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JFUE 1102

Fuel 78 (1999) 905–910

Physical properties of bagasse


M.G. Rasul a,*, V. Rudolph a, M. Carsky b
a
Department of Chemical Engineering, The University of Queensland, Brisbane, Qld 4072, Australia
b
Department of Chemical Engineering, University of Durban-Westville, Durban 4000, South Africa
Received 21 September 1998; accepted 13 January 1999

Abstract
Bagasse is a by-product of sugar milling and important fuel resource for that industry. It is a fibrous, low density material with a very wide
range of particle sizes and high moisture content. It is difficult to characterize properties of bagasse particles in the usual ways (i.e. by particle
density, size, drag co-efficient, etc.). These properties are necessary to apply normal design procedures to, for example, pneumatic conveying,
fluidization, drying, combustion, etc. In this paper techniques to determine some physical properties of the three major components of
bagasse, namely pith, fibre and rind, are demonstrated. Average material properties may then be obtained based on the weight proportions of
the components constituting the bagasse. 䉷 1999 Elsevier Science Ltd. All rights reserved.
Keywords: Bagasse; Physical properties; Experimental measurement

Nomenclature and is the fuel resource for that industry. Bagasse consists of
three components namely, pith, fibre and rind mixed in
CDt Drag coefficient
different proportions. There is a considerable difference in
D Cylindrical diameter, m
shapes and sizes of the three components. The rather regular
deq Equivalent cylinder diameter (defined by Eq.(1)),
shape of spongy pith particles with a near unity length/width
m
dhed Hydrodynamic equivalent diameter, mm ratio can be approximated by a spherical shape. The shape
of fibres with high length/width ratios can be modelled by
dp* Dimensionless diameter, m
cylinders. The large rind material roughly comprise rectan-
g Gravitational constant ( ˆ 9.81), m/s 2
gular particles with high length/width ratios. Some fibres are
L Length of bagasse fibres and rind, m
often adjacent to the inner wall of the rind particles. The
Ret Terminal Reynolds number (r gUtdhed/m)
literature provides some reports of properties of bagasse
Ut Terminal velocity, m/s
particles, for example, geometric properties and bulk
Vpore Pore volume, m 3
density [1]. The literature does not provide an appropriate
xt,xf,xr Mass fraction of pith, fibre and rind, %
r abs Absolute or skelatal density, kg/m 3 method for determining bagasse particle density. Terminal
velocity and drag coefficient of bagasse fibre has been
r bag, Particle density of bagasse, kg/m 3
published by Nebra and Macedo [2]. Both the parameters
rg Density of gas (air), kg/m 3
are functions of particle size and very important for example
rp Particle density, kg/m 3
in design of pneumatic conveying or fluidized bed systems.
r t, r f, r r Particle density of pith, fibre and rind respectively,
Typically, the equivalent cylinder diameter (deq), given in
kg/m 3
Eq.(1), is used to represent bagasse particle size [2],
m Viscosity of fluid, kg/m s
!1=2
a2 ⫹ b2
deq ˆ ; …1†
2
1. Introduction
where dimensions a and b are shown in Fig. 1. This has a
Bagasse, the crushed remnants of sugar cane stalks left general problem in that fibres will have exactly the same deq
after the extraction of juice, is a by-product of sugar milling, regardless of their lengths. As the particle surface will
significantly affect the terminal velocity and drag co-effi-
* Corresponding author. Tel.: ⫹61-7-3365-9067; fax: ⫹61-7-3365-4199 cient, this is not a convincing or suitable measure. Hydro-
E-mail address: rasul@cheque2.cheque.uq.edi.au (M.G. Rasul) dynamic equivalent diameter (dhed) provides a suitable
0016-2361/99/$ - see front matter 䉷 1999 Elsevier Science Ltd. All rights reserved.
PII: S0016-236 1(99)00011-3
906 M.G. Rasul et al. / Fuel 78 (1999) 905–910

Fig. 1. Characteristic dimension of bagasse particles (Nebra and Macedo [2]).

average length parameter in many other systems and is held at 20 kPa (abs) for two hours. The sample was
proposed here for bagasse as well. shaken several times during the evacuation period to
In this article methods to measure the particle density of assist removal of all the trapped air. This procedure
bagasse are presented. Measurements of terminal velocity of was assumed to fully wet the sample and remove all
fibre and rind bagasse in a simple fluidization column the internal air.
provide a convenient method for measuring dhed of these • The wet sample was decanted to remove most of the
particles. Correlations for predicting dhed and drag coeffi- external water. Acetone was then added into the bottle,
cient (CDt) of fibre and rind bagasse are proposed. left for a couple of minutes and then decanted off.
• Then the sample was dried quickly (over about 5 min)
with hot humid air to remove acetone solvent. At that
2. Particle density of bagasse time it was observed that the particles were separated
from each other and appeared visually to be dry on the
Particle density (r p) of a material is defined as the ratio of external surface. The sample was then divided into two
the mass of the particles to the volume enclosed by the outer approximate equal parts.
surface of the particles. For porous materials this volume • The volume of a measured mass of one part of the sample
includes void volume within the particle, for example due to was obtained using a pycnometer (density bottle) with
pores [3]. Direct measurement of particle density is not easy kerosene as a displacement liquid.
for bagasse. Particle density can be determined by measur- • The water content of a measured mass of the other part
ing the pore volume of the particles and using the following was determined by drying the sample in an oven at 105⬚C
equation [4]: until constant weight was achieved.
1 • The particle density was then calculated from the dry
rp ˆ : …2†
…1=rabs † ⫹ Vpore sample mass and the sample volume from density bottle.

The common methods for determining pore volume have


not been successfully applied to bagasse, preventing the 2.1.1.2. Method 2 (Jones [3])
simple calculation of particle density by Eq.(2). Alternative • A sample of pith bagasse is added to a container of water.
methods had to be found to determine the density of indi- The water is then brought to boil and maintained at boil-
vidual constituents of bagasse. ing condition for about 15 min. As the bagasse particles
take up moisture they sink, until all of the bagasse is
2.1. Measurement procedures lying at the bottom of the bottle. The excess water is
then decanted off.
2.1.1. Pith particle density • The wet sample was then dried as a thin layer in an oven
The procedure used is based on the filling of the pores of at 105⬚C for an hour approximately. When surface of the
the particles with water and then measuring the particle particles were just dry, the sample was removed from the
envelope volume in a density bottle, using an organic liquid oven. At this stage, the majority of the pores are still
as the displacement medium. Two methods were used: filled with water.
• Using a conventional pycnometer (density bottle) and the
2.1.1.1. Method 1
water-saturated sample, the particle density was
• About 5 g of dry sample was soaked in water for 48 h and measured by displacement with kerosene.
M.G. Rasul et al. / Fuel 78 (1999) 905–910 907

2.1.2. Fibre particle density can be carried out for spongy pith particle only, because
Twenty-seven samples of fibres were cut into 30.00 ^ these are nearly spherical in shape. The sieve size can be
0.20 mm length and were dried in an oven at 105⬚C for used with reasonable confidence for designing processing
several hours until steady weight was achieved. Considering systems such as drying, combustion, pneumatic conveying,
a fibre as a cylinder and measuring its diameter, the particle etc. The other two components, fibre and rind particles, are
density was calculated. The fibre diameter was obtained by difficult to characterize by sieving and the sieve size does
Nikon shadograph. not provide a meaningful size (diameter) measurement
owing to their strange and very non-spherical morphology.
2.1.3. Rind particle density An alternative method is necessary to determine a mean-
The particle density of rind was determined by cutting ingful characteristic length measure. For these particles,
sections of rind into rectangular slabs. The volumes of the hydrodynamic equivalent diameter (dhed) seems appropriate
rectangular slabs were calculated by measuring their dimen- for many system design requirements. The dhed can be deter-
sions using vernier callipers. As the rind particles may mined by measuring the terminal velocity and particle
contain some sugar and other solubles, these were removed density. The terminal velocity can be measured using
by immersing the samples in a relatively large quantity of fluidization technique.
water for few days before drying in an oven at 105⬚C to Given the terminal velocity of a particle, Haider and
constant weight. The density was then calculated using dry Levenspiel [7] present the following useful approximation
sample weight and measured volume of slab. Five samples for spherical particles:
were taken into account for this density measurement. 2 31=3 2 3⫺1
r 2
 5 ˆ6
18 0:591 7
Ut 4 
g
2.2. Results and discussion 4  2 ⫹  0:5 5 ; …5†
m rp ⫺ rg g d*p d*p
The particle density of pith was found to be 20 ^ 20 kg/
m 3 using method 1 and 240 ^ 10 kg/m 3 using method 2. where the dimensionless diameter d*p is given by [8]:
Clearly, both of these methods depend upon the sample
preparation procedure to get an externally dry but an intern- dhed
d*p ˆ h   i1=3 : …6†
ally fully wet sample. Both are prone to some subjective m2 =rg rp ⫺ rg g
error in this aspect. A pith particle density of 220 kg/m 3 has
been used here, as method 1 seems less liable to operator If Ut is experimentally measured, and the system proper-
discretion and arbitrary experimental judgements. The ties are known, then dhed can be calculated for a hydrodyna-
density of fibre and rind particles were found to be 520 ^ mically equivalent (fictious) sphere from Eqs. (5) and (6).
10 kg/m 3 and 550 ^ 20 kg/m 3, respectively. By contrast the When a spherical particle of size dhed falls through a fluid
skeletal density of dry bagasse using a multipycnometer was at terminal velocity (Ut), its drag co-efficient (CDt) can be
found to be 1470 ^ 30 kg/m 3. This compares with 1330 kg/ estimated from fluid mechanics by the equation of sedimen-
m 3 (Crawford [5]) and 1510 ^ 10 kg/m 3 (Pidduck [6]) for tation of a single sphere in an unlimited environment
dry fibres of bagasse. 2   3
The average particle density of bagasse was then deter- 1 4 4dhed rp ⫺ rg g 5
mined from the measured density of the components and CDt ˆ 2 : …7†
Ut 3rg
their proportions using the formula
1 x x x
ˆ t ⫹ f ⫹ r; …3†
rbag rt rf rr 3.1. Experimental
where The equipment used to determine the terminal free-fall
xt ⫹ xf ⫹ xr ˆ 1: …4† velocity was a simple fluidization column. The column was
made of perspex of inside diameter 25 mm and total height
In a typical sample, the proportion of pith at about 5%,
of 2 m, fitted with a porous plate distributor at the bottom.
fibres 73% and rind 22% by weight was found by mechan-
Air was used as a fluidizing gas. Air flow rate was measured
ical separation. Using the formula given in Eq. (3), the
by rotameters.
particle density of bagasse was found to be 492 ^ 15 kg/
Fibres and rind bagasse were loaded into the fluidization
m 3. Hence, the voidage in the porous bagasse particles was
column. The air was then gradually increased until the parti-
found to be about 66%.
cles floated near the middle of the column. From that point,
if air flow was increased further, the particles eluted from
3. Particle size and drag coefficient the column. The velocity corresponding to steady floating of
the particles was taken to be the terminal settling velocity
The particle size distribution of powder is generally and was recorded from the rotameter reading. The terminal
described by sieve analysis. For bagasse, this sieve analysis velocity was used to calculate dhed.
908 M.G. Rasul et al. / Fuel 78 (1999) 905–910

Fig. 2. Bagasse terminal velocity as a function of dhed.

3.2. Results and discussion terminal velocity increases with equivalent cylinder
diameter (deq) in the form of
The hydrodynamic equivalent diameter (dhed) of fibre and  0:397
rind particles were calculated from Eqs. (5) and (6) using Ut ˆ 2:41 deq …9†
measured terminal velocity and particle density. It was
observed that Ut of these particles increases with dhed, as for 1 ⬍ deq ⬍ 6 mm (Fig. 3). Direct comparison of terminal
expected, with the following form: velocity cannot be done with their data because insufficient
ÿ  information is recorded to calculate dhed from their data.
Ut ˆ 2:96 dhed 0:58 …8†
However, the terminal velocity calculated by their method
where dhed is in mm and Ut is in m/s. Fig. 2 shows the shows significant scatter compared with their data (Fig. 4).
relationship between Ut and dhed.Nebra and Macedo [2] The data from this study is also shown in the figure and
measured the terminal velocity of fibre bagasse in ambient compares well with the calculated values according to our
air by allowing the particles to fall from heights of 4 and method of calculation.
6 m. and recording the time required to fall. They found that The drag coefficient of these bagasse particles decreases

Fig. 3. Terminal velocity versus equivalent cylinder diameter (deq) for fibre-type bagasse (Nebra and Macedo [2]).
M.G. Rasul et al. / Fuel 78 (1999) 905–910 909

Fig. 4. Comparison of measured and calculated terminal velocities.

exponentially with terminal Reynolds number as shown in reasonable for correlation with drag coefficient, because it
Fig. 5. An empirical expression for the relationship is, implies that a long cylinder will have exactly the same drag
ÿ  coefficient as a short one. For bagasse (the hydrodynamic)
CDt ˆ Ret ⫺0:1 ; …10† equivalent spherical diameter seems a more appropriate
for 342 ⬍ Ret ⬍ 2653 with a correlation coefficient of 0.972 parameter for expressing terminal velocity and drag
and Ret ˆ r gUtdhed/mg. Drag co-efficient data of Nebra and coefficient.
Macedo [2] who used equivalent cylinder diameter for
Reynolds number calculation is shown in Fig. 6. They
expressed these data in the form of 4. Conclusions
ÿ 
CDt ˆ 2:07 Ret ⫺0:242 …11†
Particle density, hydrodynamic equivalent diameter and
for 10 ⬍ Ret ⬍ 2000. The use of the equivalent cylinder drag co-efficient of bagasse are basic data for the design of
diameter to calculate Reynolds number does not seem systems such as drying, combustion, pneumatic transport,

Fig. 5. Drag co-efficient of bagasse as a function of terminal Reynolds number.


910 M.G. Rasul et al. / Fuel 78 (1999) 905–910

Fig. 6. Drag co-efficient versus terminal Reynolds number for fibre-type bagasse (Nebra and Macedo [2]).

separation in cyclones, etc. Methods for determination of References


above physical properties of bagasse have been addressed.
A new method for particle density provides a useful addition [1] Ponce N, Friedman P, Leal D. Int. Sugar J. 1983;85(1018):291.
to the methodologies available for experimentally obtaining [2] Nebra SA, Macedo IDC. Int. Sugar J. 1988;90(1077):168.
[3] Jones PJ. 1981. Downflow of gas-solids mixtures in bottom-restrained
this information. Measured results for physical properties, vertical standpipes, Ph.D. Thesis, Dept. of Chem. Eng., University of
including particle density, terminal velocity, drag Queensland, Australia.
coefficient and hydrodynamic equivalent diameter, are [4] Geldart D. Powder Technol. 1990;60:1.
given together with simple empirical equations which [5] Crawford WR. Proc. Qld. Soc. Sugar Cane Technol. Australia
allow the properties to be easily calculated. The hydrody- 1954;21:p.132.
[6] Pidduck J. Proc. Qld. Soc. Sugar Cane. Technol. Australia
namic diameter is convenient length dimension for use in 1955;22:147.
standard hydrodynamic calculations. These methods can be [7] Haider A, Levenspiel O. Powder Technol. 1989;58:63.
used for physical properties determination of any fibrous [8] Kunii D, Levenspiel O. Fluidization engineering. 2. Butterworth Heine-
biomass. mann series in chemical engineering. Boston, MA: Butterworth, 1991.

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