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solidi
physica
Phys. Status Solidi B 247, No. 2, 269–272 (2010) / DOI 10.1002/pssb.200945513
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b
www.pss-b.com
basic solid state physics
Auxetic cellular structures through
selective electron-beam melting
,1 2 2 2
J. Schwerdtfeger* , P. Heinl , R. F. Singer , and C. Körner
1
Institute of Advanced Materials and Processes (ZMP), University of Erlangen-Nürnberg, Dr.-Mack-Str. 81, 90762 Fürth, Germany
2
Institute of Materials Science and Technology (WTM), University of Erlangen-Nürnberg, Martensstr. 5, 91058 Erlangen, Germany
This paper is concerned with the build up and characterization objects. Using SEBM we are able to produce structures of
of well-defined auxetic structures (negative Poisson ratio) from arbitrary geometry in a well-defined manner. Here, we
Ti-6Al-4V through selective electron-beam melting (SEBM). introduce a self-designed 3D-auxetic structure and determine
SEBM is a rapid prototyping/manufacturing technique allow- its mechanical properties. We also address the dependence of
ing for the direct translation of CAD models to real world Young’s modulus on relative density.
1 Introduction Auxetic cellular structures have in a highly controlled manner. This not only opens up a whole
attracted considerable interest in recent years due to their new field of possible structures, but allows for a high degree
unique mechanical properties resulting from a negative of control over the resulting mechanical properties. In this
Poisson’s ratio n [1–4]. The value of the Poisson’s ratio paper we present a self-designed three-dimensional auxetic
controls the elastic behavior of a material to the same extent structure and its build up in the SEBM process using
as, for example, the Young’s modulus E. A negative value of Ti-6Al-4V. Results for the mechanical characterization of
n leads to higher indentation resistance [5], shear resistance, the structure by compression testing are shown.
[6] and fracture toughness [7] to name only a few affected
properties. Potential applications for metal auxetics might be 2 The structure This is built up from basic elements
found in a wide area of applications as these materials allow that can be envisaged as an inverted tetrapod. These elements
for new combinations of material properties and present a are arranged in building blocks that themselves are used
new class of materials [6]. To give an example, in high- to fill a plane. The planes are stacked on top of each other
temperature systems the combination of low forces due to by turning the stacking layer by 608 (see also Fig. 1a).
thermal expansion (low E) and high shear resistance are of The resulting structure has an abab stacking order and is
great interest. Previously, auxetic cellulars have been mainly anisotropic, which makes it necessary to determine the
produced through volumetric compression of conventional mechanical properties in different directions. The coordinate
open porous polymer or metal foams (e.g. [8, 9]). The system used in the following to describe the orientation of
volumetric compression results in a complex microstructure the structure is shown in Fig. 1b.
that leads to negative Poisson ratios. The exact mechanisms
are still a matter of debate, but involve the unhinging of 3 Experimental The samples for mechanical testing
crumbled cells and rotation of rigid units (e.g. [10, 11]) were built in a SEBM system (ARCAM A2) using Ti-6Al-
within the microstructure as well as possibly more 4V powder with a maximum particle size of 105 mm and a
complicated modes of deformation [12]. Unfortunately, this mean particle diameter of 70 mm. In the process, parts are
compression process allows for very limited control over the built layerwise by depositing 100-mm layers of metal powder
resulting mechanical properties including n. However, by on a steel start plate using a rake system and melting the
using selective electron-beam melting (SEBM) we are able powder in the desired places with an electron beam gun
to build well-defined auxetic cellulars of arbitrary geometry (acceleration voltage 60 kV). After each layer the start plate
solidi
physica
status
270 J. Schwerdtfeger et al.: Auxetic cellular structures through selective electron beam melting
is lowered and a new powder layer is deposited. The whole samples were build up in 3 directions to avoid differences
process produces low impurity concentrations and good in their mechanical behavior caused by the formation process
mechanical properties comparable to cast material or better. itself. For compression, an updated Instron testing machine
A more detailed description of the process can, for example, (Inspekt Retrofit 100) and a crosshead speed of 1 mm/min
be found in Ref. [13]. was used. Strain was measured by an extensometer setup to
The geometric data of the part to be built are given as a measure the distance between the compression stamps.
CAD model. In the present study the relative density of the The Poisson’s ratio n was determined on larger samples
structures was varied by changing the energy deposited by as this allowed for better accuracy (for exact dimensions see
the electron beam per unit length (constant scan speed of Table 2). To measure the transverse strain an extensometer
160 mm/s; variable beam current of 1.9–6 mA). More energy was attached to the sample using two sharp blades. Then they
translates to a larger amount of metal to be molten. This were strained in compression with a stress up to 1.7 MPa,
results in thicker struts and higher relative densities. Relative which was situated within their elastic range and the
densities were determined geometrically, by determining resulting transverse strains measured. On both types of
sample dimensions using callipers and weighing. samples, care was taken to ensure contact planes with the
For the determination of the Young’s modulus E compression stamps as flat as possible by polishing their
rectangular samples of slightly varying dimensions were faces before testing.
used. For different orientations of the structure different
Table 1 Test specimen dimensions (compression).
dimensions were necessary in order to not cut through cells.
The exact dimensions of the compression samples are listed orientation height [mm] width [mm] thickness [mm]
in Table 1. The dimensions of a single inverted tetrapod
given by the CAD-file were A ¼ 3.75 mm and B ¼ 3 mm (see Orientation 1 39.5 17.4 17.5
Orientation 2 39.3 17.5 17.5
Fig. 1a). Four different line energies were used to build the
Orientation 3 39.6 17.4 17.5
structures resulting in four different relative densities. All
solidi
physica
status
272 J. Schwerdtfeger et al.: Auxetic cellular structures through selective electron beam melting