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JMEPEG (2014) 23:2403–2411 ASM International

DOI: 10.1007/s11665-014-0945-4 1059-9495/$19.00

Effects of Loading and Constraining Conditions


on the Thermomechanical Fatigue Life of NiTi Shape
Memory Wires
G. Scirè Mammano and E. Dragoni

(Submitted September 28, 2013; in revised form February 24, 2014; published online March 25, 2014)

The availability of engineering strength data on shape memory alloys (SMAs) under cyclic thermal acti-
vation (thermomechanical fatigue) is central to the rational design of smart actuators based on these
materials. Test results on SMAs under thermomechanical fatigue are scarce in the technical literature, and
even the few data that are available are mainly limited to constant-stress loading. Since the SMA elements
used within actuators are normally biased by elastic springs or by antagonist SMA elements, their stress
states are far from being constant in operation. The mismatch between actual working conditions and
laboratory settings leads to suboptimal designs and undermines the prediction of the actuator lifetime. This
paper aims at bridging the gap between experiment and reality by completing an experimental campaign
involving four fatigue test conditions, which cover most of the typical situations occurring in practice:
constant stress, constant-strain, constant stress with limited maximum strain, and linear stress-strain
variation with limited maximum strain. The results from the first three test settings, recovered from the
previously published works, are critically reviewed and compared with the outcome of the newly performed
tests under the fourth arrangement (linear stress-strain variation). General design recommendations
emerging from the experimental data are put forward for engineering use.

Keywords constant strain, constant stress, limited maximum Nomenclature


strain, linear stress-strain variation, SMA wires,
thermomechanical fatigue Af Austenite finish temperature Æ
As Austenite start temperature Æ
c Empirical constants in Coffin-Manson equation Æ
kb Spring rate of the backup spring in the test with linear stress-
strain variation Æ
1. Introduction Mf Martensite finish temperature Æ
Ms Martensite start temperature Æ
Shape memory alloys (SMAs) are increasingly employed to Nf Number of cycles to failure Æ
build solid-state actuators, characterized by sleek design and SME Shape memory effect ( ” De = eM eA) Æ
outstanding power density. For the rational design of shape S0 Initial stress level in the JSME fatigue test method Æ
memory actuators, a thorough knowledge of the fatigue e Wire strain Æ
behaviour of the alloy is needed (Ref 1-3). Since the actuation ea Amplitude of total strain cycle Æ
is always provided by thermal activation of the alloy, the eA Wire strain in the austenitic state Æ
fatigue incurred by the material is called ‘‘thermomechanical,’’ elim Maximum wire strain in the constant-stress test and in linear
implying that the material performs mechanical work against stress-strain cycle with limited maximum strain Æ
the external applied load when heated during the actuation eM Wire strain in the martensitic state Æ
cycle. The thermomechanical cycling can affect both the emax Maximum wire strain recorded in the cycle ( ” eM) Æ
structural performance of the alloy (fatigue fracture) and its emin Minimum wire strain recorded in the cycle ( ” eA) Æ
functional response (loss of strain recovery, elongation drift). De Shape memory effect ( ” SME = eM eA) Æ
Although the purely mechanical fatigue (i.e., at constant r Nominal stress applied to the wire Æ
temperature) of SMAs is well established in the technical r¢f Fatigue strength coefficient in Coffin-Manson equation Æ
rmax Maximum wire stress recorded in the cycle Æ
rp Pre-stress in the wire under the maximum strain in the linear
stress-strain cycle Æ
This article is an invited paper selected from presentations at the rw Fatigue limit
International Conference on Shape Memory and Superelastic
Technologies 2013, held May 20-24, 2013, in Prague, Czech
Republic, and has been expanded from the original presentation.
G. Scirè Mammano and E. Dragoni, Department of Engineering literature (Ref 4), only scanty data exist on the response of these
Sciences and Methods, University of Modena and Reggio Emilia, materials to thermomechanical fatigue. Furthermore, the few
Reggio Emilia, Italy. Contact e-mail: eugenio.dragoni@unimore.it. papers available on thermomechanical fatigue of SMAs are

Journal of Materials Engineering and Performance Volume 23(7) July 2014—2403


limited to the constant-stress loading condition and cover a very
limited number of cycles (Ref 5-7).
Test methods different from the constant-stress concept were
carried out in (Ref 8) and (Ref 9). Mertmann et al. (Ref 8)
investigated the stability of the shape memory effect (SME)
under constant-strain conditions. They observed that memory
effect is quickly lost under these conditions accompanied by a
general elongation of the specimen. Demers et al. (Ref 9) tested
the thermomechanical fatigue of a NiTi alloy after various
thermal training processes based on three steps: ‘‘stress-free
shape recovery,’’ ‘‘constrained recovery’’ (constant-strain), and
‘‘constant-stress recovery’’ (assisted-two-way-shape-memory-
effect).
The authors have lately started a systematic test campaign
on SMA wires undergoing realistic thermomechanical fatigue
cycles (Ref 10, 11). A specific testing machine has been
designed and built to implement a variety of loading conditions
likely to be encountered in practice. Test results have been
published for three loading and constraining conditions:
constant stress, constant-strain, and constant-stress cycle with
limited maximum strain (Ref 10, 11). This paper reviews those
results and presents the results from a new experimental set-up
to test SMA wires under a linear variation of stress and strain. Fig. 1 Specific tests proposed to characterize the SMA wires under
Experimental data obtained by cycling the wire against two thermomechanical fatigue: (a) constant stress; (b) constant strain; (c)
different elastic springs (one with low stiffness and the other constant stress with limited maximum strain; and (d) linear stress-
with high stiffness) are discussed and compared with the strain cycle
outcomes of the previous tests.

constant force, works between hard stops. Given the material,


2. Materials and Methods this test is fully defined by two parameters: the applied stress
and the maximum strain.
2.1 Characteristic Stress-Strain Tests Figure 1(d) describes a cyclic-stress test, in which the SMA
element undergoes a linear variation of stress and strain, with
A typical shape memory actuator comprises an active SMA
the stress level increasing during strain recovery and the
element (e.g., a wire) and a backup element (e.g., a spring) used
maximum strain limited by an external restraint. This test
to restore the reference position when the SMA element is
reproduces the situation in which the SMA element of an
deactivated. The particular load acting on the active element
actuator is backed up by a spring (or another SMA element)
strongly depends on the backup element and on the external
and works between hard stops. Given the material, this test is
load applied to the actuator. Figure 1 illustrates four test
defined by three parameters: the stress-strain slope, the
conditions in which the stress and the strain in the SMA
maximum strain, and the initial stress at the maximum strain.
element vary along specific paths representative of what can
occur in operation.
2.2 Properties of the Tested Shape Memory Alloy
Figure 1(a) describes the classical constant-stress test, in
which the SMA element undergoes variable strains under a With the aim of gathering fatigue data on shape memory
prescribed stress, provided, for example, by an applied constant materials readily available to the designer, the NiTi wire,
load. This test reproduces the situation occurring in an actuator Smartflex 150 marketed by SAES Getters, was tested in the
backed up by a constant force and operated slowly (i.e., with no experimental campaign. The wire has a diameter of 0.150 mm,
inertial effects) under no external load (such as in positioning a Ni content of 54% by weight, and the following transforma-
devices). Given the material, this test is fully defined by the tion temperatures: As = 86 C, Af = 94 C, Ms = 65 C, and
stress applied to the SMA element. Mf = 57 C. The entire experimental campaign described
Figure 1(b) describes the constant-strain test, in which the below has been covered using two different batches of the
SMA element undergoes variable stresses under prescribed wire with the above properties. One batch was used to perform
strain, provided, for example, by rigid restraints fixing the ends the tests under constant stress, constant strain, constant stress
of the sample. This test reproduces the situation in which the with limited maximum strain, and the linear stress-strain
actuator is operated in a locked position, or when the SMA variation with the highest slope (35 MPa per unit percent
element is heated up very fast against external loads with strain). The second batch was used to carry out the tests with
significant inertia. Given the material, this test is fully defined linear stress-strain variation with the lowest slope (15 MPa per
by the strain imposed to the SMA element. unit percent strain). The strain-temperature diagram provided
Figure 1(c) describes a constant-stress test with limited by the manufacturer for both batches is shown in Fig. 2. The
maximum strain, in which the SMA element undergoes variable stress-strain diagram measured on the second batch is reported
strains under prescribed stress, but the maximum strain in Fig. 3 for the wires in martensitic and austenitic states. The
achievable is limited by an external restraint. This test stress-strain tensile properties from Fig. 3 are very close to
reproduces the situation in which an actuator, backed up by a those of the first batch presented in (Ref 10).

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Fig. 2 Strain-temperature curves for the NiTi wire under examina-
tion (courtesy of SAES Getters)

Fig. 4 Details of the apparatus used to apply the four test condi-
tions of Fig. 1: (a) constant stress; (b) constant strain; (c) constant
stress with limited maximum strain; and (d) linear stress-strain cycle
Fig. 3 Quasi-static stress-strain curve for the NiTi wire under
examination
constant-stress test of Fig. 1(a). By removing the basket and
2.3 Experimental Equipment
locking the bottom end of the terminal rod as in Fig. 4(b), the
The custom-built test machine used to apply the stress-strain constant-strain test condition of Fig. 1(b) is achieved. By
conditions of Fig. 1 is described in detail in (Ref 10). Basically, placing a polymer spacer on top of the displacement sensor to
the machine comprises a primary C-shaped aluminum chassis function as a hard stop for the loading basket (Fig. 4c), the test
to which a secondary plastic frame is attached. The upper part condition in Fig. 1(c) (constant stress with limited maximum
of the plastic frame holds the primary load cell to which one strain) is performed.
end of the SMA wire under test is attached through a rigid The implementation of the test condition ‘‘linear stress-
clamp. According to the test to be performed, the lower end of strain cycle’’ (Fig. 1d) is shown in Fig. 4(d). A conventional
the SMA wire was loaded or constrained as shown in Fig. 4. compression spring, mounted between the frame and an
Heating of the wire was provided by electric current supplied adjusting nut on the sliding rod, provides the backup force
by an electronic power board. The supplied current and the on the wire according to a linear stress-strain variation. The
signals from the sensors (load cell and displacement transducer) spring rate of the spring controls the slope of the stress-strain
were picked up, processed, and controlled by a DAQ board path. The equipment accepts springs with internal diameters
(National Instruments USB 6251). The operating parameters from 6 mm and free lengths up to 60 mm. The limit maximum
were displayed on a custom-built graphical user interface strain is adjustable by a flange nut which functions as a hard
developed in LabView, and the sensors signals were stored stop for the rod. Another nut provides the desired preload of
continuously on disk. the spring. The exact preload of the spring is verified by the
In the configuration as shown in detail in Fig. 4(a), with a instrumented aluminum plate, which functions as a secondary
loading basket appended to the wire, the machine performs the load cell.

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2.4 Tests Under ‘‘Constant stress’’ and ‘‘Constant stress was endured with no failure. The experimental plan adopted in
with Limited Max Strain’’ the test campaign included five strain levels (1, 2, 3, 4, and 5%)
with three samples per level. Further details on the testing
For the tests in constant stress (both free and with limited
procedure are available from (Ref 11).
maximum strain), the wire coupons were cut from the coil, and
electrical-type ferrules (http://www.partex.co.uk/cefs.html) were
2.6 Tests Under ‘‘Linear Stress-Strain Variation’’
crimped to both ends giving a net test length of 100 mm. Each
wire was loaded by filling the basket with lead beads until the Using the set-up in Fig. 4(d), the tests under linear stress-strain
desired stress in the wire (read by the primary load cell) was variations were carried out by choosing the following three
achieved. The heating of the wire was provided by sinusoidal characteristic parameters for each test: the stress-strain slope
current oscillating from zero to a peak value capable of producing (controlled by the spring rate of the backup spring), the limits of
the full transformation of the alloy under the cooling conditions maximum strain (3 and 4% were the selected values). and the pre-
adopted. The maximum achievable frequency was limited by the stress in the wire before start (controlled by the spring preload). The
need to avoid significant force ripples in the wire due to the inertia stress-strain slope and the limit of maximum strain remained
of the moving basket and the need to achieve full transformation constant for an entire test run, with each run involving a set of single
of the alloy (M fi A, A fi M). The maximum strain rate tests performed for different pre-stresses. The pre-stress in the wire
measured during the constant-stress tests ranged between 0.150 was used as control variable much in the same way as the stress
and 0.300 s 1 during activation, and between 0.065 and level in the constant-stress tests, or the strain level in the constant-
0.150 s 1 during relaxation. The tests were terminated auto- strain tests described above. This is not only the way to perform the
matically at fracture of the SMA wire (which produced a sudden tests under linear stress-strain variations but it is also by far the
interruption of the current flowing in the sample) or when the simplest choice from an experimental point of view and the most
sample survived a prescribed number of cycles (5 9 105). realistic from a practical standpoint. Experimentally, this procedure
The constant-stress tests with limited maximum strain were allowed the entire set of results for the given maximum strain and
carried out for two levels of limit strain: elim = 3, 4%. Further given stress-strain slope (single backup spring) to be easily
information on the testing procedure is available from (Ref 11). collected and readily elaborated with standard statistical methods
(see section 3). In practical terms, this procedure fits well with the
2.5 Tests Under ‘‘Constant strain’’ normal stress-strain conditions occurring in real-life actuators
where a given backup spring with a particular spring rate fixes the
The constant-strain tests were performed on wire lengths of stress-strain slope in the active SMA element for its entire life.
100 mm cut from the same coil as that used for the constant- The tests were performed using two different backup springs
stress tests and mounted on the machine using the same end- (one relatively stiff and the other relatively soft) and adopting a
crimping technique. The prescribed strain (read by the position limit maximum strain elim = 4%. The spring rates of the springs
transducer in Fig. 4) was applied to the wire by lowering the were 0.62 and 0.27 N/mm, giving stress-strain slopes in the
restraining cross-head in Fig. 4(b). The heating of the wire was wire of 35 MPa per unit percent strain and 15 MPa per unit
provided by sinusoidal current oscillating from zero to a peak percent strain, respectively. The pre-stresses were chosen so as
value capable of producing the full transformation of the alloy to coincide with the stress levels of the constant-stress tests with
under the cooling conditions adopted. The test was terminated the maximum strain limited to the same value: elim = 4%
automatically at fracture of the SMA wire (no current flowing in (section 2.4). Starting from the maximum chosen value for the
the sample), or when a prescribed number of cycles (5 9 105) applied stress in the first test, the stress level was lowered

Fig. 5 Woehlers diagram with the fatigue results for the constant-stress tests, and the tests at constant stress with limited maximum strains
(3 and 4%)

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stepwise for the subsequent tests until no fracture in the wire Fitting the fatigue data for the constant-stress tests with
was observed after a life of 5 9 105 cycles. After accomplish- Coffin-Manson equation, gives a fatigue ductility exponent
ment of the first runout, the staircase method was performed c = 0.4894. This result is very similar to that obtained by
according to the method described in (Ref 11). Lagoudas (0.47 ‚ 0.49) in (Ref 7) for an NiTiCu alloy.
Also in this test, the heating of the wire was provided by a
sinusoidal current oscillating from zero to a peak value capable 3.2 Tests Under ‘‘Constant strain’’
of producing the full transformation of the alloy under the
The strength-life (Woehlers) curve in Fig. 6 (semi-log
cooling conditions adopted and generating a test frequency of
diagram) for the constant strain tests features only the inclined
about 1 Hz as found in the other test conditions.
part (the wire failed for all strain levels tested between 1 and
5%) and there is no indication of a strain threshold (strain
fatigue limit). The slope of the interpolating line is
e/log(Nf) = 8.28 (e expressed in percent). The fatigue life can
3. Results and Discussion be as low as 7000 cycles (for applied strain of 5%) and never
exceeded 19,000 cycles (applied strain of 1%) in the strain
3.1 Tests Under ‘‘Constant stress’’ and ‘‘Constant stress range investigated. This outcome confirms that the constant-
with Limited Max Strain’’ strain loading condition is much more demanding on the
The semi-log Woehlers chart in Fig. 5 displays the data of material than the constant-stress test, even though the maxi-
applied stress (r) and cycles to failure (Nf) obtained from the mum strains induced in the alloy are of the same order of
test campaign under constant stress (circles) and constant stress magnitude in the two tests. Figure 7 shows that the stress
with limited maximum strain (triangles and diamonds for limit induced in the wire during constant-strain cycles, rmax,
strains of 3 and 4%, respectively). In the same chart, the
bilinear interpolations of the test data are also shown with solid
line, for the constant-stress test, and with dotted and dashed
lines for the constant-stress test with limit strains of 3 and 4%,
respectively. The interpolations were obtained through statis-
tical treatment of the results according to the accelerated
staircase method (Ref 12) developed by the Japanese Society of
Mechanical Engineers (JSME). Figure 5 shows that the
inclined part of the Woehlers curves is well represented by
straight lines. The slope of the interpolating line is
r/log(Nf) = 101 MPa for the constant-stress test, and higher
for the constant-stress test with limited maximum strain (the
slope in this case is r/log(Nf) = 245 MPa, regardless of the
specific strain limit). These results demonstrate that putting a
limit, however small, to the maximum strain during constant-
stress tests is extremely beneficial to the fatigue life. It is worth
noting that limiting the maximum strain to 3% instead of 4%
does not produce further advantages because the sloped legs of
the Woehlers curves in Fig. 5 for 3% (dashed line) and 4%
maximum strain (dotted line) are very close to each other. This Fig. 6 Woehlers diagram with the fatigue results for the constant-
occurrence suggests that a threshold limit strain does exist strain tests
beyond which the described life increase is definitely obtained
with respect to constant-stress tests with unlimited strain.
The distribution of the experimental points in Fig. 5 along
the horizontal part of the Woehlers curves suggests the
existence of a true fatigue limit of the material under
constant-stress conditions, both for limited and unlimited
maximum strains. This conclusion is supported by the fact
that a sample wire which had survived the staircase method
(5 9 105 cycles) was mounted on the machine and cycled again
up to one million cycles without any sign of failure.
The fatigue limit for the constant-stress tests calculated from
Fig. 5 for the chosen life (5 9 105 cycles) is rw = 101.8 MPa.
For constant-stress tests with limited maximum strain, the
fatigue limits estimated by the JSME elaboration are greater
than for those under the constant-stress conditions and takes
values for decreasing limit strains as 108.7 and 127.3 MPa for
limit strains of 4 and 3%, respectively. All these fatigue limits
are calculated with a confidence level of 50%. Quantitatively,
the difference between the fatigue limits with limited strain and
the fatigue limit at constant stress is proportional to the Fig. 7 Evolution of the maximum stress in the wire under constant-
difference in strains achieved in the tests under these stresses. strain loading

Journal of Materials Engineering and Performance Volume 23(7) July 2014—2407


decreases exponentially with the number of cycles. The residual applied stress, r, or pre-stress, rp. For each stress level, the tables
stress just before failure falls in the range 400-500 MPa, give the number of cycles to failure, Nf, together with the
irrespective of the strain applied. Dropping of the maximum following set of data, provided both for the second cycle after
stress into this range could be adopted as a predictor of start and for the last cycle before termination: the maximum
incipient fracture of the material undergoing constant-strain stress, rmax; the minimum strain (emin ” eA); the maximum
thermal cycling of whatever amplitude. strain (emax ” eM); and the differential strain (SME ” De =
emax emin) actually measured in the wire during each test.
As shown in Tables 1 and 2, the stress increment in the
3.3 Tests Under ‘‘Linear Stress-Strain Variation’’ staircase method for the linear stress-strain variations tests was
Tables 1 and 2 collect the results obtained from the tests under 19 MPa for the greatest slope (Table 1) and 11 MPa for the
linear stress-strain variation respectively for the stress-strain lowest slope (Table 2).
slope of 35 MPa per unit percent strain and 15 MPa per unit The stress-life data from Tables 1, 2, and 3 are plotted in
percent strain, respectively. For the sake of comparison, Table 3 Figure 8 as Woehlers curves. As a benchmark, the solid line in
shows the results for the constant-stress test with same limit strain Fig. 8 represents the data for the constant-stress test with
(4%). The lines in Tables 1, 2, and 3 correspond to the value of maximum strain limited to 4% (see dashed line in Fig. 5). The

Table 1 Fatigue results for the tests under linear stress-strain variation (35 MPa per unit per cent strain) with limited
maximum strain of 4%
Second cycle after start Last cycle before termination

emin ” eA, emax ” eM, De ” SME, rmax, emin ” eA, emax ” eM, De ” SME,
Test elim, % rp, MPa Nf rmax, MPa % % % MPa % % %

1 4.0 235 8,139 363 0.86 4.03 3.18 328 1.86 4.02 2.16
2 4.0 170 18,723 291 0.65 4.00 3.35 268 1.30 3.98 2.58
3 4.0 105 21,678 245 0.56 4.00 3.44 229 0.94 3.98 3.04
4 4.0 85 500,000* 219 0.46 3.96 3.50 196 1.08 3.95 2.87
5 4.0 300 4,728 422 1.10 4.03 2.93 370 2.62 3.97 1.35
6 4.0 300 4,597 415 1.09 3.91 2.82 359 2.54 3.92 1.38
7 4.0 170 14,673 315 0.61 4.03 3.42 288 1.42 4.02 2.60
8 4.0 235 8,000 377 0.92 4.00 3.08 339 1.91 3.99 2.08
9 4.0 105 19,399 235 0.51 4.00 3.49 218 0.99 3.99 3.00
10 4.0 104 16,817 247 0.49 3.99 3.50 228 0.98 3.98 3.01
11 4.0 85 126,850 225 0.51 3.97 3.46 205 1.03 3.95 2.92
12 4.0 66 500,000* 213 0.50 3.92 3.42 188 1.11 3.92 2.80
13 4.0 85 118,671 218 0.48 4.00 3.52 195 0.94 3.98 3.04
14 4.0 66 500,000* 204 0.46 3.92 3.46 178 1.11 4.01 2.91
*Denotes run-outs

Table 2 Fatigue results for the tests under linear stress-strain variation (15 MPa per unit per cent strain) with limited
maximum strain of 4%
Second cycle after start Last cycle before termination

elim, rp, rmax, emin ” eA, emax ” eM, De ” SME, rmax, emin ” eA, emax ” eM, De ” SME,
Test % MPa Nf MPa % % % MPa % % %

1 4.0 235 8,028 312 0.68 3.99 3.31 301 1.61 3.98 2.37
2 4.0 170 13,037 238 0.48 4.00 3.52 229 1.00 4.00 3.00
3 4.0 105 500,000* 168 0.40 4.02 3.62 160 1.02 4.01 2.99
4 4.0 300 4,240 370 0.88 4.03 3.15 349 2.15 4.02 1.87
5 4.0 365 2,379 433 1.03 3.98 2.95 404 2.67 3.97 1.31
6 4.0 170 12,471 237 0.50 4.02 3.51 227 0.98 4.00 3.03
7 4.0 235 7,158 304 0.64 3.99 3.35 286 1.50 3.98 2.48
8 4.0 300 4,762 372 0.87 3.99 3.12 352 2.13 3.97 1.84
9 4.0 365 3,092 442 1.20 3.97 2.77 416 2.84 3.95 1.11
10 4.0 116 160,171 181 0.39 4.00 3.62 173 0.89 3.99 3.10
11 4.0 105 500,000* 166 0.35 4.01 3.66 157 0.93 4.00 3.07
12 4.0 116 78,905 180 0.28 4.01 3.73 173 0.69 4.00 3.32
13 4.0 105 241,426 162 0.32 4.00 3.68 156 0.89 3.99 3.10
14 4.0 94 500,000* 162 0.34 3.99 3.66 157 0.86 3.99 3.13
*Denotes run-outs

2408—Volume 23(7) July 2014 Journal of Materials Engineering and Performance


Table 3 Fatigue results for the tests under constant stress with limited maximum strain of 4%
Second cycle after start Last cycle before termination

elim, rmax, emin ” eA, emax ” eM, De ” SME, rmax, emin ” eA, emax ” eM, De ” SME,
Test % r, MPa Nf MPa % % % MPa % % %

1 4.0 235.0 8,899 241 0.35 4.00 3.65 243 1.15 4.00 2.85
2 4.0 170.0 17,693 188 0.35 3.99 3.64 174 0.81 4.00 3.19
3 4.0 105.0 500,000* 110 0.22 4.01 3.79 109 0.70 4.00 3.30
4 4.0 300.0 3,579 311 0.57 4.10 3.53 309 2.08 4.08 2.00
5 4.0 365.0 2,790 381 0.76 3.94 3.18 374 2.86 4.08 1.22
6 4.0 170.0 15,665 177 0.28 4.04 3.75 177 0.80 4.04 3.24
7 4.0 235.0 6,972 243 0.39 4.03 3.64 244 1.24 4.05 2.81
8 4.0 300.0 3,301 313 0.53 4.05 3.52 311 1.99 4.05 2.06
9 4.0 365.0 2,977 379 0.73 4.06 3.33 371 2.92 4.06 1.14
10 4.0 127.2 36,444 133 0.16 4.02 3.87 131 0.47 4.04 3.57
11 4.0 105.0 339,280 113 0.11 4.04 3.93 110 0.57 4.04 3.47
12 4.0 82.8 500,000* 85 0.08 3.95 3.88 85 0.39 3.97 3.58
13 4.0 105.0 500,000* 110 0.12 4.06 3.94 109 0.64 4.05 3.42
14 4.0 127.2 36,458 133 0.12 4.06 3.95 131 0.44 4.07 3.63

*Denotes run-outs

Fig. 8 Woehlers diagram with the fatigue results for the tests under linear stress-strain variation (high and low stiffness) and under constant
stress all with maximum strain of 4%

dotted line and the dashed line in Fig. 8 represent the linear higher the fatigue life is. Furthermore, for applied stresses
interpolation of the data for the linear stress-strain variation for above 250 MPa, both inclined legs for the linear stress-strain
the lower slope (15 MPa per unit percent strain) and for the variation tests fall to the right of the inclined leg for the pure
higher slope (35 MPa per unit percent strain). The inclined legs constant-stress test. Since in this case, the average and the
of both Woehlers curves for the linear stress-strain variation maximum stresses in the wire are much lower than for the
tests have the same inclination of r/log(Nf) = 289 MPa, which stress-strain variation tests (see Tables 1, 2, and 3), this
is higher than for the constant-stress test with the same limit outcome suggests that at high applied stresses, the fatigue life
strain (r/log(Nf) = 245 MPa, solid line in Fig. 8). is conditioned more by the strain cycle than by the stress itself.
From Fig. 8, it is worth noting that the inclined leg of the To support this conclusion, examine Fig. 9(a), which plots the
Woehlers curve for the higher stress-strain slope (35 MPa for shape memory effect, SME (=difference between maximum
unit percent strain) falls to the right of the inclined leg for the and minimum strain) against the number of cycles, N, for the
lower stress-strain slope (15 MPa per unit percent strain), three tests in Tables 1, 2, and 3 under the same pre-stress of
which means that the stiffer the backup spring the slightly 300 MPa. Figure 9(a) shows that the higher the stress-strain

Journal of Materials Engineering and Performance Volume 23(7) July 2014—2409


Fig. 9 Evolution with the number of cycles of the shape memory effect (SME) in the wire for the linear stress-strain variation tests (low and
high stiffness) and for the constant-stress tests with limited maximum strain of 4%: (a) applied pre-stress = 300 MPa; (b) applied pre-
stress = 105 MPa

Fig. 10 Effect of applied pre-stress on the shape memory effect (SME) in the wire for the linear stress-strain variation tests(low and high stiff-
ness) and for the constant-stress tests with limited maximum strain of 4%: (a) SME in the second cycle after test start; (b) SME in the last cycle
before test termination

slope of the test, the lower the shape memory effect, and hence is about one-fourth of the fatigue limit for the constant-stress
the strain cycle, which apparently contributes to the longer test (81.8 MPa against 108.7 MPa). The same degree of
fatigue lives observed in Fig. 8. On the other hand, despite this nonlinearity is confirmed by the curves of SME against the
small advantage on the structural side, Fig. 9(a) and (b) indicate number of cycles in Fig. 9(b). These results correspond to an
the loss of performance of the wire with the accumulation of applied stress of 105 MPa, close to the fatigue limits of the
cycles and is a manifestation of functional fatigue. three loading conditions investigated. Figure 9(b) shows that
The trend of the experimental points in Fig. 8 for the linear the curves for the constant-stress test (diamonds) and for the
stress-strain variation tests with limited strain suggests the linear stress-strain variation with lower slope (circles) are very
existence, as for the regular constant-stress tests with or without close to each other. In particular, both test conditions lead to
limited strain, of a genuine fatigue limit. The fatigue limit run-outs at 5 9 105 cycles. By contrast, the curve for the linear
estimated by the JSME procedure in Fig. 8 is 106.9 MPa for stress-strain variation with higher slope (squares) decays much
the lower stress-strain slope (15 MPa per unit percent strain); more quickly and leads to fracture after a few thousand cycles.
and 81.8 MPa for the higher slope (35 MPa per unit percent Figure 10 presents the SME in the wire for a selection of
strain). As expected, both these fatigue limits are lower than for applied pre-stresses for the linear stress-strain variation tests (low
the constant-stress test with the same limit strain (108.7 MPa). and high stiffness) and for the constant-stress tests with limited
However, the measured decrease of the fatigue limit depends maximum strain of 4%. Figure 10(a) refers to the second cycle
nonlinearly on the increase of the stiffness of the backup after beginning of the test, and Fig. 10(b) refers to the last cycle
system. For the lower stress-strain slope (15 MPa per unit before test termination. From Fig. 10, it is interesting to note that,
percent strain), the decrease of the fatigue limit is hardly for both reference cycles, the SME has a maximum for an applied
noticeable (106.9 MPa versus 108.7 MPa), while for the higher pre-stress of about 100 MPa, regardless of the type of test.
stress-strain slope (35 MPa per unit percent strain), the decrease Furthermore, the decrease of the SME from the second cycle after

2410—Volume 23(7) July 2014 Journal of Materials Engineering and Performance


beginning of the test and the last test before test termination is increases for increasing slope of the stress-strain cycle (hence
very low. This result suggests that 100 MPa is the optimum level for increasing stiffness of the backup element). This behaviour
of pre-stress to employ for this alloy in order to maximize the is probably due to a decrease of the SME (net recovered strain)
functional performance of the wire, and simultaneously, mini- with the number of cycles accompanying the tests with the
mize the detrimental effects of the functional fatigue. higher stress-strain slopes. The lesser recovered strain is
Figure 10 also shows that, beyond the optimum stress level apparently less detrimental to the structural fatigue of the alloy,
of 100 MPa, the SME decreases, both for the second cycle although this advantage is more than offset by the poorer
(Fig. 10a) and for the last cycle (Fig. 10b), in proportion to the functional performance implicit in the reduced shape memory
applied pre-stress. At the end of the life of the wire (Fig. 10b), effect.
the residual SME under stresses between 300 and 400 MPa is
less then one half of the initial SME (Fig. 10a) under the same
stress conditions.

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Journal of Materials Engineering and Performance Volume 23(7) July 2014—2411

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