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Cat. No.

M000-04
Rev. 02 – 4/98

R.O. DESALINATION UNIT


TECHNICAL MANUAL

IW Model
1996

Culligan reserves the right to change any technical or design specifications


CULLIGAN ITALIANA S.p.A. - Via Gandolfi, 6 - 40057 Cadriano di Granarolo E. BO (ITALY) - Phone +39/51/6017111 –
Telefax +39/51/765602

Quality System Certified according to UNI EN ISO 9001 Norm


This manual is intended for the Staff specifically appointed to
install and/or operate and/or repair the Culligan systems. Work by
unauthorised staff, or not in accordance with the instructions in the
manual, will relieve Culligan of all liability for the possible
consequences.

SAFETY WARNINGS

• All handling, maintenance and repair of systems must be carried out by suitably trained
staff.

• The room which is to house the systems, the accessory material and the consumable
products must comply with the safety, use and storage requirements envisaged by the
regulations in force.

• The water produced by each device must be used for the specific purpose for which it was
intended. Culligan is not liable for the consequences of improper use of the water produced
by its equipment.

• All system malfunctions must be reported to the Culligan Service Centre immediately.
Culligan is not liable for the consequences of protracted use of a system on which
malfunctions have occurred.

• Where necessary, chemicals must be selected, dosed and handled by professional qualified
staff, in accordance with the Culligan instructions and the Safety Technical Information.

• The system must be disconnected from the electricity and water supplies during all
maintenance or repair operations.

• Waste or consumable materials from water treatment systems must be disposed of in


accordance with the regulations in force.
GENERAL - The nominal temperature is
used for the calculation of
IW series industrial R.O. desalination units expected plant performance.
are designed and constructed to offer reliable
- The SDI value required may
operation, high efficiency, user-friendliness
be achieved by means of
and simple maintenance.
adequate pre-treatment.

The materials used for construction, - Chlorine is normally added


particularly those in contact with water, are to raw water for disinfection.
food grade and have high resistance to The excess should be
corrosion (AISI 316 stainless steel, uPVC and eliminated by means of
polyethylene). The water for treatment must activated carbon or injection
have the following main characteristics (for of suitable chemicals.
the other parameters not considered here, it - Calcium sulphate, Calcium
is supposed that the water meets drinking carbonate and Silica: the
water standards). limits indicated refer to the
Feed pressure : 0.3 bar min. prevention of scale-forming
precipitations.
Product pressure : 1.5 bar max.
Normally, on the basis of the chemical
Temperature : 2-35°C (design
analysis of water, the limits are borne in mind
temperature is
during the design phase and the necessary
20°C)
corrective pre-treatment (acidification,
Salinity : 5000 mg/l (as sequestrant injection or conditioning with
TDS) max. products such as polyphosphates, softening
on resins, etc.) is suggested.
S.D.I. : <3

pH : 4 - 11
Free chlorine : absent
DESCRIPTION
Calcium sulphate (CaSO4) : concentration in
the reject water The Aqua-Cleer IW consists basically of:
below the
solubility limit
- A skid.
Calcium carbonate
- One or more pressure vessels and
(CaCO3) : negative
relevant R.O. membranes.
Langelier index in
the reject water - Multistage centrifugal pump(s) (AP01).
Silica : concentration in - Automatic valve on raw water inlet
the reject water (SV01).
below the
- Control valves for recycle and reject
solubility limit
(RV02 and RV03, if applicable).
WARNING - Temperature out of the
permitted range could cause - Feed pressure control valve (RV01).
irreversible damage to the - Control panel with:
membranes (because of
frost or deterioration of the - pressure switch for low inlet pressure
osmotic film). (PS01)
- pressure switch for high product
pressure (PS02)

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 1


- pressure switch for high pressure pump - Flushing system with:
(PS03)
- horizontal cylindrical container
- pressure gauges
- minimum level switch (LSL01)
- product flow meter (Fl02)
- vacuum breaker
- reject water flow meter (Fl03)
- non-return product valve.
- recycle flow meter (Fl01), if applicable.

Logic of Operation
The R.O. unit is operated on level installed in
- pressure switch for low inlet pressure
the treated water accumulation tank.
PSL01
The starting procedure is as follows:
- pressure switch for high discharge
- Solenoid valve SV01 is energized, pressure pump PSH02 (detects
opening the automatic valve AV01 malfunctions)
installed at the R.O. unit inlet and allowing
- pressure switch for high pressure product
the feed water to pressurize the system.
PSH03 (to protect the R.O. membranes).
The low pressure switch PS01 controls the
pressure, and does not allow automatic Whenever the values set on the pressure
start-up of the high pressure pump AP01 switches are exceeded, the system cuts out
unless it exceeds the preset value. This and the associated alarm is signaled.
prevents damage to the pump caused by The operating pressures and flow rates are
lack of water and/or insufficient pressure. displayed on the pressure gauges and flow
Once the pump AP01 has started, the meters supplied with the unit, which are
water is pressurized and sent to the R.O. regulated with the aid of the manual valves
membranes. installed on the HP pump discharge line
A part of the feed water passes through (product RV01, recycle RV02, reject RV03).
the membranes and loses a large portion
of salts (PRODUCT), while the remainder, Once the maximum level has been reached in
with higher salt content, is rejected to the treated water tank, the unit automatically
drain (REJECT). carries out a flushing cycle.
In order to reduce the quantity of reject In the flushing phase, all the water inside the
water, some of it can be recycled by membranes is totally replaced with the
setting the regulator valve RV02 as osmotized water drawn from the flushing
appropriate, on the basis of the reading of tank.
the flow meter Fl01.
The flushing time set allows use of about 75%
The system is equipped with three safety
of the water available in the tank.
pressure switches:
At the end of the flushing phase, the unit is
switched off.

2 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98


IW R.O. DESALINATION UNITS

Description IW05 IW06 IW08 IW10 IW12 IW14 IW16 IW18 IW20 IW22 IW24 IW26 IW28 IW30 IW30A
Q.ty/ Q.ty/
Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/ Q.ty/
type typetype type type type type type type type type type type type type
Membrane BW 30-400 4 5 7 9 10 12 15 16 18 20 22 25 28 30 30

Cat. No. M000-04 - 9/97


1x4 2x3 2x5 2x5 2x6 3x4 3x4 3x5 3x6 3x6
Pressure Vessels 1x4 1x5 2x5 2x6 5x6
1x3 1x3 1x5 1x6 1x6 2x4 2x5 2x5 2x5 2x6
1x 1x 1x 1x 1x 2x 2x 2x 2x 2x 2x 2x 2x 2x 2x
Pumps SV1615 SV1615 SV1615 SV3012 SV3012 SV1615 SV1615 SV1615 SV1615 SV3012 SV3012 SV3012 SV3012 SV3012 SV3012
15 kW 15 kW 15 kW 22 kW 22 kW 2x15kW 2x15kW 2x15kW 2x15kW 2x22kW 2x22kW 2x22kW 2x22kW 2x22kW 2x22kW
Instruments:
Conductivity Meter 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
Termperature gauge 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
Pressure gauges (1) 4 4 5 5 4 4 5 5 5 5 5 5 5 4 5
(3)
Flow indicators (2) 3 3 3 3 3 3 3 3 3 3 3 3 3 3 2

IW
Pressure switches (4) 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3
HPP discharge valve 1x2” 1x2” 1x2” 1x2½” 1x2½” 1x2½” 1x2½” 1x2½” 1x2½” 1x3” 1x3” 1x3” 1x3” 1x3” 1x3”
uPVC uPVC uPVC uPVC uPVC uPVC uPVC uPVC uPVC uPVC uPVC uPVC uPVC uPVC uPVC
Pipework AISI AISI AISI AISI AISI AISI AISI AISI AISI AISI AISI AISI AISI AISI AISI
316 316 316 316 316 316 316 316 316 316 316 316 316 316 316
Control panel NOT INCLUDED
Flushing tank 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
(1)
- Single Stage: HP pump suction, HP pump discharge, reject, product.
- Double Stage: HP pump suction, HP pump discharge, reject 1st stage, reject 2nd stage, product.
(2)
- Product, reject, recycle.
(3)
- Unit without recycle.
(4)
- HP pump suction, HP pump discharge, product.

3
Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 3
4 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98
Note: Model IW 30A without recycle.

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 5


6 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98
Note: Model IW 30A without recycle.

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 7


Installation Instructions

MEMBRANE ELEMENT LOADING

Although it is very simple to load the spiral - Drain the pressure vessels as much as
wound membrane elements into the pressure possible.
vessels, it is very important that is should be - Losen pipe couplings from endcaps.
done with maximum care and attention. One
- Loosen all permeate - feedwater - and
damaged product tube or forgotten
concentrate piping/couplings from
interconnector may cause a lot of time
manifolds.
consuming labour in fault finding later on.
Therefore, the handling of element loading - Remove ends from pressure vessels and
has to be carefully conducted and supervised slide the O-Rings on the pressure vessel
free from the endcaps. Note condition of
intensively.
gasket: if cracked or damaged, replace
- Use of a membrane element loading tool
with new gasket.
is strongly advised for 8" membrane
- Place end caps on a clean surface.
elements.
- During membrane element loading the Note: in case of membrane element
location of the membrane element replacement, push the old membrane
numbers has to be recordered in the elements out in the same direction as
membrane location sheets (see Figure the flow of water.
No. 1). NEVER USE A STEEL ROD.
- Don't expose the membrane elements to (Please note: when removing old
direct sunshine, sand or dust after membrane elements, it is necessary
unpacking, lay them in a single layer on a to support them on emerging to
clean even surface. prevent product tubes from breaking,
- To prevent membrane elements from a membrane element loading tool
drying out, unpacked membrane elements would provide for this).
must be loaded within 20 minutes.
Figure No. 1

8 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98


Figure No. 2

- Wipe the pressure vessel with a clean - The piping/tubing (feedwater, product
water-soaked sponge (e.g. polyester) water and brine lines) must be
glued to a PVC pipe, and then wipe with a reconnected exactly as they were prior to
glycerin-soaked swab or sponge (see disassembly.
Figure No. 2).
Note: some units may be supplied with less
After use, the swabs should be rinsed in membranes than the available space
water. Do not permit strong oxidizing in the pressure vessels (e.g. 3
agents such as nitric or Potassium pressure vessels for 6 membranes
permanganate to contact the glycerine. each and 15 membranes only). The
number of membrane is suitable for
- The membrane elements are coupled with
producing the required amount of
element connectors (see Figure No. 3).
water under the applicable design
Inspect the O-Rings and lubricate with
conditions. The available space may
glycerine.
be used in the future to compensate
- The membrane elements are inserted one for membrane ageing.
at a time into the pressure vessel with the Great care must be taken during
concentrate end (opposite end of brine membrane loading: push the
seal) of the membrane element first (see membranes to the end of the
Figure No. 1). Lubricate the brine seal with pressure vessel connecting brine and
glycerine before the membrane element is product ports. Install the plug - Cat.
completely inserted. All lubrication has to No. R07935 + R05551 - on the
be done sparingly. membrane product tube and the cap -
- Lubricate the membrane element Cat. No. 600368 - on the adapter
connector with glycerine and position on located inside the product port of the
product tube. Use a twisting motion to pressure vessel end plate (see Figure
ease the membrane element connector No. 4).
O-Rings over the product tube and push - Then the train of membrane elements is
the membrane element connector onto the pushed in the direction of the permeate
product tube until it butts. outlet side of the pressure vessel (this can
- When the number of membrane elements be done by means of the membrane
inserted into the vessel equals the number element loading device).
for which the vessel was designed, the The distance between the front-product
product tubes on the membrane elements tube and the pressure vessel end plate
will extend to the ends of the pressure should be less than 50 mm for 8 inch
vessel. membranes.

Now replace both endcaps and insert - Assembly the endcap of the pressure
Holding Plates and Bolts. vessel. Tighten the Victaulic bolts.

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 9


MEMBRANE ELEMENT FAILURE Usually this will indicate where the problem
DIAGNOSIS lies so that the necessary action can be
determined.
The location of the O-Ring leak or failing
membrane element begins by sampling the In a multimembrane element pressure vessel,
permeate output from each pressure vessel, the data may not be conclusive and it is
until the particular pressure vessel, that sometimes necessary to remove two of the
rejects less Total Dissolved Solids (TDS) than elements in a shell in order to isolate one
it should, has been found. element.
Doing this, we have to realize that Permeate If it becomes necessary to remove membrane
TDS increases along with the R.O. assembly elements from the pressure vessel, they
as a function of the local concentration. For should not be exposed to humidity of less
these vessels which are rejecting properly, than 100% for more than a few hours. An
the next step is to isolate the failing easy method to prevent this condition is to
component. In each vessel there are two ring have a container larger than all dimensions of
joints for each membrane element, any of the membrane element and submerge the
which could cause a high TDS reading. elements as soon as removed from the
system.
The technique of determining the failing
membrane element or connection consists of First, examine the O-Rings; each O-Ring
the use of a 6-mm diameter plastic tube must be in its groove without being twisted,
(supplied with the unit) which is inserted in distorted or nicked so that perfectly seal
the permeate passage of a pressure vessel to around both its inside and outside surface,
determine the TDS of the permeate at various avoiding concentrate from entering the
points along its passage through the vessel. permeate passages. Also examine the
Insert the tube to the far end. connectors and bushings for damages or
cracks. If the feed water does not enter the
By sampling one can develop a contour of the
permeate passages, the resulting TDS
salinity at each location throughout the
reading will depend upon the portion of feed
pressure vessel by measuring the
water (high in TDS) penetrating into permeate
conductivity of the water at each position of
(low TDS). Usually there is only one failure
the probe.
but examine all connections to be sure.
Samples are tested from various positions
Secondly, consider the brine seal is a tapered
along the lenght of the vessel. A sample with
device which prevents the pressurized feed
a much higher conductivity content than the
water from by-passing a membrane element.
previous sample indicates a leak in the area
Failure will cause a drop in the permeation
from which the latter sample was taken.
rate since one membrane element has, in
The initial reading is a check of the O-Ring; effect, been removed from the normal flow of
the second reading is a ckeck of the feed water.
membrane rejection; the third reading is a
check of the next O-Ring junction etc.

10 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98


Figure No. 3

Figure No. 4

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 11


R.O. Unit Start-Up

Note: the description of the start-up


- Switch off the power supply to the control
procedure describes a unit with single
panel and close the automatic switch of
high pressure pump. If two pumps are
the pump AP01.
installed, the procedure described
applies to both pumps. - Switch the control panel power supply
back on.
After making sure that the R.O. feed water
quality is within the operating limits, the After the preset delay, if the feed water
system can be started up. pressure conditions are met, the AP01
pump will start.
- Set the safety pressure switches:
Note: check that the motor runs in the
low pressure pressure switch
direction shown by the arrow;
PSL01 = 0.3-0.5 bar
otherwise, reverse two wires on
high pressure product pressure switch the motor terminal board.
PSH03 = 1.5 bar
- Set the system correctly for the operating
high pressure pump pressure switch expectations, by adjusting the control
PSH02 = 25-28 bar valves on the pump discharge (RV01),
reject (RV03) and recycle (RV02, if
- Temporarily, connect the product water
applicable) lines.
line to drain using a flexible hose.
Note: all flow rate and pressure
- Set the control valves for high pressure
parameters can be checked
pump discharge (RV01), reject (RV03) and
immediately on the flow meters
recycle (RV02, if applicable) 50% open.
and pressure gauges supplied with
- Open the automatic switch installed to the system.
protect the high pressure pump (AP01),
- Leave the system in operation with the
the pump cannot start.
product line connected to drain for about
- Feed to the control panel and turn the two hours to eliminate any trace of
R.O. unit control switch to RUN position. chemicals from the R.O. membranes.
- The solenoid valve (SV01) will be - Restore the original connection of the
energized and the automatic valve (AV01) product water line and fill the treated water
installed on the unit inlet will immediately accumulation tank.
open to pressurize the system.
- When the tank is full the R.O. unit will
From the reject flow meter (Fl03) check
automatically switch to flushing mode. In
that all air has been expelled from the
this phase the solenoid valve (SV01) is de-
circuit (air bubbles will gradually
energized; the automatic inlet valve
disappear).
(AV01) is shut, while the motor-driven
- Vent the air from the pump AP01 using the pump unit continues running, drawing in
suitable vent port located on top of the water from the flushing tank. The R.O.
pump. unit will stop after the preset time.
- Make sure there are no leaks in the water Note: the flushing tank is equipped with
circuit. one minimum level switch to
prevent the pump from dry
running.

12 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98


CHECKING THE ALARMS below those indicated on the relevant
pressure gauges.
When the alarm condition occurs the unit cuts
out immediately and the "Pump High
R.O. UNIT LOW PRESSURE ALARM Pressure" or "Product High Pressure" light
(PAL01) illuminates on the control panel.
Restore the pressure switches to their original
Shut the manual valve at the R.O. system setting and reset the alarm.
inlet and check that the unit stops
immediately and the "Low Pressure" alarm
lights up on the general control panel.
FLUSHING TANK LOW LEVEL ALARM
Turn the manual valve back on and reset the
(LAL01)
alarm.

To check that the sensor installed in the


flushing tank is operating correctly, increase
PUMP HIGH PRESSURE (PAH02) AND the time set on the flushing timer, simulate
PRODUCT HIGH PRESSURE (PAH03) the TANK FULL condition, wait for the
ALARMS flushing tank to empty and check that the
pump stops immediately.

To check that the high pressure alarms are WARNING: great care must be taken during
working properly, modify the settings of the this procedure to avoid the pump
pressure switches themselves to values to run dry.

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 13


Operation

GENERAL PLANT PERFORMANCE LOGGING AND


DAILY CHECKS
The R.O. unit has been designed to run with
a minimum of operators attention. In order to To achieve a smooth and continuous
protect the most vulnerable parts of the plant, operation, the following items must be
it has been provided with a number of checked and logged on a daily basis.
instruments that will bring the plant to a safe - Silt density index of the feed water
emergency shut-down state when a safety The purpose of the silting index test
limit is exceeded. procedure is to obtain an indication of the
Emergency shut-down should be avoided as amount of suspended particles in the R.O.
much as possible. The various alarms will be feed water. R.O. membranes foul, because
indicated on the system panel. they retain solids, a portion of which will
Note: it is very important that right from the form a fouling layer on the membrane.
initial start-up of the plant all readings A small scale membrane filtration under
of pressure, temperature, flow, SDI and standard conditions gives information about
conductivity are logged or recorded on the fouling rate of a given feed water. To
plant log sheets and recorder rolls, determine the silt density index, follow
where provided. procedure as described in the following
section.
Daily logging, and also whenever there is an
The maximum acceptance silt density index
operator's shift change is the minimum for spiral wound membrane elements is 3.
required (SDI weekly logging is normally Results of all silt density index tests must be
acceptable).
logged, and used filters marked with the
Absence or incompleteness of plant log date of the test and stored in a filing system
sheets and recorder paper may invalidate for reference in the event of warranty
the guarantees. claims.
New membrane elements have a higher initial - Pressure drop across the cartridge filters
permeate flow, that will decrease because of The plant will shut-down on low feed
compaction of the membrane material. The pressure to the H.P. pump. When the
compaction will be higher at higher pressures cartridge filters are clogged to such extent
and temperatures and will stabilise after a that the outlet pressure gauge reads 0.7 bar
certain period of time. In the design of this less than the original value, the cartridges
plant, the compaction effects are accounted have to be replaced in the cartridge system.
for with an appropriate design margin. - Concentrate and permeate flows
The actual effect of compaction on system
Concentrate and permeate flows will vary
pressure under constant flow conditions can with varying temperature and pressure, they
best be established in practice by a might require re-adjustment by operating the
comparison between the initial system
feed control valve as well as the concentrate
pressure and the system pressure after about and recirculation control valves. Increase of
500 hrs running period. For the best permeate flow will be obtained by opening
comparison the plant should first be cleaned.
the feed control valve and closing the
After this period, compaction will progress concentrate control valve. Increase of
much more slowly and, apart from concentrate flow is obtained by opening the
temperature and fouling effects, the plant will
concentrate flow valve and opening the feed
then operate under steady conditions. control valve.

14 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98


Silt Density Index (S.D.I.) Test Procedure

GENERAL

The object of this procedure is to provide a 7) The Silt Density Index is now calculated by
means of determining the tendency of the the formula:
feed water to foul a reverse osmosis system. T1
1-
The SDI test has to be done weekly or T2
S.D.I. = x 100
whenever a change in feedwater quality is T
suspected. For a safe operation of the plant
SDI must be below 3. where T is test time in minutes (usually 15
minutes, but may be less when if 75%
plugging occurs in less than 15 minutes).
PROCEDURE
8) Note the result of the test on the plant log
sheet, mark the used filters with the date
1) The Silt Density Index test assembly of the test and keep them in a file.
consists of a pressure control valve and
Millipore filter holder type SX 0007400 and
a pressure gauge to 5 bars, in the feed
directly in front of the Millipore filter.
2) Prime the filter holder, open up the filter
holder and place by means of forceps a
new MF 0.45 micron filter concentrically on
the filter bottom.
3) When the filter is soaked, it will stick more
or less to the filter bottom and the filter
holder can be closed again.
4) Adjust the feed pressure to the filter
quickly to 2.2 bar on the pressure gauge
by means of the pressure control valve.
5) Start a stop watch and time the period to
fill a flask to the 500 ml mark. Record this
time as T1 seconds. This should take
longer than 15 seconds. A shorter time
indicates incorrect pressure or a leak on
the filter assembly. Leave the valve open
for continuous flow.
6) After 15 minutes repeat step 5. Time the
period it takes to fill the 500 ml flask.
Record this time as T2 seconds.

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 15


Membrane Cleaning

GENERAL INFORMATION

a) Introduction rated capacity.


Deposition of suspended solids, It is also recommended that the cleaning
precipitation of sparingly soluble salts or procedures described in this report are
biological growth can foul R.O. executed if it becomes necessary to
membranes if the feed water does not increase the applied pressure by as much
receive adequate pre-treatment. Fouling as 5-10% to maintain constant output.
has also been known to occur over a Fouling can be easily detected if such
period of time even when the feed water is increases are required, provided that the
from a source that has a low Silt Density feed water temperature and the recovery
Index. rate remain constant.
Symptoms of fouling are decreases in both However, increased pressure will also be
permeate flow and permeate quality. required to maintain constant output from
The earlier that fouling is detected, the clean membranes if the feed water
easier it is to clean the membranes in temperature decreases. Furthermore,
order to restore their performance. The some increase in pressure will also be
purpose of this report is to provide required if the recovery is increased while
guidelines for the detection of fouling and the concentrate flow rate is constant or if
to recommend procedures for cleaning the the concentrate is increased while the
membranes. recovery is constant. The latter factors
b) Detection of Fouling have a relatively minor effect on required
pressure increases compared to the
The permeate flow rate varies with the
temperature factor and can usually be
temperature of the water that is being
ignored. The following chart can be used
processed and the pressure to which it is
as a guide for approximating the effect of
subjected. Generally it is recommended
temperature on the pressure requirements
that the applied pressure is adjusted to
for clean membranes.
maintain constant permeate production at
MULTIPLICATION FACTOR

TEMPERATURE (°C)

16 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98


A temperature of 20°C was arbitrarily In this example, cleaning is recommended
chosen as a base point for this chart for if the pressure required to produce
plotting the multiplication factors. If a base constant output increases to:
point other than 20°C is needed, its 17.0 x 1.05 = 17.8 bar at 25°C
multiplication factor can be adjusted to or
another temperature by using the ratio of 21.5 x 1.05 = 22.6 bar at 16°C
the two multiplication factors taken from
this chart. If, for example, an R.O. plant is If operation were to be continued at higher
producing rated output at 25°C at an pressures, the deposited foulants would
applied pressure of 17 bars and if the become more compacted, and
temperature decreases to 16°C, the subsequently cleaning would not be as
approximate factors taken from the chart effective in removing them.
are 0.87 and 1.1 respectively. c) Recommended Cleaning Solutions
The pressure that will be needed to The following are a selection of cleaning
produce the same output at 16°C will then chemicals that have been shown to be
be approximately: successful at other installations. The choice
1.1 of the cleaning solution will be made by
x 17 = 21.5 bar engineering. Add the given quantities to
0.87 R.O. water product as described.

SIMPLE CLEANING SOLUTIONS FOR R.O. MEMBRANE


Cleaner 0.1% (W) 0.1% (W) 0.1% STP 0.2% 0.5% 2.0% 0.2% 1.0%
NaOH and NaOH and and 1.0% (W) (W) (W) (W) (W)
pH 12, pH 12, Na4EDTA HCl H3PO4 Citric NH2SO3H Na2S2O4
30°C max 30°C max or Acid
or 1.0% or 0.025% 0.1%TSP
(W) (W) and
Na4EDTA Na-DSS 1.0%
and and Na4EDTA
pH 12, pH 12,
Foulant 30°C max 30°C max
Inorganic Salts
(for example
CaCO3 CaSO4
BaSO4) best OK OK OK
Metal Oxides
(for example
Iron) good OK good
Inorganic
Colloids (Silt) good
Silica OK
Biofilms best good good
Organic OK good good

(W) denotes weight percent of active ingredient.


Cleaning Chemical symbols in order used: NaOH is Sodium hydroxide; Na4EDTA is the tetrasodium salt of
ethylene diamine tetraacetic acid; Na-DSS is Sodium salt of dodecylsulfate; STP is Sodium triphosphate
(Na5P3O10); TSP trisodium phosphate (Na3PO4⋅12H2O); HCl is hydrochloric acid; H3PO4 is phosphoric acid;
C3H4(OH)(CO2H)3 is citric acid; NH2SO3H is sulfamic acid; Na2S2O4 is Sodium hydrosulfite.
Foulant Chemical symbols in order used: CaCO3 is Calcium carbonate; CaSO4 is Calcium sulfate; BaSO4 is
Barium sulfate.

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 17


Cleaning Procedure with the "CLEANING KIT" System

The Cleaning Kit includes: 1) Drop in product water flow rate not
1) A chemical preparation tank justified by simultaneous decrease in feed
water temperature.
2) A mixing system
2) Increase in product water conductivity.
3) A pump
3) Increase in the ∆P across the membranes.
4) Hoses for connection to the ports provided
on the desalinator.
The flushing tank should be used for storage
of the solution used for cleaning.
PROCEDURE Fill the container to 75% of its total capacity
(check the real quantity of water present).
1) Fill the cleaning tank with R.O. water.
Disconnect the flange of the product water
2) Add the product to be used for cleaning outlet pipe to the top of the container.
(citric acid, caustic soda, etc.) to the
Connect the reject pipe to the flushing
osmotized water.
container, using a hose.
3) Supply power to the pump and recycle
Fully open the manual valves RV02 and
until the solution is thoroughly mixed RV03 on the recycle and reject line.
(when an electric stirrer is not provided).
Set the manual valve on pump discharge
4) Switch off the power supply in the general about 80% closed.
control panel.
Set the flushing time at 60 minutes using the
5) Use the hoses provided to connect to the timer provided.
R.O. unit inlet, product and reject lines Prepare the cleaning solution and pour it into
(connections already provided). the flushing container, after calculating the
6) Open the valve on the cleaning pump concentration correctly.
discharge line totally or partially, as Turn the "duty-flushing" key-switch to flushing
required. Supply power to the control and supply power to the electrical panel.
panel.
Adjust the manual valve on pump discharge
7) Recycle the solution through the line until a pressure of 6 bar approx. is
membranes for about 1 hour or until a reached.
temperature of max. 35°C is reached. Leave the system in operation until it stops
This procedure can be repeated several times automatically, checking the solution
of course changing the cleaning solution each temperature from time to time.
time. Restore the product and reject line
connections.

EMERGENCY CLEANING PROCEDURE Turn the key-switch to DUTY.


(when the system is not equipped with the Wait until the water in the flushing container
"CLEANING" KIT system) has been completely replaced, then restore
the initial parameter, pressure and flow rate
The osmotic membranes require cleaning
settings.
when malfunctions are noticed:

18 Aqua-Cleer IW Cat. No. M000-04-9/96 – R2-4/98


ENCLOSURES:

1- R.O. MEMBRANE SPECIFICATION

2- R.O. PRESSURE VESSEL SPECIFICATION

3- HP PUMP SPECIFICATION

4- PRESSURE SWITCH SPECIFICATION

5- FLUSHING TANK LEVEL SWITCH SPECIFICATION

6- FLOW INDICATORS SPECIFICATION

7- THERMOMETERS SPECIFICATION

Cat. No. M000-04-9/96 – R2-4/98 Aqua-Cleer IW 19

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