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SemustY Quality Produ,
PHYSICAL PHARMAEVTICS-T (3

re

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A
StandarD
9nDE SHIKSHAa

Ca

Ca
Sr. Date of Date of
No.
Experiment PageExperiment Submission Remarks

0LTo deleminut Aolublii of oL.

_chug atI0oM -Mptradus.
a

a
02. To deternau pka valu by 64
rm

rm

rm
hulf neurilizahim tHandersan-cq
ha

ha

ha
DS.T deeminn Surfau HOsim_ofE
given Lquid by drop wigt muhod.
lP

lP

lP
0
o5.Todekemint th partihion coefkident
el

el
Ofenzoic aid in_benzenu_nd watr
w

w
O4.Dekeinahm of Specific_1dtatim 09
re

re
ot qjiven sugar Soluhon_and also
Ca

iport percentaga olu_LOMposittm_of

given Solution_using polanlmker Ca
t6T deleriatha parhition Loetficient_Y
ibdins inwoler ond CCly
0To determiu th Surfhu tonsion1
a

of ghen liquid ny drop_coun

rm

m
ar

ar
O8.Tdeltmina th HLB number_of 19
ha

Ph

Ph
surfacbrnts by saponufiotom muttodl.
lP

09. To dektrmlnu Hh staitiy (onstant

l

l
el

el

and donor eptor ratio of pACA-

Cofeina complu.x
by solublit mHod
w

w
re

re
Ca

Ca
a

a
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- ol
Ca

Ca
pulmant NO

im To delumunu of drug oloom -emp

a

a
rm

rm

rm
, stiu,
ha

ha

ha
Requimun- fpuratus -fAmlyic balonuu, Beska, thurmosjat
lP

lP

lP
W-Visibl spectoprolomdtn pspaiti
ar
el

el
Chunl Cal Pansetamol, Distilled
w

w
re

re
Ca

Ca
soLUSTLTTY XPRESSONS
a

Deoiphive tam
rm

m
fo paut of solule.
ar

ar
ha

veuy Solubl .lOM thon

Ph

Ph
fieely Solution
lP

Splubl 0 30
el

el

Spoalngly vblu 30- 100

w

SLughty Solubl 16D- 1000

re

re

Vey Sughtly gzlubls lo00- lo0oo

Ca

Ca

auially waolublu o ingalubu MoU non lo,0000

a

a
m

m
ar

ar

ar

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Expt. Page No.

Ca

Ca
EXpcuimmunt
NO0
|im-b _dtlkimis Jolubuliti e dug at10om -Jemperahud
a

a
cleunu-Tanvir Y»Shákh Md.Rageb Vman,O1.Siro nsháukh_-
rm

rm

rm
BaMawaray endgumbla,
ysitl pharmotvlio-I Nirai rokashon.Itihi
ha

ha

ha
&equitnun Apacatu Beake, httnostat, Sht.,_
-Analylic balanu
lP

lP

lP
Uy. visible Spethophotnute eiputt.
el

el
hnuicay Panacetamol Distiled Wake
w

w
re

re
heary intiple Th solueltiy _and dissolulion propeshies of
Ca

Ca
_dvugs Perfoun a valuabluptAE olk in tn
procA) of-formvlahon deuwlopment

Soludili = Te moaimum_amount Of Solut

per l00 nl/am
padicksuhith
Con b in
discolved of solent ia
a

Calltd ADlubulitiqO druq

rm

m
ar

ar
ha

SaturakdAolunom_cí dug Anoumal trp,

masinum amount of
Ph

Ph
lP

SOluk disolvecd In solule (that_ situahn lo hichwe

l

Convnot add mok olule in ADluhiau)at noimal_mdann.

el

el
w

)_Unsaluralrd Alution_bf_dau
That SOluhon in ich add mou
re

re

3olult eAsily in Solulion

Ca

Ca

ii)Supe Aatualtd_duhion duglhat solulion which_tOntaina

Teacher's Sign
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a

a
rm

rm

rm
ha

ha

ha
lP

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el

el
w

w
re

re
Tihahm
Ca

Ca
0N
NoO
a

a
rm

m
ar

ar
ha

Ph

Ph
Ponocotomsi
lP

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Ca

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Expt. Page No. 2

Ca

Ca
mOH dissoluecd olule ihon fon_p:¢paAing
Kouitdfo a avraltd
tuhion by healinga boluhon

Impoatant Of Solueiki Deta minatin

Soluhilutyis onDh Impoltuw_panamuktrs -jo_achiev
a

a
rm

rm

rm
desired Loncwtraion o du ia Suslemalic catulahon fon
ha

ha

ha
achievino kquied phamalogical responce
Solubitildeleaminohion is impostau in -ormulain of
lP

lP

lP
dosags-am alo_pxdichim of tokillij_on dot 6E dro
el

el
w

w
Protedu 3
re

re
firstiy clean alu th mersayqlasswoe
Ca

Ca
Now, Makpths mtuaatedAoluhonm of Paracetamol by
adding in walt ot rOom empLatuu
ukenthu olutiom ung flkaolutim
NO daR hiu AatuatedL oluhon comcical-ftask
dufeunt luk L0_Vnd neouh (mcical lask)
a

daopsof phnophhaleu indicato.

rm

m
add 3-4
ar

ar
in aJoluhon
ha

Ph

Ph
No
tira thuu 30luhnwih 0N Na0H_
lP

pinkolon indicalta encd poínt

l

idi o ttu
el

el

Hhue A0luhon aud noke reading of

w

bumeite
Nou pu n fomula axd
re

re

h3 Valu Calcolat
t
Jluealiof
Ca

Ca

dug

Teacher's Sign.
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Ca

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Obstwahon_
Bitl Reoding
Avenag
I
Ponace taml
dug Aclunon T+I +TL
3
a

a
in wal
rm

rm

rm
ha

ha

ha
lP

lP

lP
el

el
w

w
re

re
Ca

Ca
Kesult Solubuli Fponacotmol an ubiu. aroom tenp
J ma idn.
a

a
rm

m
ar

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ha

Ph

Ph
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Ca

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Expt. Page No. 3

Ca

Ca
Calulakn

NV,NzV2 wh N (ont. Df panacAanol

V=Voluu_of_panutotamol|
a

a
NE NXVLVz N (oM. Of Na0H
rm

rm

rm
VVolof NaoHL
ha

ha

ha
(buudetallka )|
lP

lP

lP
Solubili Normalua_(N) MaAs_equivaltur [paacutaool) 2 olum of
el

el
otdrug Soluhonin L
w

w
re

re
ponatQambl 1S1-163
Ca

Ca
g7mst

RAult Solubulutofpauaotamol in_uakl _a

room-empirafu
a

a
rm

m
ar

ar
ha

Ph

Ph
lP

l
el

el
w

w
re

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Ca

Ca

Toacher's Sign.
a

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Xpemuu NOO02

half neuhilizatim
fri To delcmL pka Volu by
tHanderson tasetbajeh eqvahon
a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
Ceqitmonts
el

el
Apparaus > urett sud (Owial-fusR Btier
w

w
Chumiol M Na Sol m auhit aud sol, Phund pholain,
re

re
O'ilbd wa
Ca

Ca
pH pka+ logHoo/ coD
a

a
rm

m
pka pH-log CHcD Co
ar

ar
ha

Ph

Ph
lP

H+ Ch LODHH Chcetc ocidJ

l

l
el

el

Ka CHI Ch
w

CuncoD1
re

re
Ca

Ca
a

a
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Expt. Page No. 4

Ca

Ca
Apeaimunt NO= 0
Aim o delemi pka valuu by nol nuilizahom/
tHandexson Hasdbatth egyahn.
a

a
rm

rm

rm
ReketnTnvir shikha Kageb MAKman DIirag Nt eh_alawaro
BendeoumbAPhusiol PharmaQuio- I, NIoli prakuh T edihn
ha

ha

ha
.
lP

lP

lP
el

el
fpporauA Burethe staud, Conical HasRSjiitpipette
w

w
Chumirals IMNaotlAo M auticaid lPhunsptralein.
re

re
Disiludwaltr
Ca

Theory Ta piAfacelic huer An_b Ca Caltukckd rom

ha dissociatiom (DIaut (ka) Of t ROR add and
tha Concovration OF th acid andl salt usidL
DissoclaHon_o ak Acd Qud Aalks al
a

HA e H A((weak actd)_
rm

m
ar

ar
BA
ha

Cowaion effcct
Ph

Ph
lP

sy4pplyiung mass Oactim,

wdf
l

l
el

el

KaCH'](n-J
w

CHA
re

re

On Rearongk,
Ca

Ca

= CHA]
(H] ka
CA
Teacher's Sign.
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Ca

Ca
Gdtte
NaoH M)
a

a
sfand
-umetlc
rm

rm

rm
ha

ha

ha
lP

lP

lP
MAuhic phenaphalein
el

el
aud
w

w
re

re
Ca

Ca
Cpaiom dt actic ocsd (Ha( CoHH)
a

a
rm

m
ar

ar
ha

Ph

Ph
lP

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Ca

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Ca

Ca
HA Add ohd CA Salt|

CH+ kaCRcia )
CSall J
a

a
Taking-l0q &n sids
rm

rm

rm
-leg CH
ha

ha

ha
=_-lo kaCfcid)
Csals)
lP

lP

lP
-109 (H]= -bgla- log (cia)_
el

el
Sal)
w

w
lg H)pHandlbgka pka
re

re
Ca

pH pka- lbq CAci41

CSalt Ca
On KeaLanga,
pH= pkat bg Salt)
CAcid]
a

a
rm

m
ar

ar
ProceduuL
ha

Ph

Ph
Wash all_ u_ ppoial t distilled_walkI
lP

|4il burttk ih dHad IM acthic thn naw a

l

atid
el

el

bubbl Gud Su pou aF0

w

3No A LOniCaL_ f1ask -tem pwetk

re

re

ueipehk ou lo of ate utd beaRur -from_

Ca

Ca

COniol-Aauk wtk u htp ofE bulb pute.

5Noud Odd 3drop Of_phnapthatelu udicotok aud coutolfiak
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Ca

Ca
DbwvahM
Tbation Result ial
quivalunt point pH| a.3
pH ef haA nubilizai 3.2
3 2
a

a
rm

rm

rm
tlaudason Hasubatth ea
ha

ha

ha
Coloulot th pka rom albove readuno
lP

lP

lP
pH pka+ loq CSott]
el

el
CAcid3

pka3-2 -+ O
w

w
pka pH- log
re

re
pka 2-2
Ca

Ca
a

a
rm

m
ar

ar
ha

Ph

Ph
lP

Hol bilia
l

l
el

el
w

w
re

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Ca

Ca

Kesu- T pka valu, of gven Aawpla.

o b 32
a

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Expt. Page No. 6

Ca

Ca
mule
6Now (hudk pH f 45 in onicol ink_ using pH
bumtk Od JM NaOH S
NA Ne akanothtn
Ao of(DNICo awk(atetit at) througkh_butte
RTMunHhai
aAhake w_duikg itadiug
a

a
) Lik celoL Cpexemauent) Mdicaksaa end pouE
rm

rm

rm
InNst dm t eoding of buuellt _Qnd Lheuk t_pH Bf AI
ha

ha

ha
Couial flk. Cacenc_acid) w
acohe acid (wuiun plte ouF inbekr
lP

lP

lP
12) Abu),_add10 lll of
is ticalfisk un Ahakr wl_pixk tolon_diapplad
el

el
13Aga M NaOH A01 bunctt-3timu
through
w

w
uhqaun Cuck tu_pH o ol attL_HOlh €ndà point
re

re
NOWCalulat pot pka valuu ihtoughobsyotim
Ca

Ca
Losudt T_pka Valuu o gien AanmplL
ob
a

a
rm

m
ar

ar
ha

Ph

Ph
lP

l
el

el
w

w
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Ca

Ca

Teacher's Sign.
a

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Ca

Ca
puiMunt Na03
Aim To delexmintsnfau yenvin of given Aiquicl b
drop weish muthod.
a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
el

el
Rrauiemant
w

w
ChuiCalA Test sampla, dislillud waln
re

re
Appouotus Bualaer, Atalagmamutr, Ho a cven, weughig boltu,
Ca

Ca
duguta Dalanu
a

a
rm

m
ar

ar
ha

Ph

Ph
ulb
lP

l
el

el

Stalaqmomte
w

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Ca

Ca

apillg
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Expt. Page No.7

Ca

Ca
Expediment No23
dettmn SuIfau tnion of qjin uqud
by_drop
mutod
a

a
rm

rm

rm
CeahcLTanuir T: Shaikh Md.Rageed Md- Uumon_Dr. Siraj n shwkh
ha

ha

ha
BaAauWara_Sendagumblu DusitalPharmaceustta
I
Niali Aakishon-Tst edition.
lP

lP

lP
el

el
Reauv&ur
w

w
(huncals Tt samblu distilad watr
re

re
Apparahu Reakur,SalagpmonutkHot oiv OM Ighin bottie
Ca

Ca
digutal ulanttBeakev.

ThebyTh Sufau Jnsionis defind ak t r ating withing

Surfau n diretion normal o li DE
m in_
lemah
a

muthdd u
rm

m
In stalagmomskr ULd._
ar

ar
-for t Mnt
MIOAUA
SvLfaatnsion Involua (ovnting of
ha

of_drops o
fotmud hn_Lxat voluu Liquid
Ph

Ph
numbir
lP

i allo o fou souly diopuwi fiom stalaqnut

l

Capullauy0uie.
el

el

Th rotio of weigkeef drop ofLqud to that_ofl

w

W
re

re

yefererre SUDstavua falungtom Aam (opilluy

Drifte JA equal ratioOf j SUrfac_tnslam.
Ca

Ca

W +es -
is SUysacl ttniom of uid
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Ca

Ca
Obsevatim
Suufoce Hnston
wean of dnopp
. |MateuiaM
Wale
Xyu.
iO.02
0 023
12 5
69-7 find
a

a
rm

rm

rm
Caltulah om
ha

ha

ha
wt weghibott O.uug
lP

lP

lP
w ofwan dnsps|+ wugnin botul 0.92
D 0-484 (20 weln do)
el

el
da deps o.92-044q
tof
w

w
wt walu dnep =O.yg .024 4. W
re

re
2.

.
of tt liquial dupj+eahúnq 0.4o o
Ca

Ca
botty

t tt liqusd daeps 0.90- o.44g 0.469 l20deP

tf u4 et) dare
60.022
2D
Nou, (suvfau tnion wau
a

of 72
rm

m
ar

ar
aSurfou tensten ofALugud)
ha

u2
Ph

Ph
lP

W 12-1X O023
l

69.7
el

el

0024
w

w
re

re
Ca

Ca

Rsult- TH itfau tenu xylun b dADp Ough

ugkk
muthocd
iu 6 dynu mM
a

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Expt. Page No. 8

Ca

Ca
frocodu
hlyclean
LThroughly lalag momuleyUsing_chronic add/puuifitd wat
Stalaamomuler must kt mounitdin vertitoh_plan using dampa
mas of
3wkih
- th wghingoH
distilud olu mmursu H botom
a

a
beaker th do -fal
rm

rm

rm
end ofAtalaqmonuler into wat andiuJ
fallvto_pH-uxinh
ha

ha

ha
5Alou 10-20drops of dictilled woltto
id MOUh
lP

lP

lP
bh tu ughing botHe along wih p-I_diop of wakt
el

el
Repaa eAperimuat 3- tiMu
w

w
Walh Afalagmoruler uithWaktr
re

re
aiu t Aalogmomtr wt tAt Lguid
Ca

Ca
9Al 10-20drops 4 n_xLghin batHe
uMk 10-20 drope Of
I h weighing- bolile
ol-
Repeat Rxpeimnt 3-4 iu O aua.cy
JaNOw Colcuc OccoLdiug (uin) H hilp fosukaion
a

a
rm

m
o
ar

ar
Rosul- T Aur au
Ajm Xylonu ky deop ughE_
ha

Ph

Ph
Muthadis 69-7 duynn)um
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w

w
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Ca

Ca

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peimAnt No.0

Aim- DHemnahon of Aprufic oTahon af given Agan

Aaluhn and aluo epout prcAt wuCoMpocition)
9ven Aolv han v
a

a
polanlmjer
rm

rm

rm
ha

ha

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lP

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Ramuidtmunt Volumubic fask, buake, pepd stdum vapow-1awp
w

w
polaimak SUCoc diutilu o
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Ca

Ca
a

a
rm

m
ar

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Ph

Ph
lP

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Expt. Page No. 9

Ca

Ca
Expeuuer No 0
Atm Dekiminahn ospuifit.rozathnDf genuga
Aolutin And _alao VepoxtPrttnl pexAnt w/u- (ompositim
of gien Aolution_singpolauimukr
a

a
rm

rm

rm
:
Reyaenu-Tonir aukh Rageeb.Ad-Umon_Dr Sirag n sai)_ Baxauar
ha

ha

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Rendtqunilayslal_poaacauita-1 Nioli ooshan Tt_ediHen
lP

lP

lP
reman-volumebic
el

el
Reaui -10sk beaker_pipet sodivum VapDLAlamb
w

w
pDlanimutHyULIOSK disjilleA wak
re

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Ca

Ca
TharyA subsjan hith1afalks_jh_ plantA Ofpolaizd4
calued phically Quhive ageut
T th rojaion ake place inclotk wisu diuctinut u
Ldexpon rotzutory
plau in antidokuwic diretHint
ak
a

Calod levo levo Yojardry

rm

m
ar

fwo pa polaising_ elemuns

ar
ha

P Polauimmtey H Conut_of
Ph

Ph
(polaúzar)
of polaroid On Of_whith isxtd
lP

Oturs is a onaluztrCapabl Of atatin and

el

el

MDUttdL iln aqraduattd ClrcularAtall in ordtr

w

0_mAAUA. is orienjahinwth teapiet tint

re

re
Ca

Ca

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-
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beervohon

Ca

Ca
Spiaic rotuhon
S NO (on of SUuosa
S% 134

10
a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
Spaific ootahon DX
el

el
w

w
wl, Rophoctohon
re

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lngHh f polauimmtu
of Avbsjana wlv-
Ca

Ca
Conanhaion
-t for s. çol 0DX1s4
14XS I1x10

Is7 -73.4
X3s 2. 5 13
a

1XIS I7x 28
rm

m
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Ruul
Ph

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ThL Aprufe
Th rotahon of given
lP

anpl was1
l

a) foL olunon Is3.64 +)

el

el

b)-fr 1o7. Boluhion 64. +)

w

)fo 1S7. Aoluhon 33.y (+)

re

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a) for 2o oluhion 146 (+)

Ca

Ca
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Page No. 1o

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Expt.

Ca

Ca
Proceduedurt
JCleanhpolaaIur amplu u wih_dishillod wakr.
Hi_AOupla -vht wilh distlud waltr ighy-
Ih (oap inorduJo_pesunt 1eakagA Af_søl

3Plac Aambl ub in polaAmltk.

a

a
yRotatu h halves in_ Drdtto
rm

rm

rm
analyzaron boh
Viu
ha

ha

ha
SNOE t veaching atop LiLular Atole
lP

lP

lP
aMon ACalu readu Od vmbir _pf_dMsih
Louaining u
el

el
Atale 8.
6. Nott _RadungO Oftetatiag rotatim.
w

w
re

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By turning 18 louLporhM
More_ yeading
Ca

Ca
OnL
Clean t Sampli
Mluticn
juba fi wih lowe_tnerahnH
SUgor
9 Kepiot prored u rm 3 foFim
lo.NoteYeacdungAgain Uutil h tonantahm ALCoalek
a

OA MLnHOnndL
rm

m
ar

ar
ha

Resul
Ph

Ph
rotahion givenAomble WAA
Thspeibi
lP

apr SSblution 15764(+)

l

l
el

el

b)for l67. 5oluhn 647 4)

w

Der ISZ ADluhon 33.(+)

re

re

dfo 2o olwh 1bU Ct)

Ca

Ca

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No,.0O
pimsn
poritin clicieu oF banzole acd:
Aim To duermin h
bunzun and wa q
a

a
rm

rm

rm
h.
ha

ha

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lP

lP

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RequinLOv
Groduole
el

el
Apponatu Sepauatouy fmnel, uetic, conicol -fusk, piptte,
w

w
ylindunVolumaluc-flusk
re

re
Chenmico Bunzoic acil, Bunzns Diuiled akn , Sodium
Ca

Ca
yduoxide phantlpholja Lndicajdn
a

a
rm

m
ar

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Ph

Ph
lP

l
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Expt. Page No.

Ca

Ca
E2peumLnt No. O5

i To
in
dekrmina
ben2zen nd
mahim_(ocffiuent_of
walt
benzoil acid-
a

a
rm

rm

rm
RactenTonuir D: Sio n.oikh,Lanuara
Soikn_,Ma-Rageev, Md UAmon
ha

ha

ha
BenduaumblaPhystiolphaanaxcuhtu1 Nirai_prakaban,Tedrhon
lP

lP

lP
Requremont
,
el

el
Apporadus Stpaatr -funnl 8ucti,_Loniol flaAR_pipitte uaduoka
w

w
ulinday VolumuhicfIsk
re

re
Chimicola Ben xit_AidBenzenu Distillod_waltyodum nydaoxiAL
Ca

Ca
phun olputhaltin inditatne

Thaohy Pyincipl
I u Vd a -find ut thu nahuu OF
olul pautitles [unknownduwg ie_drg iA lyaphlir er
hydrophilu
a

isHy akL pahially miSubla_binay A0 thn mla drug

rm

m
ind tnat binan Ao thin Ahaks t
ar

ar
-paopuul
ha

Ph

Ph
P- Xo whuho
lP

Drug disolue in oil phas

l

Xw: Drug diuolue in walt pha^

el

el
w

w
re

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P = yophillc
Caq
Ca

Ca

PAL HydAdphulic.

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a

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rm

rm

rm
ha

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lP

lP

lP
el

el
w

w
re

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Ca

Ca
Observohionu
1) Tep Ropmtp=

Bottle
NO.
Vo.Vo Na Coa lbg Coq logCoq
a

|A
rm

m
ar

ar
ha

Ph

Ph
lP

D
l

l
el

el

Man ponhtion Coefficlevd (k)=

w

wh
re

re

Vorg Vo lymi of NaO (organc) NovqNormali of arqanik lur

Ca

Ca

Voq Volvna of NgGn (oqveau oluhien) N Nor malibty of aqvavt layer

Jtorq (onanhahm fbtnzoic (trgovit) K- Paatitiom
Cocffiuet of-
Can= Conch oF bunzoit(oqueay
lour) bunzol aud
a

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Expt.

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Page No. 12
Procedu

Ca

Ca
Phpoa appmk 110m
2atuolcdSo benzoioúd jo_ onzns 0O
UL t Atotk_ Soluhon
Hpa
botHe Qnd
iollouwingmiatua
labl um0 a A, d .
in -ou zporstion- SsppnBh 1eagtn
a

a
rm

rm

rm
Bottlo NO. Distilled whkr
(M)|Stur, ot* (n1) asrtrs(ml)
ha

ha

ha
A
50 40
lP

lP

lP
50 30 20
50
el

el
20 30
10
w

w
Placo stopptys on each boftle
r
re

re
betty
ordAhobetum 3 min
d pneudakle reproducible esult
Ca

Ca
tffecive shaking
Tower u mixtuar in sepanoling uanels labeled
i mst
AR
Cond D 0nd allbu m o stond o 10 min ta sepa@o
th Jayus.
Lollec opaAo Drgani aud 0quLOS layur in dny binker.
Pipethe but 10 m of aquous lager
dihal aqaua
a

a
rm

m
-D N SDdium hydroxid (NaoA) Solukim ing3 dropsof
ar

ar
phunolphthalein DA ndtotor. The
ha

td pbirnt
oppmrre of_pink (olor. let t iRr eadingi
dektkd_as_
Ph

Ph
th Vag.
lP

Pipte out Jo c ONganl

lay Qud Rauetr
l

to_dy_ovital
el

el

flwk usfng dy pipit ll Tibar t h agamt 0N

w

Nob So0 uSing:3 drops o phunelphthalen a indialor

re

re

The end_point isdelcdtd0A0pptaant opirRColo.

Ca

Ca

ijer eading_ Vog

Repa cp
6 nd 1p a temainin Samplos
Teacher's Stgn.
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a

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rm

rm

rm
ha

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lP

lP

lP
el

el
w

w
re

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1
Ca

Plot
t groph of &Y-0a) V.
Ccmg
Ca
aCx-axis)
a

a
rm

m
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Ph

Ph
lP

l
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Ca

Ca
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Expt. Page No. 13

Ca

Ca
Calculahm.=
aqueaUSlayer
(Oncouldalin dfbonzoic. _add in _agvoVs_10yay(Naq) oE
bstite
NiV N2V2
a

a
rm

rm

rm
N=061 AV2H_ Naq
ha

ha

ha
Concenhohm of benzoic Cauid In 0Qts loa [ Coq)
lP

lP

lP
el

el
0-01 AV2 X122
Cog molus/
w

w
re

re
Simlonly Colulatd (onceukeahn of_benzoic aud in qus lap
Ca

Ca
oFotiy_botleBand D.

ulfor orqamcayn
NV N2V2
Naq. 0TXV
a

a
rm

m
ar

ar
CDA Corg. 0.1 XV2 X122 melus/L
ha

Ph

Ph
lP

Similanly Colulálid (ocouloam-for Hu bottluu 8.C4 0

l

l
el

el

toeffkdent_of DuRo
w

palihn
re

re

distilod wal iA
Ca

Ca

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Expuumun NO- 06

hion (oeffiaet of loclina in

Atim TD dulemint tHu pauj
nofe Cly
a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
el

el
w

w
re

re
Ca

Ca
a

a
rm

m
ar

ar
ha

Ph

Ph
lP

l
el

el
w

il 2E
re

re

:
Ca

Ca
a

a
m

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Page No. 19

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Expt.

Ca

Ca
Lspoainunt No d

fim dtla im th paaitimcotffii of iodinu n uaktr

an Coakn Henathloid.cy)D
a

a
rm

rm

rm
Ceguiermentt-
tchachlonids, 0:1N
alChnitals-Disilud waltiodinn_oystals corbn
ha

ha

ha
Soaiun tiosulphät (NG,S,03)0.01 N Sodium thiosulphai Stach inditsto-
ek
lP

lP

lP
bGlauunu Sepaatinq -funngla,_Yeageut botttea beakers burettt

.
piputtt stand (oita flask eltchonit ighing mothniL
el

el
w

w
re

re
RnuTanvir saukh, Raqeeb, Md- Usman, D Sirat N uph _Baauarn_
Physial_phamoLutic-T Nirali Prakahan t eautian
Ca

Ca
Bendiugumbu

Thedy Th pauhtion o-cflitientis defind as thYatio cf

uaionized_dwg tisbibutd bloorgantphisu_andaqLxaJ_
ph a equlibnivm.
a

Moleculan tai of icdin in

both th soleut ctly-
rm

m
SAmA aA
Taud hunu th pautihm
ar

ar
d
ha

Cbeffhtient goaticallyindepclut fcomchhahin in dilutr

Ph

Ph
lP

Sol
l

Hont tnU_ dsbibutimn u Lpauhhion_coatficieut) in i sinplu

el

el

-fom MAy Dt applied

w

w
re

re

K o1L- Ca
Ca

Ca

Coua

Teacher's Sign.
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Ca

Ca
StotR (onbm
Distilud
&otttu No. wotur (mL) Solon(m) Hnadlouda (ml)

A 50 40
SD 30 20
a

a
rm

rm

rm
50 20 30

D
ha

ha

ha
10
lP

lP

lP
el

el
w

w
re

re
Ca

Ca
tcnb: Room ttmpurtw

Battl
a

Varq. Voq Moq Na

Nog
NO
JCar Coo lo Cag a
rm

m
Co
ar

ar
A
ha

Ph

Ph
lP

l
el

el

D
w

MOn poahtion Coeflicievt (K)

re

re
Ca

Ca

SOmd 0 Cxp.ro.3.
a

a
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m
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Page No. 15

Ca

Ca
aedw
D Prepa0ALapp20ximakly 1dn satualed so o_iodun in_tanbn
thaloudL and avnd
USLita AtocR sSolution
1) Phepoufolloum mlxuuin fu_sepaalu Yeagtbotil2A_and
lanl hem 0AABand D.
a

a
rm

rm

rm
SnmE AS EXP. No. 3
3Pla Atoppxs on eath botlu4 shoks fo 30 mn.
ha

ha

ha
thum
ansfethAR mixhuu in seponatig -fuonula Ca.8.40)and_allou
lP

lP

lP
thum
el

el
5ColleAc sepanat OrganavudaquiDUL layrs in y boRAL
a
w

w
Pipate Out10 m of arganlayer into cortainina
o
re

re
m wot plus gm potassium ioluds
0 (k) Using_y_pupit
Ca

Ca
and ia agains DN Sodaum thiosulphal Usig -3
drop Of stanh solunon as dn inditalorLnd point_pink to zdaudes).
EPiput Out 10 m Df Vppur aquu laya uing du
RLRLtt And bti AgauidF0.01N Socdiuhioulphatr
Lvsi'ng. dnopof swh Solulom onInditattr ( End
a

blu to0 colorleA]_

rm

m
B duing hahn
ar

ar
Shaks Camt
ha

aRapat step 6 1f_all remalnina samplus

Ph

Ph
lP

Coltnlahon
el

el

aqleouslayur
w

w
re

re

Nomalut (Nog.) a NV =N2V

Ca

Ca

VL
Ni 0.0I X
Teacher's Sign.
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Ca
a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
el

el
w

w
re

re
Ca

Ca
a

a
rm

m
ar

ar
ha

Ph

Ph
lP

I Co
l

l
el

el
w

Pouihion nefficion d jodin in tehouds

re

re

Canlon
Ca

Ca
a

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Expt. Page No. 16

Ca

Ca
Coa 0.01 X VLX126:90 -malu/L

# simalaal Lalwotfo B.Caud

a

a
Oropul layu=
rm

rm

rm
Noumal
ha

ha

ha
NiV, 7
N2Uz
Nag (N) = 0.1XVL
lP

lP

lP
o
el

el
(onconralim
w

w
Caq. = 0.01 XV2 X126.90 moles/L.
re

re
, _p._ Orqan
Ca

Ca
SimilauyCallula MLenbohn oiodiniin dthet luytr of
Ot bottlu

úraph' úraph of log oq-axis) log (og(K osis)

a

laahiton (tfuiaat (k): Caq. Coa

rm

m
JCoq
ar

ar
ha

Slop (m): J(naaest integ)

Ph

Ph
lP

l
el

el

Rexult Pashiim_tosthicicut_o iodindn Conbon tchathlord

w

Ond
re

re
Ca

Ca

Sinu m:l,iodin has ik normol molucuau nxMt_n_hotnthu solue,

oskon enachloid Ard distilud water
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Experiment:No. O7
fAim To dilenina ma xfautntien of gven
Lkquud drop coundt noc.
a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
el

el
w

w
re

re
Ca

Ca
Budb
a

a
rm

m
ar

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ha

Ph

Ph
lP

-(opilon
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l
el

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w

StolaamomuJe
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Ca

Ca
a

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Expt. Page No.

Ca

Ca
EXpemunt no. 0t
Surfau ttnsim Of given liquid ny
arop LOUntMumod
a

a
aLnLLTavh 1 saikh_,.Rageco, M. Umon, Dr.Siar Nsdikh, oawarag
rm

rm

rm
BendugumblPhysical Ohaumacgvticu 1, Nrali Prokasman tdon
ha

ha

ha
lP

lP

lP
equmunt
Py.cnomuer
el

el
AApparohus stalagmomultrpipitt_tnumomhtr
onalyHcalbolant welght box.beakar et.
w

w
re

re
b(humicals_ Benzen toluen, distillud woaler
Ca

Thebny
Surfaty ttnaion E is thaforu
Ca
per _unit lengh
that_must
b applied_parallel o tha urfac
(E surfau jtnsim
torLergh- unit =N/M.
a

a
rm

m
ar

ar
ha

Ph

Ph
Prowduug
lP

HUean thoughly all glaAuAe

l

l
el

el

Liqulda_Usig deniu bottHu.

2Dettr mia a denihtu oF_all
w

|2Mout stolagmobmultk
Ostwald n Suilabu stand in eaticol
re

re

position -oovoid unnatualfall ofdaop

Ca

Ca

Wattr In dryAplagmonult tou

i têrttta pôsitionr mak and
Sign.
Teacher's
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lP
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a

a
rm

rm

rm
ha

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lP

lP
0BSERNATION
el

el
Drop (oum nuod
w

w
iqvids Dunsiy (p) Numlbr uf dnopPs Surfau tnsin
re

re
muAn (dunu.fum)
ii
Ca

Water
Bunztn
Ca
Tolu
a

a
rm

m
ar

ar
ha

Ph

Ph
lP

l
el

el
w

w
re

re

Result Guso ni ofqiven Jhaud by dp

Ca

Ca

LOundmuhod dunulom
a

a
m

m
ar

ar

ar

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Expt. Page No.

Ca

Ca
mayk A to maukB.
tota numburof drops ormud form
LUSd-fixed volum f allLiqvida)
5 Repuat Atp 3 -r three im to obtain Lorrect _reading.
&.Defoe stax of Counting num of_drops of bunxens,
nns Aalagmonuter and tham tnen fill e
a

a
and COUn_numbty of_drops formud
rm

rm

rm
with-fresh benzea
from Maak Ao MAk &.
ha

ha

ha
Siilaulyobtoin numbr OF drops_of_Other Liquida
lP

lP

lP
el

el
ObseryanonA__
w

w
Roomm temperatu=
re

re
Ketsurfas jensiom _of waler(Y):-- dynas/cm.
Ca

Ca
uOns dropOfwaltr
drop_of_benzenl =
1VOnadrop
vOn dop oftoluL =
Calulahion
a

Surfac nsion of Lquids (ould be alulaitd.

rm

m
ar

Pn
ar
ha

Ph

Ph
P n
lP

Mtn2 os_numau
l

of_daops.
whut, PAp2 au densihe
el

el

YI a usatknsim of waktr4 unknoun_uavids

w

Ppidivel
re

re

ReAult Sufau tnsion of givtniquid oy

Ca

Ca

axop COUnE Mhod dyn-/cm

Teacher's Sign.
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CXpeinanr No 08

Aim Toditrmina HLB numbl ofSurfatants by

oponificwhm muthod.
a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
el

el
w

w
re

re
Ca

Ca
a

a
rm

m
ar

ar
ha

Ph

Ph
lP

l
el

el
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re

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Ca

Ca
a

a
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Expt. . Page No. 19

Ca

Ca
EXpeaimunt No. o8
numaw
imT delermu
Saporüfitadhion
HL
Metmod
of surfuctavts hy
a

a
Rekrenclänvir ¥. shaiukh, Ma Kageeb, Ma.xanDr.SitopN
rm

rm

rm
Bedugunbla, Phueical
á
phaamaceutiu-1, Nioli PrkoAnan
Bgaowaa
_edihion
ha

ha

ha
lP

lP

lP
el

el
aApparahus botom-fiosR RetUx condenswDuret
Round
piputtc
w

w
ConitalfAask ek
e
re

re
Cnumicalsa Distilled ulatr,Estr Glyceyl mnosjtari
Ca

Ca
S Nal KDH, StAuic acid tna0CN HaL,0.LN Na@H
Ond Pnenolphthalein indiaor

Tnebny HLB Can

numbur of surfactats h delemind
by -fol louinq.
HLB 20
a

a
rm

m
ar

ar
ww
Saponifiaton numbr of ester
ha

S
Ph

Ph
A Acid numu of-fauly aúol.
lP

l
el

el

Proredure
w

Duermnation of Saponifitahion nvm

re

re

DMtighocLUroltly 0.S qm of glyerymonasheartiand_ansfer

Ca

Ca

ino yound bottom fioAk AddIE mof alcoholic

:S Naltoholic kOH t i and refluxon boiling oler bath
Teacher's Sign.
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Ca

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a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
el

el
w

w
re

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Ca

Ca
a

a
rm

m
Obwrvoho
ar

=. ar
ha

Saponificahion Numbbr
A.
Ph

Ph
u
lP

)Voluru. of 0.N H Consumsd Sompl (v)

l

nVolum of 0. N H (onsumud y blonk, (va)= -n

el

el

.
w

fAid Valu
re

re

Volum of.0.1 N NaoH CDMsumudl

V2)= M
Ca

Ca

Resu- Th HLB Volu of given anfo caut is

a

a
m

m
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Expt. Page No.20-

Ca

Ca
forfpr YS inu.
aifor blank simultaneously- reflux SApanoktly IS m f 0.SN
olcoholic kOHon boiling- WJaler ba for about uSminukA
aA blak_reading
ii Cool
ii botth tu soutHom toroom ttmpevature and Hhoti
a

a
as t.
rm

rm

rm
Sapanalelyagains 0.S N H USíng _phunolphthaluin
ha

ha

ha
indiotor.
bA Vi_and blanB L Va
ivLer ihe readinafor samplu
lP

lP

lP
el

el
2Dumnadin Of Arid number.
w

w
iDAcuahely weiah Steoac_acid in_coniol HasR.
0sq_of of
re

re
Add itto_a- mixhureof 10m etyl alconol and 10
Ca

Ca
OF eme, waam on watr bah if 2equld. CCowhn thyl
higulyinflammablaLquidal.-
alwhol Od eths Cre
iTihok soluhionOf SRaricacid against 0. N NadH_

Using phenolphthalein
Usng the indicaor
Lii)Ler tn Yeacung V.
a

a
rm

m
Calalahns
ar

ar
ha

Sapovifiohn valul
Ph

Ph
SV=_2V,-VDx0.Sx mg of koH . -0
lP

l
el

el

Acid volul
w

AV=_To060.L X 2V3
re

re

*Suostihi eq +0 valu in_eqh) toqut HLR_numbur._

Ca

Ca

HLB valu of given surfactant_ia

Reul Tu Teacher's Sign.
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PLMA No._09

Atub'obti ontan and donoy aruptor

im-Tdahioceleruna
of pABA-Caffein CPnpluy by solubiliy nuhod
a

a
rm

rm

rm
ha

ha

ha
lP

lP

lP
ReQuire mant
)Apparatus - \blumuhic ftask, puputa
el

el
) Chumicals-PACA, aHfuins, Distilud walt
w

w
re

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Ca

Ca
a

a
rm

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Ph

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Expt. Page No. 21

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Ca

Ca
FXpeAimunt No. 09

constantand donor aceptor_aio

inTo detmlnu Atubuiij
OF poba: Cofeiu_CompleA Solulimhod.

,
a

a
lanvir Y: Saudh, Md.Bageeb, Ma: Usmon Dr. Sira N:SihBasOuwarar
rm

rm

rm
Reterenco
Berdaoun la, Pysical Dharmaceutica Niri Pralkoshan1 edthonn.
ha

ha

ha
lP

lP

lP
Renuitmurt
el

el
i)Appadtys Volumeric fioJR lipitt
amino benzoleactdCafferntu Oistilled wak
w

w
Cnemicals Para
re

re
-
Tom a_ donor accaptor mechanism
Ca

Ca
Thebrn (omplexes heuts
Detweentwo ormore differet thwmical constitvets.
various expeai mut meHnods_ar usd to dekmim th
Stabili Cousjats t omplexes. somu o thesu indud
MAAAUYe muut of_colligative properttesOptial nmeHmods alouimuhay,
a

SolubiliyStudies et.
rm

m
ar

=vaying ar
ha

Pratedure
Ph

Ph
amoun
lP

Add Of (offelhu loto 1:4 gm) in

l

ditferet volumemc fiasks.

el

el

T eadh OF thu add 0.55 gm_para _amino

w

benzoic aud PABA)

re

re

BShoko th -fosk o reath the ezillbrum

Ca

Ca

Dettrmins tu Loncenhaion of para anno benzoicadd (pAL9

UB. Molar Concentrohom of coffein o determina
Teacher's Sign.
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C

Molay
ontentaion
a

a
of PAOA
rm

rm

rm
ha

ha

ha
lP

lP

lP
Molan onundalm of Coffcano
el

el
w

w
re

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Ca

.71 Ca
a

a
rm

m
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Ph

Ph
lP

l
el

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Expt. Page No. 22

Ca

Ca
mod ot analysis
Point ASolubulitiy_of PaBA in watr. CPABAlat-polnt A
2wih t addihiom_of affeiru_t solubild Of
inueaseslinearlyOwing to omplexation.
3. PoinEBSolutionisis_saturaled withCompley_nd DABA
a

a
wih
rm

rm

rm
self Take CPABAlct_point.a_onaxis and Caffunlat
peint & on X-0nis
ha

ha

ha
4.ThComplex to formond
ContinueA to_pxdpitole -fiom t
lP

lP

lP
Sadurated_Sustem as mort_and mot _coffeins_addud.
possed uo oluton
el

el
5PointC: HL ha extess SoLid_ PABA has passed
and as been Converttdto COmpux.Lafein]_at point
w

w
C.
re

re
L6.Soma PADA combinu further wih cafieinto form higher
Ca

Ca
Comples

Dekrminaim
Smbliy (onatauh
PABA+ Coffein= PABA- Caffeins
a

Pa8A-atfeint3
rm

m
ar

ar
CPABA]caffeina)
ha

Ph

Ph
CPABA-Coffein] = CPABA) at pcint0- CPABA) at_paint
lP

A
l

l
el

el

CPAGAJ= CPABAJat poin A.

w

Caffein =CCaffeinlat point e-CPABA-affeinu]

re

re
Ca

Ca

)Stpichiomehic ratio, Donor to Leplor Ratio of

PABA-Caffeina Complex
Teacher's Sign.
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rm

rm

rm
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-
lP

lP

lP
Resu
el

el
Th Atalbilili Cutpn Of PaBA-Cosicin (ompx
ofPALA -(icin
w

w
Stoichionuhici yodio
Caplux
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i
Ca

Ca
a

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Page
No.23

Ca

Ca
Stoldniomeic_ratlo= CaffeinuLin complex.
CPALAJ in_Complu

CCaffeinin complex =Ccaffein)

ot point
L-[taffeina)at point .
a

a
CPARAJin _complex = CAGAJ total- COAA) ot point 6
rm

rm

rm
ha

ha

ha
Reul
lP

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Tu Atablily_(onstpour PA8A- (atfein CompleK ia
el

el
_Cnd Atpichio memic Yatio of pABA-affina
w

w
COmpux_
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Ca

Ca
a

a
rm

m
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Ph

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lP

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w

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Ca

Ca

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