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He concluded that a new type of ray was being emitted from the tube.
This ray was capable of passing through the heavy paper covering and
exciting the phosphorescent materials in the room. He found that the
new ray could pass through most substances casting shadows of solid
objects. Roentgen also discovered that the ray could pass through the
tissue of humans, but not bones and metal objects. One of Roentgen's
first experiments late in 1895 was a film of the hand of his wife, Bertha.
It is interesting that the first use of X-rays were for an industrial (not
medical) application, as Roentgen produced a radiograph of a set of
weights in a box to show his colleagues.
Public fancy was caught by this invisible ray with the ability to pass
through solid matter, and, in conjunction with a photographic plate,
provide a picture of bones and interior body parts. Scientific fancy was
captured by the demonstration of a wavelength shorter than light. This
generated new possibilities in physics, and for investigating the
structure of matter. Much enthusiasm was generated about potential
applications of rays as an aid in medicine and surgery. Within a month
after the announcement of the discovery, several medical radiographs
had been made in Europe and the United States, which were used by
surgeons to guide them in their work. In June 1896, only 6 months
after Roentgen announced his discovery, X-rays were being used by
battlefield physicians to locate bullets in wounded soldiers.
Radium became the initial industrial gamma ray source. The material
allowed castings up to 10 to 12 inches thick to be radiographed. During
World War II, industrial radiography grew tremendously as part of the
Navy's shipbuilding program. In 1946, man-made gamma ray sources
such as cobalt and iridium became available. These new sources were
far stronger than radium and were much less expensive. The
manmade sources rapidly replaced radium, and use of gamma rays
grew quickly in industrial radiography.
Health Concerns
Today, it can be said that radiation ranks among the most thoroughly
investigated causes of disease. Although much still remains to be
learned, more is known about the mechanisms of radiation damage on
the molecular, cellular, and organ system than is known for most other
health stressing agents. Indeed, it is precisely this vast accumulation of
quantitative dose-response data that enables health physicists to
specify radiation levels so that medical, scientific, and industrial uses of
radiation may continue at levels of risk no greater than, and frequently
less than, the levels of risk associated with any other technology.
In many ways, radiography has changed little from the early days of its
use. We still capture a shadow image on film using similar procedures
and processes technicians were using in the late 1800's. Today,
however, we are able to generate images of higher quality and greater
sensitivity through the use of higher quality films with a larger variety of
film grain sizes. Film processing has evolved to an automated state,
producing more consistent film quality by removing manual processing
variables. Electronics and computers allow technicians to now capture
images digitally. The use of "filmless radiography" provides a means of
capturing an image, digitally enhancing, sending the image anywhere
in the world, and archiving an image that will not deteriorate with time.
Technological advances have provided industry with smaller, lighter,
and very portable equipment that produce high quality X-rays. The use
of linear accelerators provide a means of generating extremely short
wavelength, highly penetrating radiation, a concept dreamed of only a
few short years ago.
While the process has changed little, technology has evolved allowing
radiography to be widely used in numerous areas of inspection.
Radiography has seen expanded usage in industry to inspect not only
welds and castings, but to radiographically inspect items such as
airbags and canned food products. Radiography has found use in
metallurgical material identification and security systems at airports
and other facilities.
Inspectors in the future will be able to peal away layer after layer of a
part to evaluate the material in much greater detail. Color images,
much like computer generated ultrasonic C-scans of today, will make
interpretation of indications much more reliable and less time
consuming.
The Electromagnetic Spectrum
X-rays and gamma rays differ only in their source of origin. X-rays are
produced by an x-ray generator and gamma radiation is the product of
radioactive atoms. They are both part of the electromagnetic
spectrum. They are waveforms, as are light rays, microwaves, and
radio waves. X-rays and gamma rays cannot been seen, felt, or heard.
They possess no charge and no mass and, therefore, are not
influenced by electrical and magnetic fields and will generally travel in
straight lines. However, they can be diffracted (bent) in a manner
similar to light.
Each photon contains a certain amount (or bundle) of energy, and all
electromagnetic radiation consists of these photons. The only
difference between the various types of electromagnetic radiation is
the amount of energy found in the photons. Due to their short
wavelength they have more energy to pass through matter than do the
other forms of energy in the electromagnetic spectrum. As they pass
through matter, they are scattered and absorbed and the degree of
penetration depends on the kind of matter and the energy of the rays.
X-rays are just like any other kind of electromagnetic radiation. They
can be produced in parcels of energy called photons, just like light.
There are two different atomic processes that can produce X-ray
photons. One is called Bremsstrahlung and is a German term meaning
"braking radiation." The other is called K-shell emission. They can both
occur in the heavy atoms of tungsten. Tungsten is often the material
chosen for the target or anode of the x-ray tube.
Bremsstrahlung Radiation
X-ray tubes produce x-ray
photons by accelerating a stream
of electrons to energies of
several hundred kilovolts with
velocities of several hundred
kilometers per hour and colliding
them into a heavy target material.
The abrupt acceleration of the
charged particles (electrons) produces Bremsstrahlung photons. X-ray
radiation with a continuous spectrum of energies is produced with a
range from a few keV to a maximum of the energy of the electron
beam. Target materials for industrial tubes are typically tungsten,
which means that the wave functions of the bound tungsten electrons
are required. The inherent filtration of an X-ray tube must be
computed, which is controlled by the amount that the electron
penetrates into the surface of the target and by the type of vacuum
window present.
In Beta Decay, a neutron from an atom will split into one positively charged
proton and a negatively charged electron.
Alpha and Beta decay are almost always accompanied by Gamma Decay. In
Gamma Decay, energy in the form of gamma radiation or rays are emitted
from the nucleus. Gamma rays are electromagnetic waves with very high
frequencies and energy.
Gamma rays are identical to X-Rays, except that X-Rays are artificially
produced and Gamma rays are naturally occurring.
Alpha Particles
Certain radionuclides of high atomic mass (Ra226, U238, Pu239)
decay by the emission of alpha particles. These alpha particles are
tightly bound units of two neutrons and two protons each (He4
nucleus) and have a positive charge. Emission of an alpha particle
from the nucleus results in a decrease of two units of atomic number
(Z) and four units of mass number (A). Alpha particles are emitted with
discrete energies characteristic of the particular transformation from
which they originate. All alpha particles from a particular radionuclide
transformation will have identical energies.
Beta Particles
A nucleus with an unstable ratio of neutrons to protons may decay
through the emission of a high speed electron called a beta particle.
This results in a net change of one unit of atomic number (Z). Beta
particles have a negative charge and the beta particles emitted by a
specific radionuclide will range in energy from near zero up to a
maximum value, which is characteristic of the particular transformation.
Gamma-rays
A nucleus which is in an excited state may emit one or more photons
(packets of electromagnetic radiation) of discrete energies. The
emission of gamma rays does not alter the number of protons or
neutrons in the nucleus but instead has the effect of moving the
nucleus from a higher to a lower energy state (unstable to stable).
Gamma ray emission frequently follows beta decay, alpha decay, and
other nuclear decay processes.
The Sequence Info button displays a chart that depicts the path of the
series with atomic numbers indicated on the vertical axis on the left,
and the number of neutrons shown along the bottom. Colored arrows
represent alpha and beta decays. To return to the main user interface,
click the "Dismiss" button.
Initially, a selected series contains all parent material, and the amount
is represented by a colored bar on a vertical logarithmic scale. Each
line represents a factor of ten. In order to step forward through the
sequence by a specified number of years, you may type the
appropriate number into the "Time Step" field and hit "Enter." A
negative time step will backtrack through the sequence.
You may choose a step interval in years and progress through each
step by pressing the "Enter" key. The "Animate" button will automate
the progress through the series. You can either choose a time step
before you animate or leave it at zero. If the time step is left at zero,
the system will choose time steps to optimize viewing performance.
Ionization
As one of the fields which obey the general inverse square law, a point
radiation source can be characterized by the diagram above whether
you are talking about Roentgens, rads, or rems. All measures of
exposure will drop off by the inverse square law. For example, if the
radiation exposure is 100 mR/hr at 1 inch from a source, the exposure
will be 0.01 mR/hr at 100 inches.
If the distance is too small, the dosage will be too high and our brave
technician will face severe medical effects. To clear the graph, select a
new material, or the same one again. Moving the mouse from the white
area to the gray will turn off the sound!
Click here to run a JavaScript application on Newton's Inverse
Square Law.
What dosage in mR/hr is considered safe? Better find out!
The red dosage lines represent 2, 5, and 100 mR/hr levels.
Exercise: Assume you are standing three feet from a a 15 Curie cobalt-
60 source. How many mR/hr dosages are you getting?
Interaction Between Penetrating Radiation
and Matter
Even when they have the same energy, photons travel different distances
within a material simply based on the probability of their encounter with one or
more of the particles of the matter and the type of encounter that occurs. Since
the probability of an encounter increases with the distance traveled, the number
of photons reaching a specific point within the matter decreases exponentially
with distance traveled. As shown in the graphic to the right, if 1000 photons are
aimed at ten 1 cm layers of a material and there is a 10% chance of a photon
being attenuated in this layer, then there will be 100 photons attenuated. This
leave 900 photos to travel into the next layer where 10% of these photos will be
attenuated. By continuing this progression, the exponential shape of the curve
becomes apparent.
The factor that indicates how much attenuation will take place per cm
(10% in this example) is known as the linear attenuation coefficient, m.
The above equation and the linear attenuation coefficient will be
discussed in more detail on the following page.
Transmitted Intensity and
Linear Attenuation Coefficient
If x is the HVL then m times HVL must equal 0.693 (since the number
0.693 is the exponent value that gives a value of 0.5).
Peak Voltage
Lead Concrete
(kVp)
Note: The values presented on this page are intended for educational
purposes. Other sources of information should be consulted when
designing shielding for radiation sources.
Sources of Attenuation
Below are other interaction phenomenon that can occur. Under special
circumstances these may need to be considered, but are generally
negligible.
Photodisintegration (PD) is
the process by which the x-ray
photon is captured by the
nucleus of the atom with the
ejection of a particle from the
nucleus when all the energy of
the x-ray is given to the nucleus.
Because of the enormously high energies involved, this process may
be neglected for the energies of x-rays used in radiography.
The applet below can be used to investigate the effect that photon
energy has on the type of interaction that the photon is likely to have
with a particle of the material (shown in gray). Various materials and
material thicknesses may be selected and the x-ray energy can be set
to produce a range from 1 to 199 KeV. Notice as various experiments
are run with the applets that low energy radiation produces
predominately photoelectric events and higher energy x-rays produce
predominately Compton scattering events. Also notice that if the
energy is too low, none of the radiation penetrates the material.
Compton effect was first observed by Arthur Compton in 1923 and this
discovery led to his award of the 1927 Nobel Prize in Physics. The
discovery is important because it demonstrates that light cannot be
explained purely as a wave phenomenon. Compton's work convinced
the scientific community that light can behave as a stream of particles
(photons) whose energy is proportional to the frequency.
The applet shows that when a photon of a given energy hits an atom, it
is sometimes reflected in a different direction. At the same time, it
loses energy to an electron that is ejected from the atom. Theta is the
angle between the scattered photon direction and the path of the
incident photon. Phi is the angle between the scattered electron
direction and the path of the incident photon.
Geometric Unsharpness
For the case, such as that shown to the right, where a sample of
significant thickness is placed adjacent to the detector, the following
formula is used to calculate the maximum amount of unsharpness due
to specimen thickness:
Ug = f * b/a
Ug = f* b/a
Filters in Radiography
For industrial radiography, the filters added to the x-ray beam are most
often constructed of high atomic number materials such as lead,
copper, or brass. Filters for medical radiography are usually made of
aluminum (Al). The amount of both the inherent and the added filtration
are stated in mm of Al or mm of Al equivalent. The amount of filtration
of the x-ray beam is specified by and based on the voltage potential
(keV) used to produce the beam. The thickness of filter materials is
dependent on atomic numbers, kilovoltage settings, and the desired
filtration factor.
Undercut
Another condition that must often
be controlled when producing a
radiograph is called
undercut. Parts with holes,
hollow areas, or abrupt thickness changes are likely to suffer from
undercut if controls are not put in place. Undercut appears as a
darkening of the radiograph in the area of the thickness transition. This
results in a loss of resolution or blurring at the transition area. Undercut
occurs due to scattering within the film. At the edges of a part or areas
where the part transitions from thick to thin, the intensity of the
radiation reaching the film is much greater than in the thicker areas of
the part. The high level of radiation intensity reaching the film results in
a high level of scattering within the film. It should also be noted that the
faster the film speed, the more undercut that is likely to occur.
Scattering from within the walls of the part also contributes to undercut,
but research has shown that scattering within the film is the primary
cause. Masks are used to control undercut. Sheets of lead cut to fill
holes or surround the part and metallic shot and liquid absorbers are
often used as masks.
Radiation Safety
The source capsule and the pigtail is housed in a shielding device
referred to as a exposure device or camera. Depleted uranium is often
used as a shielding material for sources. The exposure device for
iridium-192 and cobalt-60 sources will contain 45 pounds and 500
pounds of shielding materials, respectively. Cobalt cameras are often
fixed to a trailer and transported to and from inspection sites. When the
source is not being used to make an exposure, it is locked inside the
exposure device.
When x-rays, gamma rays, or light strike the grains of the sensitive
silver halide in the emulsion, some of the Br- ions are liberated and
captured by the Ag+ ions. This change is of such a small nature that it
cannot be detected by ordinary physical methods and is called a "latent
(hidden) image." However, the exposed grains are now more sensitive
to the reduction process when exposed to a chemical solution
(developer), and the reaction results in the formation of black, metallic
silver. It is this silver, suspended in the gelatin on both sides of the
base, that creates an image. See the page on film processing for
additional information.
Film Selection
The selection of a film when
radiographing any particular
component depends on a number of
different factors. Listed below are
some of the factors that must be
considered when selecting a film
and developing a radiographic
technique.
Film Packaging
Radiographic film can be purchased in a
number of different packaging options.
The most basic form is as individual
sheets in a box. In preparation for use,
each sheet must be loaded into a cassette
or film holder in the darkroom to protect it
from exposure to light. The sheets are
available in a variety of sizes and can be
purchased with or without interleaving paper. Interleaved packages
have a layer of paper that separates each piece of film. The
interleaving paper is removed before the film is loaded into the film
holder. Many users find the interleaving paper useful in separating the
sheets of film and offer some protection against scratches and dirt
during handling.
Industrial x-ray films are also available in a form in which each sheet is
enclosed in a light-tight envelope. The film can be exposed from either
side without removing it from the protective packaging. A rip strip
makes it easy to remove the film in the darkroom for processing. This
form of packaging has the advantage of eliminating the process of
loading the film holders in the darkroom. The film is completely
protected from finger marks and dirt until the time the film is removed
from the envelope for processing.
Film Handling
X-ray film should always be handled carefully to avoid physical strains,
such as pressure, creasing, buckling, friction, etc. Whenever films are
loaded in semi-flexible holders and external clamping devices are
used, care should be taken to be sure pressure is uniform. If a film
holder bears against a few high spots, such as on an un-ground weld,
the pressure may be great enough to produce desensitized areas in
the radiograph. This precaution is particularly important when using
envelope-packed films.
Since radiographic contrast and definition are not dependent upon the
same set of factors, it is possible to produce radiographs with the
following qualities:
Radiographic Contrast
As mentioned on the
previous page, radiographic
contrast describes the
differences in photographic
density in a radiograph. The
contrast between different
parts of the image is what forms the image and the greater the
contrast, the more visible features become. Radiographic
contrast has two main contributors: subject contrast and detector
(film) contrast.
Subject Contrast
Subject contrast is the ratio of radiation intensities transmitted
through different areas of the component being evaluated. It is
dependant on the absorption differences in the component, the
wavelength of the primary radiation, and intensity and distribution
of secondary radiation due to scattering.
Film Contrast
Film contrast refers to density differences that result due to
the type of film used, how it was exposed, and how it was
processed. Since there are other detectors besides film, this
could be called detector contrast, but the focus here will be on
film. Exposing a film to produce higher film densities will
generally increase the contrast in the radiograph.
As mentioned previously,
radiographic definition is the
abruptness of change from one
density to another. Geometric
factors of the equipment and the
radiographic setup, and film and
screen factors both have an effect
on definition. Geometric factors
include the size of the area of origin
of the radiation, the source-to-
detector (film) distance, the
specimen-to-detector (film)
distance, movement of the source,
specimen or detector during
exposure, the angle between the
source and some feature and the
abruptness of change in specimen
thickness or density.
Geometric Factors
The effect of source size, source-to-film distance and the specimen-to-
detector distance were covered in detail on the geometric
unsharpness page. But briefly, to produce the highest level of
definition, the focal-spot or source size should be as close to a point
source as possible, the source-to-detector distance should be a great
as practical, and the specimen-to-detector distance should be a small
as practical. This is shown graphically in the images below.
The angle between the radiation and
some features will also have an
effect on definition. If the radiation is
parallel to an edge or linear
discontinuity, a sharp distinct
boundary will be seen in the image.
However, if the radiation is not
parallel with the discontinuity, the
feature will appear distorted, out of
position and less defined in the
image.
Similar to the decibel, using the log of the ratio allows ratios of
significantly different sizes to be described using easy to work with
numbers. The following table shows the relationship between the
amount of transmitted light and the calculated film density.
1.0 100% 1 0
0.1 10% 10 1
0.01 1% 100 2
0.001 0.1% 1000 3
0.0001 0.01% 10000 4
0.00001 0.001% 100000 5
0.000001 0.0001% 1000000 6
0.0000001 0.00001% 10000000 7
From this table, it can be seen that a density reading of 2.0 is the result
of only one percent of the incident light making it through the film. At a
density of 4.0 only 0.01% of transmitted light reaches the far side of the
film. Industrial codes and standards typically require a radiograph to
have a density between 2.0 and 4.0 for acceptable viewing with
common film viewers. Above 4.0, extremely bright viewing lights is
necessary for evaluation. Contrast within a film increases with
increasing density, so in general, the higher the density the better.
When radiographs will be digitized, densities above 4.0 are often used
since digitization systems can capture and redisplay for easy viewing
information from densities up to 6.0.
Film density is measured with a densitometer. A
densitometer simply has a photoelectric sensor that
measures the amount of light transmitted through a
piece of film. The film is placed between the light
source and the sensor and a density reading is
produced by the instrument.
Film Characteristic Curves
Note, the Io field has a number in it. This is the initial intensity of the x-
ray beam. For large numbers, it may be necessary to use the mouse to
see the entire number. Click on the number and move the mouse as if
selecting it. The cyan pointer indicates the density on the resultant
radiograph. The two other pointers represent under- and over-
exposure by a factor of four. These may be used to judge the degree
of contrast in the resultant radiograph.
Change the material to iron and press "Calculate". Note that not
enough radiation is received to generate an image. Change the
following: kV: 320, mA: 10, time: 900 seconds, thickness: 1.25 cm, and
then click "Calculate". Note the resulting center density of 0.561. With
aluminum, the time was altered by a factor of four to change the
density. With the iron, current (mA) must be increased by a factor of
four to produce an increase in density. Change the current from 10 to
40 and calculate the results.
Controlling Radiographic Quality
Image quality indicators take many shapes and forms due to the
various codes or standards that invoke their use. In the United States,
two IQI styles are prevalent: the placard, or hole-type and the wire IQI.
IQIs comes in a variety of material types so that one with radiation
absorption characteristics similar to the material being radiographed
can be used.
Hole-Type IQIs
Wire IQIs
Placement of IQIs
IQIs should be placed on the source side of the part over a section with
a material thickness equivalent to the region of interest. If this is not
possible, the IQI may be placed on a block of similar material and
thickness to the region of interest. When a block is used, the IQI
should be the same distance from the film as it would be if placed
directly on the part in the region of interest. The IQI should also be
placed slightly away from the edge of the part so that at least three of
its edges are visible in the radiograph.
Film Processing
Viewing Radiographs
Film viewers should be clean and in good working condition. There are
four groups of film viewers. These include strip viewers, area viewers,
spot viewers, and a combination of spot and area viewers. Film
viewers should provide a source of defused, adjustable, and relativity
cool light as heat from viewers can cause distortion of the radiograph.
A film having a measured density of 2.0 will allow only 1% of the
incident light to pass. A film containing a density of 4.0 will allow only
0.01% of the incident light to pass. With such low levels of light passing
through the radiograph, the delivery of a good light source is important.
Discontinuities
Cold lap is a condition where the weld filler metal does not properly
fuse with the base metal or the previous weld pass material (interpass
cold lap). The arc does not melt the base metal sufficiently and causes
the slightly molten puddle to flow into the base material without
bonding.
Incomplete fusion is a condition where the weld filler metal does not
properly fuse with the base metal. Appearance on radiograph: usually
appears as a dark line or lines oriented in the direction of the weld
seam along the weld preparation or joining area.
Internal concavity or suck back is a condition where the weld metal
has contracted as it cools and has been drawn up into the root of the
weld. On a radiograph it looks similar to a lack of penetration but the
line has irregular edges and it is often quite wide in the center of the
weld image.
Dendritic shrinkage is a
distribution of very fine lines or small
elongated cavities that may vary in
density and are usually
unconnected.
Filamentary shrinkage usually
occurs as a continuous structure of
connected lines or branches of variable length, width and density, or
occasionally as a network.
Inclusions are nonmetallic
materials in an otherwise solid
metallic matrix. They may be less or
more dense than the matrix alloy
and will appear on the radiograph, respectively, as darker or lighter
indications. The latter type is more common in light metal castings.
In the image below left is a set of cast aluminum tensile specimens. A
radiographic image of several of these specimens is shown below
right.
CT slices through several locations of a specimen are shown in the set
of images below.
A number of slices through the object can be reconstructed to provide
a 3-D view of internal and external structural details. As shown below,
the 3-D image can then be manipulated and sliced in various ways to
provide thorough understanding of the structure.
X-Ray Inspection Simulation
For more information on how the XRSIM program operates, the users
manual is available here for downloading. The educational version of
the program is available commercially.