Raw Data Sheet

Date:
Lab ref. No.:
Batch code: Client Ref.:
Retention No.: Sample Description:
Test Method Description Unit 1 2 Temp. Humidity Date Initials

Wt of Tray Empty

Wt of Tray + Sample bef. Drying 0 0

Wt of Tray + sample aft. Drying

Total Moisture ISO 589:2008-B2 %wt
Wt of sample

Moisture ( as received)

Average 8.10

Wt of Crucible Empty 55.9853 52.8976

Wt of Crucible + sample aft.Ignition 56.1426 53.0723

Ash ISO 1171 : 2010 Wt of sample 1.1015 1.2332

Ash ( ad basis ) %wt 14.28 14.17

Average 14.22

Ash (dry basis) Calculation Ash (dry basis ) 14.26

Ash ( as received) Calculation Ash ( as received ) 13.11

Wt of Crucible Empty 27.0963 26.586

Wt of Crucible+ Sample bef. Ignition 28.1204 27.6002

Wt of Crucible + sample aft.Ignition 27.7498 27.2337

Volatile Matter ISO 562 : 2010
Wt of sample 1.0241 1.0142
%wt *

Volatile matter ( ad basis ) 35.90 35.85

Average 35.87

Volatile Matter ( dry basis ) Calculation Volatile matter ( dry basis ) 35.98

Volatile Matter ( as received ) Calculation Volatile matter ( as received ) 33.06

Wt of dish empty 64.3097 63.0138

wt of dish +sample bef. Drying 67.5775 66.2715

Wt of dish+sample aft. Drying 67.5367 66.2312

Inh. Moisture ISO 589:2008-B2 %wt
Wt of sample 3.2678 3.2577

Inh. Moisture %wt 1.25 1.24

Average 0.29
* Outsource

Analyzed By Reviewed By Approved By

Date:

page 1 of 11
 Raw Data Sheet
Date:
Lab ref. No.:
Batch code: Client Ref.:
Retention No.: Sample Description:
TOTL-SP08-F04 Issue n◦ / Date 00 / 01 April 19

Test Method Description Unit 1 2 Temp. Humidity Date Initials

Mass Of Sample gm 1.0974 1.0799

Gross C.V (QV) (ad basis) cal/gm 7129 7140
Volume of Barium Hydroxide ml 15 14.8
Gross C.V (QV) ISO 1928 Volume of hydrochloric acid ml 15.1 15.5
7089.34341283399 7099.56341872874
cal/gm
Gross C.V (QV) (ad basis) after correlation 7094.45
MJ/kg 29.70
cal/gm 7115.09
Gross C.V (QV) Calculation Gross C.V(QV)(dry basis)
MJ/kg 29.80
cal/gm 6538.77
Gross C.V (QV) Calculation Gross C.V(QV) (as received)
MJ/kg 27.38
cal/gm 6262.71
Net C.V(QP) Calculation Net C.V (QP) (as received)
MJ/kg 26.23
cal/gm 6268.05
Net C.V(Qv) Calculation Net C.V (QP) (as received) at constant volume
j/g 26200.44
QV-P j/g 27.28
Qh j/g 1067.99
Qmad j/g 7.08
Net C.V(QP) Calculation ASTM Qmar j/g 197.76
Qpad (net) (air dry) j/g 28607.03
Qpad (net) (dry Base) j/g 28697.33
Qpad (net) (as Received ) j/g 26175.08
4.90 5.10
Sulphur ISO19579 Sulphur ( air dry )
5.00
% wt
Sulphur (dry basis ) Calculation Sulphur ( dry basis) 5.01
Sulphur ( as received) Calculation Sulphur ( as received ) 4.61
72.29 71.99
Carbon ISO 29541 Carbon (air dry )
72.14
% wt
Carbon Calculation Carbon ( dry basis ) 72.35
Carbon Calculation Carbon (as received) 66.49
Hydrogen (air dry ) 4.98
Hydrogen Estimation ISO 1928 Hydrogen ( as received ) % wt 4.59
Hydrogen ( drybasis ) 4.99
4.95 4.84
Hydrogen ISO 29541 Hydrogen ( air dry )
4.90
Hydrogen ASTM D 58 Had % wt 4.86
Hydrogen Calculation Hydrogen ( drybasis ) 4.91
Hydrogen Calculation Hydrogen ( as received ) 4.51
1.27 1.26
Nitrogen ISO 29541 Nitrogen ( air dry )
1.27
% wt
Nitrogen Calculation Nitrogen ( dry basis ) 1.27
Nitrogen Calculation Nitrogen ( as received) 1.17
Oxygen ISO 1170 Oxygen ( air dry ) 2.19
Oxygen ASTM D 58 Oad % wt 1.93
Oxygen ISO 1170 Oxygen ( dry basis ) 2.19
Oxygen ISO 1170 Oxygen ( as received ) 2.02
Fixed carbon Fixed Carbon ( air dry ) 49.61
% wt
Fixed carbon ISO 17246 Fixed Carbon ( dry basis ) 49.76
Fixed carbon Fixed Carbon ( as received ) 45.73
Carbon dioxide Emission factor Directive 2007/589/EC CO2 Emission Factor (tCo2/Tj) 92.99
Hard Grove Index ISO 5074 HGI
* Outsource

page 2 of 11
 Raw Data Sheet
Date:
Lab ref. No.:
Batch code: Client Ref.:
Retention No.: Sample Description:
Analyzed By Reviewed By Approved By

Date:

TOTL-SP08-F04 Issue n◦ / Date 00 / 01 April 19

page 3 of 11
 Proximate A

Parameter Base
Total Moisture As Recei
Air Dr
Ash Dry Ba
As Recei
Air Dr
Volatile Matter Dry Ba
As Recei

Air Dr

Gross CV Dry Ba

As Recei

Net CV (ISO) at
As Recei
Constant Pressure

Net CV (ISO) at
As Recei
Constant Volume

Air Dr

Net CV (ASTM) at
Constant pressure Dry Ba
 Net CV (ASTM) at
Constant pressure

As Recei

Ultimate An

parameter Base
Air Dry
Sulfur Dry Base
As Receive
Air Dry
Carbon Dry Base
As Receive
Air Dry
Hydrogen Dry Base
As Receive
Air Dry
Nitrogen Dry Base
As Receive
Air Dry
oxygen Dry Base
As Receive

Air Dry
Fixed Carbon Dry Base
As Received

CO2 Emission FactorCO2 Emission Factor (tC

CO2 Emission FactorCO2 Emission Factor (tC
Proximate Analysis

Base Result
As Received 8.10
Air Dry 14.22
Dry Base 14.26
As Received 13.11
Air Dry 35.87
Dry Base 35.98
As Received 33.06
7094.45341578137
Air Dry
30
7115
Dry Base
29.80
6539
As Received
27.38
6263
As Received
26.23
6268.05
As Received
26200.44
6843.79
Air Dry
28.607027508076
6865.39
Dry Base
28.6973301801326
 6261.98
As Received
26.175083133034

Ultimate Analysis

Base Result
Air Dry 5.00
Dry Base 5.01
As Received 4.61
Air Dry 72.14
Dry Base 72.35
As Received 66.49
Air Dry 4.90
Dry Base 4.91
As Received 4.51
Air Dry 1.27
Dry Base 1.27
As Received 1.17
Air Dry 2.19
Dry Base 2.19
As Received 2.02

Air Dry 49.61

Dry Base 49.76
As Received 45.73

CO2 Emission Factor (tCo2/Tj) 92.99

CO2 Emission Factor (tCo2/Tj) 92.99
 10/11

CERTIFICATE OF ANALYSIS

Report Number : Client name :

Report date Client address :
Material : Sample received :
Client ref : Analysis completed :
Container Type : Sealed/Seal No. :
Sample Label :

ID Test Method Unit Result Temp Uncertainty Humidity Date

Moisture ISO 589:2008-B2 %wt 8.10
Inherent Moisture ISO 11722 %wt 0.29
Ash (AD) %wt 14.22
Dry basis ISO 1171 : 2010 %wt 14.26
As received %wt 13.11
Volatile Matter(AD) %wt 35.87
Dry basis ISO 562 : 2010 %wt 35.98
As received %wt 33.06
Gross calorific value (AD)(Qp) MJ/kg 29.70
cal/gm 7094
Dry basis MJ/kg 29.80
ISO 1928
cal/gm 7115
As received MJ/kg 27.38
cal/gm 6539
Net calorific value (AR)(QP) MJ/kg 26.23
cal/gm 6263
Calculation
Dry basis MJ/kg 28.70
cal/gm 6865
Net calorific value (AR)(Qv) MJ/kg 26.20
Calculation
cal/gm 6268
Sulfur (AD) %wt 5.00
Dry basis %wt 5.01
As received %wt 4.61
(AD): Air Dry
(AR): As Received
(QV): Constant Volume
(Qp): constant Pressure

OPINIONS/ INTERPRETATIONS ( IF NEEDED):

REVIEWED BY
ANALYZED BY AUTHORIZED BY
 11/11

CERTIFICATE OF ANALYSIS

Report Number : 0 Client name : 0

Report date 12/30/1899 Client address : 0
Material : 0 Sample received : 12/30/1899
Client ref : 0 Analysis completed : 12/30/1899
Container Type : 0 Sealed/Seal No. : 12/30/1899
Sample Label : 0

ID Test Method Unit Result Temp Uncertainty Humidity Date

Carbon (AD) %wt 72.14
Dry basis ISO 29541 %wt 72.35
As received %wt 4.61
Hydrogen (AD) %wt 4.895
Dry basis ISO 29541 %wt 4.91
As received %wt 4.51
Nitrogen (AD) %wt 1.27
Dry basis ISO 29541 %wt 1.27
As received %wt 1.17
Oxygen (AD) %wt 2.19
Dry basis ISO 1170 %wt 2.19
As received %wt 2.02
Fixed Carbon (AD) %wt 49.61
Dry basis ISO 17246 %wt 49.76
As received %wt 45.73
Carbon dioxide
2003/87/EC - 92.99
Emission factor
Hard Grove Index ISO 5074 - #REF!
(AD): Air Dry
(AR): As Received

OPINIONS/ INTERPRETATIONS ( IF NEEDED):

REVIEWED BY
ANALYZED BY AUTHORIZED BY