Professional Documents
Culture Documents
OF
OF CHEMICAL ENGINEERING
SRM UNIVERSITY,KATTANKULATHUR
NAME :
REG.NO :
SRM UNIVERSITY
(Under Section 3 of UGC Act,1956)
SRM Nagar,KATTANKULATHUR – 603203
KANCHEEPURAM DISTRICT
BONAFIDE CERTIFICATE
Register No:
Lab Incharge
Class: Reg.No:
INDEX
Exp Date Title of Experiment Page Date of Remarks
.No submission
1
10
11
12
Ex.No. Date:
SIEVE ANALYSIS
AIM:
THEORY:
Sieve analysis is one of the most important methods for accessing the size of the
mineral particles. The test sieves used in the sieve analysis are made of bronze or steel
wire drawn to a very close tolerances and are woven into a screen cloth with
standardized square aperture or openings of various size. One of the standard screen
series is Tyler standard screen series. This set of screens is based on the opening of
the 200mesh screen, which is established at 0.074mm. The area of the openings in any
one screen in the series is exactly twice that of the openings in the next smaller screen
is 2 . There are different methods of plotting the sieve analysis data. The most
widely used are given below.
PROCEDURE:
FORMULAE:
Differential analysis:
1
1
3
3.diameter,
Volume mean 1
D
x
V
X
i
3
Dpi
i 1
Cumulative analysis:
TABLE
S. Mesh Size of Average Mass Mass Cumula xi xi .DPi xi 1
no No. screen diameter retained fraction tive Dp Dpi
Dp3
opening , Xi Mass i
, D pi fraction
i
Dpi
(mm) (mm) (g) mm mm-3 mm-1
-1
mm
1
10
2
RESULT:
By Differential analysis
By cumulative analysis:
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
************
3
Ex.No. Date:
SCREEN EFFECTIVENESS
AIM:
THEORY:
PROCEDURE:
EE
E x x x x x 1 x B
B
f D
f
A B
x
D
x 2 x f 1D xf
B
Where,
MODEL GRAPH
5
TABLE 1:
S Mes Size Mass Mass Cum. Mass Mass Cum. Mass Mass Cum.
. h of retain fracti Mass retain fracti Mass retai fracti Mass
N No. scree ed on, fracti ed on, fracti n ed on, fracti
o n (g) xi on, (g) xi on, (g) xi on,
openi
ng
(mm)
1
2
3
4
5
6
7
8
9
1
0
6
RESULT:
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
********
7
Ex.No. Date:
JAW CRUSHER
AIM:
THEORY:
Crushers are slow speed machines for coarse reduction of large quantities of
solids. The main types are jaw crushers, gyratory crushers, smooth-roll crushers and
toothed-roll crushers. There are two distinct types of jaw crushers, the Blake crushers
and the dodge crusher. The Blake Jaw crusher is the commonly used crusher.
In Blake Jaw crusher feed is admitted between the two jaws, set to form a V
open at the top. One jaw, the fixed or anvil jaw is nearly vertical and does not move;
the other, the swinging jaw reciprocates in a horizontal plane. It makes an angle of 20º
to 30º with the anvil jaw. It is driven by an eccentric so that it applies great
compressive force to lumps caught between the jaws. The jaw faces are flat or slightly
bulged; they may carry shallow horizontal grooves. Large lumps caught between the
upper pacts of the jaws are broken, drop into the narrower space below, and are
recrushed the next time the jaws close. After sufficient reduction they drop out the
bottom of the machine.
In the dodge crusher the moving jaw is pivoted at the bottom .The minimum
movement is thus at the bottom and a more uniform product is obtained, but the
tendency to choke is high, so it is not mostly used.
PROCEDURE:
TABLE :
Xi = (Xi/ D pi
=
FORMULAE:
m thod:
1. Volume displacement
e Increase in
volume of water =
4
nx x x =...............mm3
r3 3
r =................mm
(mm)
By Differential analysis
By cumulative analysis
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******
Ex.No. Date:
BALL MILL
AIM:
THEORY:
Ball mill is a tumbling mill (grinder) type size reduction equipment. It has a
cylindrical Shell slowly rotating about a horizontal axis and filled to about half of its
volume with balls which act as a grinding medium. It can be operated batch-wise or
continuously.
In ball mill most of the size reduction is done by impact as the balls drop from
near the top of the Shell. When the mill is rotated, the balls are picked up by the mill
wall and carried nearly to the top, where they break contact with the wall and fall to
the bottom to be picked up again. Centrifugal force keeps the balls in contact with the
wall and with each other during upper movement. While in contact with the wall the
balls do some grinding by slipping and rolling over each other, but most of the
grinding occurs at the zone of impact.
If the speed of the mill is too high the balls are carried over and the mill is said to
be centrifuging. The minimum speed at which centrifuging occurs is called the critical
speed. Little or no grinding is done when a mill is centrifuging and operating speed
must be less than the critical speed.
PROCEDURE:
TABLE 1.
S. Mes Size of Averag Mass Mass Cumulativ xi / D pi 1/ D pi
N h screen e retained fraction e Mass
o No. opening diamete , fraction,
Dpi r, D pi xi
Xi = (Xi/ D pi
=
FORMLAE:
r =................mm
pi
D = average size of particle retained on the ith increment
Where
R= mill radius
r = ball radius
RESULT:
By Differential analysis
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******
Ex.No. Date:
HAMMER MILL
AIM:
THEORY:
Hammer mill contains a high speed rotor turning inside a cylindrical casing. The
shaft is usually horizontal. Feed dropped into the top of the casing is broken and falls
out through a bottom opening. In a hammer mill the particles are broken by sets of
swing hammers pinned to a rotor disk. A particle of feed entering the grinding zone
cannot escape being struck by the hammers. It shatters into pieces, which fly against a
stationary anvil plate inside the casing and break into smaller fragments. These in turn
are rubbed into powder by the hammers and pushed through a grate or screen that
covers the discharge opening.
Several rotor disks, 150 to 450 mm (6 to 18 in.) in diameter and each carrying
four to eight swing hammers, are often mounted on the same shaft. The hammers may
be straight bars of metal with plain or enlarged ends or with ends sharpened to a
cutting edge. Intermediate hammer mills yield a product of 25 mm (1 in.) to 20-mesh
in particle size. In hammer mills for fine reduction the peripheral speed of the hammer
tips may reach 110 m/s; they reduce 0.1 to 15 ton/h to sizes finer than 200 mesh.
PROCEDURE:
The feed sample of required size was prepared by using set of sieves.
250 g of the sample was taken.
The sample was put into hammer mill where it was ground.
The product from the mill was sieved using set of sieves.
The product present in each sieve was weighed.
The results were tabulated.
1 / Dpi Vs graph was plotted.
The size reduction ratio was calculated by differential analysis and cumulative
analysis.
OBSERVATIONS:
TABLE 1:
Xi = (Xi/ D pi
=
FORMULAE:
. 1 1
2. Power consumption, P m x Kb x , kW
Dsb Dsa
3. Kb = 0.3162 x Wi
.
4. 60
Wf x 1000 , ton/h
m tc
Where,
Wf = Weight of feed, kg
By Differential analysis
By cumulative analysis
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******
Ex.No. Date:
BATCH SEDIMENTATION
AIM:
To study the settling characteristics of slurry and to determine the area of the
continuous thickener required to concentrate the slurry from a concentration of -------
-g/l at the rate of 10,000m3/day using kynch theory.
THEORY:
The separation of slurry by gravity settling into a clear fluid and slurry of higher
solids content is called sedimentation. The mechanism of sedimentation may be best
described by observation of what occurs during a batch settling test as solids settle
from slurry in a glass cylinder. Gravity settling under hindered settling conditions is
often used to convert dilute slurry of fine particles into a clarified liquid and a
concentrated suspension. This process is carried out in large open tanks called
thickeners or clarifiers. The thickener design is generally based on measurements of
the settling rates obtained from batch tests in the laboratory.
GRAVITY THICKENER
PROCEDURE:
MODEL GRAPH:
TABLE
1 21
2 22
3 23
4 24
5 25
6 26
7 27
8 28
9 29
10 30
11 31
12 32
13 33
14 34
15 35
16 36
17 37
18 38
19 39
20 40
S.No Zi ZL L C0 Z 0 Zi Z L VL
CL VL 1 1
Zi L
C C
L U
FORMULAE:
C0 Z 0
1. Slurry concentration, , kg/m3
C L
Zi
C0 Z 0
2. Under flow concentration, , kg/m3
U
C Z
U
Zi Z L
3. Settling velocity, L, m/Sec
VL
L
Where,
F = Rate of feed, m3/s
V
Plot 1 L 1 vs CL
C C
L U
RESULT:
The area of the continuous thickener required to concentrate the slurry from
the concentration ---------------------g/lit at 10,000m3/day is---------------m2.
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******
Ex No. Date:
Aim
To calculate the loss factor Kc for sudden contraction.
Theory
Fluids are usually transported in pipe or tubing, which is circular in cross
section and available in widely varying sizes, wall thickness and materials of
construction. The methods used to join the pieces of pipe depend in part on the
properties of the material but primarily on the thickness of the wall. Thick walled
tubular products are usually connected by screwed fittings, by flanges or by welding.
Pieces of thin walled tubing are joined by soldering or by compression or flare
fittings.
When the cross section of the conduit is suddenly reduced, the fluid stream
cannot follow around the sharp corner and the stream breaks contact with the wall of
the conduit. A jet is formed, which flows into the stagnant fluid in the smaller section.
The jet first contracts and then expands to fill the smaller cross section, and down
stream from the point of contraction the normal velocity distribution eventually is
reestablished. The cross section of minimum area at which the jet changes from a
contraction to an expansion is called vena contracta. The friction loss form sudden
contraction is proportional to the velocity head in the smaller conduit and can be
calculated by the equation,
PROCEDURE
Note the following system details:
i) Length and breadth of the collection tank
ii) Diameter of the pipe
iii) Diameter of the enlarged pipe
Switch on the motor of the pump and allow water to flow through the
pipe.
Note the manometer reading.
Close the outlet valve of the collection tank.
Note the time taken for 10cm rise of water in the collection tank.
Repeat the same procedure for the different flow rates.
FORMULAE
Contraction loss:
2
Kc Vb
h fe 2g
c
Sb
K c α1 S
a
Q
V
SF
ρm ρf
h f ΔH
ρf
i) ΔHf ρ m ρ f ΔHm
ρf
ΔHf pressuredrop,( in meter of water)
ΔHm - manometerdifference, m
3
ρf - Density of water,kg/m
ρ m density of mercury,kg/m3
(ii)
LBH
Q
t
L - lenght of thecollection tank,m
B - Breadth of thecollection
tank,m H - Rise in waterlevel, m
Q
(iii) Vb
A
(iv) Pc gRm m f
Pc Dropin pressure
Rm Difference in manometerlevel
(v) h Pc
fc
f
h fc Lossduetofriction
(iv) N DVbρf
μ
Re
MODEL GRAPH
hfC
Slope,KC
2
V a /2gC
OBSERVATION
TABLE .1
S. Manometer Reading(m) Time for Qa Vb NRe Drop in Loss
10cm pressure due to 2
No. V b /2gc
rise of Pc friction
(m)
Left Right Difference
water (s) hfc
30
RESULT
The loss factor Kc for sudden contraction , Kc
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******
31
Ex No. Date:
AIM
To determine the coefficient of discharge of venturimeter.
THEORY
The venturimeter is a flow measuring device very widely used in industry. It
operates on the same principle as that of the orifice meter. It differs from the orifice
meter by the fact that there is a gradual variation in the cross-section so as to reduce
losses due to turbulence. The head loss in the orificemeter at the same conditions as
the venturimeter is many times greater. The power loss is proportionally greater and
when an orifice is inserted in a line that is carrying fluid continuously for a long
period of time, the cost of this power loss is more than the saving in the first cost. The
venturimeter are however used only for permanent installations. The venturimeter
consists of tapering sections inserted in the pipeline with the taper smooth and
gradual. At a point in the line and at the throat of the venturimeter, tapings are
provided which has to be connected with a manometer. The venturimeter itself is
connected across the pipes for which the fluid flow is to be determined.
PROCEDURE
Note the following system details:
iv) Length and breadth of the collection tank
v) Diameter of the pipe at the entrance
vi) Diameter of the pipe at the throat
Switch on the motor of the supply pump.
Open the delivery valve of the pipe.
Note the manometer reading.
Close the outlet valve of the collection tank.
Note the time taken for 10cm rise of water in the collection tank.
Repeat the same procedure for 5 different flow rates.
FORMULAE :
Where
Reynold’s number :
NRe = doVoρ / µ
where
do = diameter of venturi, m
1) β = do/D
do = diameter of venturi, m
D = diameter of pipe, m
4) Velocity, Vo = Q/Ao
5) Co-efficient of discharge of venturimeter,
ρ (1 β 4 )
Cd V o f
2g(ρm ρ f )Hm
Model Graph:
Qact
Cd
Slope,
Cd = Qact/Qt
Qt
NRe
OBSEREVATION
TABLE
35
RESULT
The venturi coefficient was calculated and required graphs were plotted. The
venturi coefficient was found to be .
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******
36
Ex. No. Date:
AIM
THEORY:
The orifice meter is an extremely simple device used to measure the flow rate of
fluids and hence widely used in practice. It normally consists of a plate with a
centrally drilled hole. The drilled plate is inserted perpendicular to the direction of
flow. Pressure taps are provided before and after the orifice plate and are connected to
a manometer. Whenever a constriction is introduced into the fluid stream, there is a
reduction in the pressure of the fluid coming through the constriction and an increase
in the velocity. A manometer is used to measure the reduction in pressure due to the
constriction between the tapings. Bernoulli’s equation provides a basis for correlating
the increase in the velocity head with a decrease in the pressure head. The equation
governing the flow in an orifice meter is :
2g(ρm ρf ) ΔH
V0 Q C m
Ao
d ρ f (1 β4 )
where
Ao = area of orifice in m2
Cd = coefficient of discharge
Since Q = Ao C 2g(ρm ρf ) ΔH
d m
ρ f (1β4 )
FORMULAE:
1) β = d/D
d = diameter of
orifice D =
diameter of pipe.
ρ (1 β 4 )
Cd V o f
2g(ρm ρ f )Hm
6) NRe = dVoρ / µ
where
do = diameter of venturi
ρ = density of fluid
Specifications :
MODEL GRAPH:
Slope,Cd = Qact/Qt
Qact
Cd
NRe
Qt
NRE
OBSERVATIONS
Table
S. Manometer Reading(m) Time for Pressure Actual Coefficient NRe
10cm rise of head discharge of
No. water (s) difference, discharge,
Qact
Cd
m of H2O m3/s
40
RESULT :
The orifice coefficient was calculated and required graphs were plotted. The
orifice
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******
41
Ex.No: Date:
FLOW MEASUREMENT USING ROTAMETER
AIM
To determine the coefficient of discharge of rotameter.
THEORY
PROCEDURE
The motor is switched on.
The water is allowed to flow through the inlet valve.
The flow rate of water is fixed using the float present in the rotameter.
Collect the outlet water in the collection tank and note the time taken
for 10cm rise of water level in the collection tank.
Repeat the same procedure for different flow rates.
FORMULAE
Qact
3. Coefficient of discharge, Cd =
Q
th
TABLE
Slope,Cd = Qact/Qt
Qact
Cd
NRe Qt
RESULT
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******
Ex. No. Date:
EFFLUX TIME
AIM
To determine the efflux time of a tank through an orifice at its bottom.
THEORY
The theory describing the efflux time of a tank has been derived by Crosby
and by Bird,Stewart, and Lightfoot , and further extended to systems with the installed
fittings by Hanesian. Consider a vertical tank that contains a Newtonian liquid up to
the level h above the bottom of the tank. The top of the tank as well as the bottom of
the drain pipe are exposed to the atmosphere. Thus, the liquid drains from the tank
under the influence of gravity. An opening in a tank through which the liquid flows is
an orifice. The liquid approaching the orifice gradually converges towards it from a
cross section called vena contracta. Let it be assumed that, it is a constant head(h).
From Bernoulli’s equation, if the orifice is small compared to h, the velocity V 2 may
be considered to be constant across the equation of continuity.
Q = s1v1 = s2v2
FORMULAE
2 ATH1 H 2
Theoretical draining time =
Ao2gC d
AT = area of tank
Ao = area of orifice
PROCEDURE
TABLE
The efflux time of a tank through an orifice was measured and the percentage
error was found to be . A graph was plotted between theoretical
draining time vs actual draining time.
Internal Assessment:
Observation(5)
Calculations(10)
Viva(5)
*******