WORKSHOP 1

Considering the slides and the diagrams shown, corresponding to a POD, PFD and P&ID, you have to
develop the following tasks:

Observe the slides and the diagrams carefully. Identify and list their components and characteristics
(30 min).

What are the differences between the three kind of diagrams you can identify and describe? (10 min)

Do the components and characteristics correspond to those defined in the standards (see next slide and
the presentation Engineering Diagrams available in the course Moodle)?

This workshop correspond to autonomous learning and requires approximately 60 min of extra-session
work. Consider the characteristics of the diagrams to produce your design engineering diagrams.

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 WORKSHOP 1
Standards and documents to develop POD, PFD and P&ID

Diagrams for the chemical and petrochemical industry -- Part 1: Specification of diagrams, ISO 10628-1:2014
Diagrams for the chemical and petrochemical industry -- Part 2: Graphical Symbols, ISO 10628-2: 2012

https://www.iso.org/standard/51840.html
https://www.iso.org/standard/51841.html

Chemical Process Equipment : Selection and Design, James R. Couper, , W. Roy Penney, James R. Fair, Elsevier Science, 2012

https://ebookcentral.proquest.com/lib/unal/reader.action?docID=1012530&ppg=38

DOE FUNDAMENTALS HANDBOOK ENGINEERING SYMBOLOGY,PRINTS, AND DRAWINGS, Volume 1 of 2.

https://www.standards.doe.gov/standards-documents/1000/1016-bhdbk-1993-v1

DOE FUNDAMENTALS HANDBOOK ENGINEERING SYMBOLOGY,PRINTS, AND DRAWINGS, Volume 2 of 2.

https://www.standards.doe.gov/standards-documents/1000/1016-BHdbk-1993-V2

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 Reception Reception Reception
Untreated Jet- A NaOH 5ºBe Demineralized water

Storing Storing Storing

Va> GE
Untreated Jet-A 0.1 mgKOH/g NaOH 5ºBe Demineralized k≤
1.036
T= environmental Note1 T= environmental Note 2 water 0.06μS/cm
P= atmospheric P= atmospheric T= environmental
P= atmospheric
Filtration
Dp≤100 μm
T=environmental
ΔPmax:=15 psi Filtration
Dp≤1 mm
Va≤
0.1 mgKOH/g
T=environmental
ΔPmax:=15 psi

Neutralization
T= environmental Decantation
ΔPmax = 5psi T= environmental
VAinitial=Va untreated Jet – A P= according to hydraulic
Mass ratio Jet –A: Solution = 4.14 calculation
(Note 3) θ= 10 min

Spent caustic Jet A Water

Continue POD 2/2 Continue POD 2/2 Continue POD 2/2

Notes: Nomenclature: Operations Diagram (POD) for the continuous

Note 1: specifications in ASTM D1655-19a Temperature: T production of Jet-A free of naphthenic acids
Note 2: aerometers include density and scale in ºBE Pressure: P
Note 3: to be performed in a falling film liquid Va: Acid value DPQYB 2021-1s POD1/2
contactor. GE: specific gravity DRW: PCNR 15/02/2021
k: electric conductivity
Dp: mean Surface área-volume CHK: AOL 21/02/2021
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 Spent caustic Jet A Water
From POD 2/2 From POD 1/2 From POD 1/2

Solvent extraction
T=environmental
Note2 ΔPmax = 5psi
Solvent:wáter mass ratio=
1:1

Decantation Filtration Adsorption with CaCl

T=environmental T=environmental T=environmental
P=according to hydraulic ΔPmax = 15psi ΔPmax = 5psi
calculation Dp= ≤100 μm Final water content≤0.001%
Note3
θ= 10 min

Adsorption with clay

T=environmental
ΔPmax = 5psi
Meet Final water content≤0.001%
Specificacions Note1

Note 4

Spent water Storing Jet – A treated

Storing spent caustic
To the refinery treatment T=environmental
T=environmental
system P=atmospheric
P=atmospheric

Notes: Nomenclature: Operations Diagram (POD) for

Note 1: defined in ASTM D1655-19a θ: residence time
the continuous production of
Note 2: to be performed in a falling film liquid contactor
Note 3: CaCl meets ASTM D98-15 Grade N4-94% min Jet-A free of naphthenic acids
Note 4: Tonsil ® Jet A supreme or similar
DPQYB POD 2/2
Designed: PCN 1/3/2019
Checked: AOL 1/3/2019
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Source: Manual de ingeniería de diseño, V15, Procedimiento de Ingeniería, Preparación de Diagramas de Proceso, PDVSA, mayo 1994
Source: Manual de ingeniería de diseño, V15, Procedimiento de Ingeniería, Preparación de Diagramas de Proceso, PDVSA, mayo 1994
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