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Construction and Building Materials 90 (2015) 36–43

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Construction and Building Materials


journal homepage: www.elsevier.com/locate/conbuildmat

Influence of different types of polypropylene fibre on the mechanical


properties of high-strength oil palm shell lightweight concrete
Ming Kun Yew a,⇑, Hilmi Bin Mahmud a, Bee Chin Ang b, Ming Chian Yew c
a
Department of Civil Engineering, Faculty of Engineering, University of Malaya, 50603 Kuala Lumpur, Malaysia
b
Centre of Advanced Materials, Department of Mechanical Engineering, Faculty of Engineering, University of Malaya, 50603 Kuala Lumpur, Malaysia
c
Department of Mechanical and Material Engineering, Lee Kong Chian Faculty of Engineering & Science, Universiti Tunku Abdul Rahman, Cheras 43000 Kajang, Malaysia

h i g h l i g h t s

 Polypropylene fibres enhanced the strength of oil palm shell lightweight concrete.
 PPTB1 of 0.5% fibre produced the highest compressive strength.
 Addition of 0.5% PPTB1 fibre achieved the highest tensile strengths.
 The highest residual compressive strength was found for 0.5% PPTB1 fibre.

a r t i c l e i n f o a b s t r a c t

Article history: This study aims to investigate the use of various polypropylene (PP) fibres with different aspect ratio and
Received 8 May 2014 geometry to enhance the mechanical properties of oil palm shell fibre-reinforced lightweight concrete.
Received in revised form 6 March 2015 The volume fractions (Vf) of 0.25%, 0.375% and 0.5% were studied for each fibre. As various PP fibres were
Accepted 12 April 2015
added into oil palm shell fibre reinforced concrete, the marginal density reduction was reported. The
Available online 16 May 2015
effectiveness of new types of PP fibres to increase the compressive strength at later ages was more pro-
nounced than at early age. It is found that low volume fractions of polypropylene twisted bundle (PPTB)
Keywords:
fibres are more effective in improving the flexural strength of OPS concrete compared to its splitting ten-
Lightweight concrete
Oil palm shells
sile strength. The average modulus of elasticity (E value) is obtained to be 13.4 GPa for all mixes, which is
Polypropylene fibres higher than the values reported in previous studies. An increase in the percentage third load compressive
Mechanical property strength of 0.5% PPTB fibre of up to 11% was reported. Hence, this new types of PP fibres is a promising
Density alternative solution to compensate lower mechanical properties for lightweight concrete.
Ó 2015 Elsevier Ltd. All rights reserved.

1. Introduction recycled concrete, recycled tyres, and recycled plastics, have been
successfully used in concrete [2–4]. Recently, a large amount of lig-
The current state of the structural lightweight aggregate con- nocellulosic wastes OPS is generated due to the increasing number
crete industry was born out of realization of sustainable construc- of plantations of oil palm trees in Malaysia, Indonesia, and Nigeria
tion. Development of sustainable structural lightweight concrete [5]. This waste is considered as one of the potential lightweight
construction using oil palm shell (OPSLWC) is due to the density aggregate (LWA) in the development of lightweight aggregate con-
limit of 2000 kg/m3 [1]. The utilization of industrial and agricul- crete (LWAC). It is reported that Malaysia contributed some
tural waste materials can be a breakthrough to make the industry 18.79 million tonnes of crude palm oil on approximately 5 million
more environmentally-friendly and sustainable. It has led to green hectares of land [6], making it a major producer of palm oil.
and sustainable construction to improve the environmental friend- Calculations show that 1.1 tonnes of shells, or 5.5% of the weight
liness of concrete by reducing the cost of construction materials of the fresh fruit bunch, is produced annually from each hectare
and waste management. The utilization of waste materials, such cultivated. There are many advantages of using OPS, especially
as natural pumice, vermiculite, shale, slate, oil palm shell (OPS), when the material cost is minimized by utilizing the waste OPS
fly ash, ground granulated blast furnace slag (GGBFS), silica fume, aggregate in construction. These include savings in reinforcement,
scaffolding, formwork and foundation costs. Furthermore, such
⇑ Corresponding author. Tel.: +60 3 79675203; fax: +60 3 79675311. concrete can be used for heat insulation, sound absorption,
E-mail addresses: davidyew@siswa.um.edu.my, yewmingkun@gmail.com better fire resistance, superior anti-condensation properties and
(M.K. Yew). increased damping [7].

http://dx.doi.org/10.1016/j.conbuildmat.2015.04.024
0950-0618/Ó 2015 Elsevier Ltd. All rights reserved.
M.K. Yew et al. / Construction and Building Materials 90 (2015) 36–43 37

Air-dry density of oil palm shell concrete (OPSC) varies in the Table 1
range of 1868–1988 kg/m3 with a corresponding 28-day compres- Chemical composition and physical properties of OPC.

sive strength of more than 40 MPa [8–13]. In a past studies, the Chemical composition (%) Physical properties
enhancement of mechanical properties of OPSC is dependent on SiO2 Fe2O3 CaO MgO Al2O3 SO3 LOI Specific Blain specific
the density, aggregate content, crushed or uncrushed particle size gravity surface area
of OPS and heat treatment on OPS aggregate [8–10]. Other factors (cm2/g)
include water-cement ratio and incorporation of cementitious 21.28 3.36 64.64 2.06 5.60 2.14 0.64 3.14 3510
materials (silica fume, fly ash and ground granulated blast furnace
slag). The influence of density on the compressive strength of OPSC
can be observed from previous studies [8–13]. Alengaram et al.
2.1.3. Water and superplasticizer (SP)
[14] showed that with a density of about 1900 kg/m3, a compres- Potable water to binder (w/b) ratio of 0.30 was used for all mixes. The SP used in
sive strength of 37 MPa with the addition of silica fume (SF) can this study was polycarboxylic ether (PCE) supplied by BASF, and complies with the
be produced. However, Yew et al. [10] reported that heat treatment ASTM C494/C494 M [23] specifications. The amount of SP was kept constant at 1.0%
of the cement weight in order to improve workability.
on OPS aggregate, having a density of about 1945 kg/m3 achieved
compressive strength of 49 MPa. Furthermore, Shafigh et al. [8,9]
2.1.4. Aggregate
have successfully produced compressive strength of up to Local mining sand was used as the fine aggregate. The specific gravity, fineness
53 MPa for a density of about 2000 kg/m3. It is generally known modulus, water absorption and maximum grain size were found to be 2.68 g/cm3,
that, high compressive strength of LWAC results in brittleness 2.72, 0.97% and 4.75 mm, respectively. A sand content of 960 kg/m3 was used in
and weak in tensile strength [15] and the density of LWAC is lim- all mixes.
Old OPS were used as the coarse aggregate in this study, indicating that they
ited to 2000 kg/m3 [1]. As a result of these characteristics, LWAC
had been discarded for more than six months. The old OPS were collected from a
could not support normal stresses and impact loads, where tensile local crude palm oil producing mill. The percentage of fibres for old OPS (less than
strength is approximately one tenth of its compressive strength. It 2%) has been selected as an aggregate, which improves contact between the mortar
can be seen from recent research that, OPSLWAC can be reinforced and OPS grains and thus increases the compressive strength of the concrete. The
advantages of using this aggregate in OPS concrete were reported by Shafigh
with discontinuous (steel, polypropylene and nylon) fibres to over-
et al. [8]. The OPS were washed and sieved using a 12.5 mm-sieve. The OPS aggre-
come high potential tensile stresses and shear stresses at critical gates retained in the sieve were collected and subsequently crushed using a
location in OPSLWC member [16–19]. However, the main disad- stone-crushing machine in the laboratory. The crushed OPS aggregates were sieved
vantage of adding steel fibres into OPSLWC in fresh state is its sig- using a 9.5 mm-sieve to remove OPS aggregates with sizes greater than 9.5 mm. The
nificant reduction in slump value and increased density. OPS aggregates were heat-treated at 60 °C over a period of 0.5 h using a
temperature-controlled laboratory oven. Once cooled to room temperature, they
Furthermore, the inclusion of polypropylene and nylon insignifi-
were weighed under dry room conditions and immersed in water for 24 h. Due to
cantly increased the mechanical properties of OPSC, particularly the high water absorption of OPS, it was subsequently air dried in the laboratory
for the tensile strength [17]. One innovative method to improve to attain a saturated surface dry (SSD) condition before mixing. The difference in
the mechanical properties of OPSC without reaching the density quality of the OPS surface between heat treatment and without heat treatment con-
dition was reported by Yew et al. [10] and shown in Fig. 1. The OPS content was set
limit is an addition of a new type of non-metallic fibre namely
constant at 330 kg/m3 for all mixes. The physical properties of the OPS used, are
polypropylene twisted bundle (PPTB). shown in Table 2.
This study is to access the effects of different types of PP fibre
and aspect ratio at various volume fractions of 0.25%, 0.375% and 2.1.5. Fibres
0.5% on mechanical properties of OPSC. The beneficial effects of The properties of different type of PP fibres are presented in Table 3. The three
new types of PP fibres are considered in the investigation on types of PP fibres are (i) polypropylene twisted bundle 1 (PPTB1); (ii) polypropylene
twisted bundle 2 (PPTB2) and (iii) straight polypropylene 1 (PPS1), respectively, as
fibre-reinforced oil palm shell concrete (FROPSC). To the best of
tabulated in Table 3.
the authors’ knowledge, so far there are no reports on the effects
of the different geometries (lengths and shapes) of PP fibres on 2.2. Mix proportions
the properties of OPSC incorporating fibres. In this study, the
mechanical properties of OPSFRC containing fibres at three differ- The proportions used for all mixes as described in Section 2.1. The volume frac-
ent percentages is evaluated and reported. The primary objective tion (Vf) of the fibres added to the concrete mix typically ranges from 0.1% to 3.0%
[24]. It is noted that fibres with a high Vf tend to ‘ball’ in the mix and create work-
of this study is to investigate the effects of PPTB fibres at various ability problems. Therefore, low volume fractions (60.5%) were used for the PP
volume fractions on the compressive strength of OPSFRC. The fibres in this study. The volume fraction of the PPTB fibres was set as 0%, 0.25%,
effects of different PP fibres on the splitting tensile strength, flexu- 0.375% and 0.5%. The amount of water and superplasticizer was kept constant for
ral strength, modulus of elasticity and residual compressive all mixes.
strength (RCS) are also investigated.
2.3. Test methods

The procedure used to mix the fibre reinforced concrete is detailed as follows.
2. Experimental details Firstly, the OPS and sand were poured into a concrete mixer and dry mixed for
1 min. Following this, the cement was spread and dry mixed for 1 min. The fibres
2.1. Materials were then distributed and mixed for 3 min in the mix, based on the volume fraction
specified above. Water and superplasticizer were then added with a mixing time of
2.1.1. Cement 5 min. Slump test was carried out prior to casting the specimens. The concrete spec-
The cement used in this study was ASTM type I ordinary Portland cement (OPC) imens were cast onto oiled moulds and a poker vibrator was used to decrease the
[20] with a specific gravity of 3.14 g/cm3 and Blaine’s specific surface area of 3510 amount of air bubbles in the mix. For each mixture, 150 mm  150 mm  150 mm
2
cm /g. The chemical compositions and physical properties of the OPC are given in cubes were used to study the compressive strength and ultrasonic pulse velocity
Table 1. A cement content of 520 kg/m3 was used for all mixes. (UPV) at 1, 3, 7, 28, 56 and 90 days. Two cylinders (diameter: 150 mm, height:
300 mm) were used to examine the modulus of elasticity. Three cylinders (diame-
ter: 100 mm, height: 200 mm) and three prisms of 100 mm  100 mm  500 mm
2.1.2. Mineral admixture were used to examine the 28-day splitting tensile strength and 28-day flexural
Silica fume (SF) is available in dry powder form and is procured from strength, respectively. The specimens were demoulded approximately 24 ± 2 h after
ScancemMaterials Sdn Bhd, Kuala Lumpur. The light gray, under the product name casting. The compression testing machine used was an ELE (Engineering Laboratory
‘‘Scancem’’ is available in 20 kg bags. The SF procured by the company satisfies all Equipment) with a load capacity of 3000 kN running of 3.0 kN/s in accordance to BS
the requirements of the International Standards; ASTM C1240 [21] and AS 3582 EN 12390-3:2009 [25]. Furthermore, RCS involves reloading the cube specimens for
[22]. The amount of densified SF at 5% of the cement weight was added as addi- further 3 cycles after reaching maximum value, the failure in the compression test
tional mineral admixture to enhance the mechanical properties of concrete. setting at 15% to ascertain the corresponding RCS.
38 M.K. Yew et al. / Construction and Building Materials 90 (2015) 36–43

(a) (b)

Fig. 1. Surface quality of OPS aggregates (a) with heat treatment and (b) without heat treatment.

Table 2 200
Physical properties of OPS aggregates. PPTB 1 PPTB 2 PPS1
180
Physical property OPS OPSa
y = -18.75x + 203.75
160 R² = 0.974
Maximum size (mm) 9.5 9.5
Specific gravity (saturated surface dry) 1.33 1.30

Slump (mm)
Compacted bulk density (kg/m3) 628 625 140 y = -17.15x + 202.85
R² = 0.9664
Water absorption (24 h) (%) 23.5 20.8
Aggregate impact value (%) 2.35 2.37 120

a
Heat-treated. 100 y = -14.5x + 200.5
R² = 0.9397
80

3. Results and discussion


60
0.000 0. 25 0 0 .3 7 5 0. 500

3.1. Workability (slump) Volume fraction of PP fibre (%)

Fig. 2. Relationship between different PP fibre volume fraction and slump.


Slump tests were carried out to determine the consistency of
fresh concrete. The use of fibres is well known to affect the work-
ability and flowability of plain concrete intrinsically [26]. In this respectively. The results indicate that, the PPS1/0.25-0.5 of shorter
study, the quantity of water and SP were kept constant for all length produced a lower slump in the range of 65–150 mm com-
mixes in order to evaluate the effects of different PP fibres on the pared to PPTB1/0.25-0.5 (90–160 mm) and PPTB2/0.25-0.5 (75–
workability of OPC. From Fig. 2, it can be seen that the slump value 155 mm), respectively. Mehta and Monteiro [26] reported that a
of fresh OPSC decreases due to an increase in PP fibre volume frac- slump value for structural lightweight concrete in the range of
tion. The addition of fibres from 0% to 0.25%, 0.375% and 0.5% for 50–75 mm is comparable to an equivalent value of slump of
PPTB1, PPTB2 and PPS1 reduces the range of slump values by 100–125 mm for NWC. This phenomenon might be attributed to
approximately 11.1–64.3%, 13.9–82.7%, and 16.7–95.8%, the shorter length of fibres have higher effective surface area for

Table 3
Properties of different type of polypropylene fibres and aspect ratio.

Fibre Fibre type Length (mm) Aspect ratio Specific gravity Tensile strength
(g/cm3) (MPa)
Monofilament-polypropylene twisted bundle 1 (PPTB1) 54 108 0.91 600

Monofilament-polypropylene twisted bundle 2 (PPTB2) 30 60 0.91 600

Monofilament-polypropylene straight 1 (PPS1) 20 40 0.91 600


M.K. Yew et al. / Construction and Building Materials 90 (2015) 36–43 39

the development of a fibre–matrix bond compared to longer fibres. concrete (NWC) taken as 2350 kg/m3, the ODD and DD for all light-
The bond increases the viscosity which restrains the mixture from weight mixes are approximately 22% and 16% lower than of ordi-
segregation and flow. The fibres have the tendency to absorb a nary concrete. Hence, there is substantial cost savings by
higher amount of cement paste to wrap around due to the high providing less dead load for LWC in this study.
fibre content and large surface area of fibres, which in turn,
increases the viscosity of the mixture [27]. Hence, PP fibres of 3.3. Compressive strength
shorter length and higher volume fraction produced lower
workability. The results of the compressive strength at different ages (1 d,
The results of Yap et al. [17] showed that the slump value 3 d, 7 d and 28 d) are presented in Table 4 for all mixes. From the
decreases upon addition of 0.5% Vf fibrillated (length: 19 mm, results of Table 4, the compressive strength of OPSC increased at
aspect ratio: 48) and multi-filament (length: 12 mm, aspect ratio: all ages with an increase in PP fibres volume fraction. It can be seen
240) polypropylene fibres into the OPS LWC. The reduction in that the early compressive strength of both OPSC and OPSFRC was
slump value was found to be 47% and 60%, respectively. Several achieved. It can be attributed to the addition of silica fume (SF)
studies attempted to overcome this problem by producing more which reacts with calcium hydroxide (CaOH) liberated from hydra-
workable concrete. This was achieved by determining the opti- tion of the cement to produce calcium silicate hydrates (C–S–H) to
mum content of sand and adding superplasticizer [28]. The addi- improve aggregate-cement paste interface of concrete and conse-
tion of superplasticizer improves the concrete’s flowability and quently minimizes the induction of micro-cracks. It has been
workability without segregation [29–32]. Campione et al. [33] reported that, not all types of lightweight aggregate are suitable
attained good workability in their mixtures by adding 1.5% of for production of HSLWC [35]. This investigation shows that the
superplasticizer by cement weight for pumice and expanded clay use of agriculture waste OPS aggregate for production of HSLWC
LWACs reinforced with steel fibres. As a general rule, a low amount is possible. Yew et al. reported that the use of heat treatment
of fibres is recommended to achieve good workability for fibre method on crushed OPS aggregate caused notable surface quality
reinforced concrete [34]. improvement and enhance adhesion between the OPS and cement
paste [10]. A slight increase in compression strength was observed
3.2. Hardened density at 130 °C for 6 h has also been reported elsewhere [36].
The 28-days compressive strength of the OPSC and OPSFRC var-
Two types of density (demoulded density (DD) and oven-dry ies between 41 and 47 MPa, which fulfilled the high-strength light-
density (ODD)) were measured for all mixes. The correlation weight concrete (HSLWC) requirements with respect to density
between the demoulded and oven-dry densities as a function of and strength [37]. It was found that the compressive strength of
fibre volume fraction is shown in Fig. 3. It can be observed that specimen PPTB1/0.5 showed the highest compressive strength
the concrete’s density decreases slightly with increasing fibre vol- compared to control specimen, with a percentage increase of
ume fraction, which is attributed to the fibres’ low specific gravity. 15.4% at 28-days. A comparison of the strength at early and later
All mixtures fulfilled the requirement of structural lightweight ages indicate that the rate of strength development was greater
concrete by having an ODD and DD within the range of 1835– as the age increased, especially for OPSC with higher PP fibres con-
1910 kg/m3 and 1897–1975 kg/m3, respectively. Newman and tent. From the results of Table 4, it can be seen that the mixes from
Owens [1] stated that, concrete with an oven-dry density (ODD) PPTB1/0.25 to PPTB1/0.5 increases the compressive strength by
of not greater than 2000 kg/m3 is defined as structural lightweight 5.9% and 10.0% at 1 d, 8.9% and 11.5% at 3 d, 7.0% and 10.6% at
concrete. This OPSFRC shows a close proximity value with the ODD 7 d, 6.4% and 10.9% at 28 d, respectively. It can be observed that,
reported in previous studies [18,19]. the OPSFRC with twisted bundle shape and higher aspect ratio pro-
The results showed that, the addition of different type and duced higher compressive strength as compared to the straight
geometry of PP fibres caused remarkable changes in the density fibres. It may be due to the twisted bundle shape fibres which have
reduction of OPSC. The inclusion of PPTB1, PPTB2 and PPS1 fibres good bond and anchorage in the matrix resulting in more strength.
produced density reduction in the ODD and DD of about 10– There is decrease in the strength with decrease in aspect ratio of
75 kg/m3 and 12–78 kg/m3, respectively. From Fig. 3, the mixes same shape of fibre. All the mixtures attained about 90–93% of
with PP straight shape fibres produced a lower ODD and DD than their 28 d compressive strength at the age of 7-days. In this study,
the PPTB1 and PPTB2 geometry (twisted bundle) fibres. At 0.5% the ratio of 1 d and 3 d strength to 28 d was 66–71% and 75–79%,
Vf, the PPS1 produced the lowest ODD and DD of about 1835 and respectively. Holm et al. reported [38] that the 7-day strength to
1897 kg/m3. In comparison to the density of normal weight 28-day strength ratio for HSLWC is between 86% and 92%.
Furthermore, Fujji et al. [39] also reported that this ratio for
PPTB1 (Demoulded) PPTB2 (Demoulded) PPS1 (Demoulded)
HSLWC was between 80% and 90%.
PPTB1 (Oven-dry) PPTB2 (Oven-dry) PPS1 (Oven-dry)
1990 Table 4
y = -10.25x + 1988.8 Compressive strength development of control concrete and OPSFRC under continuous
1970 R² = 0.9806 moist curing.
y = -10.7x + 1988.3
1950 R² = 0.99 Mix code Compressive strength (MPa)a
Density (kg/m³)

1930 1d 3d 7d 28 d
y = -10.1x + 1924.4
1910
R² = 0.9706 y = -12.3x + 1985.7 Control 28.9 (70.7%) 31.4 (76.7%) 38.1 (93.0%) 40.9
R² = 0.9714
PPTB1/0.25 28.6 (67.1%) 32.8 (77.1%) 39.3 (92.4%) 42.6
1890 PPTB1/0.375 30.3 (66.8%) 35.8 (78.9%) 42.1 (92.8%) 45.3
y = -10.85x + 1923.2
R² = 0.9915 PPTB1/0.5 31.4 (66.6%) 36.6 (77.5%) 43.5 (92.1%) 47.2
1870
PPTB2/0.25 28.9 (68.5%) 32.3 (76.6%) 39.0 (92.5%) 42.2
y = -12.4x + 1924.1 PPTB2/0.375 30.0 (66.5%) 35.5 (78.6%) 41.8 (92.6%) 45.1
1850 R² = 0.9942
PPTB2/0.5 31.2 (66.7%) 36.2 (77.3%) 43.3 (92.5%) 46.8
1830 PPS1/0.25 30.1 (71.2%) 31.9 (75.3%) 38.5 (90.9%) 42.4
0.000 0.250 0. 375 0.500
PPS1/0.375 29.8 (66.3%) 34.9 (77.6%) 41.6 (92.5%) 44.9
Volume fraction of PP fibre (%) PPS1/0.5 30.4 (65.3%) 36.1 (77.4%) 43.2 (92.7%) 46.6
a
Fig. 3. Relationship between different PP fibre volume fraction and density. The data in parentheses are percentage of 28 day compressive strength.
40 M.K. Yew et al. / Construction and Building Materials 90 (2015) 36–43

Fig. 4 shows the compressive strength development for OPSC 60


containing PP with different geometry and length. The results indi-

Compressive strength, fcu (MPa)


cate that control mix achieve saturated compressive strength after
50 fcu = 0.733 (Ut)2.9
28 d. It can be observed that, all mixes reinforced with different PP R2 = 0.97
and aspect ratio showed improvement of compressive strength as
the age increased (>28 d), especially for PPTB1/0.5 with highest
40
fibre content. As can be seen from Fig. 4, there is notable difference
between control and OPSFRC specimens containing different PP
fibres and aspect ratio pertaining to 56 d and 90 d compressive 30
strength increment. It was reported [17] that the OPSFRC with
nylon fibres showed consistent compressive strength and slightly
enhancement of about 3–6% compared to the control mix. 20
3.40 3.50 3.60 3.70 3.80 3.90 4.00 4.10 4.20
However, the results of the present investigation showed that
UPV (km/s)
OPSFRC containing different PP fibres and aspect ratio increases
the compressive strength significantly compared to the control Fig. 5. Relationship between the UPV and compressive strength up to 90 days.
specimen. The mixes from control to PPTB1/0.5, control to
PPTB2/0.5 and control to PPS1/0.5 at 28 d consistently increases inhomogeneity of concrete, as well as changes in concrete such
the compressive strength by about 4–15%, 3–14% and 4–14%, as deterioration due to aggressive chemical environment, freezing
respectively. This observation may be attributed to the higher ten- and thawing. It has been stated that concrete with UPV values
sile strength of different type of the new PP and aspect ratio com- within the range of 3.66–4.58 km/s are considered as concrete with
pared with other PP (fibrillated and multi-filament). In this study, ‘‘good’’ condition [43]. In general, it can be seen that the UPV of the
an increasing compressive loading will initiate and advance the control concrete and OPSFRC increased with increase in compres-
cracking on OPSC specimens. When the advancing crack sive strength and the values were found within the range of
approaches PP fibre, the debonding at the fibre–matrix interface 3.45–4.16 km/s. From the results, it is evident that the specimens
begins due to the tensile stresses perpendicular to the expected of different type of PP fibres have a positive effect on the UPV val-
path of the advancing crack. Once significant amount of tensile ues of OPSFRC. It was found that UPV can be correlated with its
stress was introduced in concrete, micro-cracks and subsequently corresponding cube compressive strength, as shown in Fig. 5, with
macro-cracks were formed [40–42]. This phenomenon showed a R2 value of 0.97. Eq. (1) is proposed to estimate the cube com-
that the addition of PP fibres improved aggregate-fibre-cement pressive strength based on the UPV values.
paste interface of the concrete and consequently increased the
f cu ¼ 0:733ðU t Þ2:9 ð1Þ
compressive strength.
where fcu represents the cube compressive strength (MPa) and Ut
3.4. Ultrasonic pulse velocity (UPV) represents the transverse ultrasonic pulse velocity (km/s).

The UPV is a non-destructive test method used to assess the 3.5. Splitting tensile and flexural strengths
quality of the concrete. This method can be used to estimate the
strength of concrete test specimens and also useful on-site where In this study, the low dosage of different type of PP fibres and
destructive strength test is not applicable. As shown in Fig. 5, rela- aspect ratio in concrete has positive effect on the splitting tensile
tionship between the UPV and the cube compressive strength was and flexural strengths. From the results of Table 5, the addition
measured at the ages of 1 d, 3 d, 7 d, 28 d, 56 d and 90 d. The UPV of different types of PP fibres enhanced both splitting tensile and
method can be used to detect internal cracking, voids and flexural strengths of OPSFRC. Furthermore, the increment of fibres

55
54
53
52
51
50
49
48
47
46
Compressive strength (MPa)

45
44
43
42
41
40
39
38
37
36
35
34 Control PPTB1/0.25 PPTB1/0.375
33
32 PPTB1/0.5 PPTB2/0.25 PPTB2/0.375
31
30 PPTB2/0.5 PPS1/0.25 PPS1/0.375
29
28 PPS1/0.5
27
26
25
0 20 40 60 80 100
Age (days)

Fig. 4. Development of compressive strength of control and OPSFRC.


M.K. Yew et al. / Construction and Building Materials 90 (2015) 36–43 41

Table 5
Mechanical properties of control concrete and OPSFRC.

Mix code Mechanical properties


Splitting tensile Flexural strength Modulus of elasticity
strength (MPa) (MPa) (GPa)
28 d
Control 3.10 5.45 11.64
PPTB1/0.25 3.35 7.05 12.68
PPTB1/0.375 3.85 7.12 13.62
PPTB1/0.5 4.12 7.64 15.36
PPTB2/0.25 3.42 6.43 12.55
PPTB2/0.375 3.68 6.67 13.39
PPTB2/0.5 3.95 7.09 14.82
PPS1/0.25 3.49 5.75 12.04
PPS1/0.375 3.54 5.97 13.25
PPS1/0.5 3.74 6.52 14.46
Fig. 6. Image of tested prism specimen – note the different type of PP fibres
bridging across the crack.
volume fraction had a significant effect on both splitting tensile
and flexural strengths. It can be seen that, the addition of different
types of PP fibres greatly increased the splitting tensile strength of
F - Flexural ST - Splitting Tensile
concrete. As found from this investigation, the addition of
PPTB1/0.25–0.5%, PPTB2/0.25–0.5% and PPS1/0.25–0.5% fibres PPTB1-F PPTB2-F PPS1-F PPTB1-ST PPTB2-ST PPS1-ST

enhanced the splitting tensile strength up to 8–33%, 10–27% and 8.00


y = 0.1211x + 1.8162
13–21% respectively compared to the control mix. On the other 7.50 R² = 0.7602 (PPTB1)

hand, the flexural strength of PPTB1, PPTB2 and PPS1 mixes pro- 7.00
28-day tensile strength (MPa)
duced significant improvement compared to the control concrete. 6.50 y = 0.1369x + 0.6117
R² = 0.9039 (PPTB2)
The flexural strength of PPTB1, PPTB2 and PPS1 increased with 6.00
an increase in fibres volume content. The average flexural strength y = 0.1739x - 1.6814
5.50 R² = 0.8766 (PPS1)
for PPTB1/0.25–0.5%, PPTB2/0.25–0.5% and PPS1/0.25–0.5%
5.00
increases by 7.3%, 6.7% and 6.1%, respectively. The addition of y = 0.1671x - 3.7518
4.50 y = 0.1114x - 1.295 R² = 0.9956 (PPTB1)
higher aspect ratio and twisted bundle shape of fibres provide R² = 0.9734 (PPTB2)
4.00
added strength to the fibre–matrix interface which carry part of
the applied load and the crack bridging effect as shown in Fig. 6. 3.50 y = 0.0559x + 1.0954
R² = 0.8129 (PPS1)
The content of fibres volume fraction used in this study is lower 3.00
42 43 44 45 46 47 48
compared to previous studies [17–19]. 28-day compressive strength (MPa)
However, PPS1 showed higher splitting tensile strength com-
pared to PPTB2 and PPTB1 at 0.25% volume fraction. It might be Fig. 7. Relationship between tensile strengths (splitting tensile and flexural
strengths) and compressive strength.
attributed to the lower aspect ratio (L/d) of PPS1 fibres exhibiting
higher effective surface area for the development of a fibre–matrix where ft and fcu represents the splitting tensile and cube compres-
bond compared to PPTB2 and PPTB1 fibres. Thus, the greater sur- sive strengths in MPa, respectively.
face area of PPS1 fibres was effective in transferring higher tensile An equation to correlate splitting tensile strength and compres-
stress compared to PPTB2 and PPTB1 fibres. The average splitting sive strength of OPSFRC is proposed in Eq. (4), whereby a higher
tensile and flexural strengths of PPTB1/0.25–0.5, PPTB2/0.25–0.5 coefficient of correlation is produced (accuracy = ±8%). Shafigh
and PPS1/0.25–0.5 mixes were found to be 22%, 19%, 16% and et al. reported that an accurate prediction of tensile strength of
33%, 23%, 12% higher, respectively than the control concrete. It concrete imperative in mitigating cracking problems, minimize
can be seen that, low fibre volume fraction (up to 0.375%) are more the failure of concrete in tension and increase shear strength pre-
effective in improving the flexural strength of OPSC compared to diction [45], is shown below:
splitting tensile strength. This phenomenon might be attributed
qffiffiffiffiffiffi
to the fibre geometry, which provides added strength to the matrix
f t ¼ 0:55 f cu ð4Þ
through reduces the stress concentration at the crack section and
improves the crack growth resistance [44] and consequently, Different equations have also been proposed to correlate flexu-
enhances the tensile strength of OPSFRC. ral strength to compressive strength of OPS LWAC by Alengaram
The linear relationship between tensile strength (splitting ten- et al. [46] in Eq. (5) and Yap et al. [17] in Eq. (6) for OPSFRC with
sile and flexural) and compressive strength for OPSFRC at the age PP and nylon fibres. A new equation, Eq. (7) is suggested for
of 28-day is correlated in Fig. 7. It can be observed that, the advan- OPSFRC with different PP fibres to predict the flexural strength
tage of PP fibres in the enhancement of tensile strength is more within ±12%.
evident in the OPSFRC with PPTB1 and PPTB2 compared to PPS1 qffiffiffiffiffiffi
fibres. It was stated that, different equations have been proposed f r ¼ 0:3
3 2
f cu ð5Þ
to correlate splitting tensile strength to compressive strength of
OPS LWAC by Shafigh et al. [45] and Yap et al. [17]. They predict qffiffiffiffiffiffi
3 2
splitting tensile strength based on the compressive strength of f r ¼ 0:385 f cu ð6Þ
OPSC and OPSFRC as shown in Eqs. (2) and (3):
qffiffiffiffiffiffi qffiffiffiffiffiffi
f t ¼ 0:4887 f cu ð2Þ f r ¼ 0:53
3 2
f cu ð7Þ
qffiffiffiffiffiffi
f t ¼ 0:52 f cu ð3Þ where fr and fcu are the flexural and compressive strengths in MPa,
respectively.
42 M.K. Yew et al. / Construction and Building Materials 90 (2015) 36–43

3.6. Modulus of elasticity (E) PPS1/0.5

PPS1/0.375
The modulus of elasticity (E) is an imperative test to assess the PPS1/0.25
material properties of concrete as it provides useful information on PPTB2/0.5
the ability of concrete to deform elasticity in the design of concrete
PPTB2/0.375
structures. From the results of Table 5, all OPSFRC have E in the

Mix
TLCS
PPTB2/0.25
range between 12.0 and 15.4 GPa. However, the control OPSC SLCS
mix without any fibres produced a MOE of 11.6 GPa. It can be seen PPTB1/0.5 FLCS

that, the 28-day MOE of the OPSC was found to increase with the PPTB1/0.375
addition of different types of PP fibres and aspect ratio as shown PPTB1/0.25
in Table 5. Similar finding for PP2 (multifilament) is reported by Control
Yap et al. [17]. The increase of the E for PPTB1/0.25–0.5, 0.00 10.00 20.00 30.00 40.00 50.00
PPTB2/0.25–0.5 and PPS1/0.25–0.5 mixes was in the range of 9–
Comparison of 1st, 2nd and 3rd load compressive strength at 28-days
32%, 8–27% and 3–24%, respectively. The addition of different types
of PP fibres caused improvement of MOE due to higher aspect ratio Fig. 9. Comparison of 1st, 2nd and 3rd load compressive strength at 28-days.
and geometry of fibres in arresting the original shrinkage cracks in
the concrete [47] and hence reduced the strain induced under
compression loadings, and consequently improved the E of
OPSFRC. strength values for second load compressive strength (SLCS) and
As seen from Fig. 8, a good relationship is established between E third load compressive strength (TLCS) further reduced to 67.7%
and compressive strength of concrete. The following three equa- and 39.0%, respectively. The percentage TLCS of PPTB1/0.5 mixes
tions is proposed for different type of PP fibres to relate the E produced the highest RCS values compared to PPTB2/0.5 and
and the cube compressive strength of OPSFRC. PPS1/0.5 with a value of 50.8%. It might be attributed to the higher
aspect ratio, geometry as well as content of PPTB1 fibres. Similar to
1=2
Et1 ¼ 7:49f cu  36:39 ð8Þ the previous observation, the crack bridging effect of fibres that are
existent at the crack face is capable of sustaining a higher
1=2
Et2 ¼ 6:20f cu  27:89 ð9Þ post-cracking to propagate further, compared to concrete with
low volume fraction of fibres. This indicates that, the addition of
Es1 ¼ 7:50f cu  36:86
1=2
ð10Þ fibres is expected to enhance the post-failure toughness of OPSC.
In general, all OPSFRC mixes produced high RCS and this indicates
where Et1, Et2, Es1 and fcu are the modulus of elasticity (GPa) of the imperative of this type of PP fibres in improving the
PPTB1, PPTB2 and PPS1 fibres and cube compressive strengths in post-cracking characteristics.
MPa, respectively.
4. Conclusion
3.7. Residual compressive strength (RCS)
The effects of incorporating different types of PP fibres and
The residual compressive strength (RCS) is a simplified method aspect ratio at low volume fractions up to 0.5% on the mechanical
to assess the residual strength toughness of concrete. The results properties of high-strength oil palm shell lightweight concrete
from first compressive strength are further loaded into residual have been investigated in this study. The following conclusions
strength for second and third compressive strength. The RCS pro- are drawn based on the experimental results:
vides a clearer comparison on the beneficial effects of different
type of PP fibres and volume fraction in enhancing the (1) PP fibres reduce the slump value of concrete. The reduction
post-cracking of OPSFRC. As seen from Fig. 9, the control specimen in slump value is within the range of 11–64% for different
of OPSC had the lowest RCS values as the specimen failed without type of fibres. However, the reduction in slump value is less
fibre–matrix bond when the initial compressive loading was than that for fibrillated and multi-filament PP fibres at sim-
applied on the cube specimens. The post-failure compressive ilar volume fractions.
(2) The addition of this type of PP fibres contribution to density
of concrete cannot be ignored, which reduces construction
cost in foundation design, erection and installation
15.6
15.4 PPTB1 PPTB2 PPS1 (3) The compressive strength of OPSC increases with an increase
15.2 in PP fibre content. Plain OPS concrete has a 28-day com-
15.0
14.8 E = 7.49fcu ½ - 36.39 pressive strength of 41 MPa, and this value increases to
R2 = 0.923 (PPTB1)
14.6 42–47 MPa when the concrete is reinforced with different
Modulus of elasticity ( GPa)

14.4
E = 6.20fcu½ - 27.89
14.2
R2 = 0.908 (PPTB2)
types of PP fibres at volume fractions of 0.25–0.5%.
14.0
13.8
(4) The addition of 0.5% Vf of PPTB1, PPTB2 and PPS1 fibres
13.6 increases the splitting tensile strength of OPS concrete by
13.4
13.2
33%, 27% and 12%. Based on the results, it is recommended
13.0 that the minimum volume fraction of the different type of
12.8
12.6 E = 7.50fcu ½ - 36.86 PP fibres is 0.375% after reporting the results for 0.5%.
R2 = 0.986 (PPS1)
12.4 (5) The effect of incorporating different type of PPTB fibres at
12.2
12.0
low volume fractions in improving the flexural strength of
11.8 OPS concrete is more pronounced compared to its effect on
6.45 6.50 6.55 6.60 6.65 6.70 6.75 6.80 6.85 6.90
splitting tensile strength.
Compressive strength (MPa ½)
(6) The specimens for both OPSC and OPSFRC can be categorized
Fig. 8. Relationship of compressive strength and modulus of elasticity (E) at 28- as ‘‘of good’’ condition after 7 days based on the UPV test
days. results.
M.K. Yew et al. / Construction and Building Materials 90 (2015) 36–43 43

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