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Operating manual
Filling station
type FS-D
Table of contents
I. STRUCTURE OF THE MANUAL / CLARIFICATION ................................................................ 3
II. SAFETY AND HEALTH CONCERNS ...................................................................................... 4
1 INTRODUCTION ................................................................................................................ 5
1.1 Use of the FS-D Filling station .................................................................................................... 5
2 FS-D FILLING STATION GENERAL ....................................................................................... 6
3 OPERATING PROCEDURE OF THE FS-D FILLING STATION .................................................... 7
3.1 Open Dewar................................................................................................................................ 7
4 TROUBLE SHOOTING OF THE FS-D FILLING STATION .......................................................... 8
5 MAINTENANCE OF A FS-D FILLING STATION ...................................................................... 9
6 INTERVALS AND SCOPE OF INSPECTION OF SAFETY FACILITIES. ......................................... 9
HINT
Offers suggestions/advice to the operator in order to perform certain tasks more easily.
NOTE
CAREFUL
Indicates damage to the system or directly linked equipment when the operator does not carefully
adhere to the procedures.
WARNING
Warns the operator of possible injuries if the procedures are not adhered to properly.
PERIL TO LIFE
WARNING
The operator is responsible for the safety of any assisting employee. The operator must ensure, before
starting the machine or application, that no dangerous situation can occur for the assisting employee.
NOTE
This user manual must be read by the operator as soon as possible in order for him to become familiar
with the operation of this equipment.
From the point of view of injuries to the operator, specific attention is given to the dangers that can
occur when using liquid nitrogen. On Demaco Holland bv equipment, where the operator may come
into contact with liquid nitrogen, you can find the label as shown below. It warns the operator of the
presence of coldness and it is indicated that safety glasses and gloves with wrist protection should be
worn.
This user manual should at least be available for consultation at the head of the department. We
recommend that a copy be made of this manual inserted in plastic folders, or bound, and put on view at
location with the control cabinet.
We also recommend to carefully read the Demaco safety instruction “Safety guidelines for working with
cold media”. Extensive information is provided in this manual about working with cryogenic media. A copy
of the “safety instruction” is shipped with this delivery. Should you require more copies of this instruction in
order to create a save working environment for your operator(s), additional copies can be requested from
Demaco Holland bv. Contact our sales department.
1 INTRODUCTION
1.1 Use of the FS-D Filling station
The FS-D Filling station is used to fill open Dewars with liquid nitrogen in a safe, cost- effective and
reliable way.
The connections are located at the backside of the FS-D Filling station.
Connect the LN2 IN (liquid nitrogen inlet) to the liquid nitrogen supply line.
Connect the safety valve blow off to a safe direction.
Check the tightness of the threaded connections before the start up and in cold conditions.
Mounting
The FS-D Filling station must be attached firmly to the ground with 4 anchors M12.
The FS-D Filling station is designed for outside air temperature between 0 °C and + 50 °C.
The FS-D Filling station must be protected from traffic loads or collisions using proper obstacles such
as concrete poles or a steel frame.
Identification
Information about the FS-D Filling station is given on the back of the column.
WARNING
The operator has to wear leather safety gloves (also covering the wrist), safety glasses or face shield and a
leather apron at all times.
For open Dewar filling a filling hose is available. The operator of the filling station is responsible for not
overfilling a Dewar. The operator first has to put the filling hose in the Dewar and make sure the hose cannot
fall out of the Dewar during filling. Filling starts by pressing the filling button. The filling valve opens and
nitrogen starts flowing. When the filling button is released the filling valve will close immediately. When the
Dewar is full the operator must release the filling button. In case of an emergency, the control box is provided
with a quick-stop. This stop will shut down immediately the entire filling system.
HINT
WARNING
Before operating the system the operator must read this manual, and must make himself familiar with
the equipment. The operator must be familiar with working with cryogenic liquids, and he must be
familiar with working with the Dewars to be filled. The operator must have read and understood the
safety guidelines and operating guidelines of Demaco Holland bv, the Dewar supplier and the liquefied
gasses supplier. Failing to do so may lead to severe injury.
WARNING
A Dewar containing liquid nitrogen must be positioned firmly. A tilting Dewar may spill liquid nitrogen,
causing severe injury. Read to the documentation of the Dewar supplier for proper handling of the Dewar.
3. Put the filling hose in the Dewar to be filled. Make sure the hose is held firmly, and can not be blown
out of the Dewar due to forces created by the flow of nitrogen.
WARNING
Failing to hold the filling hose firmly may lead to liquid nitrogen spilling around, causing severe injury. Wear
protective gloves, glasses and clothing at all times.
PERIL TO LIFE
During filling nitrogen gas will form. This gas is odourless and colourless. Inhaling this gas may lead to
asphyxiation. Make sure proper ventilation is present or use an independent breathing device.
6. When the filling button is released the filling valve will close, and the filling will stop.
7. Remove the filling hose from the Dewar.
WARNING
Because a small amount of liquid nitrogen may still be available in the filling hose, liquid nitrogen may poor
out of the open end of the filling hose. This may lead to severe injury when touching skin or eyes. Always
wear protective gloves, glasses and clothing.
8. The hose can be placed back in the original position and the filling station is ready for filling the next
Dewar.
WARNING
Don’t leave the hoses loose on the floor, as someone may stumble and fall causing injury.
WARNING
Before working on the system, make sure no nitrogen or nitrogen pressure is available in the supply
system!
The quick stop will shut down the FS-D Filling station completely. Trouble shooting is easy and can be
performed using commonly available tooling and equipment. Documentation of the controllers can be
found in the databook..
1. Check that power is available.
2. Check all electrical components. A description of the components is available in the Demaco databook
for reference.
3. Check (by listening) whether the valves open and close when actuated.
4. Make sure the system is warm and empty before working on the system. Replace any malfunctioning
component and test.
WARNING
During some parts of this maintenance check the system must be operational. Therefore all safety
requirements noted in this manual must be met.
Fully check the system at least once every six months by operating the equipment and checking the
following:
1. Check that the light is glowing corresponding with this manual; replace the broken light.
2. Check the quick stop by operating the stop during filling. Make sure the systems stops.
3. Check for proper operation of the system. Check that all controls are operational and that the valves
are working properly.
4. Check the hoses for cracks and leakages. Check that the braiding is solid and shows no signs of wear.
Cracked, leaking hoses, or hoses with braiding-wires sticking out must be replaced.
5. Check all electrical connections. Connections that show signs of chafing, bare wires or other signs of
wear must be replaced.
6. Report and repair any malfunction.
7. Clean the FS-D Filling station periodically using a cloth.
8. Check if the opening of the safety valve is free of any obstacles.
Operating manual
Filling station
type FS-V
Table of contents
I. STRUCTURE OF THE MANUAL / CLARIFICATION ................................................................ 3
II. SAFETY AND HEALTH CONCERNS ...................................................................................... 4
1 INTRODUCTION ................................................................................................................ 5
1.1 Use of the FS-V Filling station ..................................................................................................... 5
2 FS-V FILLING STATION GENERAL ....................................................................................... 6
3 OPERATING PROCEDURE OF THE FS-V FILLING STATION .................................................... 7
3.1 Closed Dewar.............................................................................................................................. 7
4 TROUBLE SHOOTING OF THE FS-V FILLING STATION .......................................................... 9
5 MAINTENANCE OF A FS-V FILLING STATION .....................................................................10
6 INTERVALS AND SCOPE OF INSPECTION OF SAFETY FACILITIES. ........................................10
HINT
Offers suggestions/advice to the operator in order to perform certain tasks more easily.
NOTE
CAREFUL
Indicates damage to the system or directly linked equipment when the operator does not carefully
adhere to the procedures.
WARNING
Warns the operator of possible injuries if the procedures are not adhered to properly.
PERIL TO LIFE
WARNING
The operator is responsible for the safety of any assisting employee. The operator must ensure, before
starting the machine or application, that no dangerous situation can occur for the assisting employee.
NOTE
This user manual must be read by the operator as soon as possible in order for him to become familiar
with the operation of this equipment.
From the point of view of injuries to the operator, specific attention is given to the dangers that can
occur when using liquid nitrogen. On Demaco Holland bv equipment, where the operator may come
into contact with liquid nitrogen, you can find the label as shown below. It warns the operator of the
presence of coldness and it is indicated that safety glasses and gloves with wrist protection should be
worn.
This user manual should at least be available for consultation at the head of the department. We
recommend that a copy be made of this manual inserted in plastic folders, or bound, and put on view at
location with the control cabinet.
We also recommend to carefully read the Demaco safety instruction “Safety guidelines for working with
cold media”. Extensive information is provided in this manual about working with cryogenic media. A copy
of the “safety instruction” is shipped with this delivery. Should you require more copies of this instruction in
order to create a save working environment for your operator(s), additional copies can be requested from
Demaco Holland bv. Contact our sales department.
1 INTRODUCTION
1.1 Use of the FS-V Filling station
The FS-V Filling station is used to fill liquid nitrogen transport vessels (Dewars) with liquid nitrogen in a
safe, cost- effective and reliable way.
The connections are located at the backside of the FS-V Filling station.
Connect the LN2 IN (liquid nitrogen inlet) to the liquid nitrogen supply line.
Connect the GN2 OUT (gaseous nitrogen outlet) to a blow off line.
Connect the safety valve blow off to a safe direction.
Check the tightness of the threaded connections before the start up and in cold conditions.
Mounting
The FS-V Filling station must be attached firmly to the ground with 4 anchors M12.
The FS-V Filling station is designed for outside air temperature between 0 °C and + 50 °C.
The FS-V Filling station must be protected from traffic loads or collisions using proper obstacles such
as concrete poles or a steel frame.
Identification
Information about the FS-V Filling station is given on the back of the column.
WARNING
The operator has to wear leather safety gloves (also covering the wrist), safety glasses or face shield and a
leather apron at all times.
Closed Dewar filling starts by connecting the fill hose and the return hose to the Dewar. The filling hose is
used for filling the Dewar with liquid nitrogen and the return hose is used for leading the nitrogen gases
to a safe area. The return line is equipped with a temperature sensor inside the housing. This
temperature sensor detects whether the Dewar is full. The filling valve will be closed automatically.
The system will shut down when the temperature sensor is malfunctioning. In case of an emergency, the
control box is provided with a quick-stop. This stop will shut down the entire system.
HINT
The quick stop button shuts down the entire system.
WARNING
The temperature of the gas blowing out of the FS-V Filling station may be as low as -196 C. The position
of the GN2outlet and the direction of the gas flow should be chosen in such a way that there is no danger
for people or vulnerable equipment. Secondly large ice build-ups are possible without proper insulation.
PERIL OF LIFE
When the outlet of the FS-V Filling station is exhausting in a confined space, danger of suffocation exists.
This being because the amount of nitrogen from the FS-V Filling station can displace the air (oxygen)
from the space. In this case exhausting the gas to a safe remote atmosphere is necessary.
WARNING
Before operating the system the operator must read this manual, and must make himself familiar with
the equipment. The operator must be familiar with working with cryogenic liquids, and he must be
familiar with working with the Dewars to be filled. The operator must have read and understood the
safety guidelines and operating guidelines of Demaco Holland bv, the Dewar supplier and the liquefied
gasses supplier. Failing to do so may lead to severe injury.
WARNING
Make sure the connection of the Dewar is the same type and size of coupling as provided on the hoses.
During filling pressure will be available in the system. When a coupling is not connected properly, liquid
nitrogen may be spilled, causing severe injury when touching skin or eyes.
WARNING
Make sure the fill hose and the return hose are connected properly to the connections of the Dewar.
When the hoses are interchanged, the Dewar will not fill, but will empty the containing liquid nitrogen
through the return hose very quickly. The filling will stop automatically, but will not prevent a considerate
amount of liquid nitrogen blowing through the return hose. Refer to the specifications of the blow off line
whether this line is capable of withstanding liquid nitrogen.
4. When the connections are secured the start filling button can be pressed, the light turns off.
5. The filling valve will open and the Dewar starts filling. Immediately after start filling, nitrogen gas will
flow from the return line. This will make some noise. Don't let this frighten you. As soon as the Dewar is
cold, the gas flow will reduce, and the noise will decrease. The amount of noise is depending on the
type, size and temperature of the Dewar.
6. When the temperature sensor in the degas unit detects liquid nitrogen or the operator pushes the stop
button, the filling valve will be closed. The light will glow.
7. Make sure the filling sequence has stopped and close the valves on the Dewar.
8. Press the relief button, the pressure in the hoses will be relieved.
9. Disconnect the return line from the Dewar
WARNING
Always beware of the possibility that nitrogen at cryogenic temperatures may be present while
disconnecting the hose. This may lead to severe injury when touching skin or eyes, therefore always wear
protective gloves, glasses and clothing. Only after all pressure is relieved the hose may be completely
disconnected from the Dewar.
WARNING
Always beware of the possibility that nitrogen at cryogenic temperatures may be present while
disconnecting the hose. This may lead to severe injury when touching skin or eyes, therefore always wear
protective gloves, glasses and clothing. Only after all pressure is relieved the hose may be completely
disconnected from the Dewar.
WARNING
Because a small amount of liquid nitrogen may still be available in the filling hose, liquid nitrogen may
poor out of the open end of the filling hose. This may lead to severe injury when touching skin or eyes.
Always wear protective gloves, glasses and clothing.
11. The hoses can be placed back in their original position and the FS-V Filling station is ready for filling the
next Dewar.
WARNING
Don’t leave the hoses loose on the floor, as someone may stumble and fall causing injury.
12. When no more filling is required, switch off the main power.
WARNING
Before working on the system, make sure no nitrogen or nitrogen pressure is available in the supply
system!
The quick stop will shut down the FS-V Filling station completely. Trouble shooting is easy and can be
performed using commonly available tooling and equipment. Documentation of the controllers can be
found in the databook..
1. Check that power is available.
2. Check all electrical components. A description of the components is available in the Demaco databook
for reference.
3. Check the temperature sensors (Pt100). A malfunction of this sensor (broken wire or short circuit) will
shut down the FS-V Filling station.
4. Check (by listening) whether the valves open and close when actuated.
5. The sensor at the exhaust line is a special (5-wire) Pt100. This sensor detects liquid nitrogen droplets
that enter the exhaust line when the Dewar is full. The controller is factory adjusted to stop filling when
this Pt100 reaches –183 °C.
6. Make sure the system is warm and empty before working on the system. Replace any malfunctioning
component and test.
WARNING
During some parts of this maintenance check the system must be operational. Therefore all safety
requirements noted in this manual must be met.
Fully check the system at least once every six months by operating the equipment and checking the
following:
1. Check that the light is glowing corresponding with this manual; replace the broken light.
2. Check the quick stop by operating the stop during filling. Make sure the systems stops.
3. Check for proper operation of the system. Check that all controls are operational and that the valves are
working properly.
4. Check the hoses for cracks and leakages. Check that the braiding is solid and shows no signs of wear.
Cracked, leaking hoses, or hoses with braiding-wires sticking out must be replaced.
5. Check all electrical connections. Connections that show signs of chafing, bare wires or other signs of
wear must be replaced.
6. Report and repair any malfunction.
7. Clean the FS-V Filling station periodically using a cloth.
8. Check whether the opening of the exhaust valve/piping and the opening of the safety valve is free of any
obstacles.
Table of contents
1 INTRODUCTION ................................................................................................................ 3
2 SOFTWARE INSTALLATION ON YOUR PC ........................................................................... 3
3 START UP ......................................................................................................................... 3
4 COMMUNICATION VIA USB .............................................................................................. 4
5 COMMUNICATION VIA ETHERNET .................................................................................... 7
6 EXPORT DATA TABLES ...................................................................................................... 9
1 INTRODUCTION
In this quick guide will be explained how to import data-tables from the OPLC (Vision) to your PC.
Install the latest programming software Visilogic from the Unitronics download tab:
http://www.unitronics.com/Content.aspx?page=Downloads&CatId=4
3 START UP
Select the correct OPLC as default. In our case it will be the V570-57-T20B and confirm with OK.
Go to the command bar to establish the connection between the OPLC and PC.
Install the USB driver at the USB-Installation tab by clicking the “Install USB Driver” button in the Step 1
box.
Make sure you have selected the correct COM port. To confirm the correct COM port always verify with
the “Get OPLC Information” button.
If the correct COM port is applied the software will read out the OPLC. If not, try another COM port.
Connect the OPLC to the network with an Ethernet cable (RJ45) (not in scope Demaco)
Select TCP/IP (Call) and apply the correct project settings in the project setting dialog.
If other default settings are required the software of the OPLC needs to be reprogrammed.
The IP address and the OPLC name are variable, for reprogramming they need to be created by your
system administrator.
Reprogramming is recommended to be executed by Demaco. The required software update can either be
uploaded by Demaco or by the customer using the free Unitronics Utilities on the Unitronics website
http://www.unitronics.com
For reprogramming by Demaco the IP address and the OPLC name need to be forwarded to Demaco.
Select at the left side the Table you like “USERS” or “DISPTIMES”.
Then select the table with the “Select All” button see below:
Now the conversion file is made in Excel format, ready you are.
Information Mode
Information Mode is a utility that is embedded in the operating system of the controller. Via
Information Mode, you can view data on the LCD screen, use the controllers keyboard to directly
edit data, and perform certain actions such as resetting the controller.
You can enter Information Mode at any time without regard to what is currently displayed on the
LCD screen.
Viewing data does not affect the controllers program. Performing actions, such as initializing the
controller , can influence the program.