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Fire Safety Journal, 13 (1988) 27 - 37 27

High Temperature Properties of Hot-rolled, Structural Steels for Use in Fire


Engineering Design Studies

B. R. K I R B Y and R. R. P R E S T O N
British Steel Corporation, Swinden Laboratories, Moorgate, Rotherham $60 3AR, South Yorkshire (U.K.)

SUMMARY would be in danger of collapse if the applied


stress on it equalled, or exceeded, the elevated
A n extensive programme of small-scale temperature flow stress of the steel. The
tensile tests has been carried o u t under both Building Regulations therefore require that
steady-state and transient heating conditions the load-bearing structural members can be
to provide elevated temperature data on the shown to possess specific levels of fire resis-
behaviour o f hot.rolled, structural steels tance time as measured in the ISO834 stan-
for use in fire engineering design studies. dard test. Testing the behaviour of steel
It has been demonstrated that predictions elements, sub-assemblies and frameworks in
on the behaviour o f structural steels at small a fire is extremely expensive and any one
strains from data derived under steady-state test only provides limited data. Therefore,
conditions are optimistic and information great emphasis is now being placed upon
should preferably be used from transient the development of computer-aided models
tests. However, when temperatures and capable of predicting the distortion in a
stresses corresponding to strains approaching framework as the temperature rises. However,
'runaway' or the 'limit o f deflection' are the accuracy and confidence given to these
compared, then there is negligible difference models is strongly dependent on the funda-
between the m i n i m u m properties derived mental data used and, in relation to the fire
from either type o f test. Tables o f data are engineering design of structural steelwork,
provided in a form suitable for use in fire an accurate knowledge of the elevated tem-
engineering calculations. perature properties of steel is essential.
The purpose of the present paper is to
summarize the results of an extensive pro-
1. INTRODUCTION gramme of testing undertaken to more fully
evaluate the behaviour of structural sl;eels
There are many instances where structural under simulated fire conditions of tran.,'.ient
steelwork is exposed to high temperatures, heating. These data are suitable for use in
either by design or accident, and this causes fire engineering models and, in addition, a
significant changes in the strength of the comparison is made of some of the data with
material. Steels have been used for m a n y information derived from the more tradi-
years in the construction of boilers and there tional steady-state, hot tensile tests.
is a substantial body of test data available
which characterize these materials used
under steady-state heating conditions [1]. 2. TESTING METHODS
However, in terms of relating the properties
of steels, particularly those used in the It is important to distinguish between the
manufacture of hot-rolled sections, to sim- two main methods used f o r testing the
ilar stress and thermal histories experienced variation in the flow stress of a steel sample
by members in fire, the published data are as a function of temperature.
limited.
When a fire occurs in a building, the 2.1. Tests under transient heating conditions
steelwork could be heated to temperatures In many structures, or machines, it is
in excess of 700 °C and a structural member c o m m o n for a loaded steel component to

0379-7112/88/$3.50 © Elsevier Sequoia/Printed in The Netherlands


28

be subjected to a change in temperature and to its mid-point. The specimen shape con-
it is important to know how the resulting formed to the requirements of BS18 in
deformation of the material will develop. which a gauge length of 40 mm was adopted.
For this reason, tensile tests under transient Testing was carried out in a servo-hydraulic
heating conditions have been devised [2- 7] machine fitted with a three-zone, split fur-
in which the load on a steel specimen is nace, Fig. 1. This was programmed to pro-
maintained constant while its temperature vide constant specimen heating rates of 2.5,
is increased at a given rate. The changes in 5, 10 and 20 °C/min which simulated the
gauge length are constantly recorded by average heating rates of fully loaded, steel
means of high temperature extensometers. sections surviving approximately 4, 2, 1 and
In the present series of tests, two steel 1/2 h in the ISO834 standard fire resistance
qualities were evaluated conforming to test.
BS4360: Grades 43A and 50B respectively. During the tests, the prescribed load was
These represent approximately 94% of all transmitted to the specimens by means of
the structural steel sections currently sold Nimonic pull rods passing through the ends
by the British Steel Corporation and have of the furnace and hydraulically gripped in
ambient temperature properties similar to the machine. Specimen strain was monitored
those defined in Euronorm 25-72: Grades by Nimonic extensometers fixed by pressure
Fe430 and Fe510 respectively. screws at each end of the gauge length. These
Samples were prepared by machining provided measurements of changes in elastic
round test pieces from coupons removed and plastic strain, eel ~and epl, as a result of
from the standard position, i.e., one-third the applied loads, in addition to the strain,
of the distance from the edge of the flange eth , arising from thermal expansion. In
order to eliminate the latter from the results,
separate tests were carried out under zero
applied load when eel = epl = 0. Most tests
were terminated when the specimen attained
a strain of 5%, this being regarded as the
upper limit for practical use of the flow
stress data.

2.2. Tests under steady-state heating condi-


tions
In this type of test the unloaded sample
is brought into thermal equilibrium at a
certain temperature and it is then strained
at a uniform rate while the resulting loads
experienced by it are recorded as a function
of extension. Similar tests are then repeated
at other temperatures to build up a family
of load/extension curves from which the
required strengtli/temperature data can be
extracted. Most of the existing data [1]
were obtained by this method.
In the present programme of work, de-
tailed stress/strain data were derived for the
Grade 43A and Grade 50B steels over the
temperature range 20 - 800 °C. These data
were augmented by additional results from
hot tensile tests, to BS3688, carried out on
samples from several notch-tough qualities
Fig. 1. Photograph of the equipment used for ten- of structural steel sections.
sile tests conducted under transient heating condi- The total programme included 240 indi-
tions. viduai tests.
29

3. R E S U L T S A N D D I S C U S S I O N range of section sizes. In contrast, at low


applied stresses, no distinct yielding was
3.1. Tests under transient heating conditions observed since the relevant temperatures
A series of strain (eel + ep,)/temperature would be too high for effective dislocation
curves was obtained for each steel and heating locking and pinning by interstitial atoms.
rate. Typical curves, using a heating rate of In these tests, a substantial part of the ob-
10 °C/min, are shown up to 2% strain for served strain would be due to the reduction
Grades 43A and 50B steel in Figs. 2 and 3 of Young's Modulus at elevated tempera-
respectively. The principal features comprise tures.
a small initial elastic extension, when the For the purpose of fire engineering design,
load was applied at room temperature, fol- data derived from the transient tests can be
lowed by a very gradual increase in length presented in two forms:
as the temperature was increased. (a) as a series of derived stress/strain
At the highest stress levels employed, curves at elevated temperatures;
all the steels exhibited pronounced yielding (b) as a relationship between the ratio of
when the elevated temperature flow stress the elevated temperature proof stress to the
fell to a value equal to the applied stress on yield stress at 20 °C (ax) and temperature,
the specimen. However, the magnitude of where x can be represented by plastic strains
the yield strain was not consistent from of 0.2, 1.0, 2.0 or 5.0%.
one steel type to another, and this was Considering each approach in turn:
attributed to differences in microstructure It can be seen from the test curves that,
arising from the various mill production depending upon the magnitude of the applied
processes that are used to roll the current stress, certain levels of strain are attained

Heating
Rate
= 10°C/min
II
I Applied = 250, 200, 150,
1.6 Stress 100,250 , 25
N/mm

1.2

=-

250 N/mm 2
~ 0.8

25 N/mm 2
0.4

00 200 400 600 800


Temperature, °C
Fig. 2. Tensile curves for a Grade 4 3 A steel derived f r o m t r a n s i e n t tests.
3O

2.0
Heating = 10°C/min
Rate

Applied = 350, 300, 250


Stress 200, 150, I00
50, 25, N/mm z
1.6

1.2

~" 350 N

r/? jJ
0.8

o.4

25 N/mm 2

Oo 200 400 600 800


Temperature, °C
Fig. 3. Tensile cu~es for a Grade 50B steel derived from transient tests.

at specific temperatures. Therefore, by curves of p r o o f stress ratio, ax, pl ot t ed as


selecting discrete temperatures a set of a function of temperature. These again were
stress/strain curves can be derived for each derived for a heating rate of 10 °C/min and
grade of steel. In the case of a heating rate have been corrected to record only the
of 10 °C/min {equivalent to a 1-h standard plastic strain, cpl. Use of the dimensionless
fire resistance test), these data are presented ratio, a x , allowed a single, best-fit line to
in Tables l ( a ) and l ( b ) for the samples of be drawn for bot h Grade 43A and 50B
BS4360: Grades 43A and 50B steel respec- steels.
tively. Measurements made during standard fire
It is possible to use the data at very low resistance tests on steel beams in t he U.K.
strains in Tables l ( a ) and l ( b ) , to calculate have indicated t h a t a local strain of approx-
effective Young's or tangent moduli. When imately 2 - 3 % is attained at the centre of
compared with other published information, the tensile flange when the deflection reaches
these values appear to be conservative. This the limiting value of 1/30 {span). Strains
is almost certainly due to the test m e t h o d of the order of 1% may also be experienced
and it could be argued that the moduli in column sections towards the latter stages
derived from the present tests are more of a fire test. Inspection of Figs. 2 and 3
relevant when considering the behaviour of indicates that once a strain of about 1% is
hot-rolled, cold-straightened, structural steel exceeded, a 'runaw ay' situation is entered
sections in a fire. and while strains of this order in the centre
The alternative m e t h o d of presenting of a beam or in a column would n o t cause
the data is illustrated in Fig. 4 as a series of collapse, imminent failure could be e x p e c t e d
Z ~ ~ O O o o 0 0 0 0 0 o O o O ~ O 0 0 0 0 0 ~ O 0 0 0
. . . . . 0 , o , o . . . . . o o , o o o o o o o o o o o o o
0

.m

o o o ~ o o o o o o o o o o ~ w o ~ ~ o

~ •

°.


q~

0 C
~D

~r
~D

II

o
32

o~ 0

II

0~
o

o
-~J U')

o ~a

0
"0 E 0
E'~

'0
o
0

o ° ° . . . . . . . . . . . . . . . . . ~

0
u

E
Z

o . . . . . . • . . . . . . . . . .~
C~

"0

cO

O~
0:

0~
~0

0 o. -o . . . . . . . . . . . . . .~ .

° ° . . . . . . . . . , . . . . . . . . . . . . . . . . . . . 0
0 0 0 o o o o ~ o 0 0 o 0 0 o o 0 o o 0 0 o o o o ~ ~ Z
i 33
1.o \ %
ao.2
M \ \ 1 oo
I %%%~%\ a2.0
0.8 " a5.0

.,~ -~ 0 6

au.~ \ \%'.

"%,,,
NE

~ 0

I I 1 I I I I I I I
0
200 400 600 800 1000
Temperature, °C
Fig. 4. a0.2, al.0, a2:0 and as.0 versus t e m p e r a t u r e for B S 4 3 6 0 : Grades 4 3 A and 5 0 B structural steels d e t e r m i n e d
from tensile tests c o n d u c t e d under transient heating c o n d i t i o n s .

with a relatively small further rise in tem- Similar analyses of the results obtained
perature. For these reasons, the use of the for other heating rates, namely, 2.5, 5 and
a l.0 factor is advocated to derive flow stress 20°C/min, demonstrated a small heating
data for use in fire engineering calculations rate dependence upon the limiting tem-
as this parameter reflects the behaviour of perature for steel. This has been observed
steel sections in fire, near their limit of struc- by other workers [3, 4, 8] and by taking
tural stability. into account their data, adjustments can be

600
UTS.... -.."'"
~ . ~ ........ "'. "'..
, /:/" ~. ""...
".... , J l ' 5 . o~ Ps '\',.
.- / I'-', ",,".
"'--" I ~..... k."'.
400 /2.~s ~ ~ \'...
/ / -\ ~ .,'...
z -.L.._/'1_O% PS ~ \',:'.
- ~ -. \ ~ (Bs..9)
~ ~N~" Maximum design stress
~200 0.2%. PS ~ ~'.k
%''. in tension, 165 Nlmm 2

I I I I I I I I
O0 200 400 600 800
Temperature, °C
Fig. 5. Elevated t e m p e r a t u r e strength properties o f a t y p i c a l B S 4 3 6 0 : Grade 4 3 A structural steel derived f r o m
steady-state tests.
34

made to the temperature at which 1% strain 3.2. Tests under steady-state heating condi-
is attained relative to a heating rate of 10 °C/ tions
min, by using the following factors: Figures 5 and 6 illustrate data for Grades
43A and 50B structural steel derived from
20 °C/min +15 °C
steady-state tensile tests conducted over the
5 °C/min - - 1 5 °C temperature range 20 - 800 °C. In addition,
2.5 °C/min - - 2 5 °C Figs. 7 - 1 0 show the extent of scatter in

600

.
""'.....
- UTS ...........
.... .
--.__~:'~'--''- ...
• 5.0~ PS " ~ ."'.

Z o.~, PS
0.2~ ,s~~k~: k \.'..
(Bs449)
Maximum design stres@
in tension, 230 N/mm
w
200
4m
in

0 I I I I I I I !
0 200 /400 600 8O0
Temperature, °C
Fig. 6. Elevated t e m p e r a t u r e strength properties of a typical BS4360: Grade 50B structural steel derived f r o m
steady-state tests.

¢q
300

f "~
"X

x\
\

X
\ Steady state tests
~ X X
200 ~-
~.'-. '& ~ (Bs449)
~ ~'~,'.x X% M a x i m u m design stres~
~.~ ~ %\ in tension, 165 N/ram~
0

~. 100 Minimum line ~ §\


c~ from transient ~k~ ~'X
~ -x~

|
0 T ~ I I I I I I O
400 600 800 1000
Temperature, °C
Fig. 7. Relationship b e t w e e n t e m p e r a t u r e and 0.2% p r o o f stress for BS4360 : Grade 43 structural steels.
35

4oo

X %%
%
\
\
c~ \
\
300 -~ \ / Steady state tests
Z

x ', \ Maximum design stress


\ \ in tension~ 230 N/mr,2
oo 200 ~%%k x\\

c4
d

IO0 Minimum line fro/on ~"X~t~v%.


transient tests ~X~ ,

~<'.I "~-..
-~--._~___~
~_~. , , , , , ,

o ~ - o4 0 600 800 1000


Temperature, °C
Fig. 8. Relationship between temperature and 0.2% proof stress for BS4360 : Grade 50 structural steels.

30o ×~ \\\
c~
x x \\
"<.~ ~\ ~teo~y state tests

\ (BS 449 )
o -- %~ ---~ - - Maximum design stres~
~ ~ in tension, 165 N/ms z

• 1oo Minimum l i n e
transient tests
~rom~
~" %
.,%
o ~ I I I I I I I
0 400 600 800 1000
Temperature, °C
Fig. 9. Relationship between temperature and 1.0% proof stressfor BS4360 : Grade 43 structuralsteels.
36

4oo
X\
\
Xx \ \
~k \\ Steady state tests

~.3oo
\
\
C~
\ (BS449)
Maximum d e s i g n stress
\ i n t e n s i o n , 2 3 0 N/mm 2
\
o200
p..,
g-

M i n i m u m line f r o m >
t r a n s i e n t tests \k.
100
\

C ~ I I I I I I I
400 600 800 1000
T e m p e r a t u r e , °C
Fig. 10. R e l a t i o n s h i p b e t w e e n t e m p e r a t u r e a n d 1.0% p r o o f stress for B S 4 3 6 0 : G r a d e 50 s t r u c t u r a l steels.

the 0.2 and 1.0% proof stress parameters superimposed on Figs. 7 - 1 0 . Comparison
between 400 - 1000 °C, for a wide range of of the effect of temperature on the 0.2%
Grade 43 and Grade 50 steels with signifi- proof stress, Figs. 7 and 8, shows that the
cantly different ambient temperature yield minimum values obtained from transient
stress values. The results clearly demonstrate tests are significantly below the lower limit
that, under steady-state conditions, the of the scatter band of results obtained under
maximum permitted design stresses in ten- steady-state conditions. However, when a
sion, according to BS449, (165 and 230 N/ similar comparison is made for the 1.0 proof
mm 2 for Grades 43A and 50B respectively) stress, Figs. 9 and 10, there is good agree-
would not exceed the 0.2% proof stress of ment between the two modes of testing.
the steels until temperatures in excess of Therefore, while the stress/strain curves
500 °C were reached. However, as stated derived from transient and steady-state tests
earlier, these tests were carried out at con- are dissimilar at low strains, when the strain
stant temperature and, therefore, w i t h o u t approaches values corresponding to the
reference to similar steels assessed under limits of deflection or instability in a stan-
transient conditions, they could possibly dard fire resistance test, then the data derived
give rise to misleading answers when used from either type of test can be used to
in a fire engineering analysis. predict limiting temperatures.

3.3. Comparison o f data


Curves for transient test data derived from 4. C O N C L U S I O N S
Fig. 4, in which minimum yield stress values
of 255 and 355 for steel Grades 43A and An extensive testing programme has been
50B respectively are assumed, have been carried out on BS4360: Grades 43A and 50B
37

steels t o p r o v i d e e l e v a t e d t e m p e r a t u r e d a t a ACKNOWLEDGEMENT
f o r s t r u c t u r a l fire engineering design applica-
T h e a u t h o r s wish to t h a n k D r R. B a k e r ,
tions. T h e d a t a are also o f use w h e n p l a n n i n g
Director of Research and Development,
the h o t f o r m i n g o p e r a t i o n s f o r large f a b r i c a -
British Steel C o r p o r a t i o n , f o r p e r m i s s i o n
tions.
t o p u b l i s h this p a p e r .
F r o m t h e tests c o n d u c t e d u n d e r t r a n s i e n t
h e a t i n g c o n d i t i o n s , a series o f stress/strain REFERENCES
curves have b e e n d e r i v e d f o r t h e t e m p e r a t u r e
1 J. Glen, J. West o f Scotland Iron and Steel Ins-
r a n g e 20 - 9 0 0 °C. T h e results o f t h e s e tests
titute, 65 (5) (1958) 41 - 191.
w e r e also a n a l y s e d to d e m o n s t r a t e t h e in- 2 J. Ruge and O. Winkelmann, Materialpruf, 19 (8)
f l u e n c e o f t e m p e r a t u r e o n t h e p r o o f stress (1977) 295 - 299.
ratio, ax, f o r plastic strains o f 0.2, 1.0, 2.0 3 J. Ruge and O. W i n k e l m a n n , Brandvershatten yon
a n d 5.0%. A c o m b i n a t i o n o f the p r e s e n t Bauteilen, Sonderforschungsbereich 148, Arbeits-
bericht 80, 1978, Part II, Braunschweig, June,
results a n d p u b l i s h e d d a t a has a l l o w e d rules
1980, pp. 147 - 192.
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be m a d e f o r d i f f e r e n t h e a t i n g rates. Institute TNO for Building Materials and Building
C o m p a r i s o n o f t h e results derived f r o m Structures, Delft, October, 1972.
t h e t w o m o d e s o f t e s t i n g d e s c r i b e d earlier 5 L. Twilt, Proc. CIB/RILEM Symposium on Ma-
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d e m o n s t r a t e t h a t p r e d i c t i o n s using d a t a f r o m
6 J. Witteveen and L. Twilt, On the behaviour of
s t e a d y - s t a t e tests o n t h e b e h a v i o u r o f struc- steel columns at elevated temperatures, Proc.
t u r a l s t e e l w o r k in fires are o p t i m i s t i c , w h e n Colloquium on Column Strength, International
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w h e n c o n s i d e r i n g strains a p p r o a c h i n g ' r u n - ing, Paris, 1972.
a w a y ' values, t h e r e is s o m e j u s t i f i c a t i o n in 7 D. H. Skinner and A. G. Stevens, Report MRL
6/8, Broken Hill Proprietary Co. Ltd. (BHP),
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c e d u r e t o p r e d i c t t h e b e h a v i o u r o f steel 8 D. H. Skinner, BHP Tech. Bull., (2) (November)
e l e m e n t s in fire. (1972) 22 - 37.

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