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  • Lapsem GC Bayu Krisna Sanjaya (3B)

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    Afifah Elfitra
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    1) The document presents data from gas chromatography observations of several pure sample compounds including methanol, 2-propanol, ethanol, and benzene using different columns and conditions. Retention times, peak areas, and percentages are reported. 2) A multi-sample mixture of methanol, 1-butanol, 2-propanol, and benzene in specified percentages was also analyzed using capillary and packed columns. Retention times and peak areas matching the expected percentages are reported. 3) The data was collected on March 18, 2021 by Bayu Krisna Sanjaya (student number 180705014) with Okti Juliani (student number 1707035012) listed as the assistant.

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    LAPSEM GC BAYU KRISNA SANJAYA (3B)

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    1) The document presents data from gas chromatography observations of several pure sample compounds including methanol, 2-propanol, ethanol, and benzene using different columns and conditions. Retention times, peak areas, and percentages are reported. 2) A multi-sample mixture of methanol, 1-butanol, 2-propanol, and benzene in specified percentages was also analyzed using capillary and packed columns. Retention times and peak areas matching the expected percentages are reported. 3) The data was collected on March 18, 2021 by Bayu Krisna Sanjaya (student number 180705014) with Okti Juliani (student number 1707035012) listed as the assistant.

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    © All Rights Reserved
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    6 views5 pages

    Lapsem GC Bayu Krisna Sanjaya (3B)

    Uploaded by

    Afifah Elfitra
    1) The document presents data from gas chromatography observations of several pure sample compounds including methanol, 2-propanol, ethanol, and benzene using different columns and conditions. Retention times, peak areas, and percentages are reported. 2) A multi-sample mixture of methanol, 1-butanol, 2-propanol, and benzene in specified percentages was also analyzed using capillary and packed columns. Retention times and peak areas matching the expected percentages are reported. 3) The data was collected on March 18, 2021 by Bayu Krisna Sanjaya (student number 180705014) with Okti Juliani (student number 1707035012) listed as the assistant.

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    © All Rights Reserved
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    of 5

    4.1.

    Data Pengamatan
    4.1.1. Sample Pure

    Sifat
    Sampel Kolom Volume Rt Area % Peak
    Kolom
    4,26 17641 99,99
    TA =
    Polar 17642

    3,13 20173 100,00


    Capillary Non Polar TA =
    20174
    0,02 µL

    3,87 18410 99,99


    Low Polar TA =
    18411
    Metanol

    7,83 413063 100,00


    TA =
    Polar 413064

    6,75 4169117 100,00


    Packed Non Polar 2 µL TA =
    4169118

    7,41 414829 100,00


    Low Polar TA =
    414830

    15,25 13588 99,99


    TA =
    Polar 13588

    9,86 14294 99,99


    2- Non Polar TA =
    Propanol Capillary 0,02 µL 14295

    13,52 13778 99,99


    Low Polar TA =
    13779
    Sifat
    Sampel Kolom Volume Rt Area % Peak
    Kolom
    18,89 3799824 100,00
    TA =
    Polar 3799825

    13,43 3951465 100,00


    Packed Non Polar TA =
    3951466
    2 µL
    17,05 3848338 100,00
    Low Polar TA =
    3848339

    Polar 16508 99,99


    5,11

    Capillary Non Polar 0,02 µL 3,62 99,99


    18788

    Low Polar
    17180 99,99
    4,59
    Etanol

    Polar 8,74 100


    40394

    Non Polar
    Packed 2 µL 7,23 44366 100

    Low Polar
    8,20 39651 100
    Sifat
    Sampel Kolom Volume Rt Area % Peak
    Kolom

    Polar 6,09 15671 99,99

    Capillary Non Polar


    11,72 13994 99,99
    0,02 µL

    Low Polar
    9,29 14417 99,99

    Benzena

    Polar 9,63 41889 100

    Packed Non Polar 2 µL 15,33 39824 100

    Low Polar
    12,88 42134 100

    4.1.2. Multi Sample Pure

    Sampel Persen

    Metanol 30

    1-Butanol 20

    2-Propanol 20

    Benzena 30
    Sifat
    Kolom Volume Rt Area % Peak
    Kolom

    4,24 1058 33,05


    5,08 660 20,62
    Polar
    6,04 940 29,37
    15,28 542 16,93

    3,09 1211 35,91


    Capillary 0,004 µL
    Non 3,63 751 22,27
    Polar 9,81 571 16,93
    11,73 838 24,85

    3,79 1106 34,41


    Low 4,51 689 21,44
    Polar 9,19 865 26,91
    13,45 553 17,21

    7,82 422 4,68


    Polar 8,66 2660 29,51
    9,62 1943 21,55
    18,86 3989 44,25

    Packed 0,4 µL

    6,71 491 5,33


    Non 7,25 2697 29,30
    Polar 13,43 4164 45,24
    15,35 1851 20,11
    7,48 142 1,82
    Low 8,20 2350 30,19
    Polar 12,88 1556 19,99
    17,14 3736 47,99

    Samarinda, 18 Maret 2021


    Mengetahui,
    Asisten Praktikan

    Okti Juliani Bayu Krisna Sanjaya


    NIM. 1707035012 NIM. 180705014

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