherm in a treater in normal operation
Causes:
[TZT- Ethylene CO/O2 treater A PID:0202
20120/20122/20123/20128/20129 ( >
105°C) (Voting 1oo5)] AND PZT-
20127 ( > SL = 9 barg)
OR
[TZT- Ethylene CO/O2 treater B PID:0202
20130/20132/20133/20138/20139 ( >
105°C) (Voting 1oo5)] AND PZT-
20137 ( > SL = 9 barg)
OR
FZT-20220 (LLL) Ethylene FPU outlet PID:0203

Actions:
Close XZV-20302 H2 to Ethylene CO/O2 treater PID:0202

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

AND
Close XZV-20303 H2 to Ethylene CO/O2 treater PID:0202

AND
Open (note 1) XZV-20301 Bleed H2 line to Ethylene CO/O2 treater PID:0202

Causes:
[TZT- Ethylene CO/O2 treater A PID:0202
20120/20122/20123/20128/20129 ( >
120°C) (Voting 1oo5)] AND PZT-
20127 ( > SL = 9 barg)
OR
[TZT- Ethylene CO/O2 treater B PID:0202
20120/20122/20123/20128/20129 ( >
120°C) (Voting 1oo5)] AND PZT-
20137 ( > SL = 9 barg)
Actions:

Initiate I-2304-S FPU ethylene depressurisation

Exotherm in CO/O2 treaters in regeneration


Causes:
[TZT- Ethylene CO/O2 treater A PID:0202
20120/20122/20123/20128/20129 ( >
250°C) (Voting 1oo5)] AND PZT-
20127 ( <SL = 9 barg)
OR
[TZT- Ethylene CO/O2 treater B PID:0202
20130/20132/20133/20138/20139 ( >
250°C) (Voting 1oo5)] AND PZT-
20137 ( < SL = 9 barg)
Actions:
Close XZV-20124 Regeneration Air to CO/O2 treaters PID:0202

AND
Stop H201 Regeneration Nitrogen heater PID:0212
AND
Close TZV-20316 (SIS) Regeneration Nitrogen steam heater PID:0212
AND
Close XZV-20120 (note 1) Regeneration H2 PID:0202

AND
Close XZV-20121 (note 1) Regeneration H2 PID:0202

AND

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

Open XZV-20122 (note 1) Regeneration H2 PID:0202

Notes:  Note 1: Open bleed valve when both corresponding isolation valves are
detected closed. Opening of isolation valves possible only if
corresponding bleed valve is detected closed
Minimum SIL level: 1

I-2303-S: LOW PRESSURE AT SUCTION OF ETHYLENE COMPRESSOR


Hazard: Vacuum leading to air ingress and potential explosion.
Causes:
PZT-20011 (LL) Ethylene compressor inlet pressure PID:0201
Actions:
Stop K-230 Ethylene compressor PID:0201
Notes:
Minimum SIL level: 1

I-2304-S: FPU ETHYLENE DEPRESSURISATION


Hazard: Complement actions for exotherm protection
Causes :
HZS-20001 FPU Ethylene Depressurisation PID:0203
OR
I-2302-S part 2 is activated Ethylene O2 and CO removal treaters
exotherm protection
Actions:
Close XZV-20002/XZV-20003 (note Ethylene from OSBL PID:0201
1)
AND
Close XZV-40063 (note 1) Ethylene to loop PID:0404

AND
Close XZV-40066 (note 1) Ethylene from EPU to loop PID:0404

AND
Open XZV-20204 (note 1) FPU ethylene vent to HPF PID:0203

AND
Stop K-230 Ethylene compressor PID:0201

AND

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

Close XZV-20302 H2 to ethylene O2 treater PID:0202

AND
Close XZV-20303 H2 to ethylene O2 treater PID:0202

AND
Open (note 2) XZV-20301 Bleed H2 line to ethylene O2 treater PID:0202

Notes:  Note 1: open depressurisation valves only when isolation valves are
closed
 Note 2: open bleed valve when both corresponding isolation valves are
detected closed. Opening of isolation valves possible only if
corresponding bleed valve is detected closed.
Minimum SIL level: 1 for cause “I-2302-S part 2 is initiated” and all actions

I-2305-O: ETHYLENE RECYCLE COMPRESSOR AUTO-START


Hazard: Maintain Miniflow through ethylene treaters to avoid hot spot. Complements I-2302-S.
Causes:
FZT-20220 (LL) Ethylene FPU outlet PID:0203
Actions:
Start K-230 (Note 1) Ethylene recycle Compressor PID:0201
AND
Open XV-20001 (Pulse command) Ethylene recycle Compressor discharge PID:0201
Notes:  Note 1: Interlocks which lead to trip the compressor have priority over
this interlock.
 Auto-reset: interlock.
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2306-S: LOW TEMPERATURE IN ETHYLENE O2 AND CO TREATERS


Hazard: Excessive N2 flow or loss of N2 heating during regeneration leading to low temperature and
vessel failure.
Causes:
[TZT- Ethylene CO/O2 treater A PID:0202
20120/20122/20123/20128/20129
(LL) (Voting 1oo5)]
OR
[TZT- Ethylene CO/O2 treater B PID:0202
20130/20132/20133/20138/20139
(LL) (Voting 1oo5)]

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

Actions:
Close XZV-20312 Regeneration N2 make-up PID:0212
Notes:
Minimum SIL level: 1

I-2307-S: REGENERATION AIR TO FLARE


Hazard: Oxygen introduced in flare leading to explosion (Note 1)
Causes:
ZZS-20100A Regeneration steam Not Routed to Atm PID:0202
AND
ZZS-20100B Regeneration steam Not Routed to Atm PID:0202
Actions:
Close XZV-20124 Air to ethylene CO/O2 treaters PID:0202

AND
Close FZV-20122 (SIS) Air to ethylene CO/O2 treaters PID:0202

Notes:  Note 1: Risk of O2 ingress into flare system to be reviewed by detailed


engineering.
Minimum SIL level: 2

I-2308-O: ETHYLENE CO/O2 TREATERS EXOTHERM DUE TO EXCESS H2 INJECTION


Hazard: Exotherm due to loss of nitrogen and H2 concentration rise, leading to trip and down time
required while treater is inspected for damage
Causes:
FZT-20311 (L1) Regeneration Nitrogen make-up to PID:0212
Ethylene regeneration heater
Actions:
Close XZV-20120 H2 from ISBL PID:0202
AND
Close XZV-20121 H2 from ISBL PID:0202
AND
Open XZV-20122 (Note 1) Bleed H2 line from ISBL PID:0202

Notes:  Note 1: Open bleed valve when both corresponding isolation valves are
detected closed. Opening of isolation valves possible only if
corresponding bleed valve is detected closed

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2309-S: HC RELEASED TO ATM DURING ETHYLENE TREATERS REGENERATION


Hazard: HC released to atm during HC desorption of treaters leading to HC cloud and explosion
(Note 1)
Causes:
[FZT-20311 (LLL) AND Regen. Regeneration nitrogen PID:0212
Nitrogen sent to atmosphere 3 way valve routed to Atm PID:0202
(detected by ZZS-20100A/B)]
OR
[Not TZT-20126 (SH) >100°C for Regeneration N2 downstream Ethylene PID:0202
more than T1-2309 AND 3 way O2/C2 treater to flare/atm.
valve moved from Flare to Atm
(ZZS-100A/B)]
Actions:
Close XZV-20312 Regeneration nitrogen PID:0212

Notes:  T1-2309 : timer = 15 min


 Note 1: This interlock prevents HC release by preventing the N2 purge
from opening unless the 3-way vent valve is lined up to flare. This
prevents a regeneration being started without line-up to flare. If the vent
valve is changed to flare from atm. Before the bulk of the HC is desorbed
(indicated by high temperature at the treater outlet) then the N2 supply is
tripped to prevent HC being driven to atmosphere.
This Interlock has to be developed by DE according to design
developments during detailed engineering phase.
Minimum SIL level: 1

I-2310-O: ETHYLENE CO/O2 TREATERS EXOTHERM DUE TO EXCESS O2 INJECTION


Hazard: Exotherm due to loss of nitrogen and O2 concentration rise, leading to trip and down time
required while treater is inspected for damage (Note 1)
Causes:
FZT-20311 (L2) (Note 2) Regeneration Nitrogen PID:0212
Actions:
Close XZV-20124 Regeneration air to ethylene CO/O2 PID:0202
treaters
Notes:  Note 1: risk of O2 ingress into flare system to be reviewed by detailed
engineering.
 Note 2: At the end of the catalyst life, pure air is used before returning
catalyst to the catalyst vendor. This interlock has to be overridden during

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
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PROCESS INTERLOCK DESCRIPTION

last step of oxidation when only air is used. Interlock implementation to be


developed by detailed engineering.
As guidance, the override could be set after a timer = time necessary for
the sequence to reach regeneration with pure air. Timer is launched when
the air feed isolation valve is detected open. The duration of the override
setting = regeneration time with pure air. After that time the override is
automatically removed.
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2311-O: HIGH PRESSURE AT ETHYLENE COMPRESSOR


Hazard: Avoid compressor PSV discharge lifting
Causes:
PT-20001 (HH) Ethylene Compressor discharge PID:0201
Actions:
Stop K-230 Ethylene Compressor PID:0201
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2312-O: ETHYLENE FEED TO TREATERS HEATING CUT-OFF


Hazard: Avoid ethylene compressor trip on high temperature.
Causes:
FZT-20220 (LLL) Ethylene FPU outlet PID:0203
Actions:
FMC TIC-20034 Steam condensate Ethylene heater PID:0201
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2314-O: BACKFLOW THROUGH ETHYLENE COMPRESSOR MINI FLOW LINE


Hazard: Bypass of FPU to PU. Quality issue.
Causes:
K-230 detected stopped Ethylene Compressor PID:0201
Actions:
Close XV-20001 (DCS) (Pulse Ethylene Compressor mini flow line PID:0201
command)
Notes:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 23 / 110

PROCESS INTERLOCK DESCRIPTION

Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2323-S: BACKFLOW INTO REGENERATION INSTRUMENT AIR FROM ETHYLENE


TREATERS
Hazard: Contamination of Instrument Air header by ethylene
Causes:
PZDT-20132 (LL) Regeneration IA to ethylene treaters PID:0202
Actions:
Close XZV-20124 Regeneration IA to ethylene treaters PID:0202
Notes:
Minimum SIL level: 1

I-2324-S: HC RELEASED TO ATM DURING COMONOMER OR PENTANE TREATERS


REGENERATION
Hazard: HC released to atm during HC desorption of treaters leading to HC cloud and explosion
(Note 1)
Causes:
[FZT-20311 (LLL) AND Regen. Regeneration nitrogen PID:0212
Nitrogen sent to atmosphere 3 way valve routed to Atm PID:0206
(detected by ZZS-20520)]
OR
[Not TZT-20526 (SH) >100°C for Regeneration N2 downstream treaters to PID:0206
more than T1-2324 AND 3 way flare/atm.
valve moved from Flare to Atm
(ZZS-20520)]
Actions:
Close XZV-20312 Regeneration nitrogen PID:0212

Notes:  T1-2324 : timer = 15 min


 Note 1: This interlock prevents HC release by preventing the N2 purge
from opening unless the 3-way vent valve is lined up to flare. This
prevents a regeneration being started without line-up to flare. If the vent
valve is changed to flare from atm. Before the bulk of the HC is desorbed
(indicated by high temperature at the treater outlet) then the N2 supply is
tripped to prevent HC being driven to atmosphere.
This Interlock has to be developed by DE according to design

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 24 / 110

PROCESS INTERLOCK DESCRIPTION

developments during detailed engineering phase.


Minimum SIL level: 1

I-2327-S: LOW TEMPERATURE IN ETHYLENE ADSORBERS


Hazard: Excessive N2 flow or loss of N2 heating during regeneration leading to low temperature and
vessel failure.
Causes:
TZT- Ethylene oxygenate treater A PID:0203
20200/20205/20206/20207/20208/2
0209 (LL) (Voting 1oo6)
OR
TZT- Ethylene oxygenate treater B PID:0203
20210/20215/20216/20217/20218/2
0219 (LL) (Voting 1oo6)
Actions:
Close XZV-20312 Regeneration N2 PID:0212
Notes:
Minimum SIL level: 1

I-2328-O: BACKFLOW INTO H2 FROM CO/O2 ETHYLENE TREATER


Hazard: Backflow leading to ethylene in H2 network.
Causes:
PDT-20301 (LL) Hydrogen header to Ethylene CO/O2 PID:0202
treaters
Actions:
Close XZV-20302 H2 to Ethylene CO/O2 treaters PID:0202
AND
Close XZV-20303 H2 to Ethylene CO/O2 treaters PID:0202
AND
Open (Note 1) XZV-20301 Bleed H2 line to Ethylene CO/O2 treaters PID:0202
Notes: Note 1: Open bleed valve when both corresponding isolation valves are detected closed.
Opening of isolation valves possible only if corresponding bleed valve is detected closed
SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES. DE to review the SIL
rating after identification of consequences on backflow from OSBL

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 25 / 110

PROCESS INTERLOCK DESCRIPTION

I-2410-S: COMONOMER PREPARATION UNIT ISOLATION


Hazard: Isolation to reduce consequence in case of fire or loss of containment.
Causes:
HZS-20501A Emergency comonomer preparation unit PID:0205
isolation in control room
OR
HZS-20501B Emergency comonomer preparation unit PID:0205
isolation in local area
Actions:
Stop P-241A Comonomer injection pump PID:0207
AND
Stop P-241B Comonomer injection pump PID:0207
AND
Close XZV-20550 Butene-1 from OSBL PID:0205

AND
Close XZV-20560 Hexene-1 from OSBL PID:0205

AND
Close XZV-20570 Octene-1 from OSBL PID:0205

AND
Close XZV-40902 Comonomer to Main loop separator PID:0403

AND
Close XZV-40905 Comonomer to Reactor PID:0404

AND
Close XZV-20602 Comonomer buffer drum Bottom PID:0207

Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2411-O: COMONOMER PUMPS


Hazard: Pump damage due to running dry or isolated.
Causes:
LT-20604 (LL) Comonomer buffer drum PID:0207
OR
XZV-20602 is detected not open Comonomer buffer drum Bottom PID:0207
Actions:
Stop P-241AHZS-40601 Comonomer injection pump PID:0207

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 26 / 110

PROCESS INTERLOCK DESCRIPTION

AND
Stop P-241B Comonomer injection pump PID:0207
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2412-O: COMONOMER DRUM OVERFILLING


Hazard: Overfilling leading to Backflow of comonomer to N2 header. N2 contamination.
Causes:
LT-20604 (HH) Comonomer buffer drum PID:0207
Actions:
FMC LIC-20602 Comonomer buffer drum PID:0207
AND
Close XZV-20550 Butene-1 from OSBL PID:0205
AND
Close XZV-20560 Hexene-1 from OSBL PID:0205
AND
Close XZV-20570 Octene-1 from OSBL PID:0205
Notes:
Minimum SIL level: 0

I-2416-S: COMONOMERS SIMULTANEOUS FEED


Hazard: Prevent against simultaneous injection of comonomers leading to poor degassing and off-
spec production
Causes:
HS-20502 = Butene-1 Comonomer selector PID:0205
Actions:
Close XZV-20560 Hexene-1 from OSBL PID:0205
AND
Close XZV-20570 Octene-1 from OSBL PID:0205
Causes:
HS-20502 = Hexene-1 Comonomer selector PID:0206
Actions:
Close XZV-20550 Butene-1 from OSBL PID:0205
AND
Close XZV-20570 Octene-1 from OSBL PID:0205

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 27 / 110

PROCESS INTERLOCK DESCRIPTION

Causes:
HS-20502 = Octene-1 Comonomer selector PID:0206
Actions:
Close XZV-20550 Butene-1 from OSBL PID:0205
AND
Close XZV-20560 Hexene-1 from OSBL PID:0205
Notes:
Minimum SIL level: 1

I-2417-O: COMONOMER INJECTION PUMPS


Hazard: Damage to high speed pump in case of closed outlet.
Causes:
FT-20601 (LL) Comonomer pumps discharge PID:
0207
AND
[P-241A running for more than Comonomer injection pump PID:
T1-2417 0207
OR
P-241B running for more than
T1-2417]

Actions:
Stop P-241A/B Comonomer injection pumps PID:
0207
Notes:  T1-2417: timer = 20s. Time for pump to establish flow and avoid trip on
low flow at start-up.
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2420-S: PENTANE PREPARATION UNIT ISOLATION


Hazard: Isolation to reduce consequence in case of fire or loss of containment.
Causes:
HZS-20201A Emergency pentane preparation unit PID:0209
isolation in control room
OR
HZS-20201B Emergency pentane preparation unit PID:0209
isolation in local area
Actions:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 28 / 110

PROCESS INTERLOCK DESCRIPTION

Stop P-242A Pentane injection pump PID:0209


AND
Stop P-242B Pentane start-up pump PID:0209
AND
Close XZV-20201 Treated pentane storage drum bottom PID:0209
isolation valve
AND
Close XZV-40903 Pentane make-up PID:0403

AND
Close XZV-40909 Pentane start-up PID:0403

AND
Close XZV-20242 Pentane feed to Pentane treaters PID:0208

AND
Close XZV-20205 Pentane feed to users PID:0209

Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-2421-O: PENTANE PUMPS


Hazard: Pump damage and PSV lifting
Causes:
LT-20201 (LL) Treated pentane storage drum PID:0209
OR
XZV-20201 is detected not open Treated pentane storage drum bottom PID:0209
isolation valve
Actions:
Stop P-242A Pentane injection pump PID:0209
AND
Stop P-242B Pentane start-up pump PID:0209
Causes:
PT-20223 (HH) Pentane to Main loop separator PID:0209
Actions:
Stop P-242A Pentane injection pump PID:0209
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 29 / 110

PROCESS INTERLOCK DESCRIPTION

I-2422-O: PENTANE STORAGE DRUM OVERFILLING


Hazard: Backflow to N2 header
Causes:
LT-20201 (HH) Treated pentane storage drum PID:0209
Actions:
Close XZV-20242 Pentane feed to pentane treaters PID:0208
Notes:
Minimum SIL level: 0

I-2425-S: LRU OR TEAL BACKFLOW TO PENTANE


Hazard: Contamination of pentane system by LRU or TEAL through pentane flush network
Causes:
PZDT-20205 (LL) Pentane flush header PID:0209
Actions:
Close XZV-20205 Pentane flush header PID:0209
Notes:
SIL level: 1

I-2426-O: PENTANE STORAGE DRUM AUTOMATIC REFILLING


Hazard: Refill pentane storage drum with fresh pentane
Causes:
LT-20202 (SL) Pentane storage drum PID:0209
Actions:
Open XZV-20203 Pentane fill line PID:0209
Causes:
LT-20202 (SH) Pentane storage drum PID:0209
Actions:
Close XZV-20203 Pentane fill line PID:0209
Notes:  Auto-reset interlock
 The level control is described as an interlock for convenience but can be
developed as a sequence during detailed engineering

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 30 / 110

PROCESS INTERLOCK DESCRIPTION

SIL level: No SIL requirement by INEOS Technologies

I-2439-S: LOW TEMPERATURE IN PENTANE TREATERS


Hazard: Excessive N2 flow or loss of N2 heating during Regeneration leading to low temperature
and vessel failure.
Causes:
TZT- Pentane treaters PID:0208
20251/20252/20253/20261/20262/2
0263 (LL)(Voting 1oo6)
Actions:
Close XZV-20312 Regeneration N2 PID:0212
Notes:
Minimum SIL level: 1

I-2458-S: LOW TEMPERATURE IN COMONOMER TREATERS


Hazard: Excessive N2 flow or loss of N2 heating during Regeneration leading to low temperature
and vessel failure.
Causes:
TZT-20502 / 20503 / 20504 (LL) Comonomer treater (A) PID:0206
(Voting 1oo3)
OR
TZT-20512 / 20513 / 20514 (LL) Comonomer treater (B) PID:0206
(Voting 1oo3)
Actions:
Close XZV-20312 Regeneration N2 PID:0212
Notes:
Minimum SIL level: 1

I-2470-S: HYDROGEN TREATMENT UNIT ISOLATION


Hazard: Isolation to reduce consequence in case of fire or loss of containment.
Causes:
HZS-20101A Control Room Emergency isolation H2 PID:0210
feed
OR
HZS-20101B Local Emergency isolation H2 feed PID:0210

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 31 / 110

PROCESS INTERLOCK DESCRIPTION

Actions:
Close XZV-40062 Hydrogen to PU PID:0040
4
AND
Close XZV-40067 Hydrogen to catalyst stingers PID:0404
AND
Close XZV-20401 Regeneration Hydrogen to N2 treaters PID:0214
AND
Close XZV-20403 Regeneration Hydrogen to N2 treaters PID:0214
AND
Open (note 1) XZV-20402 Regeneration bleed H2 line (N2 treaters) PID:0214
AND
Close XZV-20302 H2 to Ethylene treaters PID:0202
AND
Close XZV-20303 H2 to Ethylene treaters PID:0202
AND
Open (note 1) XZV-20301 Bleed H2 line to Ethylene treaters PID:0202
AND
Close XZV-20101/20102 H2 from OSBL PID:0210
AND
Open (Note 1)XZV-20103 Bleed H2 from OSBL PID:0210
AND
Close XZV-20120 Regeneration H2 PID:0202
AND
Close XZV-20121 Regeneration H2 PID:0202
AND
Open XZV-20122 (Note 1) Bleed regeneration H2 PID:0202

Notes:  H2 compressor kept running to ensure mini flow for cata. bed
protection.
 Note 1: Open bleed valve when both corresponding isolation valves
are detected closed. Opening of isolation valves possible only if
corresponding bleed valve is detected closed
SIL level: No SIL requirement by INEOS Technologies

I-2471-S: LOW PRESSURE AT HYDROGEN COMPRESSOR A SUCTION


Hazard: Vacuum leading to air ingress and potential explosion.
Causes:
PZT-20104 (LL) Hydrogen compressor A suction PID:0210

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 32 / 110

PROCESS INTERLOCK DESCRIPTION

Actions:
Stop K-271A Hydrogen compressor A PID:0210
Notes:
SIL level: 1

I-2474-O: HIGH PRESSURE AT HYDROGEN COMPRESSOR A DISCHARGE


Hazard: Avoid compressor PSV discharge lifting
Causes:
PT-20106 (HH) Hydrogen compressor A discharge PID:0210
Actions:
Stop K-271A Hydrogen Compressor A PID:0210
Notes:
SIL level: No SIL requirement by INEOS Technologies

I-2475-O: BACKFLOW FROM HYDROGEN TREATING SYSTEM INTO H2 OSBL


PREVENTION
Hazard: Loss of hydrogen feed from OSBL leading to backflow from users and progressive loss of
mini flow into treaters
Causes:
PT-20101 (LL) H2 from OSBL PID:0210
Actions:
Close XZV-20101/20102 H2 from OSBL PID:0210
AND
Open (Note 1) XZV-20103 Bleed H2 from OSBL PID:0210
Notes:  Note 1: Open bleed valve when both corresponding isolation valves are
detected closed. Opening of isolation valves possible only if
corresponding bleed valve is detected closed
SIL level: No SIL requirement by INEOS Technologies. DE to review the SIL rating
after identification of consequences on backflow from OSBL

I-2481-S : LOW PRESSURE AT HYDROGEN COMPRESSOR B SUCTION


Hazard: Vacuum leading to air ingress and potential explosion.
Causes:
PZT-20114 (LL) Hydrogen compressor B suction PID:0210

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 33 / 110

PROCESS INTERLOCK DESCRIPTION

Actions:
Stop K-271B Hydrogen compressor B PID:0210
Notes:
SIL level: 1

I-2484-O: HIGH PRESSURE ON HYDROGEN COMPRESSOR B DISCHARGE


Hazard: Avoid compressor PSV discharge lifting
Causes:
PT-20116 (HH) Hydrogen compressor B discharge PID:0210
Actions:
Stop K-271B Hydrogen Compressor B PID:0210
Notes:
SIL level: No SIL requirement by INEOS Technologies

I-2734-S: BACKFLOW OF H2 INTO REGENERATION NITROGEN FROM H2 TREATERS


Hazard: Backflow from H2 dryers (procedure error) , H2 into regeneration N2 leading to damage to
treaters (with catalyst bed) in regeneration and loss of containment.
Causes:
PZDT-20319 (LL) Regeneration Nitrogen to hydrogen PID:0213
adsorber
Actions:
Close XZV-20318 Regeneration Nitrogen to hydrogen PID:0213
adsorber
Notes:
Minimum SIL level: 1

I-2735-S: BACKFLOW OF HYDROGEN INTO REGENERATION NITROGEN FROM


ETHYLENE TREATERS
Hazard: Backflow from H2 treaters (procedure error) , H2 into regeneration N2 leading to damage to
treaters (with catalyst bed) in regeneration and loss of containment.
Causes:
PZDT-20323 (LL) Regeneration Nitrogen to ethylene CO/O2 PID:0213
treaters
Actions:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 34 / 110

PROCESS INTERLOCK DESCRIPTION

Close XZV-20323 Regeneration Nitrogen to ethylene CO/O2 PID:0213


treaters
Notes:
Minimum SIL level: SIL 1

I-2752-S: REGENERATION NITROGEN HEATER OVERHEATING


Hazard: Overheating leading to regeneration nitrogen heater damage and downstream treaters
damage.
Causes:
TZT-20313 (HH) Regeneration nitrogen heater Outlet PID:0212
OR
TZSHH-20314 (HH) Regeneration nitrogen heater element PID:0212
(skin)
OR
FZT-20311 (LL) Nitrogen to Regeneration nitrogen heater PID:0212
Actions:

Stop H-201 Regeneration Nitrogen heater PID:0212


AND
Close TZV-20316 (SIS) Steam heater PID:0212
Notes:
Minimum SIL level: 1 for TZT-20313 and action

I-2760-S: NITROGEN CO/O2 REMOVAL TREATERS EXOTHERM


Hazard: Exotherm during regeneration leading to thermal failure of the vessel and resultant hydrogen
jet fire.
Causes:
TZT-20425 (HH) CO/O2 removal treater (A) PID:0214
OR TZT-20421 (HH)
OR TZT-20422 (HH)
OR TZT-20423 (HH)
OR TZT-20424 (HH)
OR

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 35 / 110

PROCESS INTERLOCK DESCRIPTION

TTZ-20435 (HH) CO/O2 removal treater (B) PID:0214


OR TZT-20431 (HH)
OR TZT-20432 (HH)
OR TZT-20433 (HH)
OR TZT-20434 (HH)
Actions:
Close XZV-20401/20403 H2 regeneration PID:0214
AND
Open XZV-20402 (Note 1) Bleed H2 regeneration PID:0214
AND
Close XZV-20411 Air regeneration PID:0214
AND
Close TZV-20316 (SIS) Regeneration Nitrogen steam heater PID:0212
AND
Stop H-201 Regeneration Nitrogen heater PID:0212
Notes:  Note 1: Open bleed valve when both corresponding isolation valves are
detected closed. Opening of isolation valves possible only if
corresponding bleed valve is detected closed
Minimum SIL level: 1

I-2761-O: NITROGEN CO/O2 REMOVAL TREATERS EXOTHERM DUE TO EXCESS OF H2


INJECTION
Hazard: Exotherm during regeneration due to insufficient H2 dilution. Anticipate actions of I-2760-S
Causes:
FZT-20311 (L3) Nitrogen to Regeneration nitrogen heater PID:0212
Actions:
Close XZV-20401/20403 H2 regeneration PID:0214
AND
Open XZV-20402 (Note 1) Bleed H2 regeneration PID:0214
Notes:  Note 1: Open bleed valve when both corresponding isolation valves are
detected closed. Opening of isolation valves possible only if
corresponding bleed valve is detected closed
Minimum SIL level: No SIL requirement by INEOS Technologies

I-2764-O: N2 CO/O2 REMOVAL TREATERS EXOTHERM DUE TO EXCESS OF O2


INJECTION
Hazard: Exotherm due to loss of nitrogen and O2 concentration drop, leading to trip and down time
required while treater is inspected for damage (note 1).

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 36 / 110

PROCESS INTERLOCK DESCRIPTION

Causes:
FZT-20311 (L4) (note 2) Nitrogen to Regeneration nitrogen heater PID:0212
Actions:
Close XZV-20411 Regeneration air to nitrogen CO/O2 PID:0214
treaters
Notes:  Note 1: Risk of O2 ingress into flare system to be reviewed by detailed
engineering.
 Note 2: interlock to be overriden during last step of oxidation when only
air is used. Interlock implementation to be developed by detailed
engineering.
As a guidance, the override could be set after a timer = time necessary
for the sequence to reach regeneration with pure air. Timer is launched
when the air feed isolation valve is detected open. The duration of the
override setting = regeneration time with pure air. After that time the
override is automatically removed.
Minimum SIL level: No SIL requirement by INEOS Technologies

I-2765-O: LPN NITROGEN SUPPLY PRIORITY


Hazard: Cut N2 supply to LLDPE low priority users in case of N2 pressure drop
Causes:
PT-10090 (LL) Nitrogen from OSBL PID:0102
Actions:
Close XZV-20312 Regeneration nitrogen PID:0212
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 37 / 110

PROCESS INTERLOCK DESCRIPTION

2.3 SECTION 300

I-3060-O: COMONOMER / CATALYST COMBINATION


Hazard: Incorrect combination leading to degassing requirement outside grade slate or momentary
incorrect catalyst selection causing degassing trip settings to change (will take several
hours to return to correct values)
Causes:
XZV-20550 not closed Butene-1 BL PID:3120-
0205
Actions:
Close XZV-30210 Metallocene catalyst conveying line PID:0305
isolation valve
AND
Close XZV-30310 Metallocene catalyst conveying line PID:0305
isolation valve
AND
Close XZV-30410 Metallocene catalyst conveying line PID:0305
isolation valve
Notes:
Minimum SIL level: 0

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 38 / 110

PROCESS INTERLOCK DESCRIPTION

I-3061-S: SIMULTANEOUS INJECTION OF ZIEGLER AND METALLOCENE


Hazard: Off spec production and agglomerate (potential man entry)
Causes:
XZV-30010 Not closed Ziegler catalyst conveying line isolation PID:0303
valve
OR
XZV-30110 Not closed Ziegler catalyst conveying line isolation PID:0303
valve
Actions:
Close XZV-30210 Metallocene catalyst conveying line PID:0305
isolation valve
AND
Close XZV-30310 Metallocene catalyst conveying line isolation PID:0305
valve
AND
Close XZV-30410 Metallocene catalyst conveying line PID:0305
isolation valve
AND
Close XZV-40209 Liquid additive S1 to catalyst injection PID:0411
Causes:
XZV-30210 Not closed Metallocene catalyst conveying line PID:0305
isolation valve
OR
XZV-30310 Not closed Metallocene catalyst conveying line PID:0305
isolation valve
OR
XZV-30410 Not closed Metallocene catalyst conveying line PID:0305
isolation valve
Actions:
Close XZV-30010 Ziegler catalyst conveying line isolation PID:0303
valve
AND
Close XZV-30110 Ziegler catalyst conveying line isolation PID:0303
valve
AND
Close XZV-40207 Liquid additive (B1) feed to reactor PID:0408

Notes:
Minimum SIL NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 39 / 110

PROCESS INTERLOCK DESCRIPTION

level:

I-3069-O: ZIEGLER CATALYST (SDX) STOCK LINES BACK FLOW


Hazard: Backflow from reactor leading to stock line plugging.
Causes:
PZT-30072 (LL) Nitrogen to stock pipe PID:0301
Actions:
Close XV-30075 Stock pipe transfer valve PID:0301
AND
Close XV-30078 Stock pipe transfer valve PID:0301
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3070-S: ZIEGLER CATALYST (SDX) STORAGE HP/LP INTERFACE


Hazard: Release of catalyst leading to potential injuries to operator working around the tote bin
(flexible hoses rupture)
Causes:
PZT-30072 (HH) Nitrogen to stock pipe PID:0301
OR
XV-30075 Not closed Stock pipe transfer valve PID:0301
OR
XV-30078 Not closed Stock pipe transfer valve PID:0301
Actions:
Close XZV-30070 Stock pipe transfer valve PID:0301
AND
Close XZV-30071 Stock pipe transfer valve PID:0301
Notes:  Autoreset
Minimum SIL level: 1
Two valves are installed for process reasons (leakage), not to meet SIL
requirement

I-3071-O: HP NITROGEN OPEN PATH TO CV (SDX)


Hazard: HP nitrogen vented to CV leading to bursting disk rupture.
Causes:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 40 / 110

PROCESS INTERLOCK DESCRIPTION

XV-30074 Not closed Stock pipe depressurisation valve PID:0301


AND
XV-30079 Not closed Stock pipe depressurisation valve PID:0301
Actions:
Close XV-30072 Nitrogen to holding volume PID:0301
AND
Close XV-30073 Nitrogen to holding volume PID:0301

AND
Close XV-30076 Nitrogen to holding volume PID:0301

AND
Close XV-30075 Stock pipe transfer valve PID:0301

AND
Close XV-30078 Stock pipe transfer valve PID:0301

Notes:  Autoreset
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3077-S: ZIEGLER CATALYST (SDX) STOCK LINES BACK FLOW FROM REACTOR
Hazard: Backflow from reactor leading to stock line plugging and major outage
Causes:
PZDI-30073 (LL) (note 1) Reactor and catalyst stock line PID:0301
/ 0401
Actions:
Stop X-380A/B (DCS) Catalyst rotary valves PID:0303
AND
Close after T1-3077 XZV- Catalyst conveying line isolation valves PID:0303
30010/30110
Notes:  Note 1: PZDI-30073 = PZT-30073 – PZT-40008
 T1-3077: Timer = 30s.
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3078-O: ZIEGLER CATALYST CONVEYING LINE PLUGGING


Hazard: Prevent plugging of catalyst conveying line on low flow leading to production loss.
Causes:
FT-30010 (LL) Motive Nitrogen of catalyst injection line PID:0303

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 41 / 110

PROCESS INTERLOCK DESCRIPTION

AND
XZV-30010 Not closed for more than Catalyst conveying line isolation valve PID:0303
T1-3078
Actions:
Close XZV-30010 Catalyst conveying line isolation valve PID:0303
Causes:
FT-30010 (LL) Motive Nitrogen of catalyst injection line PID:0303
Actions:
Stop X-380A Catalyst rotary valve PID:0303
Notes: T1-3078: timer = 30s
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3079-O: ZIEGLER CATALYST CONVEYING LINE PLUGGING


Hazard: Prevent plugging of catalyst conveying line on low flow leading to production loss.
Causes:
FT-30110 (LL) Motive Nitrogen of catalyst injection line PID:0303
AND
XZV-30110 Not closed for more than Catalyst conveying line isolation valve PID:0303
T1-3079
Actions:
Close XZV-30110 Catalyst conveying line isolation valve PID:0303
Causes:
FT-30110 (LL) Motive Nitrogen of catalyst injection line PID:0303
Actions:
Stop X-380B Catalyst rotary valve PID:0303
Notes: T1-3079: Timer = 30s
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3080-O: METALLOCENE CATALYST CONVEYING LINE PLUGGING


Hazard: Prevent plugging of catalyst conveying line on low flow leading to production loss.
Causes:
FT-30210 (LL) Motive Nitrogen of catalyst injection line PID:0305
AND
XZV-30210 Not closed for more than Catalyst conveying line isolation valve PID:0305

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 42 / 110

PROCESS INTERLOCK DESCRIPTION

T1-3080
Actions:
Close XZV-30210 Catalyst conveying line isolation valve PID:0305
Causes:
FT-30210 (LL) Motive Nitrogen of catalyst injection line PID:0305
Actions:
Stop X-386A Catalyst rotary valve PID:0305
Notes: T1-3080: Timer = 30s
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3081-O: METALLOCENE CATALYST CONVEYING LINE PLUGGING


Hazard: Prevent plugging of catalyst conveying line on low flow leading to production loss.
Causes:
FT-30310 (LL) Motive Nitrogen of catalyst injection line PID:0305
AND
XZV-30310 Not closed for more than Catalyst conveying line isolation valve PID:0305
T1-3081
Actions:
Close XZV-30310 Catalyst conveying line isolation valve PID:0305
Causes:
FT-30310 (LL) Motive Nitrogen of catalyst injection line PID:0305
Actions:
Stop X-386B Catalyst rotary valve PID:0305
Notes: T1-3081: Timer = 30s
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3082-O: METALLOCENE CATALYST CONVEYING LINE PLUGGING


Hazard: Prevent plugging of catalyst conveying line on low flow leading to production loss.
Causes:
FT-30410 (LL) Motive Nitrogen of catalyst injection line PID:0305
AND
XZV-30410 Not closed for more than Catalyst conveying line isolation valve PID:0305
T1-3082
Actions:
Close XZV-30410 Catalyst conveying line isolation valve PID:0305
Causes:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 43 / 110

PROCESS INTERLOCK DESCRIPTION

FT-30410 (LL) Motive Nitrogen of catalyst injection line PID:0305


Actions:
Stop X-386C Catalyst rotary valve PID:0305
Notes: T1-3082: Timer = 30s
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3087-O: CATALYST STINGER ASSIST GAS


Hazard: Flow backup to stinger jackets. Loss of flow leading to poor catalyst dispersion,
agglomerate formation and loss of production. Normally use process gas with PHN as
backup. On loss of flow, switch to process gas first, then to PHN. Switching to ethylene
should be manual operator decision.
Causes:
FT-30204 (LL1) for more than T1- C2/Process gas/Nitrogen to catalyst PID:0305
3087 injection nozzles
Actions:
Set XZV-30203 to Process gas C2/Process gas to catalyst stinger PID:0305
direction jackets
AND
Close XZV-40067 H2 to catalyst stingers PID:0404
Causes:
FT-30204 (LL2) for more than T2- C2/Process gas/Nitrogen to catalyst PID:0305
3087 injection nozzles
Actions:
Open XV-30202 Nitrogen to catalyst stinger jackets PID:0305
Notes:  T1-3087: timer = 5 sec
 T2-3087: timer = 10 sec
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 44 / 110

PROCESS INTERLOCK DESCRIPTION

I-3169-O: ZIEGLER CATALYST (NCT) STOCK LINES BACK FLOW


Hazard: Backflow from reactor leading to stock line plugging.
Causes:
PZT-30172 (LL) Nitrogen to stock pipe PID:0302
Actions:
Close XV-30175 Stock pipe transfer valve PID:0302
AND
Close XV-30178 Stock pipe transfer valve PID:0302
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3170-S: ZIEGLER CATALYST (NCT) STORAGE HP/LP INTERFACE


Hazard: Release of catalyst leading to potential injuries to operator working around the tote bin
(flexible hoses rupture)
Causes:
PZT-30172 (HH) Nitrogen to stock pipe PID:0302
OR
XV-30175 Not closed Stock pipe transfer valve PID:0302
OR
XV-30178 Not closed Stock pipe transfer valve PID:0302
Actions:
Close XZV-30170 Stock pipe transfer valve PID:0302
AND
Close XZV-30171 Stock pipe transfer valve PID:0302
Notes:  Auto-reset
Minimum SIL level: 1
Two valves are installed for process reasons (leakage), not to meet SIL
requirement

I-3171-O: HP NITROGEN OPEN PATH TO CV (NCT)


Hazard: HP nitrogen vented to CV leading to bursting disk rupture.
Causes:
XV-30174 Not closed Stock pipe depressurisation valve PID:0302

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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Technologies RAPID L20 INE PRO DES 3200 0013


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PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 45 / 110

PROCESS INTERLOCK DESCRIPTION

AND
XV-30179 Not closed Stock pipe depressurisation valve PID:0302
Actions:
Close XV-30172 Nitrogen to holding volume PID:0302
AND
Close XV-30173 Nitrogen to holding volume PID:0302

AND
Close XV-30176 Nitrogen to holding volume PID:0302

AND
Close XV-30175 Stock pipe transfer valve PID:0302

AND
Close XV-30178 Stock pipe transfer valve PID:0302

Notes: Autoreset
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3177-S: ZIEGLER CATALYST (NCT) STOCK LINES BACK FLOW FROM REACTOR
Hazard: Backflow from reactor leading to stock line plugging and major outage
Causes:
PZDI-30173 (LL) (note 1) Reactor and catalyst stock line PID:0302/
0401
Actions:
Stop X-380A/B (DCS) Ziegler catalyst rotary valves PID:0303
AND
Close after T1-3177 XZV- Catalyst conveying line isolation valves PID:0303
30010/30110
Notes:  Note 1: PZDI-30173 = PZT-30173 – PZT-40008
 T1-3177: Timer = 30s.
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 46 / 110

PROCESS INTERLOCK DESCRIPTION

I-3269-O: METALLOCENE CATALYST STOCK LINES BACK FLOW


Hazard: Backflow from reactor leading to stock line plugging.
Causes:
PZT-30272 (LL) Nitrogen to stock pipe PID:0304
Actions:
Close XV-30275 Stock pipe transfer valve PID:0304
AND
Close XV-30278 Stock pipe transfer valve PID:0304
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3270-S: METALLOCENE CATALYST STORAGE HP/LP INTERFACE


Hazard: Release of catalyst leading to potential injuries to operator working around the tote bin
(flexible hoses rupture)
Causes:
PZT-30272 (HH) Nitrogen to stock pipe PID:0304
OR
XV-30275 Not closed Stock pipe transfer valve PID:0304
OR
XV-30278 Not closed Stock pipe transfer valve PID:0304
Actions:
Close XZV-30270 Stock pipe transfer valve PID:0304
AND
Close XZV-30271 Stock pipe transfer valve PID:0304
Notes:  Autoreset
Minimum SIL level: 1
Two valves are installed for process reasons (leakage), not to meet SIL
requirement

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 47 / 110

PROCESS INTERLOCK DESCRIPTION

I-3271-O: HP NITROGEN OPEN PATH TO CV


Hazard: HP nitrogen vented to CV leading to bursting disk rupture.
Causes:
XV-30274 Not closed Stock pipe depressurisation valve PID:0304
AND
XV-30279 Not closed Stock pipe depressurisation valve PID:0304
Actions:
Close XV-30272 Nitrogen to holding volume PID:0304
AND
Close XV-30273 Nitrogen to holding volume PID:0304

AND
Close XV-30276 Nitrogen to holding volume PID:0304

AND
Close XV-30275 Stock pipe transfer valve PID:0304

AND
Close XV-30278 Stock pipe transfer valve PID:0304

Notes: Autoreset
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-3277-S: METALLOCENE CATALYST STOCK LINES BACK FLOW FROM REACTOR


Hazard: Backflow from reactor leading to stock line plugging and major outage
Causes:
PZDI-30273 (LL) (note 1) Reactor and catalyst stock line PID:0304
/0401
Actions:
Stop X-386A/B/C (DCS) Metallocene catalyst rotary valves PID:0305
AND
Close after T1-3277 XZV- Catalyst conveying line isolation valves PID:0305
30210/30310/30410
Notes:  Note 1: PZDI-30273 = PZT-30273 – PZT-40008
 T1-3277: Timer = 30s.
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 48 / 110

PROCESS INTERLOCK DESCRIPTION

2.4 SECTION 400

I-4001-S: BATTERY LIMIT ISOLATION FOR PEG PLANT


Hazard: Isolation to reduce consequences of fire
Causes:
HZS-20002 Emergency Battery limit isolation in PID:0201
control room
Actions:
Close XZV-20002 Ethylene from OSBL PID:0201
AND
Close XZV-20003 Ethylene from OSBL PID:0201
AND
Close XZV-20550 Butene-1 BL PID:0205

AND
Close XZV-20560 Hexene-1 BL PID:0205

AND
Close XZV-20570 Octene-1 BL PID:0205

AND
Close XZV-20242 Pentane BL PID:0208
AND
Close XZV-20101 (Note1) H2 to FPU from OSBL PID:0210

AND
Close XZV-20102 (Note1) H2 to FPU from OSBL PID:0210

AND
Open XZV-20103 (Note 1) H2 bleed PID:0210
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 49 / 110

PROCESS INTERLOCK DESCRIPTION

I-4009-S: MAIN LOOP SEPARATOR ISOLATION


Hazard: Isolation to reduce consequence in case of fire or loss of containment.
Causes:
HZS-40908A Emergency Main loop separator isolation PID:0403
from control room SIS board
OR
HZS-40908B Emergency Main loop separator isolation PID:0403
from field
Actions:
Stop P-409A/B HP Liquid injection pumps PID:0403
AND
Close XZV-40908 Main loop separator bottom isolation PID:0403
valve
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-4011-S: BACK FLOW INTO ETHYLENE HEADER FROM GAS LOOP


Hazard: Backflow leading to contamination of ethylene header. Uncontrolled reaction in treater
leading to potential vessel failure due to over temperature.
Causes:
PZDT-40065 (LL) Ethylene to loop gas PID:0404
Actions:
Close XZV-40063 Ethylene to loop gas PID:0404
Notes:
Minimum SIL level: 1

I-4013-O: BACK FLOW INTO COMONOMER FEEDING FROM MAIN LOOP SEPARATOR
Hazard: Backflow leading to comonomer headers contamination.
Causes:
PDT-40910 (LL) Comonomer to Main loop separator PID:0403
Actions:
Close XZV-40902 Comonomer to Main loop separator PID:0403

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 50 / 110

PROCESS INTERLOCK DESCRIPTION

Notes:
Minimum SIL level: 0

I-4014-O: BACK FLOW INTO COMONOMER FEEDING FROM GAS LOOP (K400
DISCHARGE)
Hazard: Backflow leading to comonomer headers contamination.
Causes:
PDT-40915 (LL) Comonomer to loop gas PID:0404
Actions:
Close XZV-40905 Comonomer to loop gas PID:0404
Notes:
Minimum SIL level: 0

I-4015-S: BACK FLOW INTO LIQUID ADDITIVE B1 UNLOADING STATION DRUMS


Hazard: Release of HC or nitrogen to unloding station drums. Explosion or asphixiation.
Causes:
PZT-40209 (H) (Note 1) Liquid additive B1 vertical pipe PID:0408
Actions:
Close XZV-40204 Isolation of Liquid additive B1 station PID:0408
drums
Notes: Note 1: Interlock activated during normal operation. Alarm to be activated only
when XZV-40204 is detected open.
Minimum SIL level: 1

I-4016-S: BACK FLOW INTO VRU MAIN SEPARATOR FROM GAS LOOP
Hazard: Backflow of loop gas into VRU up to degasser. Powder degassing issue and explosion in
degasser downstream equipment.
Causes:
PZDT-40904 (LL) VRU condensate to loop PID:0403

Actions:
Close XZV-40904 VRU condensate to loop PID:0403
Notes:
Minimum SIL level: 1

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PROCESS INTERLOCK DESCRIPTION

I-4017-O: BACK FLOW INTO VRU COMPRESSOR SUCTION DRUM FROM GAS LOOP
Hazard: Backflow of loop gas into VRU up to degasser. Powder degassing issue and explosion in
degasser downstream equipment.
Causes:
PDT-40919 (LL) VRU condensate to loop PID:0403

Actions:
Close XZV-40919 VRU condensate to loop PID:0403
Notes:
Minimum SIL level: 0

I-4018-S: REACTOR FEEDS EMERGENCY ISOLATION


Hazard: Production loss and flaring + manual isolation in case of fire.
Causes:
PZT-40008 (HH) Loop gas PID:0401
OR
I-4021-S is initiated Maxi kill interlock PID:0407
Actions:
XZV-30203 set to process gas C2/Process gas to catalyst stinger jackets PID:0305
direction
AND
Stop P-455A TEAL injection pump A PID:0410
AND
Stop P-455B TEAL injection pump B PID:0410
AND
Close XZV-40521 TEAL injection pumps discharge PID:0410

AND
Close XZV-40522 TEAL injection pumps discharge PID:0410

AND
Close XZV-40207 (note 1) Liquid additive (B1) feed to reactor PID:0408

AND
Stop X-380A Ziegler catalyst rotary valve PID:0303

AND
Stop X-380B Ziegler catalyst rotary valve PID:0303
AND
Close XZV-40902 Comonomer to Main loop separator PID:0403

AND

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

Close XZV-40905 Comonomer to Polymerisation reactor PID:0404

AND
Close XZV-40903 Pentane make-up to Main loop separator PID:0403

AND
Close XZV-40909 Pentane start-up to Main loop separator PID:0403

AND
Close XZV-40904 VRU second interchanger condensate to PID:0403
Main loop separator
AND
Close XZV-40919 VRU compressor suction drum PID:0403
condensate to loop separator
AND
Close XZV-40920 VRU C8 compressor suction drum PID:0403
condensate to loop separator
AND
Set XZV-40065 to N2 Direction Ethylene/Nitrogen to purge gas system PID:0404

AND
Close XZV-40062 Hydrogen to loop PID:0404
AND
Close XZV-40063 Ethylene to loop PID:0404
AND
Close FZV-061 (SIS) HN to loop PID:0404

AND
Close XZV-40209 Liquid additive S1 to catalyst injection PID:0411

AND
Stop X-386A Metallocene catalyst rotary valve PID:0305

AND
Stop X-386B Metallocene catalyst rotary valve PID:0305
AND
Stop X-386C Metallocene catalyst rotary valve PID:0305
AND
Close XZV-40901 HC condensate to Liquid injection nozzles PID:0403

AND
Close XZV-40067 H2 to Metallocene catalyst injection PID:0404
nozzles
Notes:  Note 1: This interlock also prevents B1 and TEAL additives
entering in direct contact by isolating the respective feeds when
Main loop compressor is stopped (see I-4021-S). There is a

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PROCESS INTERLOCK DESCRIPTION

chemical reaction with heat production that could lead to piping


work failure. It can occur only when Main loop compressor is
stopped and additives are then not dispersed.
Minimum SIL level: No SIL requirement by INEOS TECHNOLOGIES

I-4019-O: BACK FLOW INTO PURGE COLUMN FROM REACTOR VIA START-UP POWDER
LINE
Hazard: Lifting relief valve / blockage
Causes:
PZT-40008 (H1) (note 1) Loop gas PID:0401
Actions:
Close XV-60081 Start-up powder to Reactor PID:0608
Notes:  Note 1: Trip activated during normal operation.
Minimum SIL NO SIL REQUIREMENT BY INEOS TECHNOLOGIES
level:

I-4020-S: TEAL SYSTEM ISOLATION


Hazard: Fire, emergency isolation.
Causes:
HZS-40502 Local TEAL emergency isolation next PID:0410
toTEAL pumps
OR
HZS-40101A Control room board TEAL emerg. PID:0409
isolation
OR
HZS-40101B Local TEAL emerg. isolation (containers) PID:0409
OR
PZT-405xx (LL) (Note 1) Plastic tubing fusible link (Containers area PID:0410
and pumps)
Actions:
Stop P-455A TEAL injection pump A PID:0410
AND
Stop P-455B TEAL injection pump B PID:0410
AND
Close XZV-40531 TEAL to loop gas PID:0410

AND
Close XZV-40521 TEAL injection pumps discharge PID:0410

AND

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

Close XZV-40522 TEAL injection pumps discharge PID:0410

AND
Close XZV-40951 TEAL to nozzles PID:0405

AND
Close XZV-40101 TEAL container isolation PID:0409
AND
Close XZV-40111 TEAL container isolation PID:0409
AND
Close XZV-40103 TEAL container nitrogen purging PID:0409
AND
Close XZV-40113 TEAL container nitrogen purging PID:0409
AND
Open XZV-40102 TEAL container venting PID:0409
AND
Open XZV-40112 TEAL container venting PID:0409
AND
Close XZV-20205 Pentane flush from Pentane storage drum PID:0209
Notes:  Note 1: Number of pressure transmitters to be determined by detailed
Engineering
Minimum SIL level: 1

I-4021-S: MAXI KILL


Hazard: Reaction runaway leading to powder melting and major reactor blockage (man entry) +
manual isolation in case of fire.
Causes:
HZS-40601 MAXI KILL initiated from control room PID:0407
OR
K-400 Detected stopped Main loop gas compressor PID:0404
OR
TIC-40046.PV > TIC-40046.SP + Reactor bed PID:0401
5°C
Actions:
Initiate I-4018-S Reactor feeds isolation
AND
Close XZV-40603 (Note 1) CO kill system bleed PID:0407
AND
Close XZV-40604 (Note 1) CO kill system bleed PID:0407
AND

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

Close XZV-40615 (Note 1) CO kill system flush PID:0407


AND
Open after T1-4021 XZV- CO kill system injection PID:0407
40611/XZV-40601/XZV-40602 then
Wait T2-4021 and close XZV-
40601/XZV-40602
Then when both XZV-40601/40602 CO kill system bleed PID:0407
confirmed closed then open XZV-
40603/40604 (Note 1, 2)
AND
Open HZV-40051 to 100% (SIS) Loop gas depressurisation PID:0402
(Note 1)
AND
Open XZV-40052 (Note 1) Loop gas depressurisation PID:0402

Notes:  T1-4021: timer = 5s


 T2-4021: timer, adjustable 2 - 15s
 Note 1: CO kill injection and Reactor depressurisation to be able to be
overriden from control room panel by operator (HZS-40602 – switch) to
avoid maxi kill in case of compressor normal stop or process start-up
phase. Override Status should be displayed in the DCS catalyst injection
display.
 Note 2: When the interlock is initiated the kill injection valves are kept in
open position until the kill timer has expired. Once the timer has expired,
the operator (HZS-40601) can initiate new kills.
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-4022-S: BACK FLOW INTO LIQUID ADDITIVE S1 UNLOADING STATION DRUMS


Hazard: Release of HC or nitrogen to unloading station drums. Explosion or asphyxiation.
Causes:
PZT-40201 (H) (Note 1) Liquid additive S1 vertical pipe PID:0411
Actions:
Close XZV-40206 Isolation of Liquid additive S1 station PID:0411
drums
Notes: Note 1: Interlock activated during normal operation. Alarm to be activated only
when XZV-40206 is detected open.
Minimum SIL level: 1

I-4023-S: BACK FLOW INTO VRU C8 COMPRESSOR SUCTION DRUM FROM GAS LOOP
Hazard: Backflow of loop gas into VRU compressor suction drum. Powder degassing issue and
explosion in degasser downstream equipment.
Causes:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

PZDT-40920 (LL) VRU C8 condensate to loop PID:0403

Actions:
Close XZV-40920 VRU C8 condensate to loop PID:0403
Notes:
Minimum SIL level: 1

I-4024-O: NITROGEN BACK-UP FOR MAIN LOOP COMPRESSOR PURGE GAS


Hazard: Loss of flush gas leading to trip of Main loop compressor and Ejector booster compressor +
blockage of tappings
Causes:
XZV-40066 Closed for T1-4024 Ethylene from FPU PID:0404
Actions:
Set XZV-40065 to direction Nitrogen to Main loop compressor PID:0404
Nitrogen
Notes: T1-4024: timer = 10 sec
Minimum SIL level: No SIL requirement by INEOS Technologies

I-4025-S: BACK FLOW INTO H2 FEED FROM REACTOR


Hazard: Backflow leading to H2 header contamination.
Causes:
PZDT-40062 (LL) Hydrogen to loop gas PID:0404
Actions:
Close XZV-40062 Hydrogen to loop PID:0404
Notes:
Minimum SIL level: 1

I-4029-O: OVERHEATING COOLING WATER LOOP PROTECTION


Hazard: High water temperature leading to cooling water pumps cavitations during start-up.
Causes:
TT-40073 (HH) Main loop condenser outlet – Water loop PID:0406
Actions:
Close XV-40070 Heated water for start-up PID:0406
Notes:
Minimum SIL level: 0

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PROCESS INTERLOCK DESCRIPTION

I-4031-S: BACK FLOW INTO H2 FROM METALLOCENE CATALYST INJECTION


Hazard: Backflow leading to H2 header contamination.
Causes:
PZDT-40059 (LL) Hydrogen to Metallocene catalyst PID:0404
injection
Actions:
Close XZV-40067 Hydrogen to Metallocene catalyst PID:0404
injection
Notes:
Minimum SIL level: 1

I-4032-O: BACK FLOW INTO PENTANE FEED OR INTO 1ST STAGE K.O. DRUM OF
RECYCLE GAS COMPRESSOR
Hazard: Production loss and flaring.
Causes:
PDT-40903 (LL) Pentane make-up to Main loop separator PID:0403
Actions:
Close XZV-40903 Pentane make-up to Main loop separator PID:0403
Causes:
PDT-40909 (LL) Pentane start-up to Main loop separator PID:0403
Actions:
Close XZV-40909 Pentane start-up to Main loop separator PID:0403
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

DEGASSING VARIABLE TRIP SETTINGS

The low and high stripping gas flow settings for the degassers and purge column are variable depending on
the groups of product. The different groups of product are identified by the reactor conditions which may
include catalyst, comonomer and temperature.
All these interlocks are implemented within the SIS system.
These conditions are then used to determine the trip settings for various interlocks.
I-4041-S: Poor degassing: Reactor Low Temperature
I-4042-S: Stop catalyst feeders: degassing capacity limit
I-6330-S: Poor degassing in Degasser: high stripping gas flow
I-6340-S: Poor degassing in Degasser: low stripping gas flow
I-6830-S: Poor degassing in C8 Degasser: high stripping gas flow
I-6840-S: Poor degassing in C8 Degasser: low stripping gas flow
I-6442-S: Poor degassing in purge column: low stripping gas flow
I-6445-S: Poor degassing in purge column: high stripping flow or high pressure

Reactor condition detection to identify the different groups of product


 The reactor temperature T is determined from the Mo3 reading of TZT-40044A/B/C
 The comonomer in use is determined from the comonomer feed valve positions.
The comonomer in use can then be determined by the following logic. This code may be common to all the
interlocks with variable trips.
IF XZV- 20550 (C4) not closed THEN comonomer = C4
IF XZV- 20560 (C6) not closed THEN comonomer = C6
IF XZV- 20570 (C8) not closed THEN comonomer = C8
If more than one comonomer valve is not closed OR fault on any valve THEN comonomer = error
An alarm in DCS warns the operator if there is an inconsistency between the reactor condition
detection and the grade selected by the operator on the GROWL.
 The catalyst type is determined from the catalyst injection valves.
The catalyst line in use can then be determined by the following logic. This code may be common to all the
interlocks with variable trips.
If XZV-30010 or XZV-30110 not closed then catalyst = Zg
If XZV-30210 or XZV-30310 or XZV-30410 not closed and then catalyst = Mt
If (tone of the Zg valve is open (not closed) at the same time of one the Mt valve) OR fault on any
valve THEN catalyst = error

Each valve position should be based on three signals: SIS command status to the valve, closed limit switch
and open limit switch, in order to achieve the necessary interlock integrity. All three signals should be
consistent before the position of the valve is determined; if they are not consistent then the valve is faulty.

Group identification

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PROCESS INTERLOCK DESCRIPTION

The group numbers are calculated from the reactor conditions


 If any reactor condition is in error or the combination does not match a group, then the group
should keep its last value.
 To avoid spurious changes the group numbers are only changed if the inputs have changed for
more than 30 minutes. The timer is held if there is no reaction detected.

Group number Group Name Reactor conditions


1 LLC4 [Comonomer = C4 And Catalyst = Zg]
for more than 30 minutes (Note 1)
2 LLC6 [Comonomer = C6 And Catalyst = Zg]
for more than 30 minutes (Note 1)
3 PFC6 [Comonomer = C6 And Catalyst = Mt]
for more than 30 minutes (Note 1)
4 LLC8-1 [Comonomer = C8 And Catalyst = Zg And T <88°C]
for more than 30 minutes. (Note 1)
5 LLC8-2 [Comonomer = C8 And Catalyst = Zg And T ≥88°C]
for more than 30 minutes. (Note 1)
6 PFC8 [Comonomer = C8 And Catalyst = Mt]
for more than 30 minutes (Note 1)
Keep last group Reactor condition error or combination not matching group
number and
send an alarm
to DCS
Note 1: The timer is held if there is no reaction detected by DT<DT_T (refer below for description of DT
and DT_T)
T is the reactor temperature as defined above

The group number is used to determine the trip matrix outputs (see below)
The SIS sends the group number to the DCS. This information is compared with group number defined in
GROWL for each grade. An alarm in DCS will be issued in case of discrepancy. This alarm may happen at
the start-up of the transition when operator will change of grade setting via the GROWL but has not yet
fulfilled the conditions to determine the group number. In steady state the group in SIS and DCS are
normally identical.

Stripping gas flow trip settings


The transition between different trip settings is performed with these following rules:
 Prior to transition the DCS operator sets the set point for the degassing flow controller in the DCS
to a ―transition‖ value independently of the changes in trip settings (refer to operating manual).
 The SIS detects the transition and change the group number
 During transition the stripping gas flow trip window is reduced to the overlap of the trip windows
before and after the transition by changing either the high or low trip value as appropriate.
 A timer is used to determine the length of the transition. This time is different for the degasser and
the purge column
 During transitions, the transition timer is held when the reaction is stopped (detected by Mo3 TZT-
40044A/B/C minus Mo3 TZT-40064A/B/C is < 5°C)
 If during the transition the matrix inputs change again, the transition is extended.

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PROCESS INTERLOCK DESCRIPTION

 When the transition is completed the high or low trip value as appropriate is changed to increase to
the operating trip window for the new reactor conditions.
 After transition the DCS operator sets the set point for the degassing flow controller in the DCS to
the required value independently of the changes in trip settings (refer to operating manual).

Trip matrix definition

 Degasser

Matrix Outputs MH ML
Matrix Inputs Group Number (I-6330-S: FZT-60514/60515 (I-6340-S: FZT-60514/60515
(HH) setting) (LL) setting)
3 3
1 3210 m /h 1550 m /h
3 3
2 3210 m /h 2130 m /h
3 3
3 3210 m /h 2370 m /h
3 3
4 2850 m /h 2130 m /h
3 3
5 2850 m /h 2130 m /h
3 3
6 3210 m /h 2370 m /h

 Degasser C8

Matrix OutputsMH ML
(I-6830-S: FZT- (I-6840-S: FZT-
Matrix Inputs-Group 60814/60815 (HH) 60814/60815 (LL)
Number setting) (Note 2) setting) (Note 2)
1 High flow = 29500 kg/h Low FZT range
(note 3) kg/h
2 High flow = 29500 kg/h Low FZT range
(note 3) kg/h
3 High flow = 29500 kg/h Low FZT range
(note 3) kg/h
4 29160 kg/h 21550 kg/h
5 25860 kg/h 8910 kg/h
6 29160 kg/h 19760 kg/h
Note 2: the values given for non-C8 products are set into the matrix to distinguish C8 operation from C4/C6
operation. It is used in some interlocks only acting in C8 operation.
Note 3: High flow for C4/C6 groups only to prevent fluidization issue in the C8 degasser

 Purge Column
Matrix Outputs MH ML
(I-6445-S: FZT- (I-6442-S: FZT-
Matrix Inputs-Group 60006A/B (HH) 60006A/B (LL)
Number setting) setting)
1 1760 kg/h 660 kg/h
2 1760 kg/h 1280 kg/h
3 1760 kg/h 1280 kg/h
4 1760 kg/h 1280 kg/h
5 1760 kg/h 1280 kg/h

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PROCESS INTERLOCK DESCRIPTION

6 1760 kg/h 1280 kg/h

Method for determining trip settings.


The matrix output is used in the following logics to determine the trip settings. Each matrix’s logic is
managed by its own code with relevant parameters.

 For high and low degassing flow trips:


The code below is applicable to degasser, degasser C8 and purge column matrix
Steady:
If ML≠TL or MH≠TH Then {Matrix outputs change indicating transition start}
Set FZALL nd F A H t transition values.}
TL = Max( TL, ML) {Transition TL is calculated as the maximum of FZALL’s}
TH = Min (TH, MH) Transition TH is calculated as the minimum of FZAHH’s}

If TL > TH Then set DCS alarm message ―POWDER CANNOT BE WITHDRAWN


FROM DEGASSER DURING THIS GRADE TRANSITION‖.

MLo = ML {Record matrix output in order to detect if reactor conditions


MHo =MH change during transition}
Reset and Start timer t {Start timer for indicating when transition is completed}
Goto Transition
Goto Steady

Transition:
If DT < DT_T Then hold timer t {Hold timer if reaction stops}
If DT ≥ DT_T Then restart timer t {Restart timer if reaction restarts}
if timer t> R Then TL = ML {If timer complete change FZALL and FZAHH trip settings to
TH = MH matrix values}
Goto Steady
If MLo≠ML or MHo≠MH Then {If matrix outputs change during transition, indicating a
Reset and restart timer t change in reactor conditions, then extend transition period
and change transition values}
TL = Max( TL, ML)
TH = Min (TH, MH)
If TL > TH Then set DCS alarm message ―POWDER CANNOT BE WITHDRAWN
FROM DEGASSER DURING THIS GRADE TRANSITION‖.

Goto transition

Where:

DT Calc Mo3 TZT-40044A/B/C minus Mo3 TZT-40064A/B/C

DT_T 5 °C Minimum temperature difference indicating reaction


MH Calc High trip output from matrix
ML Calc Low trip output from matrix
MHo Calc Previous high trip output from matrix
MLo Calc Previous low trip output from matrix
TH Calc Current trip setting for FZAHH-60514/60515 (for degasser) or

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
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PROCESS INTERLOCK DESCRIPTION

FZAHH-60814/60815 (for degasser C8) or FZAHH-60006A/B (for


purge column)
TL Calc Current trip setting for FZALL-60514/60515 (for degasser) or
FZALL-60814/60815 (for degasser C8) or FZALL-60006A/B (for
purge column)
t Transition timer

R 11.4 h for Time required before final change of FZAHH and FZALL
degasser
19.4 h for C8-
degasser
19.9 h for purge
column

I-4041-S: POOR DEGASSING: REACTOR LOW TEMPERATURE


Hazard: High level of HC in powder passed to degassing system leading to potential explosion
downstream.
Causes:
TZT-40044A/B/C (LL) voting 2oo3 Polymerisation reactor outlet – Loop gas PID:0401
(Note 1)
Actions:
Close XZV- Lock hoppers isolation valves PID:0601
60003/60005/60053/60055/60303/6 /0602/
0305/60313/60315/60323/60325 0603
Notes:  Note 1: the trip setting is grade dependent. Refer below.
Minimum SIL level: 2
Refer to section on Degassing Variable Trip Settings for how these values are determined.
The trip setting for TZT-40044A/B/C (LL) should be set according to the following matrix.
Group number
1 81°C
2 81°C
3 76°C
4 81°C
5 81°C
6 76°C
On Error 81°C

I-4042-S: STOP CATALYST FEEDERS: DEGASSING CAPACITY LIMIT


Hazard: Powder production exceeds degassing capacity limit for some grades: high level of HC in
powder passed to degassing system leading to potential explosion downstream.

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 63 / 110

PROCESS INTERLOCK DESCRIPTION

Causes:
FZT-40068 (HH) for T1-4042 (Note Ethylene feed to reactor PID:0404
1)
OR
FZT-40069 (HH) for T1-4042 (Note Ethylene feed to reactor PID:0404
1)
Actions:
Stop X-380A/B Ziegler rotary valves PID:0303
AND
Stop X-386A/B/C Metallocene rotary valves PID:0305
AND
Close XZV- Lock hoppers isolation valves PID:0601
60003/60005/60053/60055/60303/6 /0602/06
0305/60313/60315/60323/60325 03
Notes:  Note 1: the trip setting is grade dependent. Refer below.
 T1-4042: 15 min to increase availability.
Minimum SIL level: 2
Refer to section on Degassing Variable Trip Settings for how these values are determined.
The trip setting for FZT-40068 (HH) and FZT-40069 (HH) should be set according to the following matrix.
Group number
1 46 t/h
2 46 t/h
3 46 t/h
4 34 t/h
5 46 t/h
6 46 t/h

On Error 34 t/h

I-4071-S: HP LIQUID INJECTION PUMPS


Hazard: Pumps running dry leading to pump damage.
Causes:
LZT-40901 (LL) Main loop separator PID:0403
OR
LZT-40902 (LL) Main loop separator PID:0403
Actions:
Stop P-409A HP Liquid injection pump (A) PID:0403
AND
Stop P-409B HP Liquid injection pump (B) PID:0403
Notes:  Interlock implemented in safety system to increase availability.

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 64 / 110

PROCESS INTERLOCK DESCRIPTION

Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-4072-S: BACK FLOW INTO NITROGEN / ETHYLENE FROM HP LIQUID INJECTION


Hazard: Backflow leading to contamination of Nitrogen / Ethylene header. Liquid to compressors’
seal system. Damage to compressors and loss of containment.
Causes:
PZDT-40951 (LL) for T1-4072 Nitrogen / Ethylene back-up for HP liquid PID:0405
injection nozzles
Actions:
Close XZV-40952 Nitrogen / Ethylene back-up for HP liquid PID:0405
injection nozzles
Notes:  T1-4072: timer = 15 secs to avoid spurious trip
Minimum SIL level: 1

I-4080-S: LIQUID CARRY OVER TO MAIN LOOP COMPRESSOR


Hazard: Liquid carry over to Main loop compressor leading to compressor damage and loss of
production.
Causes:
LZT-40901 (HH) Main loop separator PID:0403
OR
LZT-40902 (HH) Main loop separator PID:0403
Actions:
Close XZV-40902 Comonomer to Main loop separator PID:0403
AND
Close XZV-40903 Pentane make-up to Main loop separator PID:0403
AND
Close XZV-40909 Pentane start-up to Main loop separator PID:0403
AND
Close XZV-40904 VRU second interchanger condensate to PID:0403
Main loop separator
AND
Close XZV-40919 Condensate from washing pumps to Main PID:0403
loop separator
AND
Close XZV-40920 C8 VRU Condensate from recycle pumps PID:0403
to Main loop separator
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 65 / 110

PROCESS INTERLOCK DESCRIPTION

I-4410-S: TEAL TO NITROGEN BACKFLOW


Hazard: Contamination of Nitrogen header with TEAL
Causes:
PZDT-40104 (LL) Nitrogen to TEAL system PID:0409
Actions:
Close XZV-40104 Nitrogen to TEAL system PID:0409
Notes:
Minimum SIL level: 1

I-4447-O: TEAL AND LIQUID ADDITIVES SIMULTANEOUS INJECTION


Hazard: Off-spec production
Causes:
XZV-40209 not closed Liquid additive S1 to injection PID:0411
Actions:
Close XZV-40521 TEAL pumps P-455A/B discharge PID:0410

AND
Close XZV-40522 TEAL pumps P-455A/B discharge PID:0410

AND
Close XZV-40207 Liquid additive (B1) feed to reactor PID:0408

Causes:
XZV-40521 not closed TEAL pumps P-455A/B discharge PID:0410

OR
XZV-40522 not closed TEAL pumps P-455A/B discharge PID:0410

Actions:
Close XZV-40209 Liquid additive S1 to injection PID:0411
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-4538-O: TEAL PUMP OVERPRESSURE


Hazard: Relief valve discharge lifting.
Causes:
PT-40521 (HH) TEAL injection pumps discharge PID:0410
Actions:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 66 / 110

PROCESS INTERLOCK DESCRIPTION

Stop P-455A TEAL injection pump (A) PID:0410


AND
Stop P-455B TEAL injection pump (B) PID:0410
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-4554-O: STOP TEAL INJECTION WHEN NO ZIEGLER CATALYST INJECTION


Hazard: Build-up of TEAL in reactor and reaction take-off.
Causes:
X-380A Stopped for more than T1- Ziegler catalyst rotary valve PID:0303
4554
AND
X-380B Stopped for more than T1- Ziegler catalyst rotary valve PID:0303
4554
Actions:
Stop P-455A (Note 1) TEAL injection pump PID:0410
AND
Stop P-455B (Note 1) TEAL injection pump PID:0410
AND
Close XZV-40521 (Note 1) TEAL injection pumps discharge PID:0410

AND
Close XZV-40522 (Note 1) TEAL injection pumps discharge PID:0410

Notes:  T1-4554: Timer = 15 min


 Note 1: Interlock to be designed such as TEAL pumps must be able to be
started for reactor cleaning without catalyst injection.
Minimum SIL level: 0

I-4555-S: BACK FLOW INTO TEAL FEED


Hazard: TEAL system overpressure causing safety valve lift on containers and fire.
Causes:
PZDT-40522 (LL) TEAL injection line PID:0410
OR
[P-455A Stopped TEAL injection pump PID:0410
AND
P-455B Stopped] TEAL injection pump PID:0410
OR
PZT-40523A (HH) TEAL injection pump (A)suction PID:0410

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 67 / 110

PROCESS INTERLOCK DESCRIPTION

OR
PZT-40523B (HH) TEAL injection pump (B) suction PID:0410
Actions:
Close XZV-40521 TEAL pumps discharge PID:0410
AND
Close XZV-40522 TEAL pumps discharge PID:0410
Notes:
Minimum SIL level: 2

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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Technologies RAPID L20 INE PRO DES 3200 0013


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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 68 / 110

PROCESS INTERLOCK DESCRIPTION

2.5 SECTION 600

I-6204-S: OVERPRESSURISATION OF DEGASSER


Hazard: Degasser failure
Causes:
PZT-60519 (HH2) Degasser PID:0604
OR
PZT-60522 (HH2) Degasser PID:0604
Actions:
Close XZV-60003/60053 Upflow lock hoppers top isolation valves PID:0601
AND
Close XZV-60303/60313 Downflow lock hoppers top isolation PID:0602
valves
AND
Close XZV-60323 Downflow lock hopper top isolation valve PID:0603
AND
Close XZV- Degasser polymer powder isolation PID:0604
60511/60512/60521/60522/60523 valves
Causes:
XZV-60006 Not closed (note 1, 2, 3, 1st upflow lock hopper powder take-off PID:0601
4) valve
Actions:
Close XZV-60005 (Note 4) 1st upflow lock hopper powder filling valve PID:0601
Causes:
XZV-60005 Not closed (note 1, 2, 3, 1st upflow lock hopper powder filling valve PID:0601
4)
Actions:
Close XZV-60006 (Note 4) 1st upflow lock hopper powder take-off PID:0601
valve
Notes:  Note 1: for information, the valve is equipped with 4 limit switches. A pair of
open/close limit switches are connected to SIS for interlock purpose, another
pair of open/close limit switches are connected to DCS for sequence purpose.
 Note 2: Autoreset
 Note 3: Typical interlock: to be extended to all lock hoppers (XZV-
60055/60056; XZV-60305/60306; XZV-60315/60316; XZV-60325/60326).

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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Technologies RAPID L20 INE PRO DES 3200 0013


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PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 69 / 110

PROCESS INTERLOCK DESCRIPTION

 Note 4: a pneumatic interlock between take-off and bottom lock hoppers valves
should not allow air supply to both valves. The pneumatick interlock must be
SIL 1. Refer to the valves datasheet for pneumatic interlock scheme.
Minimum SIL level: SIL 2: On high pressure, close upflow and downflow lock hoppers isolation
valves
SIL 1: interlocking of lock-hopper take-off and filling valves

I-6207-O: OVERFILLING OF DEGASSER


Hazard: Blockage of withdrawal lines
Causes:
LSHH-60511 (HH) Degasser PID:0604
Actions:
CloseXZV-60003/60053 Upflow lock hoppers top isolation valves PID:0601
AND
CloseXZV-60303/60313/60323 Downflow lock hoppers top isolation PID:0602
valves /0603
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6305-S: POOR DEGASSING IN DEGASSER: HIGH HIGH PRESSURE


Hazard: Downstream equipment explosion.
Causes:
PZT-60519 (HH1) Degasser PID:0604
OR
PZT-60522 (HH1) Degasser PID:0604
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605
Notes:
Minimum SIL level: 1

I-6329-O: OVERFILLING OF PURGE COLUMN OR CONVEYING FILTER OR CONVEYING


LINE BLOCKAGE OR OVERFILLING OF START-UP POWDER SILO
Hazard: Line/filter blockage
Causes:
[ LSHH-60024 (HH) Purge column PID:0606
AND XDX-60642 set to Purge
column

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 70 / 110

PROCESS INTERLOCK DESCRIPTION

OR
LSHH-60111 (HH) Conveying filter PID:0606
OR
LSHH-60072 (HH) Start-up powder silo PID:0608
AND XDX-60642 set to start-up silo
OR
X-641 detected stopped Conveying filter outlet rotary valve PID:0606
OR
SAL-60101 (L) Conveying filter outlet rotary valve PID:0606
OR
K-660A detected stopped Gas conveying blowers PID:0607
OR
PT-60021 (HH) ] Powder conveying line A PID:0607
AND
XDX-60639A/B routed to purge Diverters PID:0605
column
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605
AND
Stop X-661 Powder conveying feed rotary valve PID:0613
Causes:
[ LSHH-60024 (HH) Purge column PID:0606
AND XDX-60642 set to Purge
column
OR
LSHH-60111 (HH) Conveying filter PID:0606
OR
LSHH-60072 (HH) Start-up powder silo PID:0608
AND XDX-60642 set to start-up silo
OR
X-641 detected stopped Conveying filter outlet rotary valve PID:0606
OR
SAL-60101 (L) Conveying filter outlet rotary valve PID:0606
OR
K-660B detected stopped Gas conveying blowers PID:0607
OR
PT-60039 (HH) ] Powder conveying line B PID:0607
AND
XZDX-60639A routed to C8 Diverter PID:0605
degasser

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 71 / 110

PROCESS INTERLOCK DESCRIPTION

Actions:
Stop X-661 Powder conveying feed rotary valve PID:0613
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6330-S: POOR DEGASSING IN DEGASSER: HIGH STRIPPING GAS FLOW


Hazard: Downstream equipment explosion due to fluidization of powder
Causes:
Corrected FZT-60514 (HH) (Note 1, VRU Stripping gas to degasser PID:0604
2)

OR

Corrected FZT-60515 (HH) (Note 1, VRU Stripping gas to degasser PID:0604


2)
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605
Notes:  Note 1: Corrected value to get actual flow in degasser:
Corrected FZTxxxxx = FZTxxxxx * [PZI60505 + ATM] / [PZI60510 +
ATM]. ATM is absolute atmospheric pressure. Refer to project basis. The
correction must be limited between 0% below and 50% above FZTxxxxx.
Limits to be refined during commissioning.
 Note 2: the trip setting is grade dependent. Refer to section on Degassing
Variable Trip Settings for how trip settings are determined.

Minimum SIL level: 1

I-6331-O: DEGASSER OUTLET ROTARY VALVE DAMAGE


Hazard: Degasser outlet rotary valve damage leading to production loss.
This interlock in conjunction with I-6339-S and sequence 64 forces the operator to put the
degasser on recycle when initially starting the withdrawals and avoid any risk of powder
compaction in degasser. The sequence 64 prevents the withdrawals being started if the
Degasser Recycle rotary valve is stopped. When there is low level in degasser then powder
cannot be removed from Degasser except through the recycle system.
Causes:
[ (X-660 Stopped OR SSL-60561 Powder conveying feed rotary valve PID:0605
(L))
AND XDX-60601 Set to X-660] Degasser Recycle diverter valve PID:0605
OR
[ (X-632 Stopped OR SSL-60571 Degasser Recycle rotary valve PID:0605
(L))

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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LICENSOR REFERENCE Rev. Page
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 72 / 110

PROCESS INTERLOCK DESCRIPTION

AND XDX-60601 Set to Recycle] Degasser Recycle diverter valve PID:0605


Actions:
Stop X-628 Degasser outlet rotary valve PID:0604
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6333-O: DEGASSER RECYCLING LINE BLOCKAGE


Hazard: Recycling Conveying Line blockage
Causes:
PT-60581 (HH) N2 to Degasser Recycling line PID:0605
OR
FT-60581 (LL) N2 to Degasser Recycling line PID:0605
Actions:
Stop X-632 Degasser Recycle rotary valve PID:0605
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6334-O: POWDER BUILD-UP IN DEGASSER RECYCLE ROTARY VALVE


Hazard: Powder build-up prevention leading to rotary valve damage
Causes:
XDX-60601 In recycle position Degasser Recycle diverter valve PID:0605
Actions:
Set the speed to minimum X-628 Degasser outlet rotary valve PID:0604
Notes:  When the rotary X-628 is detected stopped a high priority alarm must be
initiated for operator to start recycle line.

Minimum SIL level: No SIL requirement by INEOS Technologies

I-6338-S: STOP DEGASSER FILLING WHEN IN EMPTY MODE


Hazard: Low residence time: downstream equipment explosion.
Causes:
HZS-60506 In Empty mode NORMAL / EMPTY degasser PID:0604
Actions:
CloseXZV-60003/60053 Upflow lock hoppers top isolation valves PID:0601
AND

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

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LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 73 / 110

PROCESS INTERLOCK DESCRIPTION

CloseXZV-60303/60313/60323 Downflow lock hoppers top isolation PID:0602


valves /0603
Notes:
Minimum SIL level: 1

I-6339-S: STOP POWDER FEEDING FROM DEGASSER WHEN POOR DEGASSING IN


DEGASSER: LOW RESIDENCE TIME
Hazard: Downstream equipment explosion.
Causes:
[ LZSLL-60513 (LL) Degasser PID:0604
OR
LZSLL-60514 (LL) ]
AND
HZS-60506 In Normal mode NORMAL / EMPTY Degasser PID:0604
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605
Causes:
[ LZSLL-60513 (LL) Degasser PID:0604
OR
LZSLL-60514 (LL) ]
Actions:
Open XZV-60507 Stripping gas to degasser bottom PID:0604
Notes:
Minimum SIL level: 1

I-6340-S: POOR DEGASSING IN DEGASSER: LOW STRIPPING GAS FLOW


Hazard: Downstream equipment explosion due to poor degassing.
Causes:
FZT-60514 (LL) for more than T1- VRU Stripping gas to degasser PID:0604
6340 (Note 1, 2)
OR
FZT-60515 (LL) for more than T1- VRU Stripping gas to degasser PID:0604
6340 (Note 1, 2)
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605
Notes:  T1-6340: timer = 15 min to allows backup N2 to be established and to
allow time to react on VRU.

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 74 / 110

PROCESS INTERLOCK DESCRIPTION

 Note 1: Corrected value to get actual flow in degasser: Corrected


FZTxxxxx = FZTxxxxx * [PZI60505 + ATM] / [PZI60510 + ATM]. ATM is
absolute atmospheric pressure. Refer to project basis. The correction
must be limited between 20% below and above FZTxxxxx.
 Note 2: the trip setting is grade dependent. Refer to section on
Degassing Variable Trip Settings for how trip settings are determined.

Minimum SIL level: 1

I-6341-S: HIGH HC CONTENT IN STRIPPING GAS TO DEGASSER


Hazard: Downstream equipment explosion due stripping gas with too high HC content leading to
poor degassing.
Causes:
TZT-60502A/B/C (HH) (2oo3) Stripping gas from VRU main separator PID:0612
OR
PZT-60502A/B/C (LL) (2oo3) Stripping gas from VRU main separator PID:0612
Actions:
Close FZV-60602 (SIS) Stripping gas to Degasser PID:0611
AND
Initiate Interlock I-6750-O Poor degassing in Degasser: Nitrogen
back-up
AND
CloseXZV-60602 Stripping gas to Degasser PID:0611

Causes:
LZT-60501A/B/C (HH) (2oo3) VRU main separator PID:0612

Actions:
Close FZV-60602 Stripping gas to Degasser PID:0611
AND
Initiate Interlock I-6750-O Poor degassing in degasser: Nitrogen
back-up

AND

Close XZV-60602 Stripping gas to degasser PID:0611

AND

Stop K-675 Recycle gas compressor PID:0610

AND

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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LICENSOR REFERENCE Rev. Page
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 75 / 110

PROCESS INTERLOCK DESCRIPTION

st
Close LV-60001B (DCS) Condensate from recycle compressor 1 PID:0610
stage KO drum
Notes:
Minimum SIL level: 2

I-6342-S: HIGH DIFFERENTIAL TEMPERATURE BETWEEN REACTOR AND DEGASSER


Hazard: Poor degassing due to excess concentration of C5/C6 leading to downstream equipment
explosion.
Causes:
TZDI-60511A (HH) (Note 1) Temperature difference between reactor PID:0604
and degasser
OR
TZDI-60511B (HH) (Note 1) Temperature difference between reactor PID:0604
and degasser
OR
TZDI-60512A (HH) (Note 1) Temperature difference between reactor PID:0604
and degasser
OR
TZDI-60512B (HH) (Note 1) Temperature difference between reactor PID:0604
and degasser
OR
TZDI-60520A (HH) (Note 1) Temperature difference between reactor PID:0604
and degasser
OR
TZDI-60520B (HH) (Note 1) Temperature difference between reactor PID:0604
and degasser
Actions:
CloseXZV-60003/60053 Upflow lock hoppers top isolation valves PID:0601
AND
CloseXZV-60303/60313/60323 Downflow lock hoppers top isolation PID:0602
valves /0603
AND
Stop X-660 Powder conveying feed rotary valve PID:0604
if HZS-60506 In Normal mode /0605

Notes:  Note 1:TZDI-605xxy = Mo3 of (TZT-40044A/B/C) – TZT-605xxy.


Minimum SIL level: 2

I-6368-O: N2 OR PROCESS GAS BREAKTHROUGH ON DEGASSER SAMPLING SYSTEM


Hazard: Prevent loss of N2 to vent and to degasser.
Causes:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 76 / 110

PROCESS INTERLOCK DESCRIPTION

XZV-60510 Not closed Degasser powder sampling N2 purging PID:0604


OR
XV-60508 Not closed Degasser powder sampling venting PID:0604
Actions:
Close XV-60531 Degasser powder sampling filling PID:0604
Notes:  Autoreset
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6369-S: DEGASSER POWDER SAMPLING SYSTEM OPERATOR


Hazard: Nitrogen or process gas breakthrough to sampling area leading to operator asphyxiation or
explosion (presence of H2).
Causes:
PZT-60514 (HH) Degasser powder sampling PID:0604
OR
XV-60508 Not closed Degasser powder sampling venting PID:0604
OR
XV-60531 Not closed Degasser powder sampling filling PID:0604
OR
XV-60510 Not closed Degasser powder sampling N2 purging PID:0604
Actions:
Close XZV-60509 Degasser powder sampling take off PID:0604
Notes:  Autoreset
Minimum SIL level: 1

I-6408-S: DEGASSING VENT ROUTED TO ATM AND SNUFFING SYSTEM


Hazard: Flare backpressure too high leading to purge column poor degassing and extruder feed trip.
Vent routed to safe atmophere with snuffing to dilute HC
Causes:
PZT-60061 (HH) (pulse) Purge column off gas fan suction PID:0618
Actions:
Open XZV-60061 Steam to snuffing system PID:0618
AND
When XZV-60061 Confirmed open. Purge column off gas to snuffing system PID:0618
then wait T1-6408 and open XZV-
60060
Causes:
PZT-60064 (NOT HH) Flare backpressure return to normal value PID:0618

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 77 / 110

PROCESS INTERLOCK DESCRIPTION

Actions:
Close XZV-60060 Purge column off gas to snuffing system PID:0618
AND
When XZV-60060 Confirmed closed. Steam to snuffing system PID:0618
then wait T2-6408 and close XZV-
60061
Notes:  Autoreset interlock
 T1-6408 timer = 15s
 T2-6408 timer = 60s
Minimum SIL level: SIL 1 for steam opening part of the interlock

I-6409-O: AIR INGRESS AT PURGE COLUMN OFFGAS FAN


Hazard: Downstream equipment explosion.
Causes:
PZT-60061 (LL) Purge column offgas fan suction PID:0618
Actions:
Stop K-640 Purge column off gas fan PID:0618
Notes:
Minimum SIL level: 0

I-6435-S: STOP PURGE COLUMN FILLING WHEN IN EMPTY MODE


Hazard: Low residence time: downstream equipment explosion.
Causes:
HZS-60001 In Empty mode NORMAL / EMPTY purge column PID:0606
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605
Notes:
Minimum SIL level: 1

I-6441-O: POOR DEGASSING IN PURGE COLUMN: LOW LEVEL AT STARTUP


Hazard: Prevents the purge column being fed when there is low level in purge column and powder is
not recycled. This forces the operator to put on recycle when initially starting to feed the
purge column and avoid any risk of poor degassing of powder below low level and risk of
powder compaction.
Causes:
[ X-666 is detected stopped Purge column recycle rotary valve PID:0606

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 78 / 110

PROCESS INTERLOCK DESCRIPTION

OR PID:0606
XV-60014 Not open Purge column recyling line
OR PID:0606
XDX-60604 Not set to recycling ] Purge column recycle diverter valve
AND
[ LZT-60021 (LL) OR LZT-60022 Purge column PID:0606
(LL)
OR LZT-60023 (LL) (1oo3)]
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605

Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6442-S: POOR DEGASSING IN PURGE COLUMN: LOW STRIPPING GAS FLOW


Hazard: Low degassing flow: downstream equipment explosion.
Causes:
FZT-60006A (LL) for more than T1- LN stripping gas to purge column PID:0606
6442 (Note 1)
OR
FZT-60006B (LL) for more than T1- LN stripping gas to purge column PID:0606
6442 (Note 1)
Actions:
Stop X-640 Purge column outlet rotary valve PID:0606

AND
Close XZV-60011 Purge column to extrusion isolation PID:0606
Notes:  T1-6442: timer = 5 Seconds.
 Note 1: the trip setting is grade dependent. Refer to section
on Degassing Variable Trip Settings for how trip settings are
determined.
Minimum SIL level: 2

I-6443-S: POOR DEGASSING IN PURGE COLUMN: LOW RESIDENCE TIME


Hazard: Low residence time: high level of HC in powder passed to degassing system leading to
potential explosion downstream
Causes:
[LZT-60021 (LL) OR LZT-60022 (LL) Purge column PID:0606

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


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PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 79 / 110

PROCESS INTERLOCK DESCRIPTION

OR LZT-60023 (LL)] (2oo3)


AND
HZS-60001 In Normal mode NORMAL / EMPTY purge column PID:0606
Actions:
Close XZV-60011 Purge column to extrusion isolation PID:0606
AND
Stop X-640 after T1-6443 Purge column outlet rotary valve PID:0606
AND
Open XZV-60012 (note 1) Nitrogen stripping gas to Purge column PID:0606
bottom
Notes: - When [ (X-640 stopped or XZV-60011 closed) and (X-666 stopped or XV-
60014 closed)], a high priority alarm must be initiated for operator to start recycle
line.
- Note 1: Close XZV-60012 when interlock is reset.
- T1-6443: timer = time to empty line between XZV and X-640.
Minimum SIL level: 2 (Close XZV-60011 and stop X-640 on Purge column low level)

I-6444-S: STOP STEAM INJECTION INTO PURGE COLUMN WHEN INSUFFICIENT


NITROGEN FLOW
Hazard: Blockage of purge column due to condensation leading to production loss.
Causes:
FZT-60006A/B (LLL) (1oo2) Nitrogen stripping gas to purge column PID:0606

OR

TZT-60035 (LL) Nitrogen stripping gas to purge column PID:0606


Actions:
Close FZV-60014 (SIS) Steam to purge column PID:0606
AND
Close XZV-60013 Steam to purge column PID:0606
Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 80 / 110

PROCESS INTERLOCK DESCRIPTION

I-6445-S: POOR DEGASSING IN PURGE COLUMN: HIGH STRIPPING FLOW OR HIGH


PRESSURE
Hazard: Downstream equipment explosion.
Causes:
FZT-60006A/B (HH) (1oo2) (Note 2) Nitrogen stripping gas to purge column PID:0606
OR
PZT-60031 (HH) Purge column PID:0606
Actions:
Close XZV-60011 Purge column to extrusion isolation PID:0606
AND
Stop X-640 after T1-6445 Purge column oultlet rotary valve PID:0606
AND
Close FZV-60013 (SIS) Nitrogen stripping gas to purge column PID:0606

AND

Close FZV-60015 (SIS) Nitrogen stripping gas to purge column PID:0606


bottom

AND

Close XZV-60012 (note 1) Nitrogen stripping gas to purge column PID:0606


bottom
Notes:  T1-6445: timer = time to empty line between XZV-60011 and Purge column
oultlet rotary valve.
 Note 1: This interlock has priority on Interlock I-6443-S.
 Note 2: the trip setting is grade dependent. Refer to section on Degassing
Variable Trip Settings for how trip settings are determined.
Minimum SIL level: 2 for high flow
1 for high pressure

I-6446-O: PURGE COLUMN OUTLET ROTARY VALVE DAMAGE


Hazard: Purge column outlet rotary valve damage leading to production loss.
Causes:
S-820 Detected stopped Polymer vibrating screen PID:0801
AND
XDX-80805 Set to S-820 Vibrating screen bypass diverter PID:0801
Actions:
Stop X-640 Purge column outlet rotary valve PID:0606

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 81 / 110

PROCESS INTERLOCK DESCRIPTION

Notes:
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-6462-S: PELLET WATER TOO HIGH TEMPERATURE – ABSORBED HC DRIVING OFF


PELLETS (ALL GRADES)
Hazard: High pellet water temperature leads to driving off absorbed gas in pellet silos and explosion
in silo or tanker downstream.
Causes:
TZT-80701 (HH) Pellet dryer/dewatering inlet PID:0806
Actions:
Stop X-640 Purge column outlet rotary valve PID:0606
Notes:
Minimum SIL level: 1

I-6656-S: AIR INGRESS AT CONVEYING GAS BLOWER (A)


Hazard: Downstream equipment explosion and conveying line blockage.
Causes:
PZT-60042 (LL) Conveying gas blower (A) suction PID:0607
Actions:

Stop K-660A Powder conveying blower PID:0607


Notes:
Minimum SIL level: 1

I-6657-S: AIR INGRESS AT CONVEYING GAS BLOWER (B)


Hazard: Downstream equipment explosion and conveying line blockage.
Causes:
PZT-60052 (LL) Conveying gas blower (B) suction PID:0607
Actions:
Stop K-660B Powder conveying blower PID:0607
Notes:
Minimum SIL level: 1

I-6664-O: START-UP CONVEYING LINE BLOCKAGE


Hazard: Conveying line blockage.

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 82 / 110

PROCESS INTERLOCK DESCRIPTION

Causes:
XV-60081 Detected not open Start-up powder to reactor PID:0608
OR
PT-60081 (HH) Start-up powder conveying nitrogen PID:0608
OR
FT-60081 (LL) Start-up powder conveying nitrogen PID:0608
Actions:
Stop X-667 Start-up powder rotary valve PID:0608
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6665-O: DEGASSER RECYCLE ROTARY VALVE AND START-UP POWDER ROTARY


VALVE DAMAGE
Hazard: Degasser recycle rotary valve and start-up powder rotary valve damage
Causes:
[ X-667 Detected stopped Start-up powder rotary valve PID:0608
OR
SSL-60072 (L) ] Start-up powder rotary valve PID:0608
AND
XDX-60604 Set to reactor position Purge column recycle diverter valve PID:0606
Actions:
Stop X-666 Purge column recycle rotary valve PID:0606
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6666-O: PURGE COLUMN RECYCLING LINE BLOCKAGE


Hazard: Recycling line blockage
Causes:
[ PT-60038 (HH) OR FT-60007 (LL) Purge column Recycling conveying PID:0606
] nitrogen
AND
XDX-60604 Set to recycling position Purge column recycle diverter valve PID:0606
Actions:
Stop X-666 Purge column recycle rotary valve PID:0606
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 83 / 110

PROCESS INTERLOCK DESCRIPTION

I-6667-O: START-UP SILO RECYCLING LINE BLOCKAGE PREVENTION


Hazard: Conveying line blockage
Causes:
[ PT-60079 (HH) Start-up silo recycling conveying nitrogen PID:0608
OR FT-60074 (LL) ]
AND
XDX-60690 set to Recycling Start-up silo recycle diverter valve PID:0608
Actions:
Stop X-690 Start-up silo outlet rotary valve PID:0608
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6668-O: START-UP SILO OUTLET ROTARY VALVE DAMAGE PROTECTION


Hazard: Start-up silo outlet rotary valve damage
Causes:
[X-667 detected stopped Start-up powder rotary valve PID:0608
OR SSL-60072]
AND
XDX-60690 set to reactor position Start-up silo recycle diverter valve PID:0608
Actions:
Stop X-690 Start-up silo outlet rotary valve PID:0608
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6701-S: LIQUID CARRY OVER TO RECYCLE COMPRESSOR


Hazard: Recycle compressor damage (note 1)
Causes:
LZT-60102 (HH) Recycle compressor Suction KO drum PID:0609
OR
LZT-60003 (HH) Recycle compressor first stage KO drum PID:0610
Actions:
Stop K-675 Recycle gas compressor PID:0610
Causes:
LZT-60003 (HH) Recycle compressor first stage KO drum PID:0610
Actions:
Close XZV-60008 Pentane make-up to first stage KO drum PID:0610

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 84 / 110

PROCESS INTERLOCK DESCRIPTION

AND
Close LZV-60001C (SIS) Condensate from VRU condensate PID:0610
pumps
Causes:
K-675 detected stopped Recycle gas compressor PID:0610
Actions:
Close XZV-60009 Cooling liquid to recycle gas compressor PID:0610
suction
AND
Close XZV-60010 Cooling liquid to recycle gas compressor PID:0610
st
1 stage
Notes:  To be finalised with compressor vendor
 Note 1: Liquid build-up when machine stops. Risks and protection to be
provided by detailed engineering in accordance to machine and system
low points.
Minimum SIL level: To be assessed by DE

I-6702-S: RECYCLE GAS COMPRESSOR SUCTION KO DRUM HIGH LEVEL


Hazard: Liquid overflow from KO drum to degasser. Powder degassing issue and explosion in
degasser downstream equipment
Causes:
LZT-60102 (HH) Recycle compressor Suction KO drum PID:0609
Actions:
Close XZV-60102 Liquid feed header to KO drum PID:0609
Notes:
Minimum SIL level: 1

I-6717-S: AIR INGRESS TO RECYCLE COMPRESSOR


Hazard: Recycle compressor damage or Downstream equipment explosion due to air ingress at
compressor suction
Causes:
PZT-60103 (LL) (note 1) Recycle Compressor suction PID:0609
Actions:
Stop K-675 Recycle gas compressor PID:0610
Notes:  To be finalised with compressor vendor
 Note 1: Location of PZT-60103 should be between any isolation valve
and compressor inlet
Minimum SIL level: 1

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
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LICENSOR REFERENCE Rev. Page
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 85 / 110

PROCESS INTERLOCK DESCRIPTION

I-6750-O: POOR DEGASSING IN DEGASSER: NITROGEN BACKUP

Hazard: Inject back-up nitrogen into degasser in case of VRU shutdown. The back-up nitogen flow is
ramped to prevent N2 network over draw.
Causes:
I-6341-S Activated High HC content on stripping gas to
degasser protection
Actions:
Open XV-60603 Back-up N2 for stripping gas from VRU PID:0611
AND
Set to Auto mode and ramp set point Back-up N2 for stripping gas from VRU PID:0611
of FIC-60603 T1-6750 (Note 1)
Notes:  Note 1: T1-6750: timer = 5 min corresponding to a ramp rate
= 500 kg/hr/min
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6754-O: LOW TEMPERATURE IN PIPE WORK FROM VRU MAIN SEPARATOR


Hazard: Cold temperature leading to pipe failure.
Causes:
TT-60102 (LL) Condensate to recycle compressor KO PID:0609
drum
OR
TT-60602 (LL) Condensate to main loop separator and PID:0611
HCD
Actions:
FMC LIC-60501 Condensate to recycle compressor KO PID:0612
drum, main loop separator and HCD
Notes:
Minimum SIL level: 0

I-6756-O: VRU RECYCLE PUMPS


Hazard: Prevent pump running dry
Causes:
LIC-60501 (LL) VRU main separator PID:0612
Actions:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 86 / 110

PROCESS INTERLOCK DESCRIPTION

Stop P-675A/B VRU condensate Recycle Pumps PID:0612


Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6771-O: VRU WASHING PUMPS PROTECTION


Hazard: Damage to pump. Prevents running dry
Causes:
LZT-60102 (LL) Recycle compressor suction KO drum PID:0609
Actions:
Stop P-671A VRU washing pump PID:0609
AND
Stop P-671B VRU washing pump PID:0609
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6772-O: BACK FLOW INTO RECYCLE COMPRESSOR FROM GAS LOOP


Hazard: Backflow protection, avoid fines in the VRU
Causes:
K-675 Detected stopped Recycle gas compressor PID:0610
Actions:
Close XV-40906 Recycle gas from Recycle gas PID:0403
compressor
AND
FMC FIC-60601 VRU purge PID:0611
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6776-O: RECYCLE GAS COMPRESSOR CONDENSATE PUMPS


Hazard: Prevent pumps running dry
Causes:
LZT-60003 (LL) Recycle compressor first stage KO drum PID:0610
Actions:
Stop P-672A/B Recycle compressor condensate pumps PID:0610
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 87 / 110

PROCESS INTERLOCK DESCRIPTION

I-6777-O: AUTOMATIC VRU GAS TO NITROGEN SUPPLY TO THE DEGASSER FILTER


BACK FLUSH
Hazard: Prevent degasser overhead filter pluggage on loss of VRU back flush. Prevent simultaneous
feed from nitrogen and VRU gas that could lead to backflow into nitrogen.
Causes:
K-675 Detected stopped Recycle gas compressor PID:0610
OR
XZV-60602 not open Stripping gas from VRU to degasser PID:0611
Actions:
Close XV-60604 VRU flushing gas to degasser overhead PID:0611
filter back flush
AND
Open XV-60525 Nitrogen back-up to degasser overhead PID:0604
filter back flush
Causes:
XV-60525 detected not closed Nitrogen back-up to degasser overhead PID:0604
filter back flush
Actions:
Close XV-60604 VRU flushing gas to degasser overhead PID:0611
filter back flush
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6778-O: RECYCLE GAS COMPRESSOR CONDENSATE PUMPS


Hazard: Damage to high speed pump in case of closed outlet.
Causes:
FT-60004 (LL) Recycle gas compressor condensate PID:
pumps 0610
AND
[P-672A running for more than Recycle gas compressor condensate PID:
T1-6778 pumps 0610
OR
P-672B running for more than
T1-6778]

Actions:
Stop P-672A/B Recycle gas compressor condensate PID:
pumps 0610

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 88 / 110

PROCESS INTERLOCK DESCRIPTION

Notes:  T1-6778: timer = 20s Time for pump to establish flow and avoid trip on
low flow at start-up.
Minimum SIL level: NO SIL REQUIREMENT BY INEOS TECHNOLOGIES

I-6801-S: LIQUID CARRY OVER TO C8 COMPRESSOR


Hazard: Recycle compressor damage
Causes:
LZT-60802 (HH) C8 Recycle compressor Suction KO drum PID:0614
Actions:
Stop K685 C8 Recycle gas compressor PID:0615
Notes:  To be finalised with compressor vendor
Minimum SIL level: To be assessed by DE

I-6802-S: C8 GAS COMPRESSOR SUCTION KO DRUM HIGH LEVEL


Hazard: Liquid overflow from KO drum to degasser. Powder degassing issue and explosion in
degasser downstream equipment
Causes:
LZT-60802 (HH) Recycle compressor Suction KO drum PID:0614
Actions:
Close XZV-60802 Liquid feed header to KO drum PID:0614
AND
Close XZV-60803 Pentane feed to compressor suction KO PID:0614
drum
Notes:
Minimum SIL level: 1

I-6805-S: POOR DEGASSING IN C8 DEGASSER: HIGH HIGH PRESSURE


Hazard: Poor degassing - Downstream equipment explosion.
Causes:
PZT-60819 (HH) C8 Degasser PID:0613
Actions:
Stop X-661 Powder conveying C8 feed rotary valve PID:0613
Notes:
Minimum SIL level: 1

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 89 / 110

PROCESS INTERLOCK DESCRIPTION

I-6807-O: OVERFILLING OF C8 DEGASSER OR C8 CONVEYING FILTER OR CONVEYING


LINE BLOCKAGE
Hazard: Line/filter blockage
Causes:
[LSHH-60811 (HH) C8 degasser PID:0613
OR
LSHH-60891 (HH) C8 Conveying filter PID:0613
OR
X-639 detected stopped C8 Conveying filter outlet rotary valve PID:0613
OR PID:0613
SAL-60891 (L) C8 Conveying filter outlet rotary valve PID:0607
OR
K-660A detected stopped] Gas conveying blowers
AND
XZDX-60639A routed to C8 Powder routed from C4/C6 degasser to PID:0605
degasser C8 degasser
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6817-S: AIR INGRESS TO C8 RECYCLE COMPRESSOR


Hazard: Recycle compressor damage or Downstream equipment explosion due to air ingress at
compressor suction
Causes:
PZT-60803 (LL) (note 1) C8 Recycle Compressor suction PID:0614
Actions:
Stop K-685 C8 Recycle gas compressor PID:0615
Notes:  To be finalised with compressor vendor
 Note 1: Location of PZT-60803 should be between any isolation valve
and compressor inlet
Minimum SIL level: 1

I-6830-S: POOR DEGASSING IN C8 DEGASSER: HIGH STRIPPING GAS FLOW


Hazard: Downstream equipment explosion due to fluidization of powder.
Causes:
[FZT-60814 (HH) (Note 1, 2) C8 VRU Stripping gas to C8 degasser PID:0613

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 90 / 110

PROCESS INTERLOCK DESCRIPTION

OR

FZT-60815 (HH) (Note 1, 2)] C8 VRU Stripping gas to C8 degasser PID:0613


Actions:
Stop X-661 Powder conveying feed rotary valve PID:0613
Notes:  Note 1: the trip setting is grade dependent. Refer to section on Degassing
Variable Trip Settings for how trip settings are determined.
 Note 2: The interlock is only applicable when degasser contains
undegassed C8 powder. The variable trips are disabled when running in
C4/C6 powder. Disabling of the trips is performed in the variable trip logic.
Refer to section on Degassing Variable Trip Settings.
Minimum SIL level: 1

I-6831-O: C8 DEGASSER OUTLET ROTARY VALVE DAMAGE


Hazard: Degasser outlet damage leading to production loss.

Causes:
[ (X-661 Stopped OR SSL-60861 C8 Powder conveying feed rotary valve PID:0613
(L))
AND XDX-60801 Set to X-661] C8 Degasser Recycle diverter valve PID:0613
OR
[ (X-662 Stopped OR SSL-60871 C8 Degasser Recycle rotary valve PID:0613
(L))
AND XDX-60801 Set to Recycle] C8 Degasser Recycle diverter valve PID:0613
Actions:
Stop X-638 C8 Degasser outlet rotary valve PID:0613
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6833-O: C8 DEGASSER RECYCLING LINE BLOCKAGE


Hazard: Recycling Conveying Line blockage
Causes:
PT-60881 (HH) N2 to C8 Degasser Recycling line PID:0613
OR
FT-60881 (LL) N2 to C8 Degasser Recycling line PID:0613
Actions:
Stop X-662 C8 Degasser Recycle rotary valve PID:0613

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 91 / 110

PROCESS INTERLOCK DESCRIPTION

Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6834-O: POWDER BUILD-UP IN C8 DEGASSER RECYCLE ROTARY VALVE


Hazard: Powder build-up prevention leading to rotary valve damage
Causes:
XDX-60801 In recycle position C8 Degasser Recycle diverter valve PID:0613
Actions:
Set the speed to minimum X-638 C8 Degasser outlet rotary valve PID:0613
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6838-S: STOP C8 DEGASSER FILLING WHEN IN EMPTY MODE


Hazard: Low residence time: downstream equipment explosion.
Causes:
HZS-60801 In Empty mode NORMAL / EMPTY C8 degasser PID:0613
AND
C8 operation (Note 1)
Actions:
Stop X-660 PID:0605
Notes:  Note 1: The interlock is active only in C8 operation. C8 operation is
determined with the value of the degassing trips for high and low
degassing flow in C8 operation.
C8 operation when (TH not equal to High flow and TL not equal to low
flow range).
Refer to section on Degassing Variable Trip Settings for how trip settings
are determined.
Minimum SIL level: 1

I-6839-S: STOP POWDER FEEDING FROM C8 DEGASSER WHEN POOR DEGASSING IN


C8 DEGASSER: LOW RESIDENCE TIME
Hazard: Downstream equipment explosion.
Causes:
[C8 operation (Note 1)
AND
(LZSLL-60814 (LL) C8 Degasser PID:0613

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

OR
LZSLL-60815 (LL)]
AND
HZS-60801 In Normal mode NORMAL / EMPTY C8 Degasser PID:0613
Actions:
Stop X-661 Powder conveying feed rotary valve PID:0613

 Note 1: The interlock is active only in C8 operation. C8 operation is


determined with the value of the degassing trips for high and low
degassing flow in C8 operation.
C8 operation when (TH not equal to High flow and TL not equal to low
flow range).
Refer to section on Degassing Variable Trip Settings for how trip settings
are determined.
Minimum SIL level: 1

I-6840-S: POOR DEGASSING IN C8 DEGASSER: LOW STRIPPING GAS FLOW


Hazard: Downstream equipment explosion due to poor degassing. To limit the reabsorption of C8 on
powder, N2 flow is injected into the degassing line.
Causes:
FZT-60814 (LL) (Note 1, 2) C8 VRU Stripping gas to C8 degasser PID:0613
OR
FZT-60815 (LL) (Note 1, 2) C8 VRU Stripping gas to C8 degasser PID:0613
Actions:
Stop X-661 Powder conveying feed rotary valve PID:0613
AND
Stop X-641 Conveying filter outlet rotary valve PID:0606
Causes:
FZT-60814 (LL) for more than T1- C8 VRU Stripping gas to C8 degasser PID:0613
6840 (Note 1, 2)
OR
FZT-60815 (LL) for more than T1- C8 VRU Stripping gas to C8 degasser PID:0613
6840 (Note 1, 2)
Actions:
Open PZV-60801A (SIS) N2 make-up to C8 degasser PID:0616
AND
Open XZV-60863 after T2-6840 N2 make-up to C8 degasser PID:0616

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
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PROCESS INTERLOCK DESCRIPTION

Notes:  T1-6840: timer = 15 min to allows N2 to be established and to allow time


to react on VRU.
 T2-6840: timer = 1 min to limit pressure drop in N2 header.
 Note 1: the trip setting is grade dependent. Refer to section on Degassing
Variable Trip Settings for how trip settings are determined.
 Note 2: The interlock is only applicable when degasser contains
undegassed C8 powder. The variable trips are disabled when running in
C4/C6 powder. Disabling of the trips is performed in the variable trip logic.
Refer to section on Degassing Variable Trip Settings.

Minimum SIL level: 2

I-6841-S: HIGH HC CONTENT IN STRIPPING GAS TO C8 DEGASSER


Hazard: Downstream equipment explosion due stripping gas with too high HC content leading to
poor degassing.
Causes:
TZT-60872A/B/C (HH) (2oo3) Stripping gas from C8 VRU main PID:0617
separator
Actions:
Close FZV-60865 (SIS) Gas flow from C8 VRU PID:0616
AND
Close XZV-60862 Stripping gas to C8 Degasser PID:0616

Causes:
LZT-60871A/B/C (HH) (2oo3) C8 VRU main separator PID:0617

Actions:
Close FZV-60865 (SIS) Gas flow from C8 VRU PID:0616

AND

Close XZV-60862 Stripping gas to C8 degasser PID:0616

AND

Stop K-685 C8 Recycle gas compressor PID:0615

Notes:
Minimum SIL level: 2

I-6842-S: HIGH DIFFERENTIAL TEMPERATURE BETWEEN REACTOR AND C8


DEGASSER
Hazard: Poor degassing due to excess concentration of C8 leading to downstream equipment

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

explosion.
Causes:
[TZDI-60811A (HH) (Note 1) Temperature difference between reactor PID:0613
and C8 degasser
OR
TZDI-60811B (HH) (Note 1)] Temperature difference between reactor PID:0613
and C8 degasser
AND
C8 operation (Note 2)
Actions:
Close XZV-60003/60053 Upflow lock hoppers top isolation valves PID:0601
AND
Close XZV-60303/60313/60323 Downflow lock hoppers top isolation PID:0602
valves /0603
AND
Stop X-661 if HZS-60801 In Normal Powder conveying feed rotary valve PID:0613
mode
AND
Stop X-660 Powder conveying feed rotary valve PID:0605
Notes:  Note 1:TZDI-60811y = Mo3 of (TZT-40044A/B/C) – TZT-60811y
 Note 2: The interlock is active only in C8 operation. C8 operation is
determined with the value of the degassing trips for high and low
degassing flow in C8 operation.
C8 operation when (TH not equal to High flow and TL not equal to low
flow range).
Refer to section on Degassing Variable Trip Settings for how trip settings
are determined.
Minimum SIL level: 2

I-6850-S: ENSURE ROUTING TO C8 DEGASSER WHEN IN C8 OPERATION


Hazard: Incorrect C8 powder routing leading to poor degassing powder.
Causes:
XZDX-60639A not routed to V-638 PID:0605
AND
C8 operation (Note 1)
Actions:
Stop X-660 Powder conveying feed rotary valve PID:0605
Notes:  Note 1: The interlock is active only in C8 operation. C8 operation is
determined with the value of the degassing trips for high and low
degassing flow in C8 operation.
C8 operation when (TH not equal to High flow and TL not equal to low

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 95 / 110

PROCESS INTERLOCK DESCRIPTION

flow range).
Refer to section on Degassing Variable Trip Settings for how trip settings
are determined.
Minimum SIL level: 1

I-6852-S: STOP POWDER FEEDING FROM C8 DEGASSER WHEN POOR DEGASSING IN


DEGASSER: START C8 WITH EMPTIED C8 DEGASSER
Hazard: Start-up with C8 when C8 degasser is emptied. Downstream equipment explosion if powder
is not recycled and degassed.
Causes:
LZSLL-60817 (LL) C8 Degasser pipe outlet PID:0613

OR
LZSLL-60818 (LL) C8 Degasser pipe outlet PID:0613
Actions:
Close XZV-20570 Octene-1 from OSBL PID:0205
Interlock Reset:
Causes:
LZSLL-60814 (NOT LL) C8 Degasser PID:0613

AND

LZSLL-60815 (NOT LL) C8 Degasser PID:0613

Actions:
Permissive to open XZV-20570 Octene-1 from OSBL PID:0205

Minimum SIL level: 2

I-6854-O: LOW TEMPERATURE IN PIPE WORK FROM C8 VRU MAIN SEPARATOR


Hazard: Cold temperature leading to pipe failure.
Causes:
TT-60802 (LL) Condensate to C8 recycle compressor PID:0614
KO drum
OR
TT-60873 (LL) Condensate to main loop separator and PID:0617
HCD
Actions:
FMC LIC-60871 Condensate to C8 recycle compressor PID:0617

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 96 / 110

PROCESS INTERLOCK DESCRIPTION

KO drum, main loop separator and HCD


Notes:
Minimum SIL level: 0

I-6856-O: C8 VRU RECYCLE PUMPS


Hazard: Prevent pump running dry
Causes:
LIC-60871 (LL) C8 VRU main separator PID:0617
Actions:
Stop P-684A/B C8 VRU condensate Recycle Pumps PID:0617
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-6871-O: C8 VRU WASHING PUMPS PROTECTION


Hazard: Damage to pump. Prevents running dry
Causes:
LZT-60802 (LL) C8 VRU Recycle compressor suction KO PID:0614
drum
Actions:
Stop P-681A C8 VRU washing pump PID:0614
AND
Stop P-681B C8 VRU washing pump PID:0614
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 97 / 110

PROCESS INTERLOCK DESCRIPTION

2.6 SECTION 700

I-7101-S: LIQUID RECOVERY ROUTING TO LRU OR TO DC


Hazard: Ensure open path of liquid recovery to LRU or DC
Causes:
XZV-70111 Not open Liquid HC to LRU PID:0701
Actions:
Open XZV-70112 Liquid HC to DC PID:0701
Notes:  When interlock is activated, alarm message should specify:‖ Liquid purge
routed to HCC. TEAL not allowed in liquid to HCC‖.
Minimum SIL level: 1

I-7104-O: RECOVERED LIQUID FROM LRU ROUTING TO HCD STORAGE DRUM OR TO


PROCESS
Hazard: Ensure open path of recovered liquid to HCD storage drum or to process
Causes:
XZV-70401 Not open Recovered Liquid HC to process PID:0702
Actions:
Open XZV-70211 Recovered Liquid HC to HCD storage PID:0702
drum
Notes:  Autoreset interlock. Interlock I-7105-S takes precedence on this interlock.
Minimum SIL level: No SIL requirement by INEOS Technologies

I-7105-S: LRU UNIT ISOLATION


Hazard: Isolation to reduce consequence in case of fire or loss of containment.
Causes:
HZS-70111A Emergency LRU isolation from console PID:0701
control room
OR
HZS-70111B Emergency LRU isolation from local area PID:0701
Actions:
Stop P-711 LRU column feed pump PID:0701
AND

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 98 / 110

PROCESS INTERLOCK DESCRIPTION

Close XZV-70113 HCD storage drum bottom isolation valve PID:0701


AND
Close XZV-70111 Liquid HC to LRU PID:0701
AND
Close XZV-70401 Recovered Liquid HC to process PID:0702
AND
Close XZV-70211 Recovered Liquid HC to HCD storage PID:0702
drum
AND
Close XZV-70411 Clean HC to OSBL PID:0702
AND
Close FZV-70501 (SIS) Clean HC to Clean HC drain drum PID:0701
AND
Close FZV-70402 (SIS) Concentrated HCD from LRU column PID:0702
AND
Close FZV-70211 (SIS) TEAL rich HCD to LRU recycle drain PID:0702
drum
AND
Stop P-714 Clean HC export pump PID:0702
AND
Stop K-711 LRU recycle fan PID:0701
AND
Stop P-713 LRU recycle pump PID:0702
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-7106-O: LRU COLUMN FEED PUMP PROTECTION


Hazard: Pump damage
Causes:
LT-70112 (LL) HCD storage drum PID:0701
OR
XZV-70113 not open HCD storage drum bottom isolation valve PID:0701
Actions:
Stop P-711 LRU column feed pump PID:0701
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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350 kta LLDPE PLANT 61070F 3200 SP - 013 1 99 / 110

PROCESS INTERLOCK DESCRIPTION

I-7107-O: LRU COLUMN HIGH LEVEL


Hazard: Overfilling of column leading to HCD rich in TEAL carryover to flare KO drums and OSBL.
No safety issues into flare KO drums.
Causes:
LT-70102 (HH) LRU column PID:0701
Actions:
Stop P-711 LRU column feed pump PID:0701
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies
SIL to be assessed by DE for TEAL to OSBL

I-7108-O: LRU COLUMN LOW LEVEL OR HIGH TEMPERATURE


Hazard: Keep LRU column reboiler flooded. Risk of fouling. Risk of TEAL decomposition.
Causes:
LT-70102 (LL) LRU column PID:0701
OR
TT-70105 (HH) LRU column PID:0701
Actions:
Close XV-70104 SL to LRU column reboiler PID:0701
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-7109-S: AIR INGRESS IN LRU COLUMN


Hazard: Nitrogen introduced to column in case of vacuum. Avoid air ingress and fire/explosion when
in contact with TEAL and HC
Causes:
PZT-70102 (LL) LRU column PID:0701
Actions:
Open XZV-70107 Nitrogen to LRU column PID:0701
AND
Stop K-711 LRU recycle fan PID:0701
Notes:

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

Minimum SIL level: 1

I-7110-O: CLEAN HC DRAIN DRUM HIGH LEVEL


Hazard: Overfilling of HC drain drum leading to backflow to nitrogen.
Causes:
LT-70412 (HH) Clean HC drain drum PID:0702
Actions:
FMC FIC-70501 Clean HC to Clean HC drain drum PID:0701
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-7112-O: LRU RECYCLE DRAIN DRUM HIGH LEVEL


Hazard: Overfilling of LRU recycle drain drum leading to backflow to nitrogen.
Causes:
LT-70402 (HH) LRU recycle drain drum PID:0702
Actions:
FMC FIC-70402 Concentrated HCD to LRU recycle drain PID:0702
drum
AND
FMC FIC-70211 TEAL rich HCD to LRU recycle drain PID:0702
drum
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-7113-O: BACKFLOW FROM MAIN LOOP SEPARATOR TO LRU


Hazard: Backflow to LRU – Prevent PSV lifting
Causes:
P-713 detected stopped LRU recycle pump PID:0702
Actions:
Close XZV-70401 (Note 1) Recovered Liquid HC to process PID:0702
Notes:  Note 1:Start-up override requirement to be determined by DE (No need
of start-up override if pump can be started with discharge valve closed
and no risk of pump discharge PSV pop-up).

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
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PROCESS INTERLOCK DESCRIPTION

Minimum SIL level: No SIL requirement by INEOS Technologies

I-7115-O: LRU RECYCLE FAN


Hazard: Liquid to fan leading to mechanical damage.
Causes:
LSHH-70103 (HH) LRU blower fan suction boot PID:0701
Actions:
Stop K-711 LRU recycle fan PID:0701
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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PROCESS INTERLOCK DESCRIPTION

2.7 SECTION 800

I-8249-O: 1ST EXTRUDER FEED SCREW


Hazard: Powder conveyor and upstream line blockage. Loss of production.
Causes:
M-820 is detected stopped Extruder feed screw PID:0801
OR
SSL-80041 (L) Extruder feed screw PID:0801
Actions:
Stop W-835A (Note 2) Additive feeder (A) PID:0802
AND
Stop W-835B (Note 2) Additive feeder (B) PID:0802
AND
Stop W-835C (Note 2) Additive feeder (C) PID:0802
AND
Stop X-640 (Note 1) Purge column outlet rotary valve PID:0606
Notes:  Note 1: If powder routed to feed screw.
 Note 2: DE to ensure that feeders can be started for pellet purge at
extruder start-up.

Minimum SIL level: No SIL requirement by INEOS Technologies

I-8250-O: 2ND EXTRUDER FEED SCREW


Hazard: Blockage of powder conveyor and usptream line. Loss of production.
Causes:
M-821 is detected stopped Second feed screw PID:0801
OR
SSL-80101 (L) Second feed screw PID:0801
Actions:
Stop M-820 First feed screw PID:0801
AND

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the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
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Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 103 / 110

PROCESS INTERLOCK DESCRIPTION

Stop W-835D (Note 1) Additive feeder PID:0803


AND
Stop W-835E (Note 1) Additive feeder PID:0803
AND
Stop W-835F (Note 1) Additive feeder PID:0803
AND
Stop (pulse command) X-855 Rerun pellet rotary valve PID:0807
(Note1, 2)
Notes:  Note 1: Detailed engineering to ensure that feeders can be started for
pellet purge at extruder start-up.
 Note 2: and if pellets are routed to the extruder hopper.
 This interlock must be automatically reset at extruder start-up.

Minimum SIL level: No SIL requirement by INEOS Technologies

I-8251-O: EXTRUDER STOPPED


Hazard: Extruder upstream line blockage. Loss of production.
Causes:
M-840 is detected stopped Extruder main motor PID:0805
OR
LSHH-80003 (HH) Extruder feed hopper PID:0805
Actions:
Stop M-821 Second Extruder feed screw PID:0801
Notes:
Minimum SIL level: No SIL requirement by INEOS Technologies

I-8252-O: ADDITIVE ACCUMULATION WHEN POWDER FEED TO EXTRUDER IS


STOPPED
Hazard: Additives in extruder hopper or powder feed screw without polymer powder.
Causes:
X-640 is detected stopped for T1- Purge column outlet rotary valve PID:0606
8252
OR
SSL-60011 (L) for T1-8252 Purge column outlet rotary valve PID:0606
Actions:
Stop —W-835A/B/C (Note 1) Additive feeders PID:0802

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 104 / 110

PROCESS INTERLOCK DESCRIPTION

AND
Stop W-835D/E/F (Note 1) Additive feeders PID:0803
AND
Stop (pulse command) X-855 after Rerun pellet rotary valve PID:0807
T1-8252 (Note 1, 2)
Causes:
M-820 is detected stopped for more than First extruder feed screw PID:0801
T2-8252
OR
SSL-80041 for more than T2-8252 First extruder feed screw PID:0801
Actions:
Stop W-835D/E/F (Note 1) Additive feeders PID:0803
AND
Stop (pulse command) X855 after T2- Rerun pellet rotary valve PID:0807
8252 (Note 1, 2)
Notes:  Note 1: Detailed engineering to ensure that feeders can be started for
pellet purge at extruder start-up.
 Note 2 : and if pellets are routed to the extruder hopper
 T1-8252: Residence time for the powder conveyor (20 seconds)
 T2-8252: Residence time for the 2nd powder conveyor (Hold seconds)
 This interlock must be reset automatically at extruder start-up
Minimum SIL level: 0

I-8256-S: NITROGEN AND DUST EXPLOSURE FOR OPERATOR IN ADDITIVE FIBC


UNLOADING STATIONS
Hazard: Operator asphixation or dust in building.
Causes:
FZT-80501 (LL) Additives venting header PID:0802
Actions:
Close XZV-80518 Additive antiblock unloading station slide PID:0802
valve (A)
AND
Close XZV-80528 Additive catalyst unloading station slide PID:0802
valve (B)
AND
Close XZV-80538 Additive antioxidant unloading station PID:0802
slide valve (C)
AND
Close XZV-80548 Additive antioxidant unloading station PID:0803

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 105 / 110

PROCESS INTERLOCK DESCRIPTION

slide valve (D)


AND
Close XZV-80558 Additive others unloading station slide PID:0803
valve (E)
AND
Close XZV-80568 Additive spare unloading station slide PID:0803
valve (F)
AND
Close XZV-80519 Additive 25kg sack unloading station slide PID:0802
valve (A)
AND
Close XZV-80529 Additive 25kg sack unloading station slide PID:0802
valve (B)
AND
Close XZV-80539 Additive 25kg sack unloading station slide PID:0802
valve (C)
AND
Close XZV-80549 Additive 25kg sack unloading station slide PID:0803
valve (D)
AND
Close XZV-80559 Additive 25kg sack unloading station slide PID:0803
valve (E)
AND
Close XZV-80569 Additive 25kg sack unloading station slide PID:0803
valve (F)
AND
Lock closed Additives and 25 kg X-835A/B/C/D/E/F additive and 25 kg PID:0802
sack unloading stations access sack unloading stations /0803
doors (note1)
[ZZS-80513 / 80514 / 80523 /80524
/ 80533 / 80534 / 80543 / 80544 /
80553 / 80554 / 80563 / 80564
cannot be released]
Notes:  Note 1: Access doors must also be lock closed if relevant slide valve
XZV-80518 / 80519 / 80528 / 80529 / 80538 / 80539 / 80548 / 80549 /
80558 / 80559 / 80568 / 80569 is not closed.
Minimum SIL level: 1

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 106 / 110

PROCESS INTERLOCK DESCRIPTION

I-8260-O: POLYMER VIBRATING SCREEN WASTE SKIP SYSTEM


Hazard: Nitrogen to waste skip area leading to operator asphyxiation.
Causes:
XV-80016 not closed Waste skip feeding PID:0801
Actions:
Close XV-80017 Waste skip take-off PID:0801
Notes:  Autoreset
Minimum SIL level: 0

I-8417-O: PELLET CONVEYING HOPPER OVERFILLING


Hazard: Stop extruder on pellet conveying hopper overfilling
Causes:
LSHH-80001 (HH) Pellet conveying feed hopper PID:0807
OR
X-850 is detected stopped for T1- Pellet conveying hopper rotary valve PID:0807
8417
Actions:
Stop Extruder M-840 Extruder PID:0805
Notes:  T1-8417: Timer = 7 minutes (typical value). Estimated time to fill hopper
when rotary valve is stopped.
Minimum SIL level: No SIL requirement by INEOS Technologies

I-8418-O: EXTRUDER SHUTDOWN DUE TO PELLETISER PROBLEM


Hazard: Equipment blockage downstream of Extruder. Loss of production.
Causes:
FT-80801 (LL) Water to pelletising system PID:0806
OR
PT-80801 (LL) Water to pelletising system PID:0806
OR
XZV-80802 not open (pulse) (Note Water to pelletising system PID:0806
1)
OR
PI-80005 (HH) Pelletiser pressure PID:0805
Actions:
Stop Extruder M-840 Extruder PID:0805

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 107 / 110

PROCESS INTERLOCK DESCRIPTION

Notes:  Note 1: Detect valve is moving from open to close position. It must be
possible to start extruder with valve XZV-80802 closed
 Interlock to be developed by detailed engineering and extruder vendor.
Minimum SIL level: No SIL requirement by INEOS Technologies

I-8419-O: EXTRUDER SHUTDOWN DUE TO PELLET DRYER/DEWATERING STOPPAGE


Hazard: Equipment blockage downstream of Extruder. Loss of production.
Causes:
D-847 is detected stopped Pellet dryer/dewatering PID:0806
OR
SSL-80701 (L) Pellet dryer/dewaterering low speed or PID:0806
stopped
Actions:
Stop M-840 Extruder PID:0805
Notes:  Interlock to be developed by detailed engineering and extruder vendor
Minimum SIL level: No SIL requirement by INEOS Technologies

I-8420-O: PELLET DRYER/DEWATERING


Hazard: Stoppage or overfill of the screener leads to overfill and damage to the overfill pellet
dryer/dewaterer
Causes:
LSHH-80701 (HH) Pellet screener outlet PID:0806
OR
[S-847 is detected stopped Pellet screener PID:0806
AND
XDX-706 routed to Pellet screener] Pellet screener bypass valve
Actions:
Stop D-847 Pellet dryer/dewaterer PID:0806
Notes:  Interlock to be developed by detailed engineering and extruder vendor
Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 108 / 110

PROCESS INTERLOCK DESCRIPTION

I-8470-S: PELLETIZER HOOD OPENING WHILE HOT WATER CIRCULATING


Hazard: Operator in contact with hot water leading to severe burns.
Causes:
ZZSL-80002 (NOT L) Chamber not closed PID:0805
OR
ZZSL-80003 (NOT L) Chamber not closed PID:0805
Actions:
Close XZV-80802 (Note 1) Water to pelletising system PID:0806
Notes:  This interlock must be automatically reset at extruder start-up: the water
will be required to start immediately by the extruder start-up sequence
 Note 1: Detailed engineering contractor may consider implementing a
trapped key interlock system that prevents extruder motor and pelletiser
motor starting and prevents XZV-80802 opening.
 SIL2 interlock relies on a single valve. XZV-80802 design guidance is
described in the instrument datasheet.
Minimum SIL level: 2

I-8471-S: PELLET DRYER/DEWATERING DOORS OPENING WHILE HOT WATER


DIRECTED TO PELLET DRYER
Hazard: Operator in contact with:
a) hot water or steam leading to severe burns.
b) rotating equipment pieces.
Causes:
LZAH-80005 (NOT H) Water in extruder pelletizer PID:0805
AND
LZAH-80006 (NOT H) Water in extruder pelletizer PID:0805
AND
P-848A is not running Pellet water pump PID:0806
AND
P-848B is not running Pellet water pump PID:0806
AND
D-847 is not running Pellet Dryer / Dewatering PID:0806
Actions:
Permissive to open pellet dryer and Pellet Dryer / Dewatering PID:0806
dewatering doors
Notes:  Detailed engineering contractor may consider implementing a trapped
key interlock system in order to achieve this interlock. The interlock

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 109 / 110

PROCESS INTERLOCK DESCRIPTION

should also prevent equipment starting until the doors are closed.
Minimum SIL level: 1

I-8801-O: PELLET CONVEYING LINE FROM FEED HOPPER BLOCKAGE


Hazard: Conveying line blockage. Rotary valve under purge column is also stopped to ensure the
extruder will shutdown cleanly
Causes:
LSHH-80021 (HH) (Note 1) Transfer hopper PID:0808
OR
LSHH-80031 (HH) (Note 1) Pellet blender A PID:0808
OR
LSHH-80041 (HH) (Note 1) Pellet blender B PID:0808
OR
LSHH-80501 (HH) (Note 1) Pellet purge silo PID:0807
OR
PT-80006 (HH) Conveying air to pellet conveying hopper PID:0807
OR
PT-80006 (LL) Conveying air to pellet conveying hopper PID:0807
Actions:
Stop X-850 Pellet rotary valve PID:0807
AND
Stop X-640 Purge column outlet rotary valve PID:0606
Notes:  Note 1: Interlock must take into account the destination of the pellet
conveying
 The failure routing is not included in the interlock to minimize spurious
trips. Nevertheless the route must be checked by the conveying
sequence before the transfer is started

Minimum SIL level: No SIL requirement by INEOS Technologies

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.
OWNER REFERENCE
Project Package Originator Discipline Doc. Type Unit n° Serial n°

Technologies RAPID L20 INE PRO DES 3200 0013


LICENSOR REFERENCE Rev. Page
PETRONAS RAPID PROJECT Project Unit n° Doc. Type Doc. Code Sequent. n°
350 kta LLDPE PLANT 61070F 3200 SP - 013 1 110 / 110

PROCESS INTERLOCK DESCRIPTION

2.8 LIST OF PROCESS DATA SHEETS INCLUDING INEOS TECHNOLOGIES CONTROL


SPECIFIC REQUIREMENTS

This paragraph lists all the process data sheets where specific INEOS Technologies control
requirement are described.

This list will help the DE to have an overall view to design properly the safety and control
systems.

PDS Item PDS Service

K-230 Ethylene recycle compressor

K-271A/B Hydrogen compressors

K-400 Main loop gas compressor

K-401 Ejector booster compressor

P-409A/B Liquid injection pumps

A-660 Powder conveying package

K-675 VRU Recycle gas compressor

A-675 Refrigeration package

K-685 C8 VRU Recycle gas compressor

A-684 C8 VRU Refrigeration package

A-820 Feeders package

A-825 Additives unloading package

A-840 Extruder package

A-847 Pellet dryer package

A-850 Pellet conveying package

© INEOS Commercial Services UK Limited. All rights reserved. This document is the property of INEOS Commercial Services UK Limited, and
the information and images it contains are strictly confidential and may not be altered or amended, copied, used or disclosed without the
express permission of INEOS Commercial Services UK Limited.

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