Professional Documents
Culture Documents
GAS CARBURIZING
(Process Specification)
1. SCOPE
1.1 This specification provides the required properties for gas carburized parts. It is intended to
replace Former CNH Company Carburizing Specifications listed in Table 1 and shall apply or be
specified for all gas carburizing applications.
1.2 All referenced Standards and test methods are to be latest issue unless otherwise specified.
2. APPLICATION
2.1 Gas carburizing introduces carbon into the surface of a part at an elevated temperature and when
the parts are quenched, produces a layer of hard, high carbon martensite at the material surface. Core
mechanical properties are also improved, similar to through hardening.
2.2 Commonly carburized materials are specified in MAT1051, MAT1052, and MAT1031. Typical
carburized parts are transmission shafts and gears. Carburizing provides improved bending and contact
fatigue strengths and wear resistant surfaces.
3. RELATED SPECIFICATIONS
CNH MAT1003 (86979049) Metallic Material Designations on Engineering Drawings
CNH MAT1031 (87021629) Low Carbon HR Bar
CNH MAT1051 (87021634) Low Carbon Steel Hot Rolled Alloy Bar
CNH MAT1052 (87021694) Carburized Gear Steel, Improved Quality, Low Carbon HR Alloy
CNH MAT4030D Design & Material Information, Gas Carburizing
CNH MAT4030S (87034353) Gas Carburizing, ISR
CNH ENPJ100 (86619032) Significant Characteristics
CNH MAT4110 (87034350) Metallurgical Quality, Ground, Hard Turned, Hard Hobbed Surfaces
ASTM E112 Standard Test Methods for Determining Average Grain Size
ASTM E140 Standard Hardness Conversion Tables for Metals (Relationship among Brinell, Vickers,
Rockwell, Rockwell Superficial, Knoop, and Scleroscope Hardnesses)
SAE J121 Decarburization in Hardened and Tempered Unified Threaded Fasteners
SAE J121M Decarburization in Hardened and Tempered Metric Threaded Fasteners
SAE J423 Methods of Measuring Case Depth
UNI 3245 Microscopic Exam - Ferrous Materials - Determination of Austenitic or Ferritic Grain Size
Unalloyed and Low Alloyed Steels
4 DEFINITIONS
4.1 EFFECTIVE CASE DEPTH (ECD)
ECD is the distance from the surface of the hardened case to the furthest point where a specified level of
hardness is measured.
4.1.1 For parts with a specified minimum surface hardness 55 HRC and above, the ECD is the distance
to where the microhardness converts to 50 HRC.
4.1.2 For parts with a specified minimum surface hardness less than 55 HRC, the ECD is the distance
to where the microhardness converts to five (5) HRC points lower than the minimum specified surface
hardness.
4.1.3 For pins and shaft diameters, where core hardness over 45 HRC is permitted on the drawing, the
ECD is the distance to where the microhardness converts to three (3) HRC points higher than the
maximum permitted core hardness. For gear teeth, where a core hardness above that specified in
Section 8.2.1 is permitted on the drawing, the ECD is the distance to where the microhardness converts
to three (3) HRC points higher than the maximum specified mid-tooth, half-height core hardness (Figure
1 Point Y) or as specified on the engineering drawing.
TCD is the distance from the part surface to a depth where chemical or physical properties of the case
and core can no longer be distinguished by microhardness or visual examination of etched samples.
Parts shall be clean, free of sulfur containing films from cutting fluids, and dry prior to heat treatment.
5.1 When more than one gear is integral with a shaft, the primary heat treatment goal shall be to
meet the case depth requirement for the gear with the greatest tooth thickness at the tooth half height,
unless otherwise specified on the drawing. As a result, the smaller tooth gears will generally have a
deeper case, but it should not exceed specified case depth requirements. In cases where the large tooth
gear case depth requirement will result in over-carburizing of the small tooth gear, specify individual case
depths for each integral gear on the drawing.
Although not a requirement of this specification, components are typically carburized at temperatures of
870 - 955oC (1600 - 1750oF). Prior to quenching the parts are cooled to 815 - 870oC (1500 - 1600oF).
Different processing temperatures and times can be used providing all of the mechanical and
microstructural requirements of this specification are met.
The carbon potential used during carburizing should be appropriate for achieving the specified case
properties, including the post-heat treatment surface carbon content and microstructure, see Table 2.
When a boost and diffuse process is utilized the maximum carbon potential during the boost phase shall
be 1.25%.
5.6.1 All parts shall be furnace tempered as soon as practical (within one hour is preferred) after they
reach 54°C (130°F) from quenching. Tempering shall be performed at a minimum temperature of 165°C
(330°F) for at least one hour at temperature. Higher temper temperatures may be required to achieve a
specific lower surface hardness. Tempering at 260-370°C (500-700°F) is not recommended unless
indicated on the drawing. Tempering can be verified by laboratory testing, See MAT4030D for additional
information. Required tempering is waived only if the drawing states: "TEMPERING NOT REQUIRED".
5.6.2 While not required the tempering temperature may be specified on the drawing. The
recommended drawing note for parts hardened to a surface hardness of 58-62 HRC or equivalent is
"FURNACE TEMPER AT 165°C MINIMUM TO A SURFACE HARNESS OF 58-62 HRC". See Section
14.3.3 example.
5.7 Sub-zero treatment (refrigeration) is generally not permitted except on steels with a nominal
nickel content of 2.0 wt% or greater.
6. MICROSTRUCTURE REQUIREMENTS
The core shall exhibit a microstructure consistent with quenching from a fully austenitic condition,
consisting principally of low carbon martensite produced from fine prior austenite grains. Bainite and
acicular ferrite, appropriate to the specified material grade and part section size, are permissible. Coarse
prior austenite grains (<No. 5 grain size per ASTM E112), pearlite and blocky ferrite are not permitted.
(A)
Standard Effective Case Depths and Surface Hardness Values
Table 3
and Recommended Gear Modules / DP
(B)(C)
Standard Effective Design Guide
Surface Hardness and Test Method
Case Depth Ranges Gear Module Gear DP
0.40-0.70 mm 89-91 HR15N or File Hardness #58 1.50-2.34 10.82-16.93
0.60-0.95 mm 80-82.5 HRA 2.35-3.54 7.16-10.81
0.80-1.25 mm 3.55-4.54 5.59-7.15
1.00-1.50 mm 58-62 HRC 4.55-5.69 4.47-5.58
1.25-1.80 mm 5.70-7.20 3.53-4.46
(A) Other case depth and/or surface hardness values may be specified on the drawing
(B) These are recommendations, heavier, lighter, or custom case depths may be specified on the drawing per local practice or historical usage.
(C) The mean gear module shall be used for effective case depth selection for bevel, spiral bevel, and hypoid gears.
8. HARDNESS REQUIREMENTS
8.1 SURFACE HARDNESS
The surface hardness shall be specified on the drawing. Recommended surface hardness and test
methods are given in Table 3. Lower hardness ranges may be specified. Lower load hardness scales
shall be used on shallower cases as the case might not support the Rockwell C (HRC) test load. HRC,
HRA, HR15N hardness conversions are provided in ASTM E140.
8.2 CORE HARDNESS
If necessary, a core hardness range shall be designated on the engineering drawing and should follow
the guidelines provided in MAT4030D. The specified core hardness should be consistent with the
material's hardenability, tooth size, part diameter, and the carburizing equipment used.
Where core hardness for either the root diameter or the mid-tooth, half height is specified on the
engineering drawing, the core hardness requirements above (Section 8.2.1) are superseded.
9. OTHER REQUIREMENTS
9.1.1 Portions of shafts and gears, such as areas to be welded or with threads, can be protected from
carburizing by using stop-off paint or other methods. Areas to be protected shall be indicated on the
drawing with a note stating "PROTECT INDICATED AREAS FROM CARBURIZATION". Protected areas
designated on the drawing are recommended to extend about 5 mm from the feature to be protected.
9.1.2 In protected areas the surface hardness shall be 42 HRC maximum (415 HV maximum) and
microscopic examination at 500X magnification shall not exhibit any evidence of carburization. SAE
J121 or SAE J121M may also be used to assess thread carburization.
"BORE MUST BE HARD" or "BORE MAY BE SOFT" should be placed on gear drawings as applicable.
Gears with a "BORE MUST BE HARD" requirement shall also specify a minimum ECD in the bore to be
the greater of either 0.45 mm or 50% of the minimum ECD specified for gear teeth. For ground bore
maximum metal removal and surface quality requirements, see Section 7.1.3. The surface hardness
shall be equivalent to that specified for the gear teeth, see Table 3. Where "BORE MAY BE SOFT" is
indicated, the ECD and surface hardness requirements are waived.
Figure 2.
Figure 1. Spline ECD Measurement Location
Effective Case Depth Measurement Locations
10.1 MICROSTRUCTURE
10.1.1 Case microstructure requirements and associated test methods are given in Table 2. Evaluate
case microstructure for gear teeth on the full tooth profile (tooth root mid-radius to tooth tip) and for shafts
at the surface of the largest diameter.
10.1.2 The core microstructure should be evaluated at 500X magnification. Evaluate core
microstructure for gear teeth at location X as shown in Figure 1 and for shafts at the mid-radius.
Reference pictures are given in MAT4030D and MAT4030S for comparison. Evaluation of core grain
size shall be per ASTM E112.
10.2.1.1 The effective case depth of a gear tooth is measured from the surface at the tooth half height (A-
A) and the tooth root fillet (B-B), see Figure 1. The root fillet traverse (B-B) is perpendicular to a line (C-
C) that intersects the top corner of the tooth land (E) and is tangent to the tooth surface at the root fillet
(D).
10.2.1.2 The ECD of a gear tooth may instead be measured at the pitch diameter. This alternate
measurement location must be noted on the drawing as follows: “TOOTH ECD MEASURED AT PITCH
DIAMETER”.
10.2.2 The ECD shall be measured at controlling locations after final stock removal. If for production
control the effective case depth is measured prior to grinding, the amount of anticipated stock removal
must be taken into account.
The effective case depth for spline teeth is measured from the root diameter surface towards the center
section (F-F), as shown in Figure 2.
10.4.2 Core hardness shall be measured by the method stated on the drawing or with a comparable
scale converted to the specified hardness. Core hardness of gear teeth shall be measured at both the
tooth center on the line between the tooth roots (Figure 1 point X) and at the mid-tooth, half-height
(Figure 1 point Y). The core hardness measurement location on a carburized shaft shall be the mid-
radius or as specified on the drawing.
Recommended effective case depth ranges and surface hardness based on gear tooth module or
diametral pitch are indicated in Table 3. Custom case depths may be specified on the drawing.
CNH Material
ALLOY HR ROUND, CNH MAT1051, GRADE A
Local Material
HR ROUND, ASTM A322, 8620
(Example note placed on drawing)
HEAT TREATMENT:
CARBURIZE AND DIRECT QUENCH PER CNH MAT4030
FURNACE TEMPER TO A SURFACE HARDNESS OF 80-82.5 HRA
EFFECTIVE CASE DEPTH 0.60-0.95
CNH Material
ALLOY CD ROUND, CNH MAT1050, GRADE A
Local Material
CD ROUND, ASTM A108, 8620
(Example note placed on drawing)
HEAT TREATMENT:
CARBURIZE AND DIRECT QUENCH PER CNH MAT4030
FURNACE TEMPER TO A SURFACE HARDNESS OF 80-82.5 HRA
TOTAL CASE DEPTH 0.90-1.45
14.4.1 Gear Design: Ground Gear Teeth; Design Requirement; Gear Module = 3
CNH Material
ALLOY HR ROUND, CNH MAT1052, Gr BG, CL2
Local Material
SEE CNH MAT1052
HEAT TREATMENT – PROCESSING (Note on Drawing)
FORGE
NORMALIZE PER CNH MAT4070
GAS CARBURIZE AND DIRECT QUENCH PER CNH MAT4030
FURNACE TEMPER TO A SURFACE HARDNESS 80-82.5 HRA
EFFECTIVE CASE DEPTH 0.60-0.95 mm MEASURED ON GEAR TEETH AFTER GRINDING
14.4.2 Gear Design: Non-Hard Finished Gear Teeth; Design Requirement; Gear Module = 3
CNH Material
ALLOY HR ROUND, CNH MAT1052, Gr BG, CL2
Local Material
SEE CNH MAT1052
HEAT TREATMENT – PROCESSING (Note on Drawing)
FORGE
NORMALIZE PER CNH MAT4070
GAS CARBURIZE AND DIRECT QUENCH PER CNH MAT4030
FURNACE TEMPER TO A SURFACE HARDNESS 80-82.5 HRA
EFFECTIVE CASE DEPTH 0.60-0.95 mm MEASURED ON GEAR TEETH
CNH Material
ALLOY HR ROUND, CNH MAT1052, Gr AG-S3, AG-S4, CL2
Local Material
SEE CNH MAT1052
HEAT TREATMENT – PROCESSING (Note on Drawing)
FORGE
NORMALIZE PER CNH MAT4070
GAS CARBURIZE AND DIRECT QUENCH PER CNH MAT4030
FURNACE TEMPER TO A SURFACE HARDNESS 80-82.5 HRA
EFFECTIVE CASE DEPTH 0.60-0.95 mm MEASURED ON GEAR TEETH AFTER GRINDING
MID-RADIUS CORE HARDNESS 20-25 HRC MEASURED ON DIA. 23.5