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Transformation textures in steels

R. K. Ray and J. J. Jonas

cessing is carried out in the ferrite phase, texture


During the controlled rolling of steel, the control is achieved largely by controlling the first two
parent y phase develops a crystallographic processes, i.e. deformation and annealing, or recrys-
texture which is later acquired by the material tallisation. Here, the y-to-eX transformation only
after transformation. The major components of plays a minor role by providing the starting texture
the deformation texture of austenite are the for the cold rolling operation. The effects of rolling
{110}(112) and {112}(111) which give rise, reduction, heating rate, holding temperature, and
respectively, to the {332}(113) and {113} alloying on the annealing textures formed in low
(110) orientations in the transformation
carbon and deep drawing steels have recently been
products. The recrystallisation texture of
austenite, {1OO}(001), is similarly reviewed by Mishra and Darmann1 and by Hutchin-
transformed into the {100}(011) component son,2 and so are not dealt with here.
in the ferrite. The latter orientation can also be Steels can also be employed in the normalised or as
strengthened by ferrite rolling. During hot rolled conditions, in which cases the texture
processing, the recrystallisation of y changes accompanying transformation play a much
should be avoided in order to prevent the larger role. Some of these steels are finished by
formation of {100}(011) component, which controlled rolling, in which reductions are applied in
has a deleterious effect on the delamination the unrecrystallised y region, optionally followed by
behaviour of steels~The {332} (113) is the deformation in the intercritical (eX+ y) region before
most beneficial among the transformation
controlled cooling to room temperature. Figure 1 is a
texture components from the point of view of
achieving good deep drawability and improved schematic illustration3 of the three stages of the con-
strength and toughness. The effects of trolled rolling process, as it applies to reversing mills,
compositional and processing variables, during together with the microstructural changes accom-
controlled rolling, on the overall sharpness as panying deformation at each stage. The review by
well as on the relative intensities of the Tanaka3 covers several aspects of the controlled
components of the transformation texture are rolling process, including ferrite grain refinement, the
described. While the {332}(113) component is properties of controlled rolled steels, and industrial
significantly affected by some of these controlled rolling practices. However, it does not
parameters, the {113} (110) remains relatively deal with the effect of transformation on the textures
insensitive to these factors. Variant selection found in hot and controlled rolled steels. The prop-
does not seem to occur during ferrite
transformation. By contrast, martensite erties of such materials are dictated, not only by the
textures are generally much sharper than ferrite grain size and presence of solute elements and
ferrite textures, and this is attributable to precipitates, but also by the overall crystallographic
variant selection during transformation. texture of the grains.
Several analytical tools are available for the The various kinds of transformation textures
prediction of transformation textures. With the encountered in steels and their possible modes of
aid of information obtained in this way, origin have been briefly surveyed by Inagaki4 in 1981.
suitable processing routes can be devised to This review is by no means complete and requires
produce desirable texture components in the y, updating and further elaboration. The present paper
which are then inherited by the a'. There is
much scope for research along these lines.
has therefore been prepared to bring together some
IMR/207 of the more recent results in this area and also to
present a critical assessment of the subject as a whole.
© 1990 The Institute of Metals and ASM
INTERNATIONAL. At the time the work was carried out Orientation relationships and texture·
the authors were in the Department of Metallurgical inheritance during transformation
Engineering, McGill University, Montreal, Quebec,
Depending on the type and amount of alloying
Canada. Dr Ray was on sabbatical leave from the
Department of Metallurgical Engineering, Indian Insti- elements in a given steel, the cooling rate after defor-
tute. of Technology, Kanpur, India, where he has mation processing, and the 'state' of the austenite
returned. (i.e. strain free or worked), the austenite can trans-
form: (a) by a diffusional mode to polygonal ferrite or
pearlite; (b) by a shear mode to martensite; or (c) by
Introduction mixed diffusion and shear modes to acicular ferrite or
The processes that give rise to textures and texture bainite. If the parent material (austenite in the
changes in wrought steels are of three types, namely, present instance) possesses a crystallographic
deformation, recrystallisation, and transformation. texture, the material after transformation (ferrite,
For the production of sheet materials such as the martensite, acicular ferrite or bainite) will also
aluminium killed drawing quality (AKDQ) and acquire a texture that can be related in a precise way
interstitial free (IF) steels, where most of the pro- to the texture of the parent material. Thus, textures

International Materials Reviews 1990 Vol. 35 No.1


2 Ray and Jonas Transformation textures in steels

I : Recrystallization ~ Def?rmed t
region' grams

--950°C--- - ----- --.-

Deformation
1 band'

1
a>
L-

•...
:J
o
L-
a>
.m: ( i+ tJ.) region
Co
E
a>
J- - Art

Equiaxed grains Subgrains

Strain ~

1 Schematic diagram illustrating the three stages of the controlled rolling process and changes in microstructure
with deformation in each stage (after Ref. 3)

present in the high temperature y phase can be in- relationship corresponds to a 95.3° rotation about a
herited by the transformation products. common (hkI) axis where h = -1 + Y2 + Y3, k = 1
A first step in any attempt to examine the + Y2 + Y3, and I = Y2. This has been found out
relationship between the textures of the parent and using the method of Davies et aI.lO
product phases is to specify the crystallographic ori- In an alternative approach, the transformation can
entation relationship which describes the transfor- be specified in terms of the set of Euler angles (1', (3,and
mation. In general, orientation relationships are y which relate the crystallographic axes of the parent
expressed in the following form and product phases. These angles can be determined
if A, JL, and ill are known; the appropriate
{hlklIl}/I{h2k2I2}, (UlVlWl) II (U2V2W2) (1) relationships have been presented by Davies et aI.lO
where subscripts 1 and 2 refer to the parent and Table 1 shows that, depending on the specific ori-
product structures, respectively. In the case of steels, entation relationship assumed between the lattices of
four such orientation relationships have so far been the parent and product phases, one parent ori-
employed; these are the ones proposed by Bain,5 entation can transform into a fixed number (24 in the
Kurdjumov and Sachs,6 Nishiyama7 and Wasser- case of K-S) of product orientations, also known as
mann,8 and Greninger and Troiano. 9 The last one is variants. For a given transformation, it is necessary to
intermediate between the Kurdjumov-Sachs and establish the axis-angle pair for each possible variant.
Nishiyama-Wassermann relationships. The principal
characteristics of the first three are given in Table 1.
For any specific orientation relationship, there Table 1 Orientation relationships between y and a'
exists an axis which is invariant with respect to the Lattice
transformation. In such a case, the transformation Orientation correspondence Number of Total number
may be described as a rotation of angle ill about this relationship relation alternatives of variants
axis. The invariant axis can be defined in terms of Bain (B) {001 hll {001}(1' 3
polar and azimuthal angles, A and JL, with respect to (110),,/1(110)(1' 1
3
the crystallographic axes of the parent phase. Kurdjumov-Sachs {111},,/I{011}(1' 4
According to this notation, the Bain relationship (K-S) (011),,11(111)(1' 3 24
corresponds to a 45° rotation about a (100) axis (twin related
common to each crystal, whereas the K-S variants) 2
relationship can be described as a 90°rotation about a Nishiyama- {111h/l{011}(1' 4
12
Wassermann (N-W) (112),,/1(011)(1' 3
common (112) axis. On the other hand, the N-W
International Materials. Reviews 1990 Vol. 35 NO.1
Ray and Jonas Transformation textures in steels 3

Table 2 The 24 variants of Kurdjumov-Sachs ori- The orientations of the Bain variants differ by
entation relationship; symbols y and a refer 11.06 and 9.7 from those of the K-S and N-W
0 0

to fcc and bcc crystals, respectively variants, respectively. 14The K-S and N-W relations
Symbol Variant involve the same parallelism between planes and
there is a difference of only 5.30 between the parallel
o 1. (111)yll(110)£1' [101]yll(111]£1'
directions. 15A schematic (002) pole figure of the bcc
2. [101]yll(111]£1'
3. [110]yll(111]£1' variants formed from a single (001) [100] oriented fcc
4. [110]yll(111]£1' crystal following the Bain and K-S relationships is
5. [011]yll(111]£1' presented in Fig. 3a (Ref. 14). The corresponding
6. [011]yll(111]£1'
relationship for the Bain and N-W variants is demon-
o 1. (111)yll(110)£1' [110]y II (111 ]£1'
strated in Fig. 3b (Ref. 16). The relative positions of
2. [110]yll(111]£1'
3. [1 01]yll (111]£1' the three orientation relationships in Euler space (see
4. [101]yll(111]£1' the next section) are given in Fig. 3c (Ref. 17). It can
5. [011]yll(111]£1' b.e seen from these figures that the Bain relation gives
6. [011]yll(111]£1'
rIse to a much narrower pole distribution than either
the K-S or the N-W relation. This is because each
• 1.
2.
(111)yll(110)£1' [101]yll(111]£1'
[101]yll(111]£1'
Bain variant is surrounded by a number of K-S or
3. [011 ]yll (111]£1' N-W variants. It is also evident that, because of the
4. [011]yll(111]£1' multiplicity of variants, a relatively sharp parent
5. [ 11 0 ]y II ( 111 ]£1' texture generally decreases in intensity on transfor-
6. [110]yll(111]£1'
mation.
1. (111)yll(110)£1' [011]yll(111]£1'
2. [011]yll(111]£1'
Methods of representation of
3. [11 O]yll (111]£1'
4. [110]yll(111]£1' transformation textures
5. [101 ]y II (111 ]£1' Texture description by means of
6. [101 ]yll (111]£1'
pole figures
Detailed descriptions of the X-ray methods18,19 that
Thus the Euler angles corresponding to each of the 24 lead to the determination of pole figures can be found
variants of the K-S orientation relationship can be in the monograph on textures in metals by Hatherley
obtained, for example, from the crystallographically and Hutchinson2o and in several texts on X-ray dif-
equivalent sets of A, JL, and w. fraction, e.g. by Cullity.21 From an inspection of pole
Experimental evidence indicates that the K-S ori- figure data, it is possible to describe a well developed
entation relationship is generally followed during the texture by relating the positions and intensities of
austenite ~ ferrite or martensite transformation in specific orientations with those of the specimen
steels.ll,12 All the 24 K-S variants that are possible geometry. For example, textures in rolled sheet
are g~ven in Table 2. A plot of the {002} poles for all metals are frequently represented as being of the type
these variants is illustrated in Fig. 2 on (111)1'stereo- {hkl} < uvw) , which means that the orientations of the
graphic projection.13 grains in the sheet are such that their {hkl} planes lie
parallel to the plane of the sheet (i. e. perpendicular to
the normal direction (ND)), whereas their < uvw )
directions lie parallel to the rolling direction (RD).
When the texture is more complex, which is usually
the case, it is possible to describe it as consisting of a
6. number of components of different severity such as
111

2005 texture = ~Ai . {hkl} < uvw ) (2)


3 • .0..1 60.1
6. .0..4 where Ai is a weighting factor which is introduced to
4.03
o 03 5.0...0..2
200 allow for the relative intensities or strengths of the
6
5 various components.
The positions of the (200) poles of some useful
texture components are presented in pole figure form
in Fig. 4. The copper {112} < 111), brass {110}(112),
and S {123}(634) orientations, which are the major
50 02 111
60 .1 components of the deformation texture in fcc materi-
30 -4 als (such as y), are shown in Fig. 4a. The cube, {100}
5A .6.2
(001) , which is the major component of the recrystal-
lisation texture in fcc materials, is included in this
3 figure. The (200) poles of the main components of the
6 bcc transformation textures in steels are illustrated in
Fig. 4b. Of these, the {332}(113) component forms
2 Stereographic plot showing positions of {002}a
poles for each of the 24 K-S variants in (111)y single
by transformation from the {lID} (112) orientation
crystal matrix after Ref. 13. See Table 2 for codes of present in the deformed austenite (Fig. 4a), and the
symbols and numbers {113}(110) component is derived in a similar way

International Materials Reviews 1990 Vol. 35 No.1


4 Ray and Jonas Transformation textures in steels

y y

o o
o 0
y

o Starting Orientation (1) o Starting Orientati on (1)

• Bain Variant (3) • Bain Variant (3)

o K-SVariant (24) o IN -W Variant (12)

r'r-~!-----------
I
'l' I K-S
I
I
I
B N -W
1
I
1 K-S y
1
1
I
1......:::: •••••• >-
(c) I

3 a and b schematic (002) pole figures of all variants of bcc a phase formed from (001) [100] oriented fcc y crystal
following, respectively, the Bain and K-S relationships (after Ref. 14) and the Bain and N-W relationships (after
Ref. 16); c relative positions of the three orientation relationships (Bain, K-S, and N-W) in Euler space (after
Ref. 17)

from the fcc {112} < 111) orientation. Furthermore, This difficulty can be removed by the use of the
the {100}(011) bcc component is produced from the crystallite orientation distribution function (CODF
major recrystallisation component in the austenite, or ODF), which describes the frequency of
i.e. the cube {lOO}(OOl) (Fig. 4a). These are discus- occurrence of particular orientations in a three-
sed in more detail below. Finally, some other dimensional orientation space. This space is defined
important ideal orientations, which often constitute by three Euler angles which constitute a set of three
part of the transformation texture of steels, are plot- consecutive rotations that must be given to each
ted in Fig. 4c. crystallite in order to bring its crystallographic axes
into coincidence with the specimen axes. The
complete ODF consists of the sets of rotations per-
Texture description by means of taining to all the crystallites in the specimen. Mathe-
orientation distribution functions matical models have been developed which allow the
Although pole figures provide a useful description of ODF to be calculated from the numerical data
the texture present in a material, the information they obtained from several pole figures.
contain is incomplete and at best semiquantitative.22 The most widely adopted methods are those
International Materials Reviews 1990 Vol. 35 No.1
Ray and Jonas Transformation textures in steels 5

RD RD RD

• • x X
A A 0 0

• • • • • •
• • ~• I.

• • ~ ~
• • • • • • • •
A A
~ ~ xO Ox
• •

(c)
(b)
(0)
• l110! <112>Bross • l332l <113> • (111\ <112>

A(112~ <111>Cu ~~113! <110> ~ !554~ <225>

• (123) < 634> S Dl1001 <011> ° 1111j <110>


o (100) < 001 > Cube X 1112J<110>

a major deformation and recrystallisation texture components in y; b major transformation texture components in a; c some other important
orientations in transformed a
4 (200) pole figures showing ideal positions

proposed independently by Roe23 and by Bunge, 24who metry, a three-dimensional orientation volume may be
used generalised spherical harmonic functions to rep- defined by using three orthogonal axes for cjJ1,cjJ,and
resent the crystallite distributions. A thorough math- cjJ2with each of the Euler angles ranging from 0 to 900•
ematical treatment of this subject can be found in two This volume is divided into three basic ranges in
books by Bunge and co-workers. 17,25The three Euler which each orientation appears once. The value of
angles employed by Bunge to describe the crystal the orientation density at each point in this volume is
rotations are qh, cjJ,and cjJ2,whereas the set of angles simply the strength or intensity of that orientation in
proposed by Roe are referred to as 'II, 8, and <1>, multiples of random units. Regions of higher and
respectively. lower orientation density are separated by three-
According to Bunge, an ODF may be expressed as dimensional cohtour surfaces and it is usual to take a
a series of generalised spherical harmonics in the series of parallel sections through this space for ready
form: visualisation of the data contained in the three-
+1 +1 dimensional plot.
2: 2: ernPF
m=-1 n=-1
n
( cjJ) A three-dimensional view of the Euler space is
presented in Fig. Sa. Here the location of the techno-
logically important {Ill} fibre as well as some
important ideal orientations can be clearly seen. A
where ern are the series coefficients and PFn( cjJ)are two-dimensional <I>= 450 section (Roe notation), in
which a few ideal orientations are identified, is repro-
certain generalisations of the associated Legendre
duced in Fig. 5b. The availability of ODFs has made
functions.
In Roe's notation, an ODF may be expressed as possible the quantitative comparison of textures; fur-
thermore, the higher resolving power associated with
+1 +1 ODFs has enabled researchers to recognise more
w(W, 8, <1» = 2:
1=0
L 2: WlmnZlmn( cos
m=-1 n=-1
8) clearly many details of individual textures which may
be smeared out and difficult to identify in a pole
x exp (-im'ljJ) exp (-incjJ) (4) figure.

where W1mn are the series coefficients and Zlmn( cos 8)


is a generalisation of the associated Legendre func-
tions, the so called augmented Jacobi polynomials.2
6 Technological importance of
The relationships between the Roe and Bunge angles transformation textures
are the following27 ' Transformation textures and R values
Numerous investigations of texture formation during
(5) cold rolling and subsequent recrystallisation have
been carried out with a view to producing cold rolled
Although the two methods are equivalent, there are sheets with high R values.1,2 Recently, however, the
some minor differences of detail, which are discussed demand for low cost, deep drawing quality steels has
in Ref. 28. stimulated research on developing as hot rolled sheet
For cubic/orthorhombic crystal/specimen sym- steels with satisfactory R values for use in place of

International Materials Reviews 1990 Vol. 35 No.1


6 Ray and Jonas Transformation textures in steels

(001) (113) (112) (i 11) (i 10)


: ;(001)[110) 90 ["nO] [110] [110] [110] [110]

! TDII[110] ~ (4411) (223)

I (337)(776]~
80 [110] [110]

: ; (111)[112]
.(011)[011) ; / (101)[101
70 < 111 > II ND -.:

1
:
,J"
,:(5 54)[ii 5)
~(332)(113]
60 , (111)
[121]

, ,I' ;(110)(001] be
o Q)
'"d
50
(001)
(001)[1101: _ <_, ,~3.?~(~C!.~ ~3':~~!~ 90
(013)(100) _ .(113)(1~0) .' ~l~l)[Oll)
~ 40
[010]
(337)(110~ (111)(12~/ 80 (j 10)
30 (111) [112]
(112)[110~ ' 70 30 ~
en (223)[110~ ,'~ _ 60 [01l]
(1)
• , (101)(010]
~ 50 (011)(100] :,,- _ so : (5S4)
_ ~(111)[110] 40 oeO; 20
(111) : [2is]
RDI/[110] :.: 30 ~~
70 (001)
1 20
10 [112] : ~ (332) (; 10)
(031)(100) (301)(0;0] [110]
~: [113] [001]
90
:(110)(110)

o
10
0
0
" 10 20 30 40 50 60 70 80 90
----- ~=55~ ~2=45~<111>IIND
• ideal positions e,deg
(0) (b)

5 a three-dimensional view of Euler space with locations of some important ideal orientations (Bunge notation)
and b <I>= 45° section of Euler space showing locations of some important ideal orientations (Roe notation)

certain cold rolled grades. Since the plastic aniso- and 45° ears (~R < 0). Similar predictions were
tropy of a material is very much a function of its published by Lequeu and Jonas, 30 who employed the
texture, the transformation textures produced in hot method known as the continuum mechanics of
and controlled rolled steels will determine their deep textured polycrystals (CMTP). This method
drawing capabilities. For this reason, the manufac- combines aspects of both the crystallographic
ture of deep drawing quality, as hot rolled steels will approach and a macroscopic analysis employing
require the production of suitable transformation various continuum yield functions.
textures and some knowledge of how their formation It is shown in the section 'Common transformation
and modification can be controlled. textures in steels' below that the texture components
The major transformation texture components obtained after controlled rolling in the (y + a) and a
inherited by ferrite from both recrystallised and ranges are not precisely the same as the transfor-
deformed austenite are listed in Table 3. For each mation texture components presented in Table 3. The
texture component, calcu!ated values are presented of positions of some of these modified components,
the average strain ratio R and the planar anisotropy however, are not far from those of the inherited
~R. These were estimated by Daniel29 by using components in Euler space. These latter orientations,
crystal plasticity and the relaxed constraint method; together with their relative positions via-cl-vis the
they indicate the contribution that each textur~ {332}(113)a- and {113}(110)a- components, are
component is likely to make to the deep drawability R listed in Table 4. The calculated values of R and ~R
and to the tendency to form 0 and 90° ears (~R > 0) (Ref. 29) for each ideal orientation are also 'included.

Table 3 Major transformation texture components


Table 4 Texture components obtained after control-
inherited by a from y in controlled rolled
led rolling of steel in (y + a) and a ranges
steels
Texture
Texture
component Relative position R !!J.R
component Origin !!J.R
*{554} (225)a Differs from {332}(113)a by a 4° 2·6 1·1
{332} (113)a {110}(112)YI 2·7 1·9
rotation in a- about TOil (11 0)
rolled y texture
component (brass
*{111}(112)a Differs from {332}(113)a by a 10° 2·6 0·0
rotation in a- about TOil (11 0)
component)
{113}(110)a {112}(111)YI 1·0 -1·7 *{111}(110)a Differs from {113}(110)a by 30° 2·6 0·0
rolled y texture rotation in a-about RDII(110)
component (copper {445}(110)a Differs from {113}(110)a by a 24° 1·2 -2·0
component) rotation ina- about RD" (110)

{100}(011)a {100}(001)YI 0·4 -0·8 *{112}(110)a Differs from {113}(110)a by a 10° 2·1 -2·7
recrystallised y rotation in a about RDII(110)
texture component
(cube component) * Ideal orientations observed in the textures of commercial deep
drawing quality steels.

International Materials Reviews 1990 Vol. 35 No.1


Ray and Jonas Transformation textures in steels 7

Table 5 Effect of rolling on transformation texture regarding the desirable or undesirable natures of
components (Ref. 31) individual ideal orientations. For example, it is clear
Common rotation that for good deep draw ability (high R), the
axis Orientation changes in a during rolling {332}(113), {554}(225), {111}(112), and
{Ill} (110) texture components are preferred over
RDII(110) {113} ( 110) ~ {112} ( 110 ) {111}( 110) all the others. One of the major transformation

TDII(110) {332}(113) ~ {554}(225) ~


t
{111}(112)
texture components, {332}(113), is found to possess
values of R = 2·7 and I1R = 1·9. By contrast, these
two parameters take the values 1·0 and -1·7 for the
other major component of the transformation
During rolling in the (y + a) range, the deforma- texture, {113}(110). Thus the {332}(113) leads to
tion of y followed by transformation into the a does an increase in R value and to the presence of 0 and 90°
not lead to the formation of any new texture com- ears, whereas the {113}(110) leads to a change in the
ponents. Rather, continued rolling of the y leads sign of I1R and therefore to the presence of 45° ears.
to the intensification of the copper {112}( 111) y In this way, it is clear that there is a need to control the
and brass {lID} ( 112) y components. These two C
volume fractions of these two components during
components, after transformation, are converted into processing so as to produce relatively high R, with
the {113}(110)a and {332}(113)a orientations, minimum I~RI.
respectively, as outlined in Table 3. The texture Among the other desirable components,
modifications referred to in Table 4 are produced {554}(225) and {111}(112) lie within the usual
instead by the deformation of the a phase. Rolling dispersion limits of the {332} (113) component,
simulation studies31 have clarified how the transfor- whereas the {Ill} (110) component lies relatively far
mation texture components are reoriented by from {113}(110). Thus, control of the transfor-
deformation-induced rotation of the a phase (Table mation process to produce as much of the {332}(113)
5). Comparison of Tables 4 and 5 shows that the component as possible is beneficial from the point of
texture components present after rolling can indeed view of achieving good deep draw ability . As discus-
be produced from {113}(110) a and {332}(113) a by sed below, the {332}(113) component is largely
the plane strain deformation of a (see the section derived from the {lID} (112) component of the
'Common transformation textures in steels' below). texture of the deformed austenite. This indicates
These predictions are in £eneral agreement with that, during the controlled rolling of steels, the pro-
experimental observations. 2 . duction of a large volume fraction of the {lID} (112)
SOlne plots of R versus the angle a with respect to component in y is desirable.
the rolling direction, as predicted by the relaxed An overall view of the transformation texture
constraint method,29 are given in Fig. 6: These dia- components observed experimentally and of the
grams, as well as the values of Rand I1R listed in modifications these undergo as a result of rolling in
Tables 3 and 4, lead to some simple conclusions the (y + a) and a ranges is depicted schematically in

{332}<113> {554}<225> {111}<110> {311}< 110>


5 5 5 3

4 4 4
2
3 3 3

2 2 2

1 1
0 30 60· 90 0 30 60 90 0 30 60 90 30 60 90

{1144}<110> {112}<110> {223}< 110> {100}<011 >


3 5 5 3

2 2

2 2

o o
R
30 60 90 30 60 90 0 30 60 90 0 30 60 90

a
6 Plots of R versus angle a with respect to rolling direction for selected ideal orientations predicted by relaxed
constraint method (after Ref. 29)

International Materials Reviews 1990 Vol. 35 NO.1


8 Ray and Jonas Transformation textures in steels

I y Rolling Texture I
11. {110}<112> I 12.{112}<111> I

Sharpens with decreasing


finishing temp. in unrecrys. y •
Transformed a texture

t t
• Sharpens due to presence
of small amounts ofNb, V, etc.

I {332}< 113 > I I {113}-{4 411}<110>

Sharpens with Sharpens signi- 1


Decreasingfinishing
temperature in y+a •
I~,----,
{112}<110> I
\It
,
~----.
Sharpens little
decreasing y ficantly due to by addition of Relatively in-
grain-size and addition of sub- I{554}<225> I I{223}< 110> I substitutional sensitive to
increasing cooling stitutional solutes solutes like Mn, y grain-size and

r
rate like Mn, Ni, etc. Ni, etc. cooling rate

Deformation in Q ~

I y Recrys. Texture I Yfibre <lll>IIND a fibre < 110>IIRD from


{100}<001 > {OOl}<110> to {111}<110>

t Recrystallization
I Transformed a Texture'
{100}<011 > y fibre sharpens at the expense of a fibre

7 Schematic diagram showing effect of compositional and processing variables on the two major components of
transformation texture in steel

Fig. 7. In the same diagram, the effect of different Inagaki et al. 37also calculated the anisotropy of the
compositional and processing variables on the rela- relative yield stress for various ideal texture
tive sharpness of the texture components is also components. The theoretical values of the relative
given. These will be discussed in more detail in the yield stresses obtained by them are plotted against the
section 'Common transformation textures in steels' angle with respect to the rolling direction in Fig. 9.
below. The anisotrogies of the orientation factor for brittle
fracture, cos 8, which is a measure of the toughness,
Transformation textures and strength were also calculated for various ideal orientations.37
and toughness Such plots are shown in Fig. 10.
It has long been known that, for pure bcc polycrys- From Figs. 9 and 10 it is clear that, among the
tals, the anisotropies of yield strength (YS), ultimate transformation texture components found in control-
tensile strength (UTS), and the brittle fracture initi- led rolled steels, the {113}(110) component is unde-
ation stress are closely related to the textures of these sirable because (a) it produces significant anisotropy
materials.33-36 Since, as stated above, relatively sharp in both strength and toughness, and (b) it makes the
transformation textures are encountered in many material brittle along planes oriented at 45° with
controlled rolled steels, it is to be expected that there respect to the rolling direction. By contrast, the
will be a correlation between their textures and the {332}(113) component causes much less anisotropy
relatively large directionalities of strength and in strength and toughness and also leads to more
toughness that are observed. Inagaki et al.37 desirable values for these properties. Thus, the above
attempted to establish a quantitative relationship results show that the strength and toughness of con-
between the transformation textures of such steels trolled rolled steels can be improved by controlling
and their mechanical anisotropies. Using the method the development of austenite textures so as to
of Hosford and Backofen,38 they calculated the yield strengthen the intensity of the {110}(112)
and tensile strength anisotropies, and then evaluated component. The latter, in turn, leads to the presence
the anisotropy of toughness (or brittleness) from the of the desirable {332} (113), {554} (225) and,
densities of the (100) axes lying near the test direc- {Ill} (112) components in the transformation
tion. Their predictions were in good agreement with texture.
the experimental results, as shown, for example, in
Fig. 8. Here the predicted and measured anisotropies
associated with the yield and tensile stresses for four Transformation textures and delamination
controlled rolled high strength steels, tested both at behaviour
room tem~erature and at -196°C, are plotted and It has been emphasised33 that in order to establish a
compared.37 quantitative relationship between texture and
International Materials Reviews 1990 Vol. 35 No.1
Ray and Jonas Transformation textures in steels 9

'028 Mn- %
HFT 1·28%.Mn-L FT '"55%Mn- L FT 2 OG'oMn- L FT
o

102 105
102
-196°C -196OC -196~ -196°C
100 • TS • 150
100
TS TS
98
• • 140

98 • •
98 YS
95 •

/00
• 100 130
• YS
96
• 98 YS • 115
95
N
IE 94 • 110
96 •
E 105
O'l 90
~ /00
lfl
lfl
66 /02
Q) RT
"-
+..I 62 RT 62 R.T. TS
(/)
TS TS 64 98
60 60

• • 94
62

58 80
46 YS 54

• • 76

44 48
• 72
42 .50
0 45 90 460
45 90 0 45 90 0 45 90
Angle from rolling direcfion , dfg

8 Plots showing predicted and measured anisotropies of YS, 0·2%PS, and TS for four controlled rolled steels,
tested at RT and -196°C; curves were calculated from textures, HFT and LFT indicate high and low finishing
temperatures, respectively (after Ref. 37) 1 kg mm-2 == 9·807 MN m-2

mechanical properties, the precise orientation distri- ferrite grains containing the {100} (uvw) type
bution must be taken into account, including even the texture.
minor components. An example where a minor It has also been proposed42,44 that separation could
component of the transformation texture in control- be caused by the plastic anisotropy of the banded
led rolled steels has often been referred to as being structure typically found in controlled rolled steels.
responsible for property deterioration is the case of According to this view, the pancake shaped bands are
the {100}(011) component and its association with composed of two families of grains, which can be
the delamination process. It is well known that when broadly classified into the {Ill} (110) and
a ferrite-pearlite steel is controlled rolled and fin- {100}(011) types. Under an applied stress, the dif-
ished in the (y + a) region, a lateral split frequently ferently textured bands are expected to behave dif-
occurs on the fractured surfaces of Charpy impact ferently, thus producing a discontinuity in plastic
specimens tested in the neighbourhood of the transi- strain at the boundaries of the bands, leading ulti-
tion temperature.39-48 The principal cause of such mately to intergranular fracture. However, a detailed
through thickness embrittlement is the presence of calculation by Inagaki47 has shown that the difference

1·0
4.0
5 :5
m m
c c
(1) d>
L
+-'
III
~
III
CD
"0
Qj
0>.
(1)
(1) l332}<1I3>
/ /
> >
+-' {IIO)<OOI>
0
Qj
0:: 20 (1101<001')
o
o 30 60 90 0 30 60 90
o 30 60 90 0 30 60 90 Angle from rolling direction I deg
Angle from rolling direction, deg
10 Plot of cos28 v. angle from rolling direction for
9 Plot of theoretical relative yield stress v. angle from various ideal orientations; 8 is angle between test
rolling direction for various ideal orientations (after direction and nearest {100} plane normal (after
Ref. 37) Ref. 37)

International Materials Reviews 1990 Vol. 35 No.1


10 Ray and Jonas Transformation textures in steels

in plastic anisotropy between the {100}(011) and result that it cannot be preserved at room tem-
{Ill} (110) orientations is not likely to be large perature in most commercial steels. This has necessi-
enough to cause separation. Further work by tated the use of indirect methods to study the
Inagaki48 has shown that separation is a cleavage development of texture during the deformation
fracture which is initiated by cracking in coarse pearl- and/or recrystallisation of the austenite. Both con-
ite colonies. When such colonies are surrounded by ventional pole figures and ODF analysis have been
coarse pancake shaped ferrite grains with near used in these investigations.
{100}(011) orientations, the original cracks will pro- One approach to the identification of textures in
pagate readily into these regions, ultimately causing austenite has been to take a representative pole figure
the delamination. Since such conditions can be read- or ODF for a rolled fcc metal (to simulate austenite)
ily satisfied in controlled rolled steels rolled in the and transform it according to an appropriate ori-
(y + a) region, delaminations are often observed in entation relationship (K-S or N- W) to yield a predic-
these materials, and the deleterious effects of the ted pole figure or ODF for the ferrite phase. The
{100}(011) component are now widely recognised. experimentally measured ferrite texture is then
Since {100}(011) in ferrite is known to form from the compared with the predicted texture and a goodness.
major recrystallisation texture component of aus- of fit criterion is used to assess the correctness of the
tenite, the cube or {100}(001), the importance of assumed austenite texture. Such a process of match-
preventing austenite from recrystallising during con- ing experimental and predicted textures can have a
trolled rolling is readily apparent. Similarly, heavy reasonable degree of success provided a sufficiently
rolling of ferrite is also to be avoided, as it leads to wide range of fcc textures is available. The various
strengthening of the {100} < 011) orientation (see the analytical methods available for this kind of predic-
next section). tion are summarised in the section 'Analytical meth-
ods for prediction of transformation textures' below.
Using the above approach, the rolling texture of
Common transformation textures austenite has often been assumed to be similar to that
in steels produced by cold rolling fcc materials with high stack-
ing fault energies, such as copper or aluminium.50,51
Textures in deformed and recrystallised
This texture normally consists of a continuous tube of
austenite
orientations running from {lID} (112) to near
In the upper temperature ranges of hot working (i.e. {4 4 II} (11 11 8). From the results of a number of
in the roughing range), conventional (static) recrys- studies involving the matching of predicted and
tallisation takes place. At lower hot working tem- experimental ferrite textures, 52it is now clear that the
peratures (i.e. in the finishing range), depending on general features of the austenite rolling texture in
the composition of the steel, rolling is followed by commercial steels do indeed correspond to those of
static recrystallisation (in plain C and similar steels), heavily cold rolled copper, aluminium, or nickel.
or by the absence of recrystallisation and pancaking Similarly, there is indirect evidence to show that the
(in Nb steels). major component of the austenite recrystallisation
Pancaking or strain accumulation occurs when the texture is the cube, {100}(001). The characteristics
time available for carbonitride precipitation is suffi- of the deformation and recrystallisation textures of
cient to prevent static recrystallisation (e.g. in revers- austenite referred to above agree quite well with the
ing mills). When this time is short, as in strip mills, corresponding experimental textures observed in a
and when the presence of solutes such as Nb prevents type 304 austenitic stainless steel. 53-55
rapid static recrystallisation, dynamic recrystallis- It is of interest that, whether the final product from
ation is initiated instead, followed by post-dynamic deformed austenite is ferrite or martensite, the
recrystallisation in the interpass intervals.49 All three texture consists of the same two major components,
of these processes (i.e. deformation, precipitation, {332}(113) and {113}(110) (Ref. 56). However, the
and recrystallisation) give rise to the development of sharpness of the texture and the relative intensities of
microstructural direction alities and therefore to the various components differ depending on the
anisotropy in the mechanical properties of the hot composition of the steel, amount of rolling reduction,
worked austenite. When the austenite recrystallises finishing temperature, initial austenite grain size, and
before transformation, only a weak crystallographic cooling rate during transformation. 4,50-:00 The charac-
texture is present in the transformed ferrite.4 By terisation of transformation textures in different
contrast, much sharper textures and more marked steels therefore involves an understanding of the
anisotropy are encountered in the controlled rolled effects of the above compositional and processing
steels which are finished below the 'no-recrystal- variables.
lisation' temperature.
The ferrite textures are due to the inheritance of
the preferred orientation present in the original Effect of composition on
austenite. The textures of steels finish rolled in the transformation texture
(a + y) intercritical range, on the other hand, include Investigators have shown that the chemical compo-
contributions from two sources, namely: (a) the sition of steel has a significant effect on the nature and
inheritance of texture from the austenite, and (b) the sharpness of the final transformation texture. The
development of a deformation texture in the ferrite. effect of Nb in modifying the transformation texture
The evaluation of austenite textures has been handi- of C-Mn steels has been dealt with in a number of
capped by the transformation it undergoes, with the papers,59,60 which indicate that the texture severity
International Materials Reviews 1990 Vol. 35 No.1
Ray and Jonas Transformation textures in steels 11

~ ~ g ~ ~ 9 g ~ ~
5.3p'l1\

0<D
-
M

-
......•.

~ g g g ~ ~ g ~ ~ ~ ~ g ~ ~ g ~ ~ 00

5.3p'l1\ 5.3p I 11\

~ ~ ~ £ ~ S g ~ ~ ~ ~ g ~ ~ S g 2 ~ 0° •..
5.3p'l1\ 5.3p 111\ •..

International Materials Reviews 1990 Vol. 35 No.1


12 Ray and Jonas Transformation textures in steels

increases sharply when Nb is added. The transfor- Fig. 13, which depicts the effect of Mn on the trans-
mation textures of simple C-Mn steels, which are less formation textures found in a series of steels with a
severe, can be described as a continuous distribution basic composition of 0·lC-Q·4Si-Q·05Nb. The latter
of orientations from {001}(110) to near {Ill} (110). figure shows that increasing the amount of Mn in the
The textures of C-Mn-Nb steels, on the other hand, Nb-containing steel leads to a more significant change
consist of an {hkl} ( 110) fibre centred around in the transformation texture.
{113}(110) plus some elements of the {lll}(uvw) cI> = 45° (Roe notation) sections of the 0 DFs57
fibre, as well as an enhanced {100}(011) component representing the textures of the four experimental
(Ref. 59). steels with varying Mn content (Fig. 13) are repro-
From his work on a 0·lC-"1·3Mn steel and a O·lC- duced in Fig. 14. It can be seen that the major
1·24Mn-Q·03Nb-Q·07V steel, Inagaki60 concluded . components in all four steels are the {113}( 110) and
that the addition of Nb and V affects the transfor- the {332}(113).The {113}(110) component is
mation textures of simple C-Mn steels over a wide already quite sharp at the lowest Mn concentration
range of finishing temperatures. His results are and its sharpness increases only slightly. as the Mn
presented in Fig. 11. It is apparent from this figure level is increased. The {332}(113) component, on the
that, when processed at higher finishing tem- other hand, which is rather weak at the lowest Mn
peratures, the Nb- V steel displays a significantly concentration, sharpens significantly with increasing
sharper texture than the Nb-V-free steel. The gene- Mn. These features are evident from the skeleton
ral features of the textures and their severities are, lines obtained by plotting the maximum orientation
however, similar for the two steels when lower densities in each constant 'ljJ section of the corre-
finishing temperatures are employed. The difference sponding 0D F (Fig. 15). Whether the observed
in the textures of the two steels finished above 800°C effect of Mn on the transformation texture of steels is
has been ascribed as due to the difference in the due to possible changes in the stacking fault energy of
original austenite texture.60 The austenite rolling yiron brought about by solute addition,73 or is simply
texture in the Nb- V steel is much sharper than that an alloyin~ effect on the transformation behaviour of
in the Nb- V-free steel due to suppression of y the steels, 7 is not yet clear. This aspect will be dealt
recrystallisation in the former by the precipitation of with in more detail below. It is apparent from Figs. 12
NbC and VC particles. Below 750°C, however, and 13 that Mn alone cannot produce a sharp trans-
recrystallisation in the Nb- V-free steel will also be formation texture without the addition of Nb in these
sluggish and therefore little difference in the y rolling steels. It appears, therefore, that the suppression of
texture in the two steels is expected, except for the recrystallisation in the y phase caused by the presence
obvious presence of the {001}(110) component in of Nb is essential to the formation of an intense
the Nb- V-free steel. transformation texture in such steels.
Many investigators have discussed the effect of Nb The effect of Ni on the transformation texture of a
in retarding y recrystallisation in steels.61-72This has 0·05C-Q· 26Si-1· 3Mn-Q·04Nb steel is depicted in Fig.
been attributed to: (a) the strain induced precipi- 16 (Ref. 58). It is clear from this figure that the
tation of fine Nb( C, N) particles61-63,70and (b) to a {332}(113) texture component increases in intensity
combination of solute drag and precipitation ,with the addition of Ni, and thus the effect of the
effects. 65,67,71,72 latter element is similar to that of Mn.
The effect of Mn on the transformation texture of The transformation textures in Fe-Ni alloys are
steels has been discussed in great detail by several also known to be strongly influenced by the Ni con-
invest~ators. 4,56-58Figure 12, taken from Inagaki's tent.4,74 cI> = 45 sections (Roe notation) of the ODFs
0

work, shows how the transformation texture in a of two Fe-Ni alloys containing 22·5 and 30·8%Ni are
O·06C-Q·2Si steel changes as a function of Mn con- compared in Fig. 17. The samples were heavily rolled
tent. It is interesting to compare this diagram with in the austenitic condition and then transformed to

RD RD RD

(0) (c)

a 1·6%Mn; b 2·5%Mn; c 4·1%Mn

12 (200) pole figures showing effect of Mn on transformation texture of 0·06C-0·2Si steel (after Ref. 58)

International Materials Reviews 1990 Vol. 35 NO.1


Ray and Jonas Transformation textures in steels 13

R.D. R.D.

0'5
~~1'5::3 0·5

(b)

R.D. R.D.

(c)

• {332}(113); A {331}(011);. {100}(011)


a 1·28%Mn; b 1·78%Mn; c 2·06%Mn; d 2·48%Mn

13 (200) pole figures showing effect of Mn on transformation texture of 0'1C-0'4Si-0'05Nb steel (after Ref. 58)

martensite. Comparison between Figs. 14 and 17 increase the sharpness of the transformation texture,
shows that the texture of the Fe-22·5Ni alloy is especially by increasing the intensity of the
similar to that of the 2·48 Mn steel. It is evident,
%
{332} < 113) component. The possible reasons for this
from the skeleton line in Fig. 18 that the {332}(113) behaviour are discussed below.
is also the main component of the 22·5 Ni alloy.4 %

The transformation texture of the Fe-30·8Ni alloy is Role of substitutional solutes


somewhat different: although the {332}(113) ori- Inagaki57 first considered that the experimentally
entation is the major texture component in this alloy observed effect of substitutional solutes on the trans-
as well, the {113} ,....,{112}(110) component is much formation texture could be a function of the stacking
weaker and the skeleton line has much broader fault energies of the alloys, which can modify the y
maxima. rolling textures. It is known that if the stacking fault
- jfi addition to Mn and Ni, Mo andCr have also energy of austenite decreases with increasing alloy
been found to cause a definite sharpening of the content,73 a transition in the ~ rolling texture from the
transformation texture in steels.58 copper to the brass type5~55,75 will occur. This is
Overall, substitutional solutes in steel are found to expected to produce a corresponding change in the

International Materials Reviews 1990 Vol. 35 NO.1


14 Ray and Jonas Transformation textures in steels

90 90

(nJ
O'l
60 (323)[jj1] lHal
<1J • I
"0

~ 30

30 60 90 90
e,deg

90 90
(d)

01
<1J
"0

30 60 90
e,deg
% c ~ ~ ~ ~ ~ ro ~ ~
lP, dE?g
.1332}(113) A f311} < 0 11) • {lOO} (011)
15 Variation in orientation density along skeleton
a 1·28%Mn; b 1·78%Mn; c 2·06%Mn; d 2·48%Mn lines of three of low-C-Mn-Nb steels of Fig. 14
(after Ref. 4)
14 <I>= 45° ODF sections (Roe notation) representing
transformation textures in steels with basic
composition 0'1C-0'4Si-0'05Nb as function of Mn using the K-S relationship and the assumption that all
content (after Ref. 4) variants of this relationship are equally favoured. He
observed close agreement between the calculated and
experimental textures in his two steels. Thus he con-
inherited transformation texture. However, Abe and cluded that the transformation textures were inher-
Itoh,74 who worked on a series of Fe-Ni alloys with Ni ited from the same type of y rolling texture, namely
in the range 19·9-30·20/0, observed that, although Ni the Cu type. The most important difference between
has a strong effect on the transformation texture, the the two textures was that the {332}(113) component
y rolling textures of their alloys were all of the copper was perceptibly weaker in the 1·280/0Mn steel. Since
type, irre~ective of the Ni content. these textures were assumed to form from the same
Inagaki then assumed the presence of a Cu-type y type of y rolling texture, he concluded that, during
rolling texture in his 1·28 and 2·48 % Mn steels consist- transformation, the {332}(113) component must be
ing of the {112}(111) and {110}(112) components. weakened with respect to the other major
He derived the corresponding (l' phase orientations component, the {113}(110), in the low-Mn steel.

RD RD RD

(c)

a 2·1%Ni; b 3·4%Ni; c 4·50/0Ni


16 (200) pole figures showing effect of Ni on transformation texture of 0'05C-0'26Si-1'3Mn-0'04Nb steel (after
Ref. 58). See Fig. 13 for key to components

International Materials Reviews 1990 Vol. 35 NO.1


Ray and Jonas Transformation textures in steels 15

90

80
70

60

30
F.-30.8·'. Ni
20

10

10 20 30 40 50 60 70 ~ 90
(b)

18 Variation of orientation density along skeleton


lines of Fe-Ni alloys of Fig. 17 (after Ref. 4)

process, the texture produced during the nucleation


stage can be weakened by the characteristics of the
subsequent growth process. This will occur at higher
temperatures (low Mn levels), at which there is
substantial growth; at lower temperatures (high Mn
levels), there is less growth, so the relatively sharp
30 'nucleation texture' undergoes less modification.
Some insight into the latter process can be gained
20 from the stored energy of deformation, which is
known to be strongly orientation dependent. In
heavily rolled eu single crystals, the stored energy is
i(
the greatest for the {112 111) and the least for the
{lID} < 112) orientation. 6 Assuming that the defor-
mation texture of the y phase of the Mn-containing
00 10 20 30 40 SO 60 70 eo 90 steels is similar to that of deformed copper, the
8} deg nucleation of a grains during transformation should
a 22·5%Ni; b 30·8%Ni be more frequent in {112} < 111) y grains than in
17 <I>= 45° ODF sections (Roe notation) showing effect {lID} < 112) y grains.
of Ni on transformation textures of two Fe-Ni alloys Although the precise mechanism of the transfor-
(after Ref. 4). See Fig. 5b for key to components mation of deformed austenite into ferrite is not fully
understood, the nucleation of a grains is thought to
occur at deformation bands as well as at austenite
Manganese is known to inhibit the transformation grain boundaries. At high temperatures, grain
of austenite to ferrite by increasing austenite stability. boundaries are the preferred sites for nucleation over
As a result, with increasing Mn content, the transfor- deformation bands.58 These grain boundary nuclei
mation temperature of steels is lowered significantly. grow more rapidly into the neighbouring y grains,
Inagaki suggested that, in the 1·28 Mn steel, exten-
%
with which they do not have any lattice relationship
sive growth of the a grains occurs during the higher (such as the K-S).77 Extensive growth of such inco-
temperature transformation, whereas in the 2·48% herent nuclei may occur at the higher transformation
Mn steel, grain growth is extremely limited. He rea- temperatures for steels with the lower Mn contents.
soned that if the orientation dependence of the grain This effect will be more pronounced in the
growth process differs from that of the nucleation {110}(112) grains, within which fewer (1' nuclei are
International Materials Reviews 1990 Vol. 35 No. 1
16 Ray and Jonas Transformation textures in steels

formed on the deformation bands due to stored gested that the development of fair!y sharp textures is
energy considerations. As a result, in the transfor- expected for all alloying elements which retard the
mation texture, the {332}(113) component will be transformation of austenite, such as Ni, Mo, Cr, etc.
relatively weak compared to the much stronger Yutori and Ogawa56 also studied the development
{113}(11Q) component. of transformation textures in a series of controlled
When the Mn content of the steel is increased, a rolled steels. The materials they used were basically
much finer ferritic structure is produced due to the low-C-Nb steels with additions of Mn, Si, Cr, Mo,
low temperature of transformation and this suggests and V. The total alloy content for the steels was
that the growth of the a' nuclei will be limited. The represented in terms of the equivalent Mn content
effect of grain boundary nucleation will also be much (Mneq = Mn + 4Mo + Cr + Q·1Si). Figure 19, taken
less. As a consequence, the orientation distribution from their work, shows how the orientation densities
of the a' nuclei will be retained in the final texture, of the two major components change as a function of
giving rise to a much sharper {332}(113) component total alloy content. The cooling rates used for effec-
in the texture of the higher Mn steels. The overall ting the phase transformation as well as the product
transformation texture will also be much more phases formed are also displayed in these figures.
intense. Inagaki has extended this reasoning to the It is apparent from their results that, except for
effect of the other alloying elements and has sug- the highest cooling rate, the sharpness of the

9 9
(0 ) (b)

g8 g8
"0

c: • "t!c:
~
)(
7 )( 7

6 6
?: • ?:
·iii 'iii 11131(110)
"0
~ 5 ~ 5
"0

.~ 4 1332\ (113) .§ 4
~ ~
] 3 ] 3 13321(113)
0 <5
2 2

----- FP----+----FB----~-A-- ··FP·+--- FM---.--·FBM----A--

0 0
2 3 2 3
9 9
(c) (d)

~ 8 E 8
-.--.-.--------
"0

0
c: • "0

t! 11131(110) c:
7 ~ 7 • 11131(110)

-
II(
)(

6 6
• 13321(113) ?:' -----------
~5
III
~ 5 13321(113)
c: "
'"0
tI
4 •

"0

4
c
.2 ~
43 ~ 3
C ·C
tI 0
~ 2 2

·-FP..•- --FM--- + --- ---. A --- ----- ------------- M------------_ ..


o o
2 3 1 2 3
Mn ~q.(= Mn ."Mo. CrtO.1Si) Mn ~q.(1I: Mn. 'Mo 'Cr t 0.1 Si)

a 1 K s-1; b 6 K S-1; c 16 K S-1; d 80 K S-1; A acicular ferrite, 8 ferrite.' F polygonal bainite, M martensite, P pearlite
19 Dependence of orientation densities of {332} (113) and {113} (110) texture components, on alloy content (as
represented by Mneq and cooling rate (after Ref. 56)

International Materials Reviews 1990 Vol. 35 No. 1


Ray and Jonas Transformation textures in steels 17

transformation texture increases as total alloy con- rite texture, shown in Fig. 20a, was rather weak and
tent goes up. Thus these results agee very well with consists mostly of the {100}(011) component. This
the idea put forward by Inagaki. orientation generally originates from the cube
{100}(001) component of the austenite recrystal-
lisation texture.
Effect of rolling conditions
on transformation texture Deformation in unrecrystallised r region
The inheritance of a strong texture by the a phase above Ar3
from the r during transformation depends principally From the early stages of the development of control
on the severity of the rolling texture of the parent led rolling, the importance was recognised of
austenite. The intensity of the austenite rolling deforming austenite in the unrecrystallised r region
texture depends in turn on the amount of deforma- above the Ar3. This treatment increases the surface
tion to which the r has been subjected, as well as on area of the austenite grain boundaries and introduces
the temperature of the deformation. The greater the a high density of deformation bands into the matrix.
amount of reduction at a particular temperature, the Thus, ferrite nucleation is made possible, not only at
more severe will be the r rolling texture. If the austenite grain boundaries, as in conventional hot
temperature is sufficiently high, static recrystallis working processes, but also in the grain interiors,
ation takes place after rolling, reducing the strength leading ultimately to a much finer grain size. Since
and changing the nature of the r rolling texture. recrystallisation is effectively retarded in austenite
At lower rolling temperatures, plain C steels con- deformed in this region, the strong deformation
tinue to recrystallise in the conventional manner, but textures produced by heavy amounts of deformation
Nb steels display two other types of behaviour. If the can be retained in the austenite and can finally be
interpass times are long, as in reversing mills, copious inherited by the a phase during transformation.
precipitation takes place, which prevents recrystal- Using ODF analysis, Inagaki60 showed that, for a
lisation, so that the ferrite forms from deformed aus- Nb-V steel, the texture of specimens finished at
tenite, as discussed above. If the interpass times are 850°C consists of two major components, namely
short, as in strip mills, the strain first accumulates, the {332}(113) and {113} ~ {4 411}(110). These
then dynamic recrystallisation is initiated. The latter originate, respectively, from {110}(112) and
tends to randomise the deformation texture, so that {112} (111), which are the rolling texture
ferrite forms from austenite with a less distinct components of the parent austenite. Many previous
texture. investigations4,15,36,~7,58,80,82
have also shown that
In order to understand the effect of controlled these orientations are the transformation products of
rolling on texture inheritance by the a phase from the main components of the rolling textures of steels
the parent r, the effects of the various mechanisms deformed in the unrecrystallised r range. When the
described above are examined more closely. With finishing temperature is decreased within this range,
this view in mind, the influence of the rolling there is an increase in the severity of the transfor-
parameters in the three distinct stages of conven- mation texture (Fig. 11). This phenomenon was
tional controlled· rolling (Fig. 1) on the resulting explained in terms of an increase in the sharpness of
transformation textures is described below. the original austenite rolling texture.
The effect of finishing temperature on texture
Deformation in recrystallised r region formation in a simple C-Mn steel has been observed
When steel is deformed in the recrystallised r region, to be quite different from that in the Nb- V steel. 60
grain refinement takes place through static recrystal- The textures of the specimens finished in the unre-
lisation.78 This phenomenon proceeds in a manner crystallised r range are considerably weaker than
similar to that in cold worked materials, and is those of the Nb-V steel finished at the same tem-
followed by normal grain growth. The critical amount perature (Fig. 11). The main texture components
of deformation needed for the completion of recrys- here can be broadly identified as {554}(225) (near
tallisation during hot working Ccrih is larger than at {332} (113») and {100} (011). The former
room temperature and its temperature dependence is component appears as significantly broader and of
substantially higher in Nb than in plain C steels.68 much lower intensity in the Nb-V-free steel than in
This difference can be attributed to the formation of the Nb-V steel, irrespective of the finishing tem-
strain induced Nb(C, N) precipitates in the Nb perature. This can be attributed to the greater accu-
steels,66,79so that static recrystallisation is essentially mulated strain in the no-recrystallisation and (r + a)
suppressed during rolling below 950°C (Ref. 3); i.e. regions in the micro alloyed as opposed to the plain C
as long as there is sufficient time for precipitation to steel. The {100}(011) component presumably arises
take place, as in reversing mills, or during the as a result of the inheritance by the a of the cube
roughing to finishing interval. texture formed in the partly recrystallised austenite in
The hot rolling of low-C steels at temperatures specimens of the Nb-V-free steel. Result§.similar to
above the austenite recrystallisation temperature the above were obtained by Davies et al.,59 who
generallj produces a rather weak transformation studied texture inheritance by ferrite from hot
texture. Kallend et al.8o determined the 0 DF of the deformed austenite in a series of C-Mn-Nb and
ferrite in a 0·11C--O·35Si-1·35Mn--O·052Nb steel fin- C-Mn steels.
ished at a temperature of 1000°C after 80% reduction
by rolling. The austenite was expected to be almost Deformation in (r + a) region
fully recrystallised under these conditions.81 The fer- During controlled rolling, the deformation of steel in

International Materials Reviews 1990 Vol. 35 NO.1


18 Ray and Jonas Transformation textures in steels

c-o
\.0
.~co
U)
C'1
U)
0
en
.•..
0
C\l l!1 II C
II II
t& Q)
t& t& 0
!;
LL
C
0
oQ

;i
0
0
co
'+-
~ l!1 U) 0
co ~ C
I"'- 0
II .e. II
't:s
~ ~
" Q)
I.

C)
:E
"0 I.

I.
Q)
~C'a
~ (.)
CD 0 C'1
0
0
II U) 0
t& 0
~
t& .•..
C'a_
,,0
Q)CO
.c~
en Q)
'2 a:
-:3- .0
~Q;
Q)~
C'a
.•.. Q)
en
Q)
-
.cl.
z:s
N"
Lt)Q)
. C? g
U) 0100
C'1
to I Co
C\J
II
U)
l!1 . 0
(j)
c ..
~c
Lt) .2
.-& M ••••
• C'a
IE
.- I.
cno
Lt)'+-
Men
" C
OC'a
O~
~C
~ ..:s
OC)
C.S
to .- en
l!1 "'C:s
"'t
II I"'- ~ ~
~ II

t'6't
.- '+-
,BO
.cQ)
o .t::
Q) C
••••Q)
"E 1;)
Q) ~
'+-C'a
'+-"
~~
c-
.2
........~
CD 0
':'
M
~
M
co
oJ: 0
C'1 1O C I.
II
Q)~

0"
!;S
LLCJ
C'-
O"g
I.
~ Co
a 0
N

International Materials Reviews 1990 Vol. 35 NO.1


Ray and Jonas Transformation textures in steels 19

the (y + a) region has been found to produce finer a visible in Fig. 21, which shows the development of
grain sizes.3 In addition to grain refinement, substan- texture in a Nb steel as a function of the amount of
tially improved yield and ultimate tensile strengths deformation in the two-phase region. 85 This steel was
are also achieved.68,83,84 During such rolling, the initially deformed in the unrecrystallised y region to
following processes take place in the steel:4 produce a weak texture comprised of the {112}(110)
and {554}(225) components. Increasing the amount
(i) crystal rotation of the parent y phase
of deformation in the (y + a) region led to an increase
(ii) y ~ a phase transformation, and
in the severity of the original texture of the material
(iii) crystal rotation and possible recrystallisation
along with some modifications, such as the sharpen-
of the product a phase.
ing of the {554}(225) component.
The resultant texture of the steel is therefore quite Inagaki and Kodama6o,88 studied the development
complex and largely influenced by the relative contri- of texture in several Nb and Nb--V steels· finished at
butions of these three processes which, in turn, various temperatures. They found that, for speci-
depend on the composition (presence of precipi- mens finished at just above the Ar3 temperature,
tates), temperature, and amount of reduction in each the main orientations of the a texture were
pass, and above all on the finishing temperature. {332}(113) and {113} -- {112}(110). These orien-
Thus the final texture is made up of the accumulated tations get progressively modified as a result of
components of the y ~ a transformation texture and deformation of the a phase when the finishing tem-
the hot rolling texture component of the a phase. perature is lowered. The changes that have been
The finish rolling temperature in the (y + a) region identified are the following:
plays an important role in texture development.
(i) {332}(113) ~ {554}(225) ~ {111}(112)
When the finishing temperature lies in the upper (y +
a) range, the amount of a phase formed, before the and
final pass, is relatively small. In such a case, the (ii) {113}(110) ~ {112}(110) ~ {223}(110).
contribution of crystal rotation in the a phase to the The orientations listed in (i) have a common (110)
overall texture is not particularly significant. By con- direction parallel to TD, whereas the orientations in
trast, when the finishing temperature lies in the lower (ii) have a common (110) direction parallel to RD.
(y + a) range, most of the y phase has already been Theoretical calculations, based on crystal plasticity
converted to a before the final passes. The ferrite and the relaxed constraint method, have been carried
grains formed earlier at higher temperatures, which out to simulate the rotations in the a phase during
inherit the y rolling texture, experience further rolling.31 The results indicate that the successive
deformation at lower temperatures, which further orientations listed in (i) above can indeed be obtained
sharpens the texture of the a phase. The remaining by rotation of the a about the (110)IITD axis, with
austenite grains are deformed continuously as the {Ill} (112) as the end texture. However, with regard
temperature is lowered in the (y + a) region, result- to the orientations in (ii), the rotation of {113}(110)
ing in an increase in the sharpness of the y texture about the (110)IIRD axis only produces the
that is, eventually, inherited by the transformed a {112}(110) component, which is too stable to
phase. undergo any further reorientation. Thus the
A number of early investigators4,59,68,83-87 have
{113}(110) component of the transformation texture
suggested that the texture developed in steels as a is not in fact converted into components of the y fibre
result of rolling below the Ar3 consists of two major ({Ill}lND), which are the ones responsible for good
components, namely: (a) a partial fibre texture deep drawability in steels. The simulations have
having (110) axes parallel to the rolling direction shown instead that the end orientation in (i) above,
with orientations lying in the range between namely the {Ill} (112), is gradually converted by
{001}(110) and {111}(110); and (b) the rolling into the {111}(110) component, as summa-
{Ill} (uvw) fibre texture. These features are clearly rised in Table 5 above. Both the above orientations
are important components of the y fibre. Thus the
.: !0011<110>,.: (112l<110>; ,: f554~<225> crystal plasticity calculations clearly point to the

.--.
<110>IIRO
desirability of starting with {332}(113) as the main
component of the transformation texture before
further processing of the steel in the (y + a) and a
ranges. They also underline the importance of the
deformation of the a phase, which is discussed in
more detail in the next section.
In plain C steel, rolling below the Ar3 temperature
also leads to the development of a strong {100}(011)
o 9,d(lg 90
.--...
e,d(lQ

<11o>IITD
texture component, apparently due to the grain
rotations taking place in the deformed a phase.31,60

a 0%; b 10%; c 60% Deformation in a region


21 <I>= 45° sectiJn (Roe notation) of ODF of Nb steel,
Although the deformation of steel in the a region
deformed initially in unrecrystallised y range, followed by cooling to room temperature does not
followed by deformation in (y + (1') region (after lead to any phase transformation, the salient features
Ref. 85) of this process are considered here because of its

International Materials Reviews 1990 Vol. 35 NO.1


20 Ray and Jonas Transformation textures in steels

technological importance. During controlled rolling, rolled pure iron has also been found to consist of a
finish rolling is occasionally carried out in the a region partial fibre with (110) parallel to the normal direc-
to improve the mechanical properties.84 This is tion.95 Furthermore, the intensity of the surface
sometimes referred to as 'continuum rolling' when it texture of intercritically rolled steel increased with
involves successive reductions in the y, (y + a), and a increasing volume fraction of the a phase. This sug-
regions. 89From his work on a simple C-Mn steel and gests that the surface texture produced during the
on another containing Nb and V, Inagaki60 concluded warm rolling of steels is due to shear of the a phase.
that, since the textures formed by rolling in the lower Such results are also in agreement with the findings of
(y + a) range should already be near the stable end Williams,96 who observed that the main components
orientations of the a rolling texture, further changes of the shear texture of a-Fe consist of {112}(111)
during deformation in the a region will not be signifi- plus orientations falling between {110}(001) and
cant. This is also apparent from Fig. 11, taken from {110}(111).
his work. Dillamore and Roberts97 have shown that surface
Recently, there has been increased interest in extra texture is generally related to the texture at the centre
low carbon steels9Q-94which, when deformed in the of the specimen by rotation about the transverse
high a range with or without a subsequent recrystal- direction, the angle of rotation bying affected by the
lisation anneal, can yield materials with high R values. extent of lubrication and the rolling temperature.
It has generally been agreed that the deformation of This general rule has been found to be more or less
steel in the a region produces the bcc rolling texture satisfied.6o The inhomogeneity of the texture in the
consisting of an a fibre* with (110)IIRD stretching through thickness direction in warm rolled steels is
from {001}(110) to {111}(110), and a yfibre* with also reflected in the R values. Figure 22, from the
{lll}lND. It has been found92 that, for finishing work of Senuma and Yada,91 displays the variation in
temperatures lower than 750°C, the intensity of the R as a function of distance from the surface of the
{Ill} component increases as the deformation tem- sheet in one of their steels. It is evident from this
perature decreases and the amount of strain increases figure that the surface texture decreases the overall
(see Table 5). Such rolling is of commercial R value of the sheet and consequently the deep
importance because the transformation texture drawability.
components produced from deformed austenite, i.e. The inhomogeneity in both the microstructure and
the {332}(113) and {113}(110), do not lead to Rand texture of steel sheets warm rolled in the a' region
~R values as desirable as those contributed by the seems to persist even after these are subsequently
{Ill} fibre and the {554} (225) component (see completely recrystallised.9o Figure 23 shows the
Tables 3 and 4). _variation in relative intensity of the various texture
Recrystallisation carried out after deformation in components in an extra low carbon steel as a function
the a range sharpens the y fibre component in the a of distance from the sheet surface when rolled both
(with the maximum intensity at {11J}{112») at the with and without lubricant, in the as rolled as well as
expense of the a fibre component.90 Hashimoto recrystallised conditions. 93The effectiveness of using
et al.93,94 have reported that, in interstitial free lubricants to keep the intensity of the {Ill}
steels, rolling in the ferrite no-recrystallisation region component uniformly high throughout the thickness
yields the {112}(110) texture, which changes upon
recrystallisation to {554}(225) with a concomitant
high R value. It is now more or less agreed that the distance from)
following conditions have to be fulfilled in order to • ( the surface
2.0
produce warm or hot rolled steels with textures that Tt
give rise to high R values: (a) finish rolling should be !t
carried out in the ferrite no-recrystallisation region; 8
(b) Ti or Nb should be added to extra low carbon
AI-killed steels so as to raise the ferrite no-recrystal-
lisation temperature; (c) the solute carbon content
during rolling must be minimised by precipitating the
C as TiC or NbC; and (d) good lubrication between
the rolls and the workpiece must be employed during
finish hot rolling. 90-9
It has been pointed out that a major problem
associated with the warm rolling of steels in the (y +
a) or a region is inhomogeneity of the texture in the
through thickness direction. Inagaki60 reported that, o Experimental results
in his steels, a surface texture developed when the t Thickness of the specimen
finishing temperature was below 750°C. It consisted
of a partial fibre with (110) parallel to the normal
direction and weak {113}(332) to {4 4 11}(1111 8) o ~ 1~
components. The surface texture of heavily cold Angle between tensile direction
and rolling direction

22 Plot showing variation of R as function of distance


* These terms are not to be confused with the £l' and y phases in t from surface of warm rolled sheet steel (after
steel. Ref. 91)

International Materials Reviews 1990 Vol. 35 No. 1


Ray and Jonas Transformation textures in steels 21

without lubricant with lubricant ( tall ON) without lubricant with lubricant (taltON)

(222)
( 222)

-. (200)
::~::~_.~::.8::'':~ (211)
(211) -.> •.~~.~-:~-<>- -0-..00
(200) .••••.•••.•

( 110)
(110)

(b)
o 10 20 ~ J.Q 50 0 10 20 l:) 40 50 o 10 20 ~ /ij 50 0 10 20 ~ 40 50
Through thickness location, -I. of 1hickness Thr~h thickness location, -I. of thickness
a as rolled condition; b recrystallised condition
23 Effect of lubrication condition on variation of pole intensity along through thickness direction (after Ref. 93)

is clearly illustrated in the figure. This improvement soaked at 1100°C (smaller y grain size) is sharper
in texture is also reflected in the increase in R value than that of the specimen soaked at 1250°C (larger
for the material (Fig. 24). y grain size).
The transformation textures formed in steels by the
martensitic transformation also seem to be influenced
Effects of austenite grain size and cooling by the initial austenite grain size.88 A 0·lC-1·7Mn-
rate on transformation texture 0·04Nb-O·08V steel was soaked at two different tem-
Transformation textures in steels are influenced by peratures, 1250 and 1050°C, then controlled rolled
the initial austenite grain size, which is determined by and finished at 760°C, followed by quenching into
the soaking temperature of the steel before control- water to produce a martensitic structure. The <I>= 45°
led rolling begins. For example, a 0·lC-O·3Si-1·6Mn- sections (Roe notation) of the ODFs of these speci-
0·04Nb steel was soaked at two different tem- mens are presented in Fig. 26. It is apparent from this
peratures, namely 1100 and 1250°C, then controlled figure that, although the major orientations are the
rolled to a finishing temperature of 800°C to produce same in the two cases, the {332}(113) component is
a ferrite-pearlite structure. 58 Figure 25 illustrates the strengthened noticeably when the smaller initial y
effect of soaking temperature (or y grain size) on the grain size (lower soaking temperature) is used. By
transformation texture of this steel. It can be seen contrast, the {113}(110) component remains
from the figure that the texture of the specimen essentially insensitive to soaking temperature.

Effect of cooling rate during transformation


2·0 The cooling rate during phase transformation after
controlled rolling in the r or (y + £1') region has been
found to have a significant effect on the resulting
transformation texture.4,56 Although the major
components of the transformation texture of marten-
site, bainite and ferrite have consistently been identi-
fied as {113}(110) and {332}(113), the sharpness of
the overall texture as well as the relative intensities of
the components seem to vary as a function of cooling
rate. Figure 27 represents <I>= 45° sections (Roe
notation) of the ODFs of some controlled rolled
hot roll steels with various transformation products.98 It is
FET: 700°C
evident from this figure that the intensities of the
major components are quite sharp and comparable in
red.: 4 . 5 - 1· 3 m m
the case of martensite and acicular ferrite. On the
(700/0) other hand, these components are decidedly weaker
annea I: 750°C I 3h in intensity in the ferrite-pearlite.
1·0
That the· transformatfon texture is generally
weaker when y is transformed into ferrite-pearlite by
o 10 20 30
slow cooling than when quenched into martensite has
Load drop by lubrication ,0/0 been reported by a number of workers. 11,50,58,98 The
24 Effect of lubrication conditions on R value (after combined effect of cooling rate during transfor-
Ref. 93) mation and alloy composition on the intensities of the

International Materials Reviews 1990 Vol. 35 NO.1


22 Ray and Jonas Transformation textures in steels

RD RD

Q'5
1·0

(0) ( b)

a 11 OO°C; b 1250°C
25 (200) pole figures showing effect of soaking temperature on texture of 0·1C-0·3Si-1·6Mn-0·04Nb steel (after
Ref. 58)

major texture components in a number of controlled formation texture components of steel, i.e. the
rolled steels is depicted in Fig. 19. There it is {332}(113) and {113}(110), are summarised sche-
shown that, whereas the {332}(113) component is matically in Fig. 7. This diagram gives an overall view
strong only after fast cooling, the {113}(110) of the types of transformation in texture components
component is relatively insensitive to the rate of encountered in controlled rolled steels, their modifi-
cooling. Yutori and Ogawa56 replotted the data of cations as a function of the rolling schedule, as well as
Fig. 19 to produce Fig. 28, which displays the change the effects of different compositional and processing
in orientation density of the {332}(113) component variables on their relative sharpness. Thus, this dia-
as function of cooling rate. The different product gram may be used as a guideline towards producing
phases formed as well as the alloy contents of the tailored transformation textures during the con-
steels (represented by their Mn equivalents) are also trolled rolling of steels.
marked in this diagram. Figure 29, again replotted
from Fig. 19, shows that there is, in fact, a simple
Relation between transformation texture
relationship between the transformation texture and
and austenite rolling texture
the mode of transformation.
The effects of factors such as solute content of the It is now clear that in order to have a marked transfor-
steel, finishing temperature during rolling, soaking mation texture in steel it is necessary to deform the
temperature, cooling rate, etc., on the major trans- material by a significant amount in either the unre-
crystallised y region or in the intercritical (y + a)
range. The orientations in the aphase produced from
90 90 the {110}(112) and {112}(111) y rolling texture
80 80 components, can be derived using matrix algebra via
70 70 any of the lattice relationships of Table 1 (Ref. 99).
60 60
For example, by assuming that all the lattice variants
of the K-S relationship are e~ually favoured during
~ SO SO
"0 the transformation, Inagaki 8 calculated the ori-
-:3- 40 40 entations resulting from these y orientations and
30 30 superimposed the former on the experimental ODF
20 20 for a 2·48%Mn steel. Four constant 'II sections (Roe
notation) of that ODF are represented in Fig. 30. It is
10 10
interesting to note that the calculated orientations
o 0 agree reasonably well with the experimental ori-
o 10 20 30 40 50 60 70 80 90 0 10 20 30 40 50 60 70 80 90 entation distribution. Furthermore, the observed
e,deg {113}(110)~ peaks are surrounded by a group of
a 1250°C; b 1050°C orientations derived mainly from {112} (111 )y,
26 Effect of soaking temperature on texture of mar- whereas the observed {332} (113) ~ peaks are
tensite in 0·1C-1· 7Mn-0·04Nb-0·08V steel; <I>= 45° surrounded by another group of orientations derived
section, Roe notation (after Ref. 88). See Fig. 5b for mainly from {II O} ( 112) y. These observations indi-
key to components cate that the transformation texture components of

International Materials Reviews 1990 Vol. 35 No.1


Ray and Jonas Transformation textures in steels 23

• (001\ <110> 9
~P13~<110>
--.. '3321(113)
O{112} <110> E0 8
., (332~ <113> "0

c Mn eq.
",'- 7 •
A A A 3.30 M

/2.45
)(.
• • •
6 A
- ~
II)
c 5
"0
~
C
.2 4
--
os
c

FB FBM
~ 3
'\:
0

FP
2 FP

(a)

0
10 100
1
Cooling ra te I K 5-

28 Change in orientation density of {332} (113)


component as function of cooling rate and alloy
composition (after Ref. 56)

the a phase, namely {332}(113) and {113}(110),


originate from the ytexture components, {110}(112)
(brass) and {112}( 111) (Cu) , respectively. Similar
results have been obtained by the present authors.IOO
It has been further shown that at least some of the
(b) intensity of the two major transformation texture
o components is due to components derived via trans-
formation from the third major y rolling texture
90 component, the S{123} (634) (Ref. 100).

Stability of transformation textures


InagakilOI hot rolled a 0·lC-1·35Mn-0·03Nb steel to
a finishing temperature of 800°C to prepare a material
with a strong initial texture. As can be seen from the
<I>= 45° section (Roe notation) of the corresponding
ODF, the specimen had a strong transformation
texture consisting of {332}(113) and {113}(110) as
30 the main components (Fig. 31a). The textures
obtained after the specimen was reheated at 1250 or
1150°C for 1 h followed by water quenching, are
shown in Fig. 31h and c, respectively. The similarity
with the initial texture of the specimen before heat
(c) treatment is striking and indicates that the former is
90 quite stable. This can happen if, during reheating, the
o 30
ferrite transformation texture is reconverted into the
6,deg
original {110}(112) and {112}(111) Ytexture; these
a polygonal ferrite-pearlite; b acicular ferrite; c martensite components subsequently transform during water
quenching, into the martensite texture, again consis-
27 <I>= 45° sections (Roe notation) of ODFs showing
transformation textures of controlled rolled steels
ting of {332}(113) and {113}(110) as the major
with various structures (after Ref. 98) orientations.

International Materials Reviews 1990 Vol. 35 NO.1


24 Ray and Jonas Transformation textures in steels

These experimental results indicate that when a given


7
grain within a particular population transforms
shear
•I mode
according to one of the, say, 24 variants of the K-S
relationship, on retransformation into the original
• ------ •• phase, it does not select at random just any variant,
E
"0
0
6

/
/:: •
but reverts back to the original orientation using the
specific variant relationship previously employed. In
c
other words, individual grains possess some kind of
L
0 I mixed • memory regarding the exact transformation path they
><
•......
>.
5
I
I mode
• have followed during entire sequences of transfor-
+-' I mation from a' ~ Y~ £1'.
II)
I
c
QJ I
Analytical methods for prediction of
"0

4 I
c I
transformation textures

·••
0
+-I I
0 /
+-I The hot working of steel is largely carried out when
c
QJ
3 ./ / the material is in the austenitic condition. Attempts
L
0 to improve the properties of as rolled steels at ambi-
M enttemperatures by manipulating their textures must
'-'
N
2

diffusion
therefore involve methods of influencing the textures
developed in the parent austenitic phase. However,
M
~ mode experimental difficulties generally preclude the meas-
urement of austenite textures before transformation.
Hence it has been necessary to use indirect methods
to study texture development during the deformation
of austenite. Several analytical techniques have been
proposed for this purpose and these are discussed in
o turn below.
29 Relationship between intensity of {332} (113) Methods based on use of
texture component and mode of transformation
texture components
(after Ref. 56)
The simplest procedure for the prediction of transfor-
mation textures is based on the description of the
In an earlier work,88 a specimen taken from the parent austenite texture as .an assembly of
mid section of a controlled rolled O·08C-2·2Mn- components, as given in equation (2). Each
O·4Mo-O·3Ni-Q·04Nb steel having an acicular ferrite component is operated on in turn according to the
structure was heat treated to produce either marten- precise transformation relationship assumed to exist
site or ferrite. A fairly strong texture, similar to the between the parent and product phases. The resulting
original texture but less sharp, was obtained after components are then taken to constitute the product
these two heat treatments, although the microstruc- texture. For sim~le transformations, known transfor-
ture had changed completely from the original one. mation matrices 02 may be used for determining the
In fact, it was observed in earlier investigations that indices of the product texture components; in more
transformation textures in steels can be relatively well complex cases, a sequence of operations may be
preserved, even after repeated reheating cycles.4,39 necessary. Using a K-S orientation relationship,

• a. derived from (110) <112>y


• a. derived from 1112~<111 >y

90 (0) 90

o o

a 0°; b 40°; c 65°; 'd 90°


30 Constant 'If sections (Roe notation) of experimental ODF for 2·48°kMn steel: orientations derived from Cu
{112} (111) and brass {110} (112) positions in y via K-S relationship are superimposed (after Ref. 58)

International Materials Reviews 1990 Vol. 35 No. 1


Ray and Jonas Transformation textures in steels 25

90

80

70

~ 50
"0

~40

30
• (3 3 2~< 11 3 >
20
• (311J <011>

a 10 20 30 40 50 60 o 10
8, deg
a initial texture; b texture after heating to 1250°Cfor 1 h and water quenching; c texture after heating to 1150°Cfor 1 h and water quenching
31 <I>= 45° sections (Roe notation) of ODFs for 0·1C-1·35Mn-0·03Nb steel (after Ref. 101)

Jones and Walkerlo3 predicted the ferrite textures product structures are known. Thus the coefficients
which are expected to result from the transformation W1mn of the product texture are related to the coeffi-
of a range of austenite textures. They did this by cients mmn of the parent texture by the expression
expressing the parent texture as a number of ideal
orientations and also by assuming that all the 24 2 )1/2 1

possible variants of the K-S orientation relationship W1mn = ( 21 +1 P~l WlmpZlpn


occur with equal probability during transformation.
They compared the predicted pole figures with the X (cos f3) exp (ipa) exp (iny) . (6)
experimentally measured ferrite pole figures in order
If, in the absence of physical constraints, the selection
to ascertain whether austenite recrystallisation had
of variants takes place in a random fashion, equation
occurred prior to transformation.
(6) may be rewritten as
A variation of this method was used by Haslam
et a1.,50 who employed the ODF of 80% cold rolled 2 )1/2 1 N 1
copperl04 to represent the deformed austenite texture
in terms of a set of components. They then tried to
Wlmn = ( 21 +1 p~lmmp ~1 N Zlpn
predict the ferrite texture by transforming these X (cos f3i) exp (ipai) exp (inYi) (7)
components using the K-S relationship. This resulted
in the prediction of a number of textures which were where N is the total number of transformation
found to be similar to those for a range of hot rolled variants. Where some selection of variants occurs,
steels. However, this approach, like that of Jones and this can be allowed for by replacing the term 1/N in
Walker, suffers from the disadvantage that the equation (7) by a factor Ii which gives the relative
description of the parent texture was oversimplified frequency of occurrence of each variant. In that case,
and no quantitative correlation was apparent. equation (7) has the form

Methods based on distribution


function analysis
It has become evident that the accurate prediction of
transformation textures requires the more complete
description of parent textures than can be done in Based on equation (7), Davies et ai.lO have written a
terms of ideal components. The ODF is better suited computer program to calculate the transformed
to this purpose, and when the precise crystallographic texture coefficients W1mn from the experimentally
relationship between the parent and product is determined texture coefficients mmn for the fcc ~ bcc
known, it is possible to calculate the orientation of the phase transformation. The form of the transfor-
product phase by using the appropriate transfor- mation is described by specifying the polar angles of
mation matrix. Roe23 has shown that when the an invariant axis and the angle of rotation about that
texture is represented by an ODF, the original set of axis. The K-S orientation relationship was used for
series expansion coefficients, W1mn (equation (4)), the calculation and it was assumed that all 24 variants
can be transformed into a new set of expansion of the transformation were equally probable. A simi-
coefficients, W1mn, for the product ODF, provided lar approach was em,rloyed by Pospiech et ai.105 using
the Euler angles a, f3, and Yspecifying the rotations the Bunge notationl ,25to explain the bainite textures
relating the crystallographic axes of the parent and formed from hot rolled austenite.

International Materials Reviews 1990 Vol. 35 No. 1


26 Ray and Jonas Transformation textures in steels

Methods based on use of misorientation the parent crystal. Thus, in the case of cubic crystals,
distribution function a peak at the orientation (hkl) [ uvw] means that the
The procedure outlined above assumed that it is (hkl) planes in the product are parallel to the (001)
possible to describe the transformation in terms of a planes in the parent and that the [uvw] direction in the
set of orientation relationships. If, however, a more product is parallel to the [100] direction in the parent.
generalised transformation takes place, as for Indexing charts have also been published for cubic107
example, during recrystallisation, a continuous distri- and hexagonal108 crystal systems and these can be
bution of orientation relationships can develop used to assist in the interpretation of MODFs.
between the parent and product crystals. This, in The existence of a set of equations relating the
turn, involves a continuous distribution of the Euler coefficients WImn, W1mn, and TImn suggests that, given
angles ll', f3, and y relating the two phases. In such a any two of these sets of coefficients, it is possible to
situation, as shown by Sargent,106 the distribution of derive the third set. The procedure for deriving the
angles can again be described in terms of spherical coefficients of the parent texture, WImn, from the
harmonics, leading to the so called misorientation known coefficients TImn of the MODF and the meas-
distribution function (MODF) ured coefficients W1mn of the product texture is
known as 'untransformation' and has been described
a 1 1
in detail by Kallend et al.80 The untransformation
t( ll', f3, y) = 2: 2: 2: m=-I n=-I
TImnZImn procedure is of considerable potential value for the
1=0 study of texture development in high temperature
x (cos f3) exp (-ima) exp (-iny) (9) phases, such as hot rolled austenite, where the direct
measurement of texture is handicapped by experi-
where TImn are the coefficients of the MODF. mental difficulties.
According to Sargent,106 if the parent and product An example of untransformation was presented
textures, described by the coefficients WImn and above in Fig. 20b where the parent austenite texture
W1mn, respectively, are related by the MODF with was obtained from the product ferrite texture (Fig.
coefficients TImn, then the relationship between all 20a) by using this procedure. In this case, the predic-
these coefficients can be expressed in the form ted ODF for the hot rolled austenite was found to
consist largely of the cube {100}(001) component, .
2 )1/2 1 which in fact is a prominent orientation of recrystal-
W1mn = ( -21
+
1 4,n2 2:
p=-I
WImpTIpn (10)
lised fcc metals with high stacking fault energies.109

The above is a general expression for a set of (21 + 1)


equations with (21 + 1) unknowns which can be Limitations of transformation texture prediction
solved to evaluate the coefficients TImn. Once these At this stage, it is not out of place to discuss briefly the
coefficients have been determined, the function can discreteness of the transformation textures predicted
be computed from equation (9) and then plotted in by the analytical methods outlined above. As shown
Euler space in the same manner as an ODF. It must below, reasonably good correspondence has often
be remembered, however, that in this case the func- been obtained between predicted and observed
tion represents the distribution of orientations of the textures. However, the results of various studies have
product crystals with respect to the reference axes of clearly illustrated the problems faced in resolving

cD=o

.t
6 0 0
o 0 0
/)

~=45 ~=56'3 ~ = 33·7

6

6
~

o ~ 0
(a) (b) 0
<I> = 71·6 <I> = 90 q>=63'4 <;P=71' 6 <1l = 90

32 MODFs for y ~ £l' transformation using a the K-S orientation relationship and b the N-W orientation
relationship, without any variant selection in each case (after Ref. 15)

International Materials Reviews 1990 Vol. 35 No.1


Ray and Jonas Transformation textures in steels 27

small differences between the predictions. The ori- selection.lO,80,82,11Q--113 It appears that when the
entation relationships suggested for the austenite- transformation is diffusion controlled, as in the case
to-ferrite transformation, such as the Bain,5 of the austenite ~ ferrite transformation in steels,
Kurd j umov-Sachs, 6 Nishiyama-Wassermann, 7,8and there is no strong evidence for variant selection.lo
Greninger-Troiano,9 differ between themselves by The experimental ODF for the ferrite obtained in the
only a few degrees (Fig. 3c). Furthermore, the case of a hot rolled 0·12C-1·47Mn-Q·05Nb steel
analytical methods described above predict textures finished at 815°C after 80% reduction is illustrated
which do not show any clear cut distinction between in Fig. 34a. The analytically predicted 0DF for the
the different orientation relationships. It has been same phase (Fig. 34b) was calculated from the ODF
suggested15 that this may be due to two factors: (a) of 60% cold rolled high purity Al using the K-S
the experimental limitations of the available tech- orientation relationship, without any variant
niques for the measurement of texture, and (b) the selection.lo The resemblance between the experi-
non-ideal nature of the transformation itself. Again, mental and analytically derived textures is striking
the MODFs for the various relationships, for and demonstrates that analytical methods based on
example the K-S and the N-W, are essentially identi- distribution function analysis can be used to make
cal (Fig. 32). Hence these cannot be used to make satisfactory predictions regarding textures when
distinctions between orientation dependent transfor- orientation-dependent transformations take place.
mations which differ by only a few degrees, and a Similar agreement has been reported between the
choice can be made instead on the basis of physical analytical predictions and experimental textures of
considerations, which favour the use of the K-S the ferrite transformed from a 0·18C-1·28Mn-
relation. 0·03Nb-Q·04V austenite.lOO
In contrast to the behaviour of ferrite, several
studies of shear transformations (such as austenite ~
Correspondence between analytically predicted
martensite in steels) indicate that the product textures
and experimentally determined textures
predicted by the analytical methods without assuming
The worth of an analytical prediction lies in how well any variant selection are not in agreement with the
it fits the experimentally determined texture. As experimental textures. 4,50,52,57,73,82,100,110,112,114-118
stated above, because of experimental difficulties, it For example, Fig. 35a represents ¢2 sections at 10°
is often impossible to measure the texture of the high intervals of the experimental ODP of the bcc marten-
temperature austenite phase in commercial steels, sitic phase in an Fe-30Ni alloy which was cold rolled
deformed or otherwise, before transformation. Thus 80% in the austenitic condition and then quenched in
the austenite rolling texture is frequently assumed to liquid nitrogen.118 The corresponding sections of the
be similar to the texture produced by cold rolling a ODFs predicted using the K-S and Bain relationships
high stackin fault energy fcc metal such as copper or are shown in Fig. 35b and c, respectively.loo These
sl
aluminium. 1,104Furthermore, other fcc metals such latter textures were calculated from the ODF of a
as nickel, which is close to iron in the periodic table, can 950/0cold rolled Ni-40Co alloy without assuming any
be used for this purpose. In fact, an alloy of Ni with 30 variant selection. This particular alloy has a stacking
wt-% Co has a stacking fault energy similar to that of fault energy not very different from that of the experi-
y-Fe (Ref. 100). Figure 33 a-d shows ¢2 sections of mental Fe-30Ni alloy.lOOIt is apparent from Fig. 35
the ODF of a 95% cold rolled Ni-30Co alloy as well that, although the positions of the orientation max-
as the ¢l sections of the ODFs obtained by transform- ima in the various sections of the three ODFs more or
ing it according to the Bain, K-S, and N-W less coincide, the experimental texture is far more
relationships.loo (It is usual to go through the ¢2 severe than the one predicted using the K-S
sections for fcc and the ¢l sections for bcc materials relationship. On the other hand, although the ori-
since most of the important orientations in these entation density values for the experimental ODF
materials appear in these sections.) It is clear from the and the one calculated by using the Bain relationship
above figures that, although the general features of more or less tally in several sections, the latter shows
the three transformed ODFs are similar, the one some quite prominent peaks in other sections which
obtained using the Bain relationship is much sharper are essentially absent in the experimental ODF.
in intensity than the other two. The ODFs obtained These results indicate that the transformation
by transformation according to the K-S and N- W variants do not occur with the same probabilities, i.e.
relationships are similar. An explanation for the some kind of variant selection takes place .during
above can be found in Fig. 3. As has already been martensite transformation. Similar conclusions were
mentioned, experimental evidence indicates that, reached by Hu and Kallend52 on the basis of their
during the y ~ a transformation in steels, the K-S work on a medium-C-5Ni steel.
relationship is generally followed.11,12 It should be
noted that, because of the multiplicity of variants in Importance and criteria of
this transformation, the a textures always appear less
intense than the y textures from which they are variant selection
derived. The observations of the previous section demonstrate
The three transformed ODFs presented in Fig. 33 the importance of variant selection during martensitic
were all calculated by assuming the absence of variant transformation in steels and iron base alloys. Marten-
selection. Many examples have been reported in the site formation is generally accompanied by a change
literature, for both ferrous and non-ferrous materi- in volume and a transformation shear. It can,
als, where transformation occurs without any variant therefore, be anticipated that the course of the

International Materials Reviews 1990 Vol. 35 NO.1


28 Ray and Jonas Transformation textures in steels

+ 13 13 12 15
o 11 11 9 7
o
E 16 15 16 14 E 6 7 7 6
x 12 14 14 15 x 8 10 10 8
o 16 15 14 12 o 6 5 6 6
E 12 12 13 level s 0 2 4 6 ... E 667 levels 0 2 4 6 .. ,
+
(0) ( b)

cf> .
rrcfo
<p 20
O~
25
10 15
3035
40 45 5055
60 65 7075
80 85 90 <1>1
4 4 3 4 4 4 4 4
o o
E 3 3 3 3 E 4 3 3 4
x 4 3 3 4 x 4 4 4 4
o 3 3 3 3 o 4 3 3 3
E 3 3 f 3 3 3 levels 0 1 2 3 ...
3 levels 0 1 2 3 ... ( d)
(c)

33 a ¢2 sections of experimental ODF corresponding to 95% cold rolled Ni-30Co alloy (Bunge notation) and
b-d ¢, sections of ODFs obtained by transforming Fig. 33a according to Bain, K-S, and N-W relationships,
respectively, (Bunge notation) (after Ref. 100)

International Materials Reviews 1990 Vol. 35 No.1


Ray and Jonas Transformation textures in steels 29

"tJ

M
.•..co
Q)

~ ~ 0 OS
~ lO
(j) CJ
N
II
II caCJ
II
t9f t&
~ .•..Q)
..
0t:

..
Q)
'+-

0
'+-
C
'0
C\l
~co
.•..
0
v ~ C
(X)
lO
v ~
•..•...•
Q)
0
II
II
~
.e. t& ~ u.
C
0
"tJ
.•..CJ
Q)

:s
..
Q)
c.
~
~ caCJ
•..•...•
M
0 M <D ~
"
M II
ca
t& II
iG-t C
'9t co
<D oQ

1
"tJ
•.....• C
.c co
Q)
---+-3- .•..U)Q)
.Q
Z
in
0
6
I
C
~•....
"'t
(,0 c: 0 ~
<D
N
(,0
lO
(j)
II
0
N
II
tfr
~
t& t9f 6
"tJ
.!
"0..
.•..0
.c
c-
0_0
"tJ~
Q)~
C Q)
~
(X) lO
~
(,0

;::
....•.
on; a:
.QQ)
II 0:::
.e. t& t& Q)~
:t::-
t:«
Q)"tJ
'+-Q)

- ..
'+- -
0-
0
c"tJ
0-
~S
•••• '+-
00
C Q)
~ Q) ••
":'
M M o =
0
II
M <D a:1(
-Q)
~ u. .•.•
<D
t& iG-t
ce
00

I --+ -3-
a
~~
lII:t
('t)

International Materials Reviews 1990 Vol. 35 No.1


30 Ray and Jonas Transformation textures in steels

followed by a critical assessment of their relative


validities.

Variant selection models


The important variant selection models proposed to
date are the following:
(i) the 'shape deformation' (SD) model by Patel
and Cohen 119
(ii) the 'Bokros-Parker' (BP) model by Bokros
and Parker120
(iii) the 'active slip system' (AS) model proposed
by a number of workers50,73,82,11o,117
(0)
(iv) the 'twinning shear' (TS) model by Higo et
al.121
(v) the 'Bain strain' (BS) model by Furubayashi et
al.14,122
(vi) the 'geometrical parameters' (GP) model pro-
posed by Humbert et al.118
The nomenclature for models (i)-(v) was suggested
by Furubayashi et al.14
Because of the fact that martensite formation
involves a shear deformation, there is an external
f@>cD shape change, and this has been regarded by Patel
2 2 2 2 00 1~ 2030 and Cohen1l9 as an influential factor in variant
3 3 3 2 <p 40506070
8090 selection in the SD model. They considered the inter-
2 2
action of an applied stress with the displacive shear
(b) <h occurring during martensite formation and suggested
that the applied stress can aid the total shape change.
Goodchild et al.123 extended the analysis of Patel
and Cohen to estimate the effect of stress on the
formation of a particular a' variant. They have shown
that the magnitude of the work done by the applied
stress will indicate which martensite variants should
be favoured. Similar analyses were carried out by
Stone and Thomas13 and Kato and Mori.124,125
Detailed examination of the experimental results
obtained by these workers on a number of steels and
iron base alloys has clearly shown that many of the a'
martensite variants that were favoured by the calcu-
lations based on the SD model were simply not
(c)
present in the actual transformed materials. Thus the
SD model has not been found suitable for variant
selection during the martensitic transformation in
35 a ¢2 sections of experimental ODF of martensite in steels.
Fe-30Ni alloy (Bunge notation) (Ref. 118) and b, C The BP model suggested by Bokros and Parker120
¢2 sections of bcc ODFs predicted for Ni-40Co alloy
is based on the interaction of slip systems and habit
using K-S and Bain relationships, respectively
(Bunge notation) (after Ref. 100)
plane variants. In an early study of martensite burst
formation in strained Fe-Ni single crystals, they
accounted for the selection observed by noting that
transformation islikely to be affected by the elastic and the variants that were favoured were those whose
plastic deformations which result from these phe- habit planes were nearly perpendicular to the active
nomena. Depending on the inhomogeneities in tem- slip plane. Conversely, the group of variants that had
perature, strain, and initial microstructure, as well as habit planes which were nearly perpendicular to the
on the physical configuration of the specimen, some active slip direction were suppressed. This behaviour
variants can be favoured over others during transfor- was suggested to be a consequence of the anisotropic
mation.52 Rules or criteria for variant selection must substructure introduced during deformation. A simi-
therefore be postulated, and in order to be successful lar form of variant selection was also reported in
in predicting the product from the parent texture, much later work on an Fe-26·4Ni-O·24C alloy by
models of texture transformation are needed that can Durlu and Christian.126
also take into account the relative weights of all the Borik and Richman114 have also presented experi-
variants. Several variant selection models have been mental data to support the BP model. Their results
proposed over the past few decades. Brief descrip- showed that, in general, the martensite orientations
tions of all the important ones are given below, could be derived from the preferred orientations of
International Materials Reviews 1990 Vol. 35 No.1
Ray and Jonas Transformation textures in steels 31

the austenite in their heavily deformed experimental experimentallx determined pole figures obtained by
steel according to either the K-S or the N-W Abe et al.74,1l The latter authors studied Fe-25·7Ni
relationship. However, one-third of the predicted and Fe-30·2Ni alloys that were heavily rolled in the
orientations were observed to be missing from the austenite condition before transformation into mar-
transformation texture. These missing orientations tensite. It was found128 that both the BP and AS
were, in fact, the ones suppressed according to the models led to wider pole distributions than the
criterion of Bokros and Parker. experimental figures (Fig. 36). By contrast, much
Furubayashi et al.14 contend that Borik and better agreement with the experimental pole figures
Richman's description of the parent austenite was provided by the theoretical pole figures calcu-
texture, in terms of a limited number of components, lated by the TS model using the applied stress as being
is inadequate for the study of transformations and of opposite sign to the rolling stress (Fig. 36).
does not permit the quantitative strength of the pro- The Bain strain (BS) model proposed by Furu-
duct texture to be predicted from the parent texture. bayashi et ale 14,122
is based on the interaction between
Thus, their work may not be considered detailed the applied stress (of rolling) and the Bain strain
enough for a test of the validity of the BP model. characteristic of the martensitic transformation. They
Bateman and Daviesl17 have also used the assump- termed the compression axis associated with the Bain
tions of the BP model to predict the transformation strain the 'Bain compression axis' or BCA. For the
texture of martensite from the experimental texture y-to-a' transformation, the BCA for each of the three
(ODF) of the austenite in an Fe-30Ni alloy. The Bain variants is parallel to the [001], [010], or [100]
predicted texture contained systematic deviations axis of the austenite. It is easy to understand that, if
from the experimental ODF of the martensite. Thus an external compressive stress is applied along the
the BP model has been shown to be only partially [001] axis, the variant having [001] as its BCA will be
successful in providing criteria for variant selection assisted more effectively by the applied stress than
during martensite transformation. the other two. This, of course, leads directly to
In a number of investigations,50,73,82,110,117variant variant selection. The BS model postulates that dur-
selection has been linked to the active slip systems in ing stress induced martensitic transformation, the
the y and in particular to the slip systems subj ected to Bain variant that is selected is the one that will lead to
the largest shear stresses during rolling before trans- the maximum work bein£ done by the applied stress
formation. The variants produced were those which against the Bain strain. 1 2
contained, in the transformation relationship, those Unlike previous models, this model also predicts
slip systems which sustained the maximum resolved the possibility that the texture of martensite might
shear stress during rolling. The above criteria for
variant selection have been grouped together under RD
the'label of active slip system (AS) model. Predic-
tions of the martensite texture (ODF) from the
parent austenite texture incorporating the above
variant selection criteria have generally resulted in
textures that are less severe than the experimental
ones. 117
The TS or twinning shear model was proposed by
Higo et al.121 They proposed that the first shear (i.e.
the twinning or twin-forming shear of the y phase) in
the double shear mechanism127 for the fcc-to-bcc
transformation is the deformation which gets affected (0) (b)
by the applied stress. This model could account for
the observed frequency of the various a' variants RD
produced during stress induced martensite formation
by postulating that the critical atomic movement to
initiate a' formation is the first shear along the
{111}y(2ll)y direction, followed by a suitable spon-
A::i~ ,;"',"~1..
.-?r:~"--"-~~"',:':.
j'::"\~

taneous complementary second shear that completes


the transformation.12l Later work by Kato and
Mori124,125supports the postulations of the TS model.
In order to assess the validity of the various variant
selection criteria, Furubayashi128 carried out
computer simulations of the martensitic textures '''-.---.-:.,/
formed from warm rolled austenite having a Cu-type
rolling texture. For this purpose, using random num- (c) Cd)
bers, he generated 360 or 720 initial orientations to a experimental; b BP model~ c AS model; d TS model
represent the rolling texture of the austenite; the 36 a experimental (002) pole figure for transformation
individual orientations were transformed into mar- texture of martensite obtained from heavily rolled
tensitic orientations according to the various variant austenite in Fe-25·7Ni alloy (after Refs. 74, 110) and
selection models using the Bain, K-S, and N-W b-d simulated (002) pole figures of transformation
relationships. The {002} pole figures of the simulated texture of martensite using the BP, AS, and TS
martensite textures were then compared with the models, respectively (after Ref. 128)

International Materials Reviews 1990 Vol. 35 NO.1


32 Ray and Jonas Transformation textures in steels

vary in response to the timing of deformation by which induce maximum deformation along the nor-
rolling with respect to transformation (timing effect) . mal direction of the sheet when the sheet is thin and
In fact, Furubayashi et al.14,122 prepared steel speci- only contains a few grains across the thickness; in
mens in which the lath martensite structure was pro- model 2, the selected variants are those which produce
duced in two different ways: (a) by transformation the minimum deformation in the plane of the sheet.
after rolling (TAR), and (b) by transformation during A computer simulation carried out by Humbert
rolling (TDR). et al.118 produced ODFs of the martensite phase in
Computer simulated pole figures drawn according accordance with these two models. Figure 38b and c
to the BS model were found to correspond very well shows the ¢2 sections of the 0D Fs calculated
with the experimental pole figures for Fe-Ni marten- according to their two models. When these are
site determined earlier by Abe et al.74,110 and Grewen compared with their experimental ODF for the mar-
and Wassermann.129 Furthermore, the theoretical tensite phase (Fig. 38a), it is apparent that the corre-
pole figures calculated by this model could also spondence between the experimental and model 1
account for the so called 'timing effect' (Fig. 37). ODFs is poor, both in terms of the positions of the
Recently, Humbert et al.118 described results of an different maxima and their relative intensities. On
experiment in which several sheets of an Fe-30Ni the other hand, the model 2 ODF is in good
alloy in the austenitic condition were rolled to dif- agreement with the experimental ODF. These
ferent degrees of reduction before transformation simulations indicate that the geometrical parameters
into martensite. A few samples were also annealed of the samples play an important role in variant
before transformation in order to relax the residual selection.
stresses induced by rolling. They observed that,
irrespective of the amount of rolling reduction in the
Critical assessment of variant
y phase or the annealing treatment before transfor-
selection models
mation, variant selection was particularly strong and
of the same type. Thus they concluded that the rolling All the models described above deal with the effect of
reduction or residual stress does not have a para- an applied or developed stress on variant selection. In
mount effect on the nature of the y ~ a transfor- this regard, they are relevant to the martensitic trans-
mation, at least for their samples. Instead, according formation in controlled rolled steels where a signifi-
to them, it was the dimensional parameters of the cant amount of deformation is normally given to the
samples that influenced the mechanism of variant austenite before transformation. Of the six, the
selection during transformation. They postulated two TS,121BS?4,122 and Gp1l8 models are the most pro-
models: in modell, the selected variants are those mising since these can account for the experimental
martensite textures in a number of steels and iron
base alloys with reasonable accuracy. Of the three,
the TS and BS models have a common character in
RD RD
that the directionality of martensite formation is
taken into account in both. As far as the BS model is
concerned, the justification for using the Bain
orientation relationship may be questioned, since
experimentally it has been repeatedly shown that it is
the K-S and N- W relationships that are generally
obeyed in steels. However, Furubayashi et al.14 con-
tend that, although the Bain variants deviated by
0 0
11.06 and 9.7 from the K-S and N-W variants,
respectively, such differences are not large compared
(0) with the wide orientation distributions that are
attained experimentally. A close look at the relative
positions of the Bain, K-S, and N-W variants shown
RD RD in pole figure form in Fig. 3 seems to justify this
argument.
'.

.~ Y~""~:
II • ;,;". "!'~I~'
;~~'.:r:-~~'
'.1)
II

1\','
Humbert et al., 118with the help of their second

.( <,.
.~';:'I . Ut.J. model, were able to explain the martensite texture
'y)~ ~~

I~f .~~~ obtained experimentally in thin sheets of an Fe-30Ni

;; ...... \,·~hl

J'.
. •.~'
.~'':j,
:. ·.~~l'.;:~.;:~··,,~ .•. ;....1-\'~·:·1
'.

~
..:>~
.J1~-
alloy. Their observations point to the importance of
the dimensional parameters of actual samples in
variant selection .
The various models for variant selection discussed
.••:.,!.)~.
.. . •.:,...• ',·v"· .I:····.~."':··.,.
, ., so far have clearly arisen out of the necessity to
explain the textures obtained by different investiga-
(d tors in experiments which were rather varied in terms
a experimental TAR; b experimental TOR; c simulated TAR; of the materials investigated, specimen dimensions,
d simulated TOR the surfaces across the specimens on which the
37 {002} pole figures of transformation texture of texture was measured, and the thermal and mechani-
martensite obtained from rolled austenite with cal treatments the specimens were subjected to
Cu-type texture (after Ref. 122) before transformation. Therefore, in order to derive
International Materials Reviews 1990 Vol. 35 No. 1
Ray and Jonas Transformation textures in steels 33

thermo mechanical processing, coupled with


computer modelling studies, should be able to throw
much light on this phenomenon in the near future.

Summary and conclusions


The major purpose of this work has been to carry out
an up to date review of several aspects of transfor-
mation textures, especially in controlled rolled steels.
In the preceding sections, an attempt has been made
to highlight the technological importance of transfor-
mation textures and their relationship to mechanical
properties. The different kinds of transformation
textures normally encountered in steels have been
discussed and the effects of compositional and pro-
cessing variables on their development have been
enumerated. The various analytical tools available to
predict the texture of the product phase from the
parent texture have been discussed. An attempt was
also made to compare the analytically predicted
textures with experimentally determined ones and
the extent of correspondence between the two has
been noted and analysed in the light of variant
selection. Finally, a critical assessment has been
made of the importance and criteria of variant
selection during transformation from austenite. The
major conclusions of this work are enumerated
below.
1. During the controlled rolling of steels, the parent
austenite phase develops a crystallographic texture.
Thus, the material after transformation (ferrite, mar-
tensite, acicular ferrite, or bainite) also acquires a
texture which is related in a precise way to the texture
of the parent material. The latter is known as the
transformation texture.
2. The texture of deformed austenite is made up of
two major components, namely, (a) Cu {112}(111)
and (b) brass {II O}( 112). The texture of recrystal-
lised austenite is made up predominantly of the cube
component, {100}(001).
3. Irrespective of the nature of the product phase,
the transformation textures derived from deformed
austenite consist of two major components, the (a)
{332}(113) and (b) {113}(110). These orientations
originate from the {110}(112) and {112}(111)
components, respectively, of the deformed austenite.
The texture of steel obtained from recrystallised
austenite is made up predominantly of {100} < 011),
which comes from the {100}(001) texture of the
(c)
parent phase.
38 a experimental ODF of martensite obtained from 4. Of the two major components of the transfor-
heavily rolled austenite in Fe-30Ni alloy (Bunge mation texture, the {332}(113) is the more beneficial
notation), b ODF predicted according to assump- from the point of view of achieving good deep draw-
tion 1 of GP model (Bunge notation), and c ODF ability and improved strength and toughness. This
predicted according to assumption 2 of GP model indicates that, during controlled rolling, producing a
(Bunge notation) (after Ref. 118) larger volume fraction of the {110}(112) component
in austenite is desirable. As the {100}(011) texture
component has a deleterious effect on the delami-
a more generalised theory that can explain the nation behaviour of steels, the formation of this
complicated phenomenon of variant selection during component during transformation should be avoided
the y ~ a' (or a) transformation, a thorough ana by preventing austenite recrystallisation during prior
systematic investigation of a variety of steels and processing.
Fe-base alloys, carried out under controlled condi- 5. Heavy amounts of deformation and lower
tions, is called for. Carefully designed experiments finishing temperatures sharpen the overall trans-
which simulate the conditions encountered during formation texture. The presence of substitutional

International Materials Reviews 1990 Vol. 35 NO.1


34 Ray and Jonas Transformation textures in steels

solutes such as Cr, Mo, Mn, and Ni, a finer austenite 4. H. INAGAKI: in Proc. 6th Int. Conf. on 'Textures of materials',
grain size, and a faster cooling rate promote the Vol. 1, 149; 1981, Tokyo, The Iron and Steel Institute of
Japan.
intensity of the {332}( 113) component. On the other 5. E. c. BAIN: Trans. AIME, 1924, 70, 25.
hand, the intensity of the {113}(110) component is 6. G. KURDJUMOV and G. SACHS: Z. Phys., 1930, 64, 225.
relatively insensitive to these factors. 7. Z. NISHIYAMA: Sci. Rep. Res. Inst., Tohoku Univ., 1934-35,
6. The addition of Nb and V to steels sharpens the 23,638.
8. G. WASSERMANN: Arch. Eisenhuttenwes., 1933, 16, 647.
transformation texture because of their strong effects 9. A. B. GRENINGER and A. R. TROIANO: Trans. AIME, 1949, 185,
on the retardation of y recrystallisation. This leads to 59.
the inheritance of a stronger ferrite texture. 10. G. 1. DAVIES, J. S. KALLEND, and P. P. MORRIS: Acta Metall.,
7. The Kurdjumov-Sachs relation, without any 1976, 24, 159.
variant selection, leads to the accurate prediction of 11. H. INAGAKI: Z. Metallkd., 1984, 75, 510.
12. H. INAGAKI: Z. Metallkd., 1988, 79, 716.
ferrite textures. By contrast, variant selection seems 13. G. STONE and G. THOMAS: Metall. Trans., 1974, SA, 2095.
to play an important role in martensitic transfor- 14. E. FURUBAYASHI, H. MIYAJI, and M. NOBUKI: Trans. Iron Steel
mation. Inst. lpn, 1987, 27, 513.
8. When strong textures are produced in rolled y, 15. G. 1. DAVIES: inProc. 5th Int. Conf. on 'Textures of materials',
Vol. 2, 121; 1978, Berlin, Springer-Verlag.
the texture inherited by the transformed a'is invari- 16. Ph. CHAPELLIER: MEng thesis, McGill University, Montreal,
ably much weaker due to the multiplicity of the 1989.
transformation variants. Therefore, promotion of the 17. H. J. BUNGE: 'Texture analysis in materials science'; 1982,
presence of desirable components in the transfor- London, Butterworths.
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19. B. F. DECKER, E. T. ASP, and D. HARKER: l. Appl. Phys., 1948,
rolling in the a' range. 19, 388.
9. Owing to the deformation induced rotation of a', 20. M. HATHERLEY and w. B. HUTCHINSON: 'An introduction to
the {113}( 110) transformation texture component is textures in metals'; 1979, London, The Institution of
converted into the {112}(110), which is too stable to Metallurgists.
21. B. D. CULLITY: 'Elements of X-ray diffraction'; 1978, Reading,
undergo any further reorientation. By contrast, the MA, Addison-Wesley.
inherited {332}(113) component is first converted 22. K. LUCKE: in Proc. 6th Int. Conf. on 'Textures of materials',
into the {554}(225) during a' rolling, and then into Vol. 1, 14; 1981, Tokyo, The Iron and Steel Institute of
the {111} < 112) . On further deformation, the Japan.
{111}(112) component is rotated into the 23. R. 1. ROE: l. Appl. Phys., 1965, 36, 2024, 2069.
24. H. 1. BUNGE: Z. Metallkd., 1965, 56, 872.
{111}(110), which is an important constituent of the 25. H. J. BUNGE: 'Mathematische Methoden der Texturanalyse';
y fibre. 1969, Berlin, Akademie Verlag.
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order to produce warm rolled steels with textures that Vol. 11,454; 1968, New York, Plenum Press.
27. 1. HANSEN, 1. POSPIECH, and K. LUCKE: 'Tables for texture
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rolling; (b) finish rolling in the ferrite no-recrystal- 28. H. 1. BUNGE and c. ESLING (eds.): 'Quantitative texture
lisation region; (c) the presence of Ti or Nb in the steel analysis', 271; 1982, Oberursel, FRG, Deutsche Gesellschaft
to raise the ferrite no-recrystallisation temperature; fur Metallkunde and Societe Fran~aise de Metallurgie.
and (d) minimisation of the solute carbon content of 29. D. DANIEL: PhD thesis, McGill University, l\10ntreal, 1990.
30. PH. LEQUEU and 1. 1. JONAS: Metall. Trans., 1988, 19A, 105.
the steel by the precipitation of C as TiC or NbC. 31. L. S. T6TH, R. K. RAY, and 1. 1. JONAS: Metall. Trans., in press.
32. H. INAGAKI and T. SUDA: Texture, 1972, 1, 129.
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Acknowledgments 279.
The authors are grateful to the Natural Sciences and 34. R. PRIESTNER and N. LOUAT: Acta Metall., 1965, 13, 563.
35. T. H. WEBSTER: Acta Metall., 1970, 18, 683.
Engineering Research Council of Canada (NSER C), 36. T. NAKAMURA, T. SAKAKI, Y. ROE, E. FUKUSHIMA, and R.
the Canadian Steel Industry Research Association INAGAKI: Trans. Iron Steel Inst. lpn, 1975, 15, 561.
(CSIRA), and the Ministry of Education of Quebec 37. H. INAGAKI, K. KURIHARA, and I. KOZASU: Trans. Iron Steel
(FCAR Program) for financial support. They would Inst, lpn, 1977, 17, 75.
like to thank Dr L. S. T6th of the Department of 38. w. E. HOSFORD and W. A. BACKOFEN: 'Fundamentals of defor-
mation processing', 259; 1964, New York, Syracuse Uni-
Metallurgical Engineering, McGill University for versity Press.
numerous helpful discussions. Thanks are also due to 39. R. SHOEFIELD, G. ROWNTREE, N. V. SARMA, and R. T. WEINER:
Messrs. Ph. Chapellier and D. Daniel, research Met. Technol., 1974, 1, 325.
students of the same department, for kindly making 40. G. R. SPEICH and D. S. DABKOWSKI: in 'The hot deformation of
austenite', 557; 1977, New York, American Institute of
available some of their unpublished results. The Mining, Metallurgical and Petroleum Engineers.
extremely able secretarial help of Ms Lorraine Mello 41. B. L. BRAMFIT and A. R. MARDER: Metall. Trans., 1977, 8A,
and Ms Joanne Guimond is also gratefully acknow- 1263.
ledged. One of the authors (RKR) would like to 42. HUNG-CHI CHAO: Metall. Trans., 1978, 9A, 509.
express his gratitude to the Indian Institute of Tech- 43. G. BALDI and G. BUZZICHELLI: Met. Sci., 1978, 12, 459.
44. S. MATSUDA and Y. KAWASHIMA: in Proc. 6th Int. Coni. on
nology; Kanpur for granting him a sabbatical leave 'Textures of materials', Vol. 1, 659; 1981, Tokyo, The Iron
during the tenure of his work. and Steel Institute of Japan.
45. D. L. BOURELL: Metall. Trans., 1983, 14A, 2487.
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