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ACI MATERIALS JOURNAL TECHNICAL PAPER

Title no. 106-M46

Short-Term Mechanical Properties of High-Strength


Concrete
by Andrew Logan, Wonchang Choi, Amir Mirmiran, Sami Rizkalla, and Paul Zia

A comprehensive experimental program was undertaken to determine high-performance concrete (HPC), with some specimens
the short-term mechanical properties of high-strength concrete referred to as “very high strength,” with 28-day compressive
(HSC). Modulus of rupture beams and two different sizes of strengths ranging from 8 to 13.4 ksi (55 to 92 MPa).6 The
concrete cylinders with three different target compressive strengths study found that the ratio of the compressive strength of the
ranging from 10 to 18 ksi (69 to 124 MPa) were subjected to three
6 x 12 in. (150 x 300 mm) cylinders to that of the 4 x 8 in.
different curing methods and durations. Test results were combined
with data from the literature to improve predictive equations for (100 x 200 mm) cylinders ranged from 0.91 to 0.98,
the elastic modulus and modulus of rupture of HSC. Of the three depending on the type of coarse aggregates used.6 The study
different curing methods, cylinders moist-cured for 7 days exhibited also determined that the proposed equation of Carrasquillo et
the highest compressive strengths at ages of 28 and 56 days. In al.4 (and ACI 363R-925) underestimated the elastic modulus
contrast, 1-day heat curing generally resulted in the lowest of HSC. With regards to the modulus of rupture, the study
compressive strength. The study shows that a Poisson’s ratio of 0.2 showed that at the design age, the ratio of the observed value
can be adequately used for HSC. to that predicted by ACI 318-053 was 1.06 for concrete made
with fly ash and 1.15 for concrete made with silica fume.
Keywords: compressive strength; elastic modulus; high-strength concrete; Comparing the measured values to those predicted by
modulus of rupture; Poisson’s ratio.
Carrasquillo et al.4 (and ACI 363R-92 5), the ratio was as
low as 0.686.
INTRODUCTION
The development of high-strength concrete (HSC) has led Mokhtarzadeh and French7 studied 142 concrete mixtures
to more efficient design of buildings and bridges, with shallower with 28-day compressive strengths ranging from 8 to 18.6 ksi
members and longer spans. Although some design specifications (55 to 128 MPa). Their data showed the ACI 318-053 equation
have addressed the use of HSC, many have implicitly or to overestimate the elastic modulus of HSC, whereas the
explicitly placed restrictions on its use, primarily because ACI 363R-925 equation was found more favorable. Also, the
of limited research data.1 For example, the American Association ACI 363R-925 equation for the modulus of rupture was
of Highway and Transportation Officials (AASHTO) LRFD found acceptable for the moist-cured specimens, whereas the
Bridge Design Specifications2 limits its applicability to modulus of rupture of the heat-cured specimens fell in
concrete compressive strength of 10 ksi (69 MPa) unless between the values predicted by the ACI 363R-925 and
physical tests are conducted. Furthermore, many design ACI 318-053 equations. The study proposed a new modulus
provisions in both ACI 318-053 and AASHTO-LRFD2 are of rupture equation with a coefficient of 9.3 to be used
based on test data obtained from specimens with compressive instead of the 7.5 in the ACI 318-053 equation.
strengths up to 6 ksi (41 MPa) and, therefore, do not accurately Légeron and Paultre8 reported that curing conditions
reflect the mechanical properties of HSC. significantly affected the measured value of the modulus of
In the late 1970s, Carrasquillo et al.4 tested specimens rupture. They also compiled data from the literature and
from three concrete mixtures with 53-day compressive proposed predictive equations for the minimum, average,
strengths ranging from 4.6 to 11.1 ksi (31.7 to 76.5 MPa). and maximum values of the modulus of rupture. They
Some of the specimens were moist-cured for 7 days and were suggested that the minimum values be used for service limit
then allowed to dry until tested at an age of 28 days. Others states to control deflections and cracking, whereas the
were moist-cured for 28 days and then allowed to dry until maximum values should be used for the ultimate limit state
tested at an age of 95 days. The control group was moist- to ensure ductility of flexural members. Burg and Ost9 found
cured until 2 hours prior to testing. The data suggested that that the ratio of the moduli of rupture of moist-cured specimens
drying of HSC cylinders resulted in a lower compressive to air-cured specimens ranged from 1.54 to 2.02.
strength and modulus of rupture, in contrast to the normal- In the last few years, the AASHTO has addressed the need
strength concrete (NSC). The reduction in the modulus of to expand the applicability of its LRFD Specifications2 to HSC
rupture was more significant than that of the compressive with a number of research projects conducted through the
strength. The study also revealed that the compressive National Cooperative Highway Research Program (NCHRP).
strength of 6 x 12 in. (150 x 300 mm) cylinders was, on This paper reports on one of these projects (NCHRP 12-64),
average, approximately 90% of that of the 4 x 8 in. (100 x which focused on flexure and compression design provisions
200 mm) cylinders, irrespective of the compressive strength
or the age at testing. Carrasquillo et al.4 then proposed equations
for both modulus of elasticity and modulus of rupture of HSC, ACI Materials Journal, V. 106, No. 5, September-October 2009.
which were later included in the ACI 363R-92 report.5 MS No. M-2008-005 received January 3, 2008, and reviewed under Institute publication
policies. Copyright © 2009, American Concrete Institute. All rights reserved, including the
The Strategic Highway Research Program (SHRP) of the making of copies unless permission is obtained from the copyright proprietors. Pertinent
discussion including authors’ closure, if any, will be published in the July-August 2010
early 1990s also focused on the mechanical properties of ACI Materials Journal if the discussion is received by April 1, 2010.

ACI Materials Journal/September-October 2009 1


Table 1—Concrete mixture proportions
Andrew Logan works for a civil engineering firm in Leesburg, FL. He received his
BS and MS in civil engineering from the University of Florida, Gainesville, FL, and Target compressive strengths
North Carolina State University, Raleigh, NC, respectively. His research interests 10 ksi 14 ksi 18 ksi
include short-term mechanical properties of high-strength concrete. Materials (69 MPa) (97 MPa) (124 MPa)
Wonchang Choi received his PhD from North Carolina State University, and his BS Cement (Type I/II), lb/yd3 (kg/m3) 703 (417) 703 (417) 935 (555)
and MS in civil engineering from Hongik University, Seoul, Korea. His research interests 3 3
include the flexural behavior of prestressed girders using high-strength concrete. Densified microsilica fume, lb/yd (kg/m ) 75 (44) 75 (44) 75 (44)
Fly ash, lb/yd3 (kg/m3) 192 (114) 192 (114) 50 (30)
Amir Mirmiran, FACI, is Professor and Interim Dean of the College of Engineering
and Computing at Florida International University, Miami, FL. He is a member of Sand, lb/yd3 (kg/m3) 1055 (625) 1315 (780) 1240 (736)
ACI Committees 440, Fiber Reinforced Polymer Reinforcement, and E803, Faculty
1830 1830 1830
Network Coordinating Committee, and Joint ACI-ASCE Committee 343, Concrete Rock (diabase 78M), lb/yd3 (kg/m3) (1085) (1085) (1085)
Bridge Design. His research interests include high-strength concrete and advanced
composite materials for bridge applications. Water, lb/yd3 (kg/m3) 292 (173) 250 (148) 267 (158)
Sami Rizkalla, FACI, is Distinguished Professor of Civil Engineering and Construction at High-range water-reducing admixture
17 (1110) 24 (1565) 36 (2345)
North Carolina State University. He serves as Director of the Constructed Facilities (HRWRA), oz/100 lb (mL/100 kg)*
Laboratory as well as the NSF I/UCR Center on Repair of Structures and Bridges at
NC State. He is a member of ACI Committees 440, Fiber Reinforced Polymer Reinforcement, Retarding agent, oz/100 lb (mL/100 kg)* 3 (195) 3 (195) 3 (195)
and E803, Faculty Network Coordinating Committee, and Joint ASI-ASCE Committees w/cm 0.30 0.26 0.25
423, Prestressed Concrete, and 550, Precast Concrete Structures.
Average 28-day compressive strength of 11.45 14.37 17.09
ACI Honorary Member Paul Zia is a Distinguished University Professor Emeritus at laboratory batch, ksi (MPa) (78.9) (99.1) (117.8)
NC State University. He is an ACI Past President and is currently a member of the *
Ounces per 100 lb of cementitious materials (mL per 100 kg cementitious materials).
Concrete Research Council, ACI Committee 363, High-Strength Concrete; Concrete
Research Council; and Joint ACI-ASCE Committees 423, Prestressed Concrete; and
445, Shear and Torsion.
the trial batches and the selected mixture proportions can be
found elsewhere.11
for HSC.10 As part of this project, an effort was made to
characterize the short-term mechanical properties of HSC. Specimen preparation and curing procedures
Concrete was batched in a ready mixed concrete plant
RESEARCH SIGNIFICANCE AND OBJECTIVES using commercial production procedures. The 4 x 8 in.
The main objective of this study was to improve predictive (100 x 200 mm) and 6 x 12 in. (150 x 300 mm) cylinders
equations for short-term mechanical properties of HSC, were used for the compressive strength and elastic modulus
including its elastic modulus, modulus of rupture, and of concrete, and 6 x 6 x 20 in. (150 x 150 x 510 mm) beams
Poisson’s ratio. The significance of this research is not only were used for the modulus of rupture. Cylinders were cast in
to improve the predictive equations, but also to enhance the plastic molds, and the beams were cast in steel molds. The spec-
test database for HSC with three different target compressive imens were made according to AASHTO T23 (ASTM C31)
strengths, different specimen sizes, and different curing (ACI 363.2R-9812). Table 2 shows the test matrix. Testing ages
conditions. The database is especially significant because it were 1, 7, 14, 28, and 56 days. On each testing day, two of the
is based on ready mixed concrete delivered from batch 4 x 8 in. (100 x 200 mm) cylinders were used to determine the
plants, and not laboratory-scale mixtures. Although not elastic modulus before being tested to failure.
directly the focus of this paper, it is also important to note
The specimens were subjected to one of the three
that the specimens for short-term mechanical properties
following curing conditions: 1) 7-day moist curing to represent
were made and tested side-by-side and as part of a larger test
typical curing procedures for reinforced concrete members;
matrix, which included reinforced concrete columns and
2) 1-day heat curing similar to that used in precast concrete
beams and prestressed girders.
plants for prestressed structural members; and 3) continual
moist curing until the day of testing according to the ASTM
EXPERIMENTAL PROGRAM standards used for the purposes of quality control and certifying
Materials and mixture design
Three different concrete mixtures with target compressive the compressive strength of concrete in the industry.12 The heat-
strengths of 10, 14, and 18 ksi (69, 97, and 124 MPa) were cured specimens were placed in a chamber with a heating
prepared using ready mixed concrete delivered from a batch regime ramping up to a constant temperature of 150 to 160° F
plant. The mixture proportions were selected from a large (66 to 71°C), and back to room temperature in 24 hours.
number of trial laboratory batches and are shown in Table 1.
The mixtures for the 10 and 14 ksi (69 and 97 MPa) Testing procedures and instrumentations
compressive strengths were proportioned to exceed their The cylinders were ground at both ends before testing to
target values by 10 to 20%, assuming that there would be a remove any surface irregularity and to also ensure that the
strength reduction due to the large batch size and the ends would be perpendicular to the sides of the specimen.
increased difficulty in maintaining quality control in truck- Compression tests were performed using a Universal testing
mixed batches. In both cases, however, as will be discussed machine for both the 4 x 8 in. (100 x 200 mm) and the 6 x 12 in.
later, the compressive strengths of the truck-mixed batches were (150 x 300 mm) cylinders. Tests followed ASHTO T22
approximately the same as those of the laboratory batches. (ASTM C39) at a loading rate of approximately 0.04 ksi/s
The coarse aggregates were crushed stone quarried in (0.28 MPa/s). The loading rate was selected at the higher end
Butner, NC, with a nominal maximum size of 3/8 in. (9.5 mm). of the standard range to avoid prolonged loading, which could
Manufactured sand made from the same type of rock was used possibly cause extensive microcracking in concrete cylinders.
as fine aggregates because the lab mixtures had clearly The elastic modulus was determined using the 4 x 8 in.
shown that it would increase the compressive strength of (100 x 200 mm) concrete cylinders and in accordance with
concrete. The cement was Type I/II. Additional details on ASTM C469. Deflections were measured using potentiometers

2 ACI Materials Journal/September-October 2009


Table 2—Description of test specimens for each target strength
Testing age (days)
Specimen Test type Curing method 1 7 14 28 56 Total
7-day moist curing 3 3 3 3 3 15
4 x 8 in. (100 x 200 mm) cylinders Axial compression 1-day heat curing 3 3 3 3 3 15
Continual moist curing 3 3 6
Total number of 4 x 8 in. (100 x 200 mm) cylinders 36
7-day moist curing 3 3 6
6 x 12 in. (150 x 300 mm) cylinders Axial compression 1-day heat curing 3 3 6
Continual moist curing 3 3 6
Total number of 6 x 12 in. (150 x 300 mm) cylinders 18
7-day moist curing 3 3 3 3 3 15
6 x 6 x 20 in. (150 x 150 x 510 mm) beams Modulus of rupture 1-day heat curing 3 3 3 3 3 15
Continual moist curing 3 3
Total number of 6 x 6 x 12 in. (150 x 150 x 510 mm) beams 33

Fig. 1—Fully instrumented 4 x 8 in. (100 x 200 mm)


cylindrical specimen.

Fig. 3—Compressive strength of 4 x 8 in. (100 x 200 mm)


cylinders at 28 days.

TEST RESULTS AND DISCUSSIONS


Compressive strength
The compressive strengths for the first two concrete
mixtures exceeded their target values, whereas the third
batch failed to reach its target value (Table 1). The tests,
however, still provided useful information for expanding and
Fig. 2—Modulus of rupture test setup. adding to the knowledge base on mechanical properties of HSC.
The effects of curing procedures on the compressive
strength measured from the 4 x 8 in. (100 x 200 mm) cylinders
attached to two fixed rings (Fig. 1). Four vertical potentiometers
at 28 days are illustrated in Fig. 3. The 7-day moist-cured
measured axial deflections, while two horizontal potentiometers
specimens showed the highest compressive strengths at 28 days
attached at midheight measured lateral dilation of concrete.
in each of the three batches. The 1-day heat curing increased
The apparatus consisted of two aluminum rings with screws
strength gain at an early age, but weakened it at later ages. This
for attachment to the specimen. Prior to attaching the apparatus behavior was attributed to rapid hydration, which causes the
to the specimen, the rings were joined by three aluminum bars. structure of the cement paste to be more porous than when
The spacing between the screws on the top ring and the cement paste hydrates slowly. The higher porosity, in turn,
screws on the bottom ring when the aluminum bars were leads to decreased strength. Although the majority of the
attached was 5 in. (127 mm), which served as a gauge length strength gain in heat-cured specimens occurred within the
for calculating axial strains from the measured deformations. first few days, their strength continued to increase until 56 days,
The modulus of rupture beams were placed in the testing albeit at a slow rate. The average 28-day strength of the 7-day
frame, oriented in such a way that the specimen was turned moist-cured specimens were 1.17, 1.10, and 1.16 times those
on its side with respect to its molded position, as specified in of the heat-cured specimens for the 10, 14, and 18 ksi
ASTM C78 (Fig. 2). The load was applied using a hand (69, 97, and 124 MPa) target strengths, respectively. The
pump. The loading rate was controlled such that the stress at continually moist-cured specimens exhibited a slightly
the extreme bottom fiber of the beam would increase at a rate lower strength, with failure closer to the surface, primarily
of 0.15 ksi/s (1.03 MPa/s). because of the remaining moisture in the capillary pores.

ACI Materials Journal/September-October 2009 3


Fig. 4—Strength gain over time expressed as percentage
of 28-day strength. Fig. 6—Predictions of over 4400 data points using proposed
equation.

Fig. 5—Elastic modulus versus compressive strength. (Data Fig. 7—Statistical comparisons for modulus of elasticity.
from References 4 and 13 to 18).
Figure 5 shows test results from this research project as
The strength gain of concrete over time is depicted in Fig. 4. compared to the ACI 318-053 (AASHTO-LRFD2) and the
For the 10 and 14 ksi (69 and 97 MPa) target strengths, the heat- ACI 363R-925 equations. In the same figure, data by
cured specimens reached approximately 90% of their 28-day others4,13-18 are also shown for comparison. The measured
strength during the first day of curing. The specimens made values are generally in agreement with the predicted values
from the 18 ksi (124 MPa) target strength concrete also calculated using the ACI 363R-925 equation, regardless of
gained the majority of their 28-day strength in the first day, the curing method. The data also support the statement in
but at a lower rate. This was attributed to: 1) higher heat of ACI 363R-925 that the ACI 318-053 (AASHTO-LRFD2) equa-
hydration resulting from the larger cement content in the tion consistently overestimates the elastic modulus for HSC.
mixture; and 2) the larger dose of high-range water-reducing A total of 4388 test data for elastic modulus, with concrete
admixture in the mixture. strengths between 3.7 to 24 ksi and unit weight between
90 to 176 lbf, were collected from the literature19 (see
Elastic modulus Reference 20 for details). Based on the collected data, the
The current code equation in ACI 318-053 and the following equation for the elastic modulus of concrete with
AASHTO-LRFD2 for estimating the elastic modulus of compressive strength up to 18 ksi (124 MPa) is proposed20
concrete is as follows

1.5 Ec (ksi) = 310,000K1[wc(kip/ft3)]2.5 × [fc (ksi)]0.33


E c = 33w c f c  psi 
(1) Ec (MPa) = 0.000035K1[wc(kg/m3)]2.5 × [fc (MPa)]0.33 (3)
1.5
E c = 0.043w c f c  MPa 
where K1 is the correction factor to account for the source of
where w is the unit weight of concrete, and fc is the 28-day aggregates, which may be taken as 1.0 unless determined by
compressive strength. ACI 363R-925 suggests the following physical tests. The collected data, including results from this
alternative equation study, are compared with the proposed equation in Fig. 6.
The figure indicates that the collected data are still scattered,
Ec = (40,000(fc )0.5 + 106)(wc /145)1.5 (psi) however, with an improved R2 = 0.76. Figure 7 shows the
probability distribution of the modulus of elasticity data as a
Ec = (3320( fc )0.5 + 6900)(wc /2320)1.5 (MPa) (2) function of the predicted over the measured value for the

4 ACI Materials Journal/September-October 2009


Fig. 8—Poisson’s ratio for various concrete strengths.

three different equations using statistical analysis. The


figure shows that the ACI 318-053 (AASHTO-LRFD2)
equation overestimates the elastic modulus. Although
the ACI 363R-92 5 equation has the lowest standard deviation
among the three predictions, its predictions are slightly
conservative. The proposed equation, on the other hand,
has the best normal distribution, although its standard deviation
is slightly higher than that of the ACI 363R-925 equation.

Poisson’s ratio
Following ASTM C469,12 Poisson’s ratio was determined
using the measured lateral and axial strains of the cylinders
tested in compression, based on two points on the stress-
strain curve. The lower point was defined by an axial strain
value of 0.00005, while the upper point was defined by an
axial stress value of 40% of the peak stress. The measured
Poisson’s ratios for concrete had large variations, as shown
in Fig. 8. Test results do not show an apparent correlation
between the Poisson’s ratio and the measured compressive
strength. In addition, it was observed that curing procedures
and age of concrete had little or no effect on the Poisson’s
ratio. The average Poisson’s ratio for all tested cylinders is
0.17 with a standard deviation of 0.07. The generally
accepted range for the Poisson’s ratio of NSC is between
0.15 and 0.25, while it is generally assumed to be 0.2 for
analysis.21 Test data from this project suggest that it is
reasonable to use 0.2 as Poisson’s ratio for HSC up to
compressive strength of 18 ksi (124 MPa).

Modulus of rupture
Effect of curing methods on the modulus of rupture for the
three different target strengths are shown in Fig. 9. Test
results suggest that the modulus of rupture is significantly
affected by curing conditions for all target strengths. The Fig. 9—Effect of curing process on modulus of rupture for
trend indicates that removal of the beam specimen after 7 days concrete compressive strength: modulus of rupture versus
from the curing tank causes a significant reduction of the time for (a) 19 ksi (69 MPa) target strength; (b) 14 ksi (97 MPa
modulus of rupture. Similarly, the 1-day heat-cured beams target strength; and (c) 18 ksi (124 MPa) target strength.
showed low values of the modulus of rupture due to the cannot evaporate as quickly as the surface moisture. This
dryness after removal from the molds, which had prevented
relative shrinkage difference causes microcracking of
moisture loss during the first day of curing. In both cases, the
reduced modulus of rupture is attributed to the microcracks concrete. Therefore, the specimens that were moist-cured up
initiated by drying shrinkage. The low permeability of the to the day of testing showed much higher modulus of rupture
HSC is expected to cause differential shrinkage strains than those cured differently.
across the depth of the specimen due to the fact that the Figure 10 shows test data from material study tested in
moisture trapped in the interior part of the specimens this program along with the data collected from the litera-

ACI Materials Journal/September-October 2009 5


(124 MPa).
• The modulus of rupture was reduced significantly for
specimens removed from their sealed or moist environments
and allowed to dry. The continuously moist-cured
specimens developed modulus of rupture values, in
some cases twice as much as those obtained from the
7-day moist-cured specimens.
• The upper bound equation specified by the AASHTO-
LRFD2 provided a good estimate of the modulus of
rupture for the continuously moist-cured specimens,
but overestimated the modulus of rupture for the 1-day
heat-cured and 7-day moist-cured specimens. The
lower bound equation specified by the AASHTO-
LRFD2 overestimated the measured modulus of rupture
for 1-day heat-cured and 7-day moist-cured specimens.
Based on the test results, a better predictive equation,
Fig. 10—Modulus of rupture versus compressive strength. lower bound of the test data, was proposed for HSC up
to 18 ksi (124 MPa).
ture.1,7,13,16,19 Two equations for modulus of rupture given
in Section 5.4.2.6 of the current AASHTO-LRFD2 are also ACKNOWLEDGMENTS
shown in the figure. Some of the tests results correspond This study was sponsored by the American Association of State Highway
better to the current upper bound of the AASHTO-LRFD.2 and Transportation Officials in cooperation with the Federal Highway
This is mainly due to the curing condition and moisture Administration, and was conducted as part of the National Cooperative
content of the specimens. Test results suggest that the Highway Research Program Project 12-64, which is administered by the
Transportation Research Board of the National Research Council, Senior
current lower bound of the AASHTO-LRFD2 overestimates Program Officer D. Beal. The experiments were carried out at the
the modulus of rupture for HSC. A better predictive equation, Constructed Facilities Laboratory at North Carolina State University. The
which is the lower bound of the test data, fr = 0.19 f c   ksi  (fr contributions of consultants—H. Russell of Henry Russell, Inc. and R. Mast
= 0.5 f c  MPa  ), is proposed for HSC up to 18 ksi (124 MPa). of Berger/ABAM Engineers, Inc.—are greatly acknowledged. The assistance of
Ready Mixed Concrete, Boral Material Technologies, Degussa Admixtures,
Roanoke Cement, Carolina SunRock , and Elkem are also greatly appreciated.
CONCLUSIONS AND RECOMMENDATIONS Z. Wu, S. Kim, and H. C. Mertol provided significant assistance during all
A total of thirty-six 4 x 8 in. (100 x 200 mm) cylinders, aspects of this research program. The findings and opinions expressed in
eighteen 6 x 12 in. (150 x 300 mm) cylinders, and thirty- this paper, however, are those of the authors alone and not necessarily the
views of the sponsoring agency.
three 6 x 6 x 20 in. (150 x 150 x 510 mm) beams were
prepared with three different target compressive strengths of
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6 ACI Materials Journal/September-October 2009


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