Professional Documents
Culture Documents
Process Table E
Annealing N
Normalizing N
Stress-Relieving N
Process Table F
Low Pressure Carburizing N
Process Table G
Sinter Hardening N
Process Table G
Ion Nitriding N
Personnel Contacted:
Name: Title: Phone: Email:
Spencer Lee General Manager 886-918068066 spencer@kenos.com.tw
Auditors/Assessors:
Name: Company: Phone: Email:
Spencer Lee Kenos industrial Co., 886-7-6229969 spencer@kenos.com.tw
Assessment
2
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
3
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
4
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
5
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
6
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
It is criticalSection 1 - Management
that all customer Responsibility & Quality Planning
requirements and lot
identification be adequately transferred to internal
heat treat documents. The facility shall ensure
that the data entered in the receiving system
match the information on the customer's shipping
1. Computers staff should check and make
documents. Documented processes and evidence
sure all customers providing information
Does the facility ensure that of compliance shall exist, e.g., shop travelers,
prior to the computer process.
the data entered in the work orders, etc. Sometimes the material
2.1 receiving system matches the received does not precisely correspond to v
2. The parts receiving staffs shall check
information on the customer's customer shipping documents. The facility shall
the parts' quantities, size, and quality
shipping documents? have a detailed process in place to resolve
condition and confirm them with
receiving discrepancies.
customer's providing infprmation .
The requirements stated above also apply to
captive heat treat departments. This process
refers to receiving and shipping the parts in and
out of the heat treat department.
7
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
1. Formen or operators
Section 1 - Management Responsibility should check
& Quality Planning
Containers handling customer product shall be inside of bins/barrels after finishing
free of inappropriate material. After emptying and feeding parts and remove all parts when
before re-using containers, containers shall be the parts are remained in the inside of
inspected to ensure that all parts and inappropriate container.
Are containers free of
2.6 material have been removed. The source of v
inappropriate material?
inappropriate material shall be identified and 2. The operators working at parts
addressed. This is to ensure that no receiving site should check and clean the
nonconforming heat treated parts or inappropriate inside of container, If the parts are found in
material contaminate the finished lot. the inside of container, they should
remove all parts.
1. The formen or operators should get the
weigh of each batch before feeding to
furnace.
Furnace loading parameters shall be specified,
documented, and controlled. Examples include
Is furnace loading specified, 2.The weight of each batch are recorded
2.7 feed rate, belt speed, number of parts per fixture, v
documented and controlled? at the back of label and daily production
and load weight. Refer to Process Tables, Section
report.
3.0, for frequency of checks.
3. Feeding rate , belt speed of each batch
are recorded at the computer
Unplanned or emergency downtime greatly raises
the risk of improper processing. Operators shall
1. The parts in process will be isolated
be trained in material handling, containment
when power is shutdown over 30 miniutes.
Are operators trained in action, and product segregation in the event of an
( per working instruction W-P-20
material handling, equipment emergency including power failure.
emergency responsse while power failure)
containment action and Training shall be documented. Work instructions
2.8 product segregation in the specifically addressing potential types of v
2. All non-confirming parts affected by
event of an equipment equipment emergencies and failures shall be
power failure will be moved to non
emergency including power accessible to and understood by equipment
confirming area and place a red card in
failure? operators. These instructions shall address
the container to control them.
containment actions related to all elements of the
heat-treating process, e.g., loading, austentizing,
quenching, tempering.
1. All parts are properly stored at the
Handling, storage, and packaging shall be inside of warehouse
adequate to preserve product quality. The heat
treater’s furnace loading system, in-process 2. All hoppers have been instaledl the
handling, and shipping process shall be assessed plastic plate ensuring all parts cannot be
Is the handling, storage and
for risk of part damage or other quality concerns. damaged when parts are contacted
2.9 packaging adequate to v
Some equipment includes conveyors and other mutually or steel hoppers.
preserve product quality?
moving components that may not be able to
handle all part configurations. Other practices 3. All inside of containers should be
such as stacking of overloaded containers can cleaned and placed several papers to
also increase the risk of part damage. prevent oil contamination.
8
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
9
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
Product testSection
equipment1shall
- Management
be verified. Test Responsibility
1. QC shall issue a&schedule
Quality Planning
of yearly
equipment shall be verified/calibrated per calibration to specify which testing
applicable customer-specific standard or per an instruments and when should be
applicable consensus standard such as those calibrated.
Is product test equipment
2.16 published by ASTM, DIN, EN, ISO, JIS, NIST, v
verified?
SAE etc. Verification/calibration results shall be 2. All testing instruments shall be posted a
internally reviewed, approved, and documented. tag to verify these instruments have been
Refer to Process Tables, Section 1.0, for calibrated and complied with the
frequency of checks. calibration schedule.
Section 3 - Equipment
The heat-treat equipment including furnaces,
generators, and quench systems shall have proper The quenching time,temperature and
Do furnaces, generators, and process controls and related equipment. Examples carbon potential, quenching oil
3.1 quench systems have proper include temperature, carbon potential/dew point, temperature and tempering temperature v
process control equipment? gas flows, quench monitoring system including and time are controlled by PLC and
agitation, temperature control, etc. as listed in the computer automatical control system.
applicable Process Tables, Section 1.0.
1. Thermal couples, temperature and CP
controller, standard temperature testing
The calibration and certification of the process instrument and quenching temperature
Are process equipment equipment shall be checked at regular specified profile have been completely calibrated in
3.2 calibrations and/or verification intervals. Refer to the applicable Process Tables, 2017. v
certified, posted, and current? Sections 1.0 and 2.0, for equipment calibration or
certification time tables. 2. The calibration of quenching and
tempering belt speed have been done in
2017.
1. The thermal couples have been
The thermocouples and protection tubes shall be renewed 10 pcs because the deviation is
Are thermocouples &
checked or replaced in compliance to a preventive over 5°C when calibrated in 2017
3.3 protection tubes checked or v
maintenance schedule. Refer to the applicable
replaced per Process Tables?
Process Tables, Section 2.0. 2. Thermal couples shall be changed after
using 5 years althought it is available.
Assessment
11
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
Section
Ammonia pick-up 1 -undesirable
can be Management Responsibility
in parts and & Quality Planning
heat treat processes not specifying/requiring
ammonia as an addition.
1. Operators shall follow the notification
The heat treater shall perform a minimum 3 hours
written on the shop order to shut off
purge prior to processing product not requiring
Is there a miniumum of 3 hour ammonia flow meter valve and purge
ammonia as an addition. Reduction of 3 hours
purge of the furnace ammonia for 3 hours minimum.
purge requires conclusive test data of the
atmosphere when switching
3.10 atmosphere to show no significant amount of v
from an ammonia bearing 2. The purge time for removing ammonia
residual ammonia is present in the furnace
atmosphere to a non- shall be recorded on the computer.
atmosphere.
ammonia bearing?
Log book, data logger, or other records shall
document the actual purge time and that sufficient
time has been allocated to remove ammonia from
the furnace prior to processing parts in heat treat
processes not specifying ammonia.
The heat treater shall periodically have the 1. Oil suppliers will take samples of each
quenching medium analyzed for specific furnace once a month and will send us the
quenching characteristics, e.g., cooling curve, test report including physical, chemical
water content, salt concentration, as specified in properties and cooling rate for reference
the applicable Process Tables, Section 5.0. This after 2 weeks.
Is the quenching medium does not include Process Table G & H.
3.14 V
analyzed? • The quench media characteristic tolerances shall 2. Kenos shall take 4 parts to test their
be specified by the quench medium supplier or the core hardness and record them everyday.
heat treater. When the core hardness after testing is
• Analysis shall be reviewed for conformance by lower than standard level, we will fill in the
the heat treater. This review shall be documented. oil addtives immediately.
12
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
Assessment
Section
The heat treater 1 - Management
shall control the energy or powerResponsibility & Quality Planning
for each part.
• A signature monitor for each machine is
preferred. A signature monitor gives the energy
Does the heat treater control
unit (voltage, kilowatt, etc.) vs. time or distance
3.16 the energy or power for each V
(for scanning systems).
part?
• An energy monitor or equivalent is acceptable if
approved by the authorized customer
representative.
13
CQI-9
Special Processes: Heat Treat Systems Assessment
Version 3, Issued 10/11
Job Identity:
Customer:
Shop Order Number:
Part Number:
Part Description:
Material:
Heat Treat Requirements:
4.7 Is the proper recipe or process 1.5 The recipe and process
specification (cycle times, 1.6 specification is properly
temperature, atmosphere, etc.) 2.1 created and saved at
used? Refer to Process Tables, 2.14 computer.
YES YES Pass
Section 3.0, for specific 2.15
parameters. List parameters that
were verified in this audit in the
spaces provided below.
4.8 What are the product inspection 2.15 Customer specification
requirements?
4.8.1 Requirement: (1) Core hardness Test result
Test Method: Rockwell (HRC)
Test frequency or quantity: 4
Selection of samples: 4
Specification: HRC 32 ~ 38
4.8.2 Requirement: (2)
Test Method:
Test frequency or quantity:
Selection of samples:
Specification:
4.8.3 Requirement: (3)
Test Method:
Test frequency or quantity:
Selection of samples:
Specification:
4.8.4 Requirement: (4)
Test Method:
Test frequency or quantity:
Selection of samples:
Specification:
Operator or Inspector Responsibilities
4.9 Were appropriate process steps 1.4 Foreman and assistant
signed off? 2.2 foreman signed their
YES YES Pass
2.3 name on the shop order
2.14
4.10 Were all inspection steps, as 1.2 Meet control plan
documented in the control plan 1.4 YES YES requirement Pass
performed?
4.11 Were steps/operations performed 1.2 Meet control plan
that were not documented in the 1.4 NO NO requirement Pass
control plan? 1.6
4.12 If additional steps were performed, 1.2 Foreman will get the
were they authorized? 1.4 management authority
1.6 YES YES prior to performing the Pass
1.11 additional process
1.17
4.13 Does the governing specification 1.11 Per work instruction
YES YES Pass
allow reprocessing or rework?
4.14 If the order was certified, did the 2.14 Supervisor daily check
certification accurately reflect the 2.15 YES YES the operating history Pass
process performed? record via the computer
4.15 Was the certification signed by an 1.17 Operator has the
YES YES Pass
authorized individual? signature on the label
4.16 Are the parts and containers free of 2.6 Operator should check
inappropriate objects or 2.11 and remove oil and
YES YES Pass
contamination? remaining parts for
container
Packaging Requirements
4.17 Are packaging requirements 2.9 Per customer request
YES YES Pass
identified?
4.18 Are parts packaged to minimize 2.9 The containing level of
mixed parts (for example, parts YES YES container is 90% max. Pass
packed over height of container)?
Shipping Requirements
4.19 Were the parts properly identified? 2.3 The square flag insert
2.9 the container or square
YES YES Pass
paper punch on the tag
when quality is OK
Were the containers properly 2.3 Each container has a
YES YES Pass
4.20 labeled? 2.9 label
14
CQI-9
Special Processes: Heat Treat Systems Assessment
Version 3, Issued 10/11
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat
treater is conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #'
NA - Requirement not applicable
Temperature uniformity tolerance for hardening furnaces shall be +/- 15 oC (or +/- 25oF). Temperature uniformity tolerance for
tempering furnaces shall be +/- 10 oC (or +/- 20oF). OK
A2.5 3.5 Recorded temperature(s) for austentizing processes shall be controlled within +/- 10 oC (or +/- 15oF) of the set point as
evidenced by continuous recording pyrometers. Furnace temperature shall be controlled with soak times starting at the lower
tolerance limit (as defined above).
For Continuous Furnaces, this requirement applies to the Qualified Work Zone. OK
A2.6 3.5 Recorded temperature(s) for tempering and precipitation hardening processes shall be controlled within +/- 5 oC (or +/- 10oF)
of the set point as evidenced by continuous recording pyrometers. Furnace temperature shall be controlled with soak times
starting at the lower tolerance limit (as defined above). OK
A2.7 3.2 Infrared pyrometers shall be calibrated annually using proper calibration methods or an approved manufacturer's procedure. NA
Batch Continuous Atmosphere
3.0 PROCESS MONITOR FREQUENCIES OK / NOK / NA
Furnace Furnace Generation
A3.1 1.4 Monitor primary temperature control Continuous recording with Continuous recording with Sign-off required
2.14 instrument(s). sign-off every 2 hours or sign-off every 2 hours or for each shift for
each batch for processes each lot for processes generators.
under 2 hours. Alarm under 2 hours). Alarm
systems (if set per limits in systems (if set per limits in
A2.5 and A2.6) satisfy the A2.5 and A2.6) satisfy the
sign-off requirement. sign-off requirement
OK
CQI-9
Special Processes: Heat Treat Systems Assessment
Version 3, Issued 10/11
A3.2 1.4 Monitor atmosphere generation as applicable. Generators shall
2.14 be continuously
3.7 monitored and
alarmed. Other
systems, such as
nitrogen-methanol
systems, may
either be
continuously
monitored and
alarmed, or sign-
off every 2 hours.
OK
A3.3 1.4 Monitor primary furnace atmosphere control(s) Continuous recording with Continuous recording with
2.14 sign-off every 2 hours or sign-off every 2 hours or
3.7 each batch for processes each lot for processes
under 2 hours. Alarm under 2 hours). Alarm
systems (if set per systems (if set per
acceptable limits) satisfy acceptable limits) satisfy
the sign-off requirement. the sign-off requirement
OK
A3.4 1.4 Verify primary furnace atmosphere control Daily Daily
2.14 method by back-up method
3.7
3.8 OK
A3.5 1.4 For austentizing salt baths: Salt chemistry Daily
2.14 (soluble oxides) or decarburization on the parts
3.13 shall be checked. OK
A3.6 1.4 Quench Media Process Parameters OK
2.12 Temperature Continuous recording with Continuous recording with
sign-off every 2 hours or sign-off every 2 hours or
each batch for processes each lot for processes
under 2 hours. Alarm under 2 hours). Alarm
systems (if set per systems (if set per
acceptable limits) satisfy acceptable limits) satisfy
the sign-off requirement. the sign-off requirement
OK
Quench Level Continuous monitor with alarm or daily verification. OK
Agitation Daily visual check, or monitor the agitation during the
quenching operation with alarm systems set at
acceptable limits.
OK
A3.7 1.4 Monitor time in furnace, cycle time or belt speed. Each batch Twice/shift & after any
2.14 change in the belt speed.
OK
A3.8 1.4 Monitor load size or fixturing or loading rate as Each batch Twice/shift & after any
2.7 applicable. change in loading rate.
OK
A3.9 1.4 Quench Delay Time - Each batch Each basket for pusher-
2.12 Quench delay time shall be based on the time type continuous furnaces
that the furnace door starts to open to the time the where the loaded basket is
load is at the bottom of the quench tank. quenched.
A5.1 2.12
3.14
Cooling Curve Analysis Semi-annually Semi-annually NA
A5.2 2.12 Water Quench Media
3.14 Suspended solids Semi-annually Semi-annually NA
A5.3 2.12 Salt Quench Media
3.14 Analysis & Contaminants Semi-annually Semi-annually NA
A5.4 2.12 Brine or Caustic Quench Media
3.14 Concentration and/or Specific Gravity. Daily Daily NA
Suspended solids Semi-annually Semi-annually NA
A5.5 2.12 Oil Quench Media
3.14 Water content, suspended solids, viscosity, Semi-Annually Semi-Annually
cooling curve, total acid, and flash point. OK
A5.6 2.13 Rust Preventive - Soluble Oil
Concentration 2x / week 2x / week OK
A5.7 2.11 Washers
Concentration of cleaner Daily Daily OK
Temperature of solution (required if temperature Each shift Each shift
is specified to be above ambient temperature). OK
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat treater is conforming
to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #'
NA - Requirement not applicable
Item # Related
HTSA Category/Process Steps
Question #
1.0 OK / NOK / NA
PROCESS AND TEST EQUIPMENT REQUIREMENTS
B1.1 3.1 All furnaces, generators and quench systems shall have temperature indicating instruments.
3.7
B1.2 3.1 Continuous strip charts and/or data loggers are required for temperature and carbon monitoring unit, e.g., dew point, oxygen probe, IR gas
3.7 analyzer, etc. For salt bath, only temperature is required to be recorded.
B1.3 1.18 A program for furnace and generator burnout is required. Not required for retort gas nitriding.
B1.4 3.2 Furnace weigh scales shall be verified quarterly and calibrated annually at a minimum.
B1.5 3.2 Dew pointers and gas analyzers, used to verify proper atmosphere in furnaces, shall be calibrated annually at a minimum.
B1.6 2.16 All hardness test equipment (for each scale used) shall be calibrated annually minimum, and verified daily or prior to use, per the applicable ASTM
standard, ISO standard, JIS standard, or approved standard.
B1.7 2.16 Files for testing hardness shall be verified per the Customer requirement.
B1.8 3.2 Refractometers (typically used to check polymer quenchants and washer solutions) shall be verified prior to use (with distilled water) and calibrated
annually (per manufacturer's requirements) at a minimum.
2.0 OK / NOK / NA
PYROMETRY
B2.1 3.2 Thermocouples and calibration of thermocouples shall conform to Section 3.1.
3.3
B2.2 3.2 Pyrometry Instrumentation and Calibration of instrumentation shall conform to Section 3.2
3.3
B2.3 3.2 CQI-9 requires a System Accuracy Test (SAT) check of the control thermocouple in the Qualified Work Zone per Section 3.3
3.3
B2.4 3.4 TUS shall be performed annually and after major rebuild per Section 3.4.
For Continuous Furnaces, this requirement applies to the Qualified Work Zone.
B2.6 3.2 Infrared pyrometers shall be calibrated annually using proper calibration methods or an approved manufacturer's procedure.
B3.3 1.4 Monitor primary furnace atmosphere control(s). Each batch (rotary Continuous recording with Daily
2.14 furnaces only) or sign-off every 2 hours.
3.7 continuous recording with Alarm systems satisfy the
3.8 sign-off every 2 hours. sign-off requirement
Alarm systems satisfy the
sign-off requirement
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat treater is conforming
to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #'
NA - Requirement not applicable
Item # Related
HTSA Category/Process Steps
Question #
B3.4 1.4 Dissociation of ammonia shall be checked in gas Each batch and every 4 Every 4 hours Daily N/A
3.7 nitriding. hours minimum
B3.5 1.4 Gas ratios for ferritic nitrocarburizing shall be Each batch Every 2 hours minimum
3.7 checked.
B3.6 1.4 Check salt chemistry (soluble oxides) in salt baths Daily
2.14 used for austenitizing, or decarburization on the parts.
3.13
B3.7 1.4 Quench Media Process Parameters
2.12 Temperature Each batch or continuous Each lot or continuous Each batch or
recording with sign-off recording with sign-off continuous
every 2 hours. Alarm every 2 hours. Alarm recording with
systems satisfy the sign-off systems satisfy the sign-off sign-off every
requirement. requirement. 2 hours.
Alarm
systems
satisfy the
sign-off
requirement.
Quench Level Continuous monitor with alarm or daily verification. Daily
Agitation Daily visual check, or monitor the agitation during the Daily
quenching operation with alarm systems set at
acceptable limits.
B3.8 1.4 Monitor time in furnace, cycle time or belt speed. Each batch Twice/shift & after any Each batch
2.14 change in the belt speed.
B3.9 1.4 Monitor load size or fixturing or loading rate as Each batch Twice/shift & after any Each batch
2.7 applicable. change in loading rate.
B3.10 1.4 Quench Delay Time if applicable - Each batch Each basket if applicable. Each batch
2.12 Quench delay time shall be based on the time that the
furnace door starts to open to the time the load is at
the bottom of the quench tank.
B4.2 1.4 Surface hardness Each batch Every 2 hours minimum Each batch
2.15
B4.3 1.4 Core hardness (when specified) Each batch Every 4 hours Each batch
2.15
B4.4 1.4 Case depth (when specified) Each batch Every 4 hours Each batch
2.15
5.0 QUENCHANT AND SOLUTION TEST Batch Continuous
Generators Salt Bath OK / NOK / NA
FREQUENCIES Furnace Furnace*
Quench Media Controls If Applicable
B5.1 2.12 Polymer Quench Media
3.14 Concentration Daily Daily
Quenchability Check; e.g., cooling curve, viscosity, or Semi-annually Semi-annually
titration.
B5.2 2.12 Water Quench Media
3.14 Suspended solids Semi-annually Semi-annually
B5.3 2.12 Salt Quench Media
3.14 Analysis & Contaminants Semi-annually Semi-annually Semi-annually
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat treater is conforming
to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #'
NA - Requirement not applicable
Item # Related
B5.7 2.11
HTSA Category/Process Steps
Question #
- Temperature of solution (required if temperature is Each shift Each shift Each shift
specified to be above ambient temperature).
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat
treater is conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
C1.2 3.1 Continuous strip charts and/or data loggers are required for temperature sensors.
C1.3 2.16 All hardness test equipment (for each scale used) shall be calibrated annually minimum, and verified daily or prior to use, per
the applicable ASTM standard, ISO standard, JIS standard, or approved standard.
C1.4 3.2 Furnace weigh scales shall be verified quarterly and calibrated annually at a minimum.
C1.5 3.2 Refractometers (typically used to check polymer quenchants and washer solutions) shall be verified prior to use (with distilled
water) and calibrated annually (per manufacturer's requirements) at a minimum.
C2.4 3.4 Temperature Uniformity Survey (TUS) TUS frequency shall be quarterly and after major rebuild per Section 3.4.
Temperature Uniformity tolerance for solution and aging furnaces shall be +/- 5 oC (+/- 10oF).
Temperature Uniformity tolerance for annealing furnaces shall be +/- 15 oC (+/- 25oF)
Minimum and maximum temperature ranges shall be defined. Exception: If the operating range of the Qualified Work Zone
is equal to or less than 85oC (155oF) then only one temperature is required to be tested. The test temperature shall be within
the operating range of the Qualified Work Zone.
For Continuous Furnaces, this requirement applies to the Qualified Work Zone.
C2.5 3.5 For Solution Treating and Aging: Recorded temperature(s) shall be controlled within +/- 5C (or +/- 10F) of the set point as
evidenced by continuous recording pyrometers. Furnace temperature shall be controlled with soak times starting at the
lower tolerance limit (as defined above).
For Continuous Furnaces, this requirement applies to the Qualified Work Zone
C2.6 3.5 For Annealing Furnaces: Recorded temperature(s) shall be controlled within +/- 10C (or +/- 15F) of the set point as
evidenced by continuous recording pyrometers. Furnace temperature shall be controlled with soak times starting at the
lower tolerance limit (as defined above).
For Continuous Furnaces, this requirement applies to the Qualified Work Zone
C2.7 3.2 Infrared pyrometers shall be calibrated annually using proper calibration methods or an approved manufacturer's procedure.
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat
treater is conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing
the job audit, the auditor shall verify heat treater is conforming to the customer's requirements.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
D1.1 2.16 All hardness test equipment (for each scale used) shall be calibrated annually
minimum, and verified daily or prior to use, per the applicable ASTM
standard, ISO standard, JIS standard, or approved standard.
D1.2 2.16 Files for testing hardness shall be verified per the Customer requirement.
D1.3 3.2 Refractometers (typically used to check polymer quenchants and washer
solutions) shall be verified prior to use (with distilled water) and calibrated
annually (per manufacturer's requirements) at a minimum.
2.0 PYROMETRY
D2.1 3.2 Infrared pyrometers shall be calibrated annually using proper calibration
methods or an approved manufacturer's procedure.
All process parameters shall be checked the beginning of every shift, tool change, or any equipment
repair. In absence of process parameter alarms, also check process parameters at end of shift or lot
(whichever is the greater frequency).
D3.1 1.4
2.12 Quench Temperature Alarm system for high and low
temperature is required.
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing
the job audit, the auditor shall verify heat treater is conforming to the customer's requirements.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing
the job audit, the auditor shall verify heat treater is conforming to the customer's requirements.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
Item
D5.1# Related
2.12HTSA Category/Process Steps
Question
3.14 #
Cooling Curve Analysis Every four months (complete
replacement of the quench
media and cleaning of the
quench tank within four months
satisfies this requirement).
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the aud
shall verify heat treater is conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
E1.1 3.1 All furnaces, generators and quench systems (where applicable) shall have temperature indicating instruments.
3.7
E1.2 3.1 Continuous strip charts and/or data loggers are required for temperature and carbon monitoring unit, e.g., dew
3.7 point, oxygen probe, IR gas analyzer, etc.
E1.3 3.2 Furnace weigh scales shall be verified quarterly and calibrated annually at a minimum.
E1.4 3.2 Dew pointers, 3-gas analyzers, spectrometers, and carbon IR combustion analyzers (shim stock analysis), used
to verify carbon potential in furnaces, shall be calibrated annually at a minimum. This is applicable when used in
controlling carbon-bearing atmospheres.
E1.5 3.2 Verification of calibration of spectrometers, and carbon IR combustion analyzers, shall be checked daily or prior
to use. This is applicable when used in controlling carbon-bearing atmospheres.
E1.6 3.2 Verification of calibration of 3-gas analyzers with zero gas and span gas shall be performed weekly at a minimum.
This is applicable when used in controlling carbon-bearing atmospheres.
E1.7 3.2 Oxygen probe controllers shall be calibrated quarterly (single-point or multi-point calibration) or semi-annual (multi-
point calibration only; single-point calibration not allowed). This is applicable when used in controlling carbon-
bearing atmospheres.
E1.8 2.16 All hardness test equipment (for each scale used) shall be calibrated annually minimum, and verified daily or prior
to use, per the applicable ASTM standard, ISO standard, JIS standard, or approved standard.
E1.9 3.2 Refractometers (typically used to check polymer quenchants and washer solutions) shall be verified prior to use
(with distilled water) and calibrated annually (per manufacturer's requirements) at a minimum.
2.0 PYROMETRY
E2.1 3.2 Thermocouples and calibration of thermocouples shall conform to Section 3.1.
3.3
E2.2 3.2 Pyrometry Instrumentation and Calibration shall conform to Section 3.2.
3.3
E2.3 3.2 CQI-9 requires a System Accuracy Test (SAT) check of the control thermocouple in the Qualified Work Zone per
3.3 Section 3.3.
E2.4 3.4 TUS shall be performed annually and after major rebuild per Section 3.4.
Temperature uniformity tolerance for furnaces operating at austenitizing temperatures shall be +/- 15 oC
(or +/- 25oF). Temperature uniformity tolerance for tempering furnaces shall be +/- 10 oC (or +/- 20oF).
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
PROCESS TABLE E - Annealing / Normalizing / Stress-Relieving
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the aud
shall verify heat treater is conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
For Continuous Furnaces, this requirement applies to the Qualified Work Zone.
3.0 PROCESS MONITOR Continuous
Batch Furnace Generators
FREQUENCIES Furnace
E3.1 1.4 Monitor primary temperature Continuous Continuous Sign-off required for each shift for
2.14 control instrument(s). recording with sign- recording with generators.
off every 2 hours or sign-off every 2
each batch for hours or each lot
processes under 2 for processes
hours. Alarm under 2 hours).
systems (if set per Alarm systems (if
limits in E2.5) satisfy set per limits in
the sign-off E2.5) satisfy the
requirement. sign-off
requirement.
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the aud
shall verify heat treater is conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
E3.6 1.4 Monitor time in furnace, Each batch Twice/shift & after
2.14 cycle time or belt speed. any change in the
belt speed.
E3.7 1.4 Monitor load size, fixturing or Each batch Twice/shift & after
2.7 loading rate as applicable. any change in
loading rate.
4.0 IN-PROCESS/FINAL TEST Batch Furnace Continuous
FREQUENCIES Furnace
E4.1 1.4 Microstructure shall be Each batch Each production
2.15 checked at a minimum run or each shift
magnification of 100x and, at a minimum.
400x or above 400x.
Microstructural visual
references shall be
available.
E4.2 1.4 Surface hardness (when Each batch Every 4 hours
2.15 specified)
E4.3 1.4 Core hardness (when Each batch Every 4 hours
2.15 specified)
5.0 SOLUTION TEST Continuous
Batch Furnace
FREQUENCIES Furnace
E5.1 2.13 Rust Preventive - Soluble
Oil
Concentration 2x / week 2x / week
E5.2 2.11 Washers
Concentration of cleaner Daily Daily
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify
treater is conforming to the customer's requirements.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
F1.3 3.1 Recording instruments are required for temperature and, hydrocarbon flow and pressure.
3.7
F1.4 3.2 Furnace weigh scales shall be verified quarterly and calibrated annually at a minimum.
F1.5 3.2 Hydrogen sensors and carbon IR combustion analyzers used to verify carbon potential in furnaces, shall be calibrated annually
at a minimum.
F1.6 3.2 Verification of calibration of spectrometers and carbon IR combustion analyzers, shall be checked daily or prior to use.
F1.8 2.16 All hardness test equipment (for each scale used) shall be calibrated annually minimum, and verified daily or prior to use, per
the applicable ASTM standard, ISO standard, JIS standard, or approved standard.
F1.9 2.16 Files for testing hardness shall be verified per the Customer requirement.
F1.10 3.2 Refractometers (typically used to check polymer quenchants and washer solutions) shall be verified prior to use (with distilled
water) and certified annually per manufacturer's requirements at a minimum.
2.0 PYROMETRY
F2.1 3.2 Thermocouples and calibration of thermocouples shall conform to Section 3.1.
3.3
F2.2 3.2 Pyrometry Instrumentation and Calibration of instrumentation shall conform to Section 3.2.
3.3
F2.3 3.2 CQI-9 requires a System Accuracy Test (SAT) check of the control thermocouple in the Qualified Work Zone per Section 3.3.
3.3
F2.4 3.4 TUS shall be performed annually and after major rebuild per Section 3.4.
Temperature uniformity tolerance for hardening and tempering furnaces shall be +/- 10 C or +/- 20 F.
F2.5 3.5 Recorded temperature(s) for austentizing and tempering processes shall be controlled within +/- 5 C or +/- 10 F of the set point
as evidenced by continuous recording pyrometers. Furnace temperature shall be controlled with soak times starting at the lower
tolerance limit (as defined above).
3.0 PROCESS MONITOR FREQUENCIES
F3.1 1.4 Monitor primary temperature control instrument(s). Continuous recording with sign-off every 2 hours or each batch for
2.14 processes under 2 hours. Alarm systems (if set per limits in F2.5) satisfy the sign-off requirement.
F3.2 1.4 Monitor primary furnace atmosphere control(s) or hydrocarbon flows. Continuous recording with sign-off every 2 hours or each
2.14 batch for processes under 2 hours. Alarm systems (if set per acceptable limits) satisfy the sign-off requirement.
F3.3 3.7
1.4 Monitor pressure in the carburizing and gas quenching process. Continuous recording with sign-off every 2 hours or each batch
2.14 for processes under 2 hours (carburizing process). Continuous recording with sign-off each batch (quenching process). Alarm
systems (if set per acceptable limits) satisfy the sign-off requirement.
F3.4 1.4 Verify primary atmosphere control method by back-up method by microstructural evaluation of parts or coupon, or carbon
2.14 analysis of shim stock or carbon bar. Verification shall be daily.
3.7
3.8
F3.5 1.2 Prior to production (APQP), the surface area of the parts shall be calculated and documented for each load configuration.
2.7
F3.6 1.4 Quench Media Process Parameters - Oil FREQUENCY
2.12 Temperature Continuous recording with alarm system is required.
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify
treater is conforming to the customer's requirements.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
F3.6 1.4
2.12HTSA
Item # Related
Category/Process Steps
Question #
Quench Level Daily check or alarm system is required.
Cooling water temperature and flow rate Monitor each load. Alarm system is required
F4.1 1.4 Microstructure shall be checked at a minimum magnification Daily per furnace (may rotate cells) or any time one of the
2.15 of 100x and, 400x or above 400x. Microstructural visual process parameters is out of specification.
references shall be available.
F4.2 1.4 Surface hardness Each batch
2.15
F4.3 1.4 Core hardness (when specified) Daily per furnace (may rotate cells) or any time one of the
2.15 process parameters is out of specification.
F4.4 1.4 Case depth (when specified) Daily per furnace (may rotate cells) or any time one of the
2.15 process parameters is out of specification.
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat treate
conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
G1.1 3.1
All furnaces, generators and quench systems shall have temperature indicating instruments.
3.7
G1.2
3.1 Continuous strip charts and/or data loggers are required for temperature and carbon monitoring unit, e.g., dew point, oxygen probe, IR
3.7 gas analyzer, etc.
G1.5 3.2 Dew pointers, 3-gas analyzers, spectrometers, and carbon IR combustion analyzers (shim stock analysis), used to verify carbon potential
in furnaces, shall be calibrated annually at a minimum (applies to carbon bearing atmospheres).
G1.6 3.2 Verification of calibration of spectrometers, and carbon IR combustion analyzers, shall be checked daily or prior to use (applies to carbon
bearing atmospheres).
G1.7 3.2 Verification of calibration of 3-gas analyzers with zero gas and span gas shall be performed weekly at a minimum (applies to carbon
bearing atmospheres).
G1.8 3.2 Oxygen probe controllers shall be calibrated quarterly (single-point or multi-point calibration) or semi-annual (multi-point calibration only;
single-point calibration not allowed). This applies to carbon bearing atmospheres.
G1.9 2.16 All hardness test equipment (for each scale used) shall be calibrated annually minimum, and verified daily or prior to use, per the
applicable ASTM standard, ISO standard, JIS standard, or approved standard.
2.0 PYROMETRY
G2.1 3.2 Thermocouples and calibration of thermocouples shall conform to Section 3.1.
3.3
G2.2 3.2 Pyrometry Instrumentation and Calibration of instrumentation shall conform to Section 3.2.
3.3
G2.3 3.2 CQI-9 requires a System Accuracy Test (SAT) check of the control thermocouple in the Qualified Work Zone per Section 3.3.
3.3
G2.4 3.4 TUS shall be performed annually and after major rebuild per Section 3.4.
Temperature uniformity tolerance for hardening furnaces shall be +/- 15ºC (or +/- 25ºF). Temperature uniformity tolerance for tempering
furnaces shall be +/- 10ºC (or +/- 20ºF).
G2.5 3.5 Recorded temperature(s) for sintering processes shall be controlled within +/- 10ºC (or +/- 15ºF) of the set point for processes operating
less than 1000ºC (1830ºF) and +/- 20ºC (+/- 35ºF) for processes operating greater than 1000ºC (1830ºF) as evidenced by continuous
recording pyrometers. Furnace temperature shall be controlled with soak times starting at the lower tolerance limit (as defined above).
For Continuous Furnaces, this requirement applies to the Qualified Work Zone.
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat treate
conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
G3.4 1.4 Verify primary atmosphere control method by back-up Daily Daily
2.14 method**. FOR ENDOTHERMIC ATMOSPHERE
3.7 ONLY.
3.8
G3.6 1.4 Quench Media Process Parameters - Oil
2.12
CQI-9
Special Process: Heat Treat System Assessment
Version 3, Issue 10/11
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat treate
conforming to the customer's requirements.
Continuous furnace frequencies are per lot (work order) or as specified, whichever is more frequent.
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
Cooling water temperature and flow rate Monitor each load. Alarm system is required
G3.8 1.4 Monitor time in furnace, cycle time or belt speed. Each batch Twice/shift & after any
2.14 change in the belt speed.
G3.9 1.4 Monitor load size or fixturing or loading rate as Each batch Twice/shift & after any
2.7 applicable. change in loading rate.
G3.10 1.4 Quench Delay Time - Each batch Not applicable for belt
2.12 Quench delay time shall be based on the time that the furnaces.
furnace door starts to open to the time the load is at
the bottom of the quench tank (oil) or the start of the
gas pressure quenching (gas quench).
G4.1 1.4 Microstructure shall be checked at a minimum Per customer requirement Per customer
2.15 magnification of 100x and, 400x or above 400x. as specified in control requirement as specified
Microstructural visual references shall be available. plan. in control plan.
The customer may have additional requirements, e.g., inspection testing, greater frequencies, etc. When performing the job audit, the auditor shall verify heat treater is conforming to the
customer's requirements.
Please note that the corresponding gas nitriding is Table "B" and the Plasma Ion Nitriding is is Table "H"
OK - Complies to requirement
NOK - Does not comply to requirement (Explain noncompliance in 'Related HTSA Question #')
NA - Requirement not applicable
H1.3 1.18 Vessel is to be free of contamination that may affect the process.
H1.5 3.2 Gas ratios controller / meters shall be calibrated / verified as recommended by the manufacturer. As an option gas composition may be analyzed using gas
mixture analyzer semi- annually and calibrated as recommended by the manufacturer.
H1.6 2.16 All hardness test equipment (for each scale used) shall be calibrated annually minimum, and verified daily or prior to use, per the applicable ASTM standard,
ISO standard, JIS standard, or approved standard.
H1.7 2.16 Files for testing hardness, if used, shall be verified per the Customer requirement.
H2.5 3.5 Temperature shall be controlled with thermocouples in the load for each batch placed as practical to represent the extremes of the load (max and min
temperatures) as evidenced by recording.
H2.6 3.2 Infrared pyrometers shall be calibrated annually using proper calibration methods or an approved manufacturer's procedure.
H3.3 1.4 Pump down of 75 microns per hour or less and leak up of 90 microns per hour or less Each Batch
2.11 are required prior to initiating the cycle
2.12
H3.5 1.4 Monitor time in furnace, cycle time. Each batch
2.14
H3.6 1.4 Monitor load size or fixturing as applicable. Each batch
2.7
4.0 IN-PROCESS/FINAL TESTS FREQUENCY OK / NOK / NA
H4.1 1.4 Microstructure characteristics including compound zone and etched zone shall be Each Batch
2.15 checked. Microstructure shall be checked at a minimum magnification of 100x and,
400x or above 400x. Microstructural visual references shall be available.
H4.2 1.4 Surface hardness Each Batch
2.15
H4.3 1.4 Core hardness (when specified) Each Batch
2.15
H4.4 1.4 Case depth (when specified) Each Batch
2.15
5.0 SOLUTION TESTS FREQUENCY OK / NOK / NA
H5.1 2.13 Rust Preventive - Soluble Oil
Concentration - when not purchased as a mixed solution 2x / week or as appropriate for cleaning the parts or per customer
and Control Plan
55