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Designation: D8316 − 20
INTRODUCTION
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This test method is under the jurisdiction of ASTM Committee D02 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Subcommittee D02.L0 on Industrial Lubricants and Engineering Sciences of High Standards volume information, refer to the standard’s Document Summary page on
Performance Fluids and Solids. the ASTM website.
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Current edition approved May 1, 2020. Published May 2020. DOI: 10.1520/ Available from Deutsches Institut für Normung e.V.(DIN), Am DIN-Platz,
D8316-20. Burggrafenstrasse 6, 10787 Berlin, Germany, http://www.din.de.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D8316 − 20
DIN 51631:1999 Mineral Spirits – Special Boiling Point 3.1.11 Rvk, n—reduced valley height according to DIN EN
Spirits – Requirements ISO 13565-2:1998; Rvk is the mean depth of the valley
DIN 51834-4 Tribological Test in the Translatory Oscillation reaching into the material below the core profile section.
Apparatus (Part 4: Determination of friction and wear data 3.1.12 Rz, (DIN), n—in measuring surface finish, the aver-
for lubricating oils with the cylindrical roller-disk geom- age of all Ry values (peak to valley heights) in the assessment
etry) length.4
DIN EN ISO 13565-2:1998 Geometrical Product Specifica-
3.1.13 wear, n—damage to a solid surface, generally involv-
tions (GPS) – Surface Texture: Profile Method; Surfaces
ing progressive loss of material, due to relative motion between
Having Stratified Functional Properties – Part 2: Height
that surface and a contacting substance or substances. G40
Characterization using the Linear Material Ratio Curve
(replacement of DIN 4776:1990) 3.2 Definitions of Terms Specific to This Standard:
3.2.1 seizure, n—localized fusion of metal between the
3. Terminology rubbing surfaces of the test pieces. D5706
3.1 Definitions: 3.2.1.1 Discussion—In this test method, seizure is indicated
3.1.1 break-in, n—in tribology, an initial transition process by a sharp rise in the coefficient of friction, over steady state,
occurring in newly established wearing contacts, often accom- of greater than 0.2 for over 20 s. In severe cases, a stoppage in
panied by transients in coefficient of friction or wear rate, or the motor will occur.
both, that are uncharacteristic of the given tribological system’s 3.3 Abbreviations:
longterm behavior. (Synonym: run-in, wear-in) G40 3.3.1 FZG, n—commonly referred to Forschungstelle für
3.1.2 coeffıcient of friction, µ or f, n—in tribology, the Záhnräder und Getriebebau (German); Research Site for Gears
dimensionless ratio of the friction force (Ff) between two and Transmissions) Visual Method (English translation) D5182
bodies to the normal force (Fn) pressing these bodies together. 3.3.2 SRV, n—Schwingung, Reibung, Verschleiss (German);
G40 oscillating, friction, wear (English translation).
µ 5 ~ F f ⁄ F n! (1) 4. Summary of Test Method
3.1.3 EP lubricating oil, n—a liquid lubricant containing an 4.1 This test method is performed on an SRV test machine
extreme pressure (EP) additive. using a test roller oscillated at constant frequency and stroke
3.1.4 extreme pressure (EP) additive, n—in a lubricant, a amplitude and under constant load (Fn), against a test disk that
substance that minimizes damage to metal surfaces in contact has been wetted with the lubricant specimen. The movement of
under high stress rubbing conditions. the roller is inclined/deflected by 10° to the oscillating axis (see
3.1.5 Hertzian contact area, n—the apparent area of contact Fig. 1). The test disk receiving block to which the test disk is
between two nonconforming solid bodies pressed against each attached is held at a constant temperature.
other, as calculated from Hertz’s equations of elastic NOTE 1—The frequency of oscillation, stroke length, test temperature,
deformation. G40 test load, test duration, and test roller and disk material can be varied from
3.1.6 Hertzian contact pressure, n—the magnitude of the those specified in this test method. The test roller yields Hertzian line
contact geometry. To obtain point or area contact, test pieces of differing
pressure at any specified location in a Hertzian contact area, as configurations can be substituted for the test roller.
calculated from Hertz’s equations of elastic deformation.
4.2 The friction force, Ff, is measured by a piezo-electric
D7421
device in the test disk assembly. Peak values of coefficient of
3.1.6.1 Discussion—The Hertzian contact pressure can also
friction, f, are determined and recorded as a function of time
be calculated and reported as maximum value Pmax in the
center of the contact or as Paverage as average over the total
contact area.
3.1.7 lubricant, n—any material interposed between two
surfaces for the purpose of reducing the friction or wear, or
both, between them. G40
3.1.8 Pgeom, n—geometric contact pressure describes the
load carrying capacity at test end (see 9.3.6).
3.1.9 Ra (C.L.A.), n—in measuring surface finish, the arith-
metic average of the absolute distances of all profile points
from the mean line for a given distance.4
3.1.10 Rpk, n—reduced peak height according to DIN EN
ISO 13565-2:1998; half the Rpk value is the mean height of the
peak sticking out above the core profile section.
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4.3 After the preset test period, the test machine and data
acquisition are stopped and the wear scar widths on the roller
and disk are measured using a microscope. If a profilometer is
available, a trace perpendicular to the wear track on the test
disk and to the scar on the roller can also be used to obtain
additional wear quantities.
5. Significance and Use
5.1 This test method can be used to determine antiwear
properties and coefficient of friction of EP lubricating oils at
selected temperatures and loads specified for use in slip-rolling
contacts in which high-speed vibrational or start-stop motions
are present for extended periods of time under initial high
Hertzian line contact pressures. It has found application as a
screening test for lubricants used in gears, rolling bearings or
cam/follower systems. Users of this test method should deter-
mine whether results correlate with field performance or other
applications. In comparison to the ball-on-disk geometry as per
Test Method D6425, the initial contact pressure is better
retained over test time in this roller-on-disk geometry.
6. Apparatus
6.1 SRV Test Machine5, illustrated in Figs. 2 and 3 consists
of a linear oscillation drive, a test chamber (see Fig. 3) and a
loading device with a servomotor and a load cell. The machine
is operated by a control device for the oscillating drive, a timer,
a load control, a frequency control, a stroke control, a data
amplifier to determine the friction coefficient, and a switch and
a controller for the heating. An oscilloscope may be used for
monitoring of quantities. Friction coefficients are recorded in
relation to time by data acquisition in a computer.
6.1.1 The roller is mounted in the holder so that the
longitudinal axis of the roller is deflected by 10° to the sliding FIG. 2 SRV Test Machine (Model 5)
direction. This test is limited to SRV IV&V models, because
SRVIII and older models do not execute a movement of the
readable to 0.005 mm. Magnification should be sufficient to
roller exactly parallel to the disk surface.
allow for ease of measurement.
6.1.2 On the firmly mounted receiving block (1) in the test
chamber (see Fig. 2 and Fig. 3), there is a piezoelectric device 6.3 Syringe, suitable for applying 0.3 mL of the lubricating
(2) to measure the friction force, Ff, and the friction coefficient, oil under test.
f, the holder for the test disk (3) with a thermostat-controlled 6.4 Tweezers, straight, round, about 200 mm long, with
electrical resistance heating element (4); a resistance thermom- non-marring tips.
eter (5); the oscillation drive rods (6); an exchangeable holder
6.5 Torque Wrench, initial torque 0.5 Nm to 5 Nm.
for the test roller (7); and the load rods of the loading device
(8). 6.6 Ultrasonic Cleaner.
6.1.3 The design of the receiving block for the test disk
7. Reagents and Materials
should be such that it has integrated cooling coils, or that
cooling coils are wound around it, so that the receiving block 7.1 Test Roller6 in AISI 52100 Steel, 60 HRC hardness 6
must be capable to maintaining test temperatures down to 2 HRC hardness, 0.025 µm 6 0.005 µm Ra (C.L.A.) polished
233 K. The test disk (9) and the test roller (10) are inserted into surface finish, is a cylinder Ø 6 mm × 8 mm with crowned
their respective holders (3, 4) (see Fig. 2 and Fig. 3). ends, so that the contact length l1 at the beginning of the test is
6.1.4 Disks are generally used as the lower test piece. 4 mm. The shape and geometry of the roller is as per DIN
5402, Part 1.
6.2 Microscope, equipped with a filar eyepiece graduated in
0.005 mm divisions or equipped with a micrometre stage 7.2 Test Disk7 vacuum arc remelted (VAR) AISI 52100
steel with an inclusion rating using method D, Type A, a
5
The sole source of supply of the apparatus known to the committee at this time
6
is Optimol Instruments, Prüftechnik GmbH, Flößergasse 3, D-81369 Munich, ASTM Handbook, “Friction, Lubrication, and Wear Technology,” Vol 18,
Germany. If you are aware of alternative suppliers, please provide this information October 1992.
7
to ASTM International Headquarters. Your comments will receive careful consid- Zaretsky, E. V., “Tribology for Aerospace Applications,” STLE SP-37, 1997, p.
eration at a meeting of the responsible technical committee,1 which you may attend. 358.
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NOTE 5—Depending on the software version, names and availability of
the parameters can vary.
8.2.1 Start conditions (thermostatic stabilization):
Temperature: for exmaple +80 °C ± 1 K
Test load: 50 N ± 1 N
Start delay: 600 s (is displayed by all versions of the SRV software).
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9.2.2 Then set the test load unit to 50 N and tighten the disk 10.1.1.7 Test disk material, and
clamps to a torque of 2.5 Nm. 10.1.1.8 Test oil sample with denomination.
9.2.3 The heater control starts automatically and heats up to 10.2 Report both wear width d1 of the scar on the roller and
the pre-set and desired temperature: for example, +80 °C. the width d2 of the track on the disk (see Fig. 1).
9.2.4 Follow the directions in the Assistant for starting a test
in the SRV control software until the automated test run mode 10.3 Report all measurements of the coefficient of friction,
(waiting for reaching start conditions) is started. The test starts fmin, fmax, f15, f30, f90, f120, fend and the magnitude of any strong
automatically when the pre-set delay (for example, 300 s) has fluctuations in the coefficients of friction, and when required by
expired. The test can also be started manually. The test machine specification, include a copy of the evolution of coefficient of
will automatically stop. friction.
10.4 Report the depth of the wear track on the lower
NOTE 8—If, due to seizure, the friction coefficient exceeds the limit f =
0.35, the test should be terminated. If the machine does not automatically specimen disk if a profilometer reading was made.
shut down at this point, it may have to be switched off manually or a
higher set point was chosen. 11. Precision and Bias
9.3 Evaluation Procedure: 11.1 Data for the precision calculations of this test method
9.3.1 Remove and clean the test roller and disk in accor- were obtained from interlaboratory tests in 2017 and 2018.
dance with 9.1. Fourteen cooperators tested in 2017 three lubricating oils and
9.3.2 Place the cleaned test roller on a suitable holder, and sixteen cooperators in 2018 three lubricating oils, all oils with
using a microscope, measure to the nearest 0.01 mm the scar known FZG load stages of >12 in the SRV apparatus. The test
width (d1) on the roller. Place the disk under a microscope and load was 1100 N with a test temperature of +80 °C, the
measure to the nearest 0.01 mm the track width (d2) on the disk frequency was 50 Hz under a stroke of 2000 mm. These results
(see Fig. 1). and statistical analysis of the interlaboratory tests in 2017 and
9.3.3 Although not specifically part of the procedure, when 2018 were filed as new research report.8
additional wear analysis is required, perform a profilometric
NOTE 9—The repeatability and reproducibility values depend on the oil
trace in the center and perpendicular to the wear track on the being used and its chemistry. The values stated in 11.2.1, 11.2.2, and
test disk and/or profilometric traces in the center of the wear 11.2.3 represent maximum values. In singular cases, smaller values were
scar on the roller in accordance with the profilometer manu- determined in RR tests.
facturer’s instructions. 11.2 Precision—The precisions of this test method, as de-
9.3.4 Measure the minimum and maximum coefficients of termined by statistical examination of the interlaboratory test
friction (fmin’fmax) and the coefficients at 15 min, 30 min, results, described in 11.1 are:
90 min, 120 min, and test end (f15, f30, f90, f120, fend) from 11.2.1 Average Width of Wear Scar on Roller d1:
computer screen, with a precision of 0.001. 11.2.1.1 Repeatability—The difference between successive
9.3.5 If a strong fluctuations (band width ≥0.005) in the results obtained by the same operator with the same apparatus
coefficient of friction are indicated in the charts at which the under constant operating conditions on identical test material
coefficient is measured, report additionally the sliding average would, in the long run, in the normal and correct operation of
out of an interval of the last 30 s and the band-width of the the test method, exceed the following value in only one case in
original signal within this interval. twenty.
9.3.6 The load carrying capacity can be additionally re-
ported as geometric contact pressure Pgeom. at test end accord- 0.073 mm
ing to the following equation: 11.2.1.2 Reproducibility—The difference between two
single and independent results obtained by different operators
Fn
P geom 5 (2) working in different laboratories on the identical test material
l 1d 1
would, in the long run, in the normal and correct operation of
where: the test method, exceed the following value in only in one case
Fn = normal force (test load), in twenty.
Pgeom = geometric contact pressure,
l1 = mean length of wear scar on roller, and 0.230 mm
d1 = mean width of wear scar on roller. 11.2.2 Average Width of Wear Track on Disk d2:
11.2.2.1 Repeatability—The difference between successive
10. Report results obtained by the same operator with the same apparatus
under constant operating conditions on identical test material
10.1 Report the following information: would, in the long run, in the normal and correct operation of
10.1.1 All parameters used to evaluate materials as follows: the test method, exceed the following value in only one case in
10.1.1.1 Test temperature, °C, twenty.
10.1.1.2 Test break-in load, N,
10.1.1.3 Test frequency, Hz,
10.1.1.4 Test stroke, mm, 8
Supporting data have been filed at ASTM International Headquarters and may
10.1.1.5 Constant load, N, be obtained by requesting Research Report RR:D02-1930. Contact ASTM Customer
10.1.1.6 Test roller material, Service at service@astm.org.
5
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0.100 mm working in different laboratories on the identical test material
11.2.2.2 Reproducibility—The difference between two would, in the long run, in the normal and correct operation of
single and independent results obtained by different operators the test method, exceed the following value in only one case in
working in different laboratories on the identical test material twenty.
would, in the long run, in the normal and correct operation of
the test method, exceed the following value in only one case in 0.03
twenty. 11.3 Bias—The evaluation of friction and wear properties of
0.290 mm lubricating oil by this test method has no bias because
11.2.3 Coeffıcient of Friction, f: coefficients of friction and wear scar and track widths can be
11.2.3.1 Repeatability—The difference between successive defined only in terms of the test method.
results obtained by the same operator with the same apparatus
under constant operating conditions on identical test material 12. Keywords
would, in the long run, in the normal and correct operation of 12.1 coefficient of friction; EP additives; EP lubricants;
the test method, exceed the following value in only one case in lubricating oil; oscillation; roller; SRV; wear
twenty.
0.01
11.2.3.2 Reproducibility—The difference between two
single and independent results obtained by different operators
APPENDIX
(Nonmandatory Information)
FIG. X1.1 Animated View through the Disk to the Contact Area
with the Wear Scar Visible on Roller
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