December 2011

Total No. of Questions : 12] [Total No. of Pages : 2

[4064] - 542
P1138
B.E. (Chemical)
ADVANCED SEPARATION PROCESSES
(Sem. - I) (409342(E)) (2008 Course) (Elective - II)
Time : 3 Hours] [Max. Marks :100

Y
Instructions to the candidates:
1) Answers to the two Sections should be written in separate answer books.

EM
2) Neat diagrams must be drawn wherever necessary.
3) Figures to the right indicate full marks.
4) Use of logarthmic tables, Slide rule, Mollier charts, electronic pocket

AD
calculator and steam tables is allowed.
5) Assume suitable data, if necessary.

Q1) a)
b)
AC
SECTION - I
What is an adsorption isotherm. Give the five types [6]
Explain temperature swing regeneration giving details of stripping and
heat limited process. [6]
c) What are various applications of chromatography in separation of
RE

enzymes and proteins. [6]

OR
UA

Q2) Give the types of chromatography and explain in detail Liquid chromatography
separation system. [18]

Q3) Explain the following term: [16]

Q

a) Fouling.
TS

b) Liquid emulsion membrane.

c) Dialysis.
d) Gas permeation.
SE

OR
Q4) a) Explain Osmotic Pressure. [4]
b) Explain in detail Membrane configurations. [8]
c) Give the classification of the main types of membrane separation process.
[4]

P.T.O.
 Q5) What are the advantages of reactive distillation and where is it suitable to
explore for separation purpose. Explain with suitable example. [16]

OR
Q6) a) Explain in detail Separation based on reversible chemical complexation.
[10]
b) What is reactive crystallization. [6]

Y
SECTION - II

EM
Q7) a) Give the classification of flotation technique based on mechanism and
size of material. [9]
b) Explain collapse and drianage phenomena. [9]

AD
OR
Q8) a) Give applications of bubble and foam separation methods to protein
and enzyme separation and waste water treatment. [10]
b)

Q9) a)
AC
What is electrophoresis? Explain in detail.

State the classification of adductive crystallization.

[8]

[8]
b) What are the molecular sieves? State its applications. [8]

OR
RE

Q10)Write detail note on: [16]

a) Zone Refining.
b) Clathrates and Adducts.
UA

Q11)a) What is centrifugation. Give the classification of centrifuges by size of

dispersed particles. [8]
Q

b) Explain Ultracentrifuge in detail. [8]

OR
TS

Q12)a) Explain in detail the Ring over technology. [8]

b) Explain selection of separation process with detailed case study. [8]
SE

[4064]-542 2
 May 12

Total No. of Questions : 12]

SEAT No. :
P1646 [Total No. of Pages : 2
[4164]-614
B.E. (Chemical)
ADVANCED SEPARATION PROCESSES
(2008 Pattern) (Elective - II) (Sem. - I)

Y
Time :3 Hours] [Max. Marks :100

EM
Instructions to the candidates:
1) Answer to the two sections should be written in separate books.
2) Neat diagrams must be drawn wherever necessary.

AD
3) Figures to the right indicate full marks.
4) Use of logarithmic tables, slide rule, Mollier charts, electronic pocket
calculator and steam tables is allowed.
5) Assume suitable data, if necessary.

 
            SECTION - I
AC
Q1) Explain in detail Liquid chromatography separation system and
characterization of chromatography processes. [18]
RE

OR
Q2) a) What are various applications of chromatography in separation of
enzymes and proteins. [6]
UA

b) Discuss all aspects of pressure swing regeneration. [6]

c) What is adsorption selectivity. [6]
Q

Q3) a) Explain various types of membranes . [8]

b) State advantages of membrane separation processes over conventional
TS

processes. [8]
OR
Q4) a) Explain Osmotic pressure with appropriate equation. [4]
SE

b) Discuss all aspects of dialysis. [6]

c) Explain Pressure Swing Adsorption (PSA) technique used for separation
of gas mixtures. [6]

P.T.O.
 Q5) Write short notes on : [16]
a) Separations based on reversible chemical complexation.
b) Reactive distillation.
OR
Q6) a) Distinguish between pervaporation and gas permeation processes. [8]
b) Explain reactive crystallization in detail. [8]

Y
SECTION - II

EM
Q7) a) Give the classification of flotation technique based on mechanism and
size of material. [9]
b) Explain collapse and drianage phenomena. [9]

AD
OR
Q8) a) Explain modes of operation of foam fractionation equipment. [9]
b) State and explain the adsorption properties of foam. [9]

Q9) Write note on :

a) Counter current electrophoresis.
AC [16]

b) Adductive crystallization.
OR
RE

Q10) a) What is zone refining. [8]

b) What are molecular sieves and state its advantages. [8]
UA

Q11) Explain the following terms in detail. [16]

a) Recoil method.
b) Exchange Reaction.
Q

OR
TS

Q12) a) Explain selection of separation processes with one case study. [10]
b) Write note on Ultracentrifuge in detail. [6]
SE

ïïï

[4164]-614 2
 May 2013

UNIVERSITY OF PUNE

[4364]-662
B. E. (Chemical) Examination - 2013
ADVANCED SEPARATION

Y
PROCESSES
(2008 Pattern)

EM
[Time : 3 Hours] [Max. Marks : 100]
Total No. of Questions : 12 [Total No. of Printed Pages :2]

AD
Instructions :
(1) Answers three questions from Sections I and three questions
from Section II.
(2) Answers to the two sections should be written in separate

AC
answer-books
(3) Neat diagrams must be drawn wherever necessary.
(4) Use of logarithmic tables, slide rule, Mollier charts,
electronic pocket calculator and steam tables is allowed.

SECTION I
RE
Q1) a) Explain the basic concept of chromatography process. [6]
b) Give the application of chromatography in separation of enzymes and proteins. [6]
c) Explain adsorption mechanism in separation of fluid-solid system. [6]
OR
UA

Q2) a) Give the details of chromatography column design and fidling. [6]
b) Explain in detail ‘Adsorption Cycle’ with neat sketches. [12]

Q3) a) Give the advantages of membrane separation process over other separation [8]
Q

technique.
b) Explain four basic types of RO module currently manufactured. [8]
TS

OR
Q4) a) Calculate the osmotic pressure of a solution containing 0.10 gmol NaCl/1000 g [6]
H2O at 250C. Density of water = 997.0 kg/m3.
SE

b) Give the classification of the membrane process. [6]

c) Explain the following terms: [4]
i) Permeability
ii) Osmotic Pressure

Q5) a) Give the characteristics of the complexing agent used in [8]

1
 chemical-complexation.
b) Explain the reactive distillation process in detail. [8]
OR
Q6) a) Give the solution characteristics of chemical complexation process. [8]
b) Explain ‘Reactive crystallization’ process in detail. [8]

Y
SECTION II

EM
Q7) a) Give the flotation techniques classification on the basis of mechanism [9]
of separation and size of material separated.
b) Explain ‘Collapse and drainage phenomena’. [9]
OR

AD
Q8) a) Give the design and development of flotation equipment. [9]
b) Give the application of flotation technique. [9]

Q9) a) Explain the adsorption properties and applications of molecular sieve. [8]

AC
b) Explain Zone refining process in detail. [8]
OR
Q10) Write short notes on: [16]
a) Zone Electrophoresis
b) Adductive Crystallization.
Q11) Explain the classification of unit operations based on the property difference. [16]
RE

OR
Q12) Write short notes on: [16]
a) Exchange Reaction
UA

b) Ring oven technology application.

Q
TS
SE

2
 December 2014

Total No. of Questions : 12] SEAT No. :

P2128 [Total No. of Pages : 3

[4659] - 299
B.E. (Chemical) (Semester - I)
E : ADVANCED SEPARATION PROCESSES
(2008 Pattern) (Elective - II)

Y
EM
Time : 3 Hours] [Max. Marks : 100
Instructions to the candidates:
1) Answer three questions from Section - I and three questions from Section - II.

AD
2) Answers to the two sections should be written in separate books.
3) Neat diagrams must be drawn wherever necessary.
4) Figures to the right indicate full marks.

AC
5) Use of logarithmic tables slide rule, Mollier charts, electronic pocket
calculator and steam tables is allowed.
6) Assume suitable data, if necessary.
RE

SECTION - I

Q1) a) Explain the details of chromatography column design and fidling. [6]
UA

b) Explain in detail ‘Adsorption Cycle’ with neat sketches. [12]

OR
Q2) a) Explain the basic concept of chromatography process. [6]
Q

b) Give the application of chromatography in separation of enzymes and

TS

proteins. [6]
c) Explain adsorption mechanism in separation of fluid-solid system. [6]
SE

Q3) a) Give the advantages of membrane separation process over other separation
technique. [8]
b) Describe four basic types of Reverse Osmosis module currently
manufactured. [8]

P.T.O.
 OR
Q4) a) Calculate the osmotic pressure of a solution containing 0.10 gmol NaCl/
1000 g H2O at 250 C. Density of water = 997.0 kg/m3 [6]
b) Write down the classification of the membrane process. [6]
c) Explain the following terms : [4]
i) Rejection

Y
ii) Permeate

EM
Q5) Discuss the following in detail :
a) Characteristics of the complexing agent used in chemical -

AD
complexation. [8]
b) Reactive distillation process. [8]
OR
AC
Q6) a) Give the solution characteristics of chemical complexation process. [8]
b) Write short note on ‘Reactive crystallization’ process. [8]
RE

SECTION - II

Q7) a) Give the flotation techniques classification on the basis of mechanism of

UA

separation and size of material separated. [9]

b) Explain ‘Collapse and drainage phenomena’. [9]
OR
Q

Q8) Discuss the following :

TS

a) Design and development of flotation equipment. [9]

b) Application of flotation technique. [9]
SE

Q9) a) Explain the adsorption properties and applications of molecular sieve.[8]

b) Explain Zone refining process in detail. [8]

[4659] - 299 2
 OR
Q10) Write short notes on : [16]
a) Zone Electrophoresis
b) Adductive Crystallization

Q11) Explain the classification of unit operations based on the property

Y
difference. [16]

EM
OR
Q12) Write short notes on : [16]
a) Exchange Reaction

AD
b) Ring oven technology application

zzz AC
RE
Q UA
TS
SE

[4659] - 299 3
 May 2015

Total No. of Questions : 12] SEAT No. :

P2021 [Total No. of Pages : 2
[4759]-279
B.E. (Chemical)
ADVANCED SEPARATION PROCESSES
(2008 Course) (Semester-II) (Elective-II) (409342)

Y
Time : 3 Hours] [Max. Marks : 100
Instructions to the candidates:

EM
1) Answer three questions from Section-I and three questions from Section-II.
2) Answers to the two sections should be written in separate books.
3) Neat diagrams must be drawn wherever necessary.
4) Figures to the right indicate full marks.

AD
5) Use of logarithmic tables slide rule, Mollier charts, electronic pocket calculator
and steam tables is allowed.
6) Assume suitable data, if necessary.

Q1) a)
SECTION-I
AC
Explain the details the design of chromatography. [6]
b) Explain in detail ‘Adsorption Cycle’ with neat sketches. [12]
OR
RE

Q2) a) Explain the basic concept of HPLC process. [6]

b) Give the application of chromatography in separation of enzymes and
proteins. [6]
UA

c) Explain adsorption mechanism in separation of fluid-solid system. [6]

Q

Q3) a) Give the advantages of membrane separation process over other

separation technique. [8]
TS

b) Explain the basic types of modules used in Reverse Osmosis. [8]

OR
Q4) a) Calculate the osmotic pressure of a solution containing 0.10 gmol
SE

NaCl/1000g H2O at 250C. Density of water = 997.0 kg/m3. [6]

b) Write down the classification of the membrane process. [6]
c) Explain the following terms: [4]
i) Rejection.
ii) Permeate.
P.T.O.
 Q5) Discuss the following in detail
a) Characteristics of the complexing agent used in chemical-complexation.
[8]
b) Reactive distilation process. [8]
OR
Q6) a) Give the solution characteristics of chemical complexation process. [8]

Y
b) Write short note on ‘Reactive crystallization’ process. [8]

EM
SECTION-II

Q7) a) Give the flotation techniques classification on the basis of mechanism of

separation and size of material separated. [9]

AD
b) Explain ‘Collapse and drainage phenomena’. [9]
OR
Q8) Discuss the following:
a)
b) Application of flotation technique.
AC
Design and development of flotation equipment. [9]
[9]

Q9) a) Explain the adsorption properties and applications of molecular sieve.

RE

[8]
b) Explain Zone refining process in detail. [8]
OR
UA

Q10)Write short notes on: [16]

a) Zone Electrophoresis.
Q

b) Adductive Crystallization.
TS

Q11)Explain the classification of unit operations based on the property difference.

[16]
OR
SE

Q12)Write short notes on: [16]

a) Exchange Reaction.
b) Ring oven technology application.

•••••
[4759]-279 2
 December 2015

Total No. of Questions : 12] SEAT No. :

P3207 [Total No. of Pages : 3

[4859] - 274
B.E. (Semester - II)
CHEMICAL ENGINEERING
Advanced Separation Processes

Y
(2008 Pattern)

EM
Time : 3 Hours] [Max. Marks : 100
Instructions to the candidates:
1) Answers three questions from sections I and three questions from section II.

AD
2) Answer to the two sections be written in separate books.
3) Neat diagrams must be drawn wherever necessary.
4) Figures to the right indicate full marks.
5) Use of logarithmic tables slide rule, Mollier charts, electronic pocket

6) Assume suitable data, if necessary.

AC
calculator and steam tables is allowed.

SECTION - I
Q1) a) What is cross flow filtration? What are its advantages over dead end
RE

filtration? [6]
b) Explain in detail ‘Adsorption Cycle’ with neat sketches. [10]
OR
UA

Q2) a) Explain the details the design of chromatography. [6]

b) Explain the basic concept of HPLC process. [10]
Q

Q3) a) Give the application of chromatography in separation of enzymes and

proteins. [8]
TS

b) Explain adsorption mechanism in separation of fluid-solid system. [8]

OR
SE

Q4) a) Give the advantages of membrane separation process over other separation
technique. [8]
b) Explain the basic types of modules used in Reverse Osmosis. [8]

P.T.O.
 Q5) a) Calculate the osmotic pressure of a solution containing 0.10 gmol
(NaCl/1000g) H2O at 250C. Density of water = 997.0 kg/m3 [6]
b) Write down the classification of the membrane process. [8]
c) Explain the following terms: [4]
i) Rejection
ii) Permeate

Y
OR

EM
Q6) Discuss the following in detail.
a) Characteristics of the complexing agent used in chemical-complexation.
[9]

AD
b) Reactive distillation process [9]

Q7) a)
SECTION - II
AC
Write down the flotation techniques classification on the basis of
mechanism of separation and size of material separated. [9]
b) Explain ‘Collapse and drainage phenomena’. [9]
OR
RE

Q8) Write short notes on

a) Design and development of flotation equipment. [9]
UA

b) Application of flotation technique. [9]

Q9) a) Explain the adsorption properties and applications of molecular sieve.[8]

Q

b) Adductive Crystallization. [8]

TS

OR
Q10)Write short notes on :
SE

a) Zone Electrophoresis [8]

b) Differentiate between electrophoresis and dielectrophoresis and discuss
advantages of dielectrophoresis over electrophoresis techniques? [8]

[4859] - 274 2
 Q11)Explain the classification of unit operations based on the property difference.
[16]

OR

Q12)Write short notes on : [16]

a) Exchange Reaction

Y
b) Describe mechanism and applications of supercritical fluid extraction in
chemical & biochemical industry?

EM
AD
AC
RE
Q UA
TS
SE

[4859] - 274 3
 May 2016

Total No. of Questions : 12] SEAT No. :

P3965 [4959]-274
[Total No. of Pages : 3

B.E. (Chemical)
e-ADVANCED SEPARATION PROCESSES
(2008 Course) (Semester - I) (409342) (Elective - II)

Y
Time :3 Hours] [Max. Marks : 100

EM
Instructions to candidates:
1) Answers three questions from Section I and three questions from Section II.
2) Answers to the two sections should be written in separate books.
3) Neat diagrams must be drawn wherever necessary.

AD
4) Figures to the right indicate full marks.
5) Use of logarithmic tables slide rule, Mollier charts, electronic pocket calculator
and steam tables is allowed.
6) Assume suitable data, it necessary.
AC
SECTION - I
Q1) a) What is cross flow filtration? What are its advantages over dead end
filtration? [6]
RE

b) What is the principle and working of Ultrafiltration? Discuss its

application. [10]
OR
UA

Q2) a) Explain the detail working of chromatography. [6]

b) Explain the basic concept of HPLC process. [10]
Q
TS

Q3) a) Give the application of chromatography in separation of enzymes and

proteins. [8]
b) Explain adsorption mechanism in separation of fluid-solid system. [8]
SE

OR

Q4) a) Discuss the classification of membrane processes along with its

applications. [8]

b) Explain the basic types of modules used in Reverse Osmosis. [8]

P.T.O.
 Q5) a) Calculate the osmotic pressure of a solution containing0.10 gmol NaCl/
1000 g H2O at 250ºC. Density of water = 997.0 kg/m3 [6]

b) Write down the classification of the membrane module. [8]

c) Explain the following terms: [4]

i) Rejection

Y
ii) Permeate

EM
OR

Q6) Discuss the following in detail.

AD
a) Characteristics of the complexing agent used in chemical-complexation.[9]

b) Reactive distillation process. [9]

AC
SECTION - II

Q7) a) Write down the flotation techniques classification on the basis of

RE

mechanism of separation and size of material separated. [9]

b) Explain ‘Collapse and drainage phenomena’. [9]

UA

OR

Q8) Write short notes on

Q

a) Design and development of flotation equipment. [9]

TS

b) Application of flotation technique. [9]

SE

Q9) a) Explain the adsorption properties and applications of molecular sieve.[8]

b) Adductive Crystallization. [8]

OR

[4959]-274 2
 Q10)Write short notes on:

a) Zone Electrophoresis. [8]

b) Differentiate between electrophoresis and dielectrophoresis and discuss

advantages of dielectrophoresis over electrophoresis techniques? [8]

Y
Q11)Explain the classification of unit operations based on the property difference.
[16]

EM
OR
Q12)Write short notes on: [16]

AD
a) Exchange Reaction.
b) Describe mechanism and applications of supercritical fluid extraction in
chemical & biochemical industry?

O O
AC O
RE
Q UA
TS
SE

[4959]-274 3
 December 2016

Total No. of Questions :12]

SEAT No. :
P2132 [Total No. of Pages : 2
[5059]-272
B.E. (Chemical)
ADVANCED SEPARATION PROCESSES
(2008 Course) (409342) (Semester-II)

Time : 3 Hours] [Max. Marks :100

Instructions to the candidates:
1) Answers three questions from sections I and three questions from Section II.
2) Answer to the two sections should be written in separate books.
3) Neat diagrams must be drawn wherever necessary.
4) Figures to the right indicate full marks.
5) Use of logarithmic tables slide rule, Mollier charts, electronic pocket calculator
and steam tables is allowed.
6) Assume suitable data if necessary.

SECTION-I

Q1) a) What is the process of surface based solid-liquid separations involving a

second liquid? [8]
b) What is reverse osmosis? Explain the process and derive the equations
of flux for once through continuous operation mode? [8]
OR
Q2) a) Explain the details the design of chromatography. [8]
b) Explain the basic concept of HPLC process. [8]

Q3) a) Give the application of chromatography in separation of enzymes and

proteins. [8]
b) Explain adsorption mechanism in separation of fluid-solid system. [8]
OR
Q4) a) Give the advantages of membrane separation process over other
separation technique. [8]
b) Explain the basic types of modules used in Reverse Osmosis. [8]
P.T.O.
Q5) Describe mechanism and applications of supercritical fluid extraction in
chemical & biochemical industry? [18]
OR
Q6) Differentiate between electrophoresis and dielectrophoresis and discuss
advantages of dielectrophoresis over electrophoresis techniques? [18]

SECTION-II

Q7) a) Write down the flotation techniques classification on the basis of

mechanism of separation and size of material separated. [9]
b) Write down the Applications of flotation technique. [9]
OR
Q8) a) Explain ‘Collapse and drainage phenomena’. [9]
b) Write short note on Design and development of flotation equipment.[9]

Q9) Write short notes on.

a) Temperature Swing Adsorption (TSA) [8]
b) Pressure Swing Adsorption (PSA) [8]
OR
Q10)Write down the applications of chromatography in separation of enzymes
and proteins, industrial examples in detail. [16]

Q11) Write short notes on. [16]

a) Adductive Crystallization.
b) Zone Electrophoresis
OR
Q12)a) Explain the adsorption properties and applications of molecular sieve.[8]
b) Explain Continuous Adsorption process. [8]

T T T

[5059]-272 2