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Warm Mix Asphalts Research, Analysis and Evaluation
Warm Mix Asphalts Research, Analysis and Evaluation
Abstract. With increasing concerns of global warming and increasing exhaustion of greenhouse gases, the asphalt
industry is looking for alternatives for hot mix asphalt (HMA). Reasonable solution for that is a use of warm mix
asphalt (WMA) technologies which allow to lower the temperatures at which asphalt pavement material is mixed and
placed on the road. The advantages of WMA are reduced energy consumption, reduced emissions and improved
workability. WMA technologies can be used with regular HMA for easier compaction in extreme weather conditions
and longer haul distances. This article presents the overview of different WMA production technologies, advantages
and disadvantages of these technologies. It also represents experimental researches which were done in order to de-
velop the optimal amount of chosen additives, their influence to physical mechanical asphalt mix properties and to
determine the optimal additive for selected mixture. Water bearing, chemical and organic additives were used for
WMA production and temperature of produced asphalt varied from 150 °C to 120 °C.
Keywords: Hot mix asphalt, warm mix asphalt, asphalt additives, Marshall stability, Marshall flow, indirect tensile
strength.
150
nia in order to determine optimal WMA technology or – Increased time available for compaction,
additive most suitable for this region. thereby for example extended paving season
into the colder months of the year.
2. Advantages and disadvantages of WMA 3. Easier compaction (by using regular HMA mixing
temperatures), which are beneficial:
Emissions of hazardous materials (greenhouse – During extreme weather conditions;
gases) during WMA production are significantly lower – For reducing amount of roller passes to reach
than during hot mix asphalt production. According to necessary compaction.
Gonzalez et al. (2009) WMA with Cecabase RT additive 4. The possibility to use 50 % and more of reclaimed
production reduces different pollutants emissions from asphalt in warm mix asphalt.
14 % to 36 % compared to traditional HMA. A reduction The use of WMA technologies in reclaimed asphalt
of about one third of the CO produced was obtained with pavement (RAP) has been investigated by Lee et al.
the reduction of 40 °C in asphalt mix production. Field (2009), Gonzalez et al. (2009) during past years. Mucinis
tests showed that virtually no fumes have been seen com- et al. (2009) defined that the greatest values of RAP that
ing from the asphalt mixture near the paver using WMA can be used in recycled asphalt mix vary depending on
with Cecabase RT additive (Gonzalez et al. 2009). the type of its homogeneity (content of bitumen or min-
Gaudefroy et al. (2009) determined that total organic eral aggregates). Asphalt pavement durability depends
compounds emissions provided by half-warm bitumen not only from RAP homogeneity, properties of the binder
mixes are lower than HMA according to the manufactur- are very important also. Lee et al. (2009) investigated
ing temperature difference. Emissions reduction advan- characteristics of WMA binders (with zeolite Aspha Min
tage of WMA has been already cited in several occasions and wax Sasobit) containing aged binders. He summa-
(D’Angelo et al. 2008; Anderson et al. 2008). Laying of rized that Aspha Min and Sasobit along with virgin and
asphalt pavements in half or fully – closed sites, e.g. in aged bitumen increases binders’ resistance to rutting. It
tunnels, makes a negative impact on the road workers’ was also determined that recycled binders with WMA
health since the exhausted smoke and fumes are cleared additives have significantly lower resistance on low tem-
away much slower than in an open area. In these cases, perature cracking.
lower emissions of WMA mixtures would be a consider- Warm mix asphalt production disadvantages are
able advantage. bound to lack of the research on these mixes and condi-
The reduced energy consumption is another benefit tionally with short usage of time. Warm mix asphalt pro-
of WMA. Energy consumption for a WMA production is duction and consumption weaknesses are as follows:
60 % – 80 % of that for HMA production, depending on 1. According to the most researches warm mix as-
how much the production temperature is lowered. Gon- phalt physical and mechanical characteristics
zalez et al. (2009) determined that a reduction of energy are worse than hot mix asphalt. Warm mix as-
(gas) in asphalt plant is from 20 % to 24 % during pro- phalt characteristics vary depending on used
duction of WMA with Cecabase RT additive. Reduction technology;
depended on asphalt mix type used. The importance of 2. Lower aggregates drying temperature requires
this benefit depends on what sort of energy is used for the to use cohesion properties between mineral ma-
production process and how polluting and expensive it is. terials and bitumen improving additive;
In Lithuania the energy cost is relatively high and has 3. The incensement in price for the asphalt using
been continuously rising, therefore this benefit can be warm mix asphalt technology because of addi-
very important for the asphalt producers. On the basis of tional additive price or asphalt plant modifica-
the review of scientific investigations it could be stated tion;
that lower fuel consumption in the production of WMA 4. The prolongation of asphalt mixing cycle due to
mixtures has not been estimated as one of the main ad- addition of additives (not all technologies).
vantages of these mixtures.
Major advantages of WMA are related to the lower 3. Experimental research of warm mix asphalt
viscosity of the asphalt mix. Generally, improved worka-
bility can have various effects throughout the production 3.1 Laboratory research
and placement process. Improved workability has follow-
ing advantages (Kristjansdottir 2006): Two experimental researches were done in order to
1. Lower working temperatures: develop the optimal amount of chosen additives, their
– Energy savings during production; influence to physical mechanical properties of asphalt
– Reduced emissions; mix and to determine the best suitable additive for se-
– Decreased cooling rate due to smaller differ- lected mixture. AC 16 PD asphalt mixture was selected. It
ence between ambient and compaction tem- is typically used one layer bituminous mixture in Lithua-
peratures. nia roads with light load. AC 11 VS asphalt mixture was
2. Increased temperature gap between mixing and studied in the first experimental research also, for more
compaction (by using regular HMA mixing tempera- about this mixture research analysis read (Vaitkus et al.
tures): 2009).
– Increased haul distances; First experimental research was carried out in July
of 2008 by the Road Research Laboratory of Department
151
of Roads of Vilnius Gediminas Technical University. produced and four with different amount of Sasobit and
Two asphalt mix temperature lowering technologies were Rediset additives in 120 °C. Cohesion properties between
selected: Iterlene T and Cecabase represented chemical mineral materials and bitumen improver Iterlene IN/400L
additives technology; Aspha Min and natural zeolite – were used for asphalt mixes with Sasobit. Rediset itself
water bearing technology. Asphalt mix with chemical had that type of improver.
additives was produced from dolomite aggregates and Asphalt mixtures were compacted using a Marshall
asphalt mix with water bearing additives – gravel aggre- compactor and tested for stability, bulk density, air voids.
gates. Amount of additives varied from 0,1 % to 0,6 % Indirect tensile strength test was carried out also to meas-
(Iterlow T and Cecabase RT by total weight of asphalt ure the tensile strength of compacted asphalt mix.
mix; Aspha Min and natural zeolite by total weight of
asphalt binder). 3.2 Analysis and evaluation of research results
For each additive 8 mixtures were mixed, two con-
trol mixtures in 150 °C and 120 °C temperatures without Asphalt mix specimens density results were scat-
additive and six mixtures in 120 °C with different amount tered and depended on technology (Fig 1). Water bearing
of selected additives. All mixtures were produced from Aspha Min and zeolite technologies with gravel aggre-
the bitumen 70/100. Chemical additives Iterlene IN/400L gates showed the lowest asphalt mix density results. As-
(for chemical technologies) and Gripper L (for water phalt mix produced in 120 °C temperature with different
bearing technologies) were added to improve cohesion amount of Iterlow T and Cecabase chemical additives
properties between mineral materials and bitumen. These density results were not scattered and varied from
asphalt mixtures were then compacted using a Marshall 2453 kg/m3 to 2462 kg/m3, however they were lower than
compactor and tested for stability, flow, bulk density and control mixture results. By increasing amount of Rediset
air voids in a standard way. Stability of Marshall speci- in asphalt mixture, asphalt mix specimens density results
mens represents the greatest asphalt pavement resistance increases. Asphalt mixes with different amount of Rediset
to deformation, flow of Marshall specimens – deforma- or Sasobit did not reach control mixture density. However
tion with maximum load. density results difference between asphalt mixes with
However warm asphalt mixes with water bearing organic and chemical additives and control mixture were
additives Aspha Min and natural zeolite did not show very small. Therefore the use of optimal amount of Iter-
expected results so they became difficult to analyze. At low T, Cecabase, Sasobit and Rediset allows to reduce
that moment asphalt mixes with Cecabase and Rediset asphalt mix production and compaction temperatures
could only be compared to each other, so the demand on from 150 °C to 120°C without major asphalt pavement
the use of other type of additives in AC 16 PD asphalt density reduction.
mixture occurred. Therefore the second experimental 0,1 % (1 %) in Figs 1 – 4 represents the dosage of
research was carried out in August of 2009. Identical type additives in asphalt mix. 0,1 % shows amount of natural
of bituminous mixture was selected (AC 16 PD) and zeolite, Aspha Min (by the mass of the mix) and Ceca-
made with dolomite aggregates. Organic additives tech- base, Iterlow T (by the mass of the binder) dozed in the
nology was now chosen. Sasobit and Rediset were used mixture. (1 %) represents amount of Sasobit and Rediset
to produce WMA. Amount of additives varied from (by the mass of the binder) dozed in asphalt mix. All
1,0 % to 2,5 % by total weight of asphalt binder. Two asphalt mixtures with additives were compacted in
control mixtures in 150 °C and 120 °C temperatures were 120 °C temperature.
2490
3
Asphalt specimens density, kg/m
2480
2470
2460
2450
2440
2430
150 °C 120 °C 0,1 % (1 %) 0,2 % (1,5 %) 0,3 % (2 %) 0,4 % (2,5 %)
Fig 1. Distribution of asphalt mix specimens density with different temperature lowering
additives and different amounts of them
152
Marshall specimens compacted from asphalt mixes compared to other four temperature lowering additives. It
with natural zeolite and Aspha Min stability results is possible to compare only asphalt mixes produced with
showed that optimal amount of these additives is 0,3 % Iterlow T, Cecabase, Sasobit and Rediset additives as
(by the mass of the mix) as then the greatest stability they all were produced according to identical asphalt mix
values were reached (Fig 2). However asphalt mix with project. Marshall specimens compacted from asphalt mix
0,3 % amount of natural zeolite stability results were with Sasobit and Rediset additives stability values is
scattered and did not reach control mixture stability. The about 20 % higher than specimens with Iterlow T and
same amount of Iterlow T and Cecabase additives (0,3 % Cecabase. According to these results it is clear that the
by the mass of binder) is optimal in asphalt mixes be- use of organic additives in asphalt mixes increases their
cause of the highest Marshall stability values then. stability.
By increasing Rediset amount in asphalt mixture (by Flow values of Marshall specimens compacted from
the mass of the binder) Marshall stability results increases asphalt mix with natural zeolite, Aspha Min, Iterlow T
and the highest value is reached at 10,7 kN with 2,5 % and Cecabase were scatered and depended on technology
amount of Rediset. Highest stability results for asphalt (Fig 3). However the less scatered flow values were
specimens with Sasobit were determined with 2,0 % (by reached with the use of 0,2 % amount of these additives.
the mass of binder) of this additive in the mix, as then a It was determined that the use of Sasobit in asphalt mixes
very similar to asphalt specimens with Rediset stability reduces flow of Marshall specimens. The greatest flow
value was reached (10,8 kN ). Marshall specimens com- reduction was reached with 2,5 % amount of Sasobit and
pacted from the mix with these amounts of Rediset and was about 16 % lower compared to the flow of specimens
Sasobit additives stability results were higher compared of control mixture. Asphalt mix specimens with different
to control mixtures compacted in 150 °C temperature. As amoun of Rediset flow values were not scatered and
the amount of Sasobit in mixture increases to 2,5 %, Mar- varied from 4,8 mm to 5,3 mm.
shall stability value decreases.
Generally asphalt mixes with organic additives Re-
diset and Sasobit Marshall stability values were highest
11,0
Marshall stability, kN
10,0
9,0
8,0
7,0
6,0
150 °C 120 °C 0,1 % (1 %) 0,2 % (1,5 %) 0,3 % (2 %) 0,4 % (2,5 %)
Fig 2. Distribution of asphalt mix stability with different temperature lowering additives and amounts of them
7,5
6,5
Marshall flow, mm
5,5
4,5
3,5
150 °C 120 °C 0,1 % (1 %) 0,2 % (1,5 %) 0,3 % (2 %) 0,4 % (2,5 %)
Fig 3. Distribution of asphalt mix flow with different temperature lowering additives and amounts of them
153
0,001100
0,001000
0,000950
0,000900
0,000850
150 °C 120 °C 1,00% 1,50% 2,00% 2,50%
Rediset Sasobit
Fig 4. Distribution of asphalt mix indirect tensile strength with different amounts of Rediset and Sasobit additives
Indirect tensile strength test was made to Marshall – Natural zeolite and Aspha Min could not be
specimens compacted from asphalt mix with Rediset and tested properly under laboratory conditions,
Sasobit additives. Research results show that by therefore much greater amounts of mixtures in
increasing amount of these additives indirect tensile asphalt plant should be tested;
strength increases (Fig 4). The greatest values were – The use of organic additives in asphalt mixes
reached with 2,5 % (by amount of the binder) for each of increases asphalt pavement stability;
additive. Asphalt mix with Rediset in all senses showed – Asphalt mixes with Zeolite, Iterlow T and Ce-
higher indirect tensile strength values compared to cabase additives stability values did not
asphalt mix with Sasobit. Marshall specimens compacted matched to traditional HMA stability values;
from the mix with these amounts of Rediset and Sasobit – The use of Sasobit in asphalt mixes decreases
additives indirect tensile strength results were higher asphalt pavement deformation (flow);
compared to the control mixture compacted in 150 °C – By increasing amount of Rediset and Sasobit
temperature. Indirect tensile strength of control asphalt additives indirect tensile strength increases;
mixture produced in 120°C temperature decreases about – Rediset showed the best Marshall stability, flow
17 % compared to control mixture produced in 150 °C and indirect tensile strength results compared to
and WMA mixes with 2 % of Rediset and Sasobit other studied additives.
Optimal amount of Sasobit and Rediset additives is
2,0 % by the mass of the binder according to stability, Conclusion
flow and indirect tensile strength results. Highest asphalt
mixes with Sasobit stability results were reached with this Based on the results presented in this paper and on
amount of additive. In order to avoid great reduction in their analysis, the main conclusions that can be drawn
asphalt pavement resistance on low temperature cracking from this study are the following:
more than 2,0 % of Sasobit (by the mass of the binder) 1. Field and laboratory researches carried out by
should not be used. Decrease in flow values confirms the scientists of various countries show that the
that. Same notice could be applied to asphalt mixes with values of the properties of WMA mixtures are
Rediset. scattered and inconstant if compared to that of
HMA mixtures.
3.3 Experimental research conclusion 2. When asphalt is produced at lower tempera-
tures, there are many potential benefits such as
According to laboratory research analysis it was de- reduced energy consumption (fuel) in asphalt
termined that: plant and reduced noxious gases emissions, in-
– Optimal amount of temperature lowering addi- creased workers’ safety due to reduce of smoke
tives in asphalt mix is 0,3 % (by the mass of the emissions, possibility to place asphalt mix in
mix) for natural zeolite and Aspha Min; 0,3 % cooler ambient temperatures and to haul farther
(by the mass of the binder) for Iterlow T and distances without compromising workability;
Cecabase. At these amounts of additives the possibility to use 50 % and more of reclaimed
greatest Marshall stability values were reached; asphalt in warm mix asphalt.
– Optimal amount of Sasobit and Rediset addi- 3. Optimal amount of asphalt mix temperature
tives is 2,0 % by the mass of the binder; lowering additives, determined by this research,
– The use of optimal amount of Iterlow T, Ceca- is 0,3 % (by the mass of the mix) for natural
base, Sasobit and Rediset allows to reduce as- zeolite and Aspha Min; 0,3 % (by the mass of
phalt mix production and compaction tempera- the binder) for Iterlow T and Cecabase; 2,0 %
tures from 150 °C to 120 °C without major (by the mass of the binder) for Sasobit and Re-
compacted asphalt pavement density reduction; diset.
154
4. The use of organic additives in asphalt mixes rence. Environmentally friendly roads. Enviroad 2009.
increases asphalt pavement stability. The use of Warsaw, October 15–16.
Sasobit in asphalt mixes decreases asphalt Kristjansdottir, O. 2006. Warm Mix Asphal for Cold Weather
pavement flow. Paving. University of Washington Civil and Environ-
5. Sasobit and Rediset additives increases asphalt mental Engineering, Seattle.
pavement tensile strength, however more than Lee, S.J.; Amirkharian, S.N.; Park, N. –W.; Kim, K.W. 2009.
2,0 % of Sasobit and Rediset (by the mass of Characterization of warm mix asphalt binders containing
the binder) should not be used in order to avoid artificially long – term aged binders, Construction and
great reduction in asphalt pavement resistance Building Materials 23(6): 2371 – 2379.
doi:10.1016/j.conbuildmat.2008.11.005
on low temperature cracking.
6. The properties of WMA mixture produced in Metzker, K.; Witsuba, M. P. 2009. Comparative study on wax
modified bitumen, in II international conference. Envi-
120 °C by the Rediset technology showed best
ronmentally friendly roads. Enviroad 2009. Warsaw, Oc-
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Stability, flow and indirect tensile strength val-
Mucinis, D.; Sivilevicius, H.; Oginskas, R. 2009. Factors de-
ues were less scattered compare to other se-
termining the inhomogeneity of reclaimed asphalt pave-
lected additives and similar to control mixture ment and estimation of its components content variation
produced in 150 °C temperature. Therefore Re- parameters, The Baltic Journal of Road and Bridge Engi-
diset is most suitable for lowering temperature neering 4(2): 80–86.
for AC 16 PD asphalt mix. Silva, H. M. R. D.; Oliveira, J. R. M.; Ferreira, C. I. G.; Pereira,
7. It is recommended to extend the research and to P. A. A. 2009. Assessment of the Performance of Warm
construct asphalt pavement section using Re- Mix Asphalts in Road Pavements, in II international con-
diset technology. During and after construction ference. Environmentally friendly roads. Enviroad 2009.
evaluation of asphalt pavement physical and Warsaw, October 15–16.
mechanical properties should be done. Sivilevicius, H.; Sukevicius, Š. 2009. Manufacturing technolo-
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