Profile Plus

Series ICP
The Affordable PMT Based ICP
The Profile Plus Family of ICP Spectrometers
Profile Plus makes ICP simple and very fast. This system
will quickly become your laboratory workhorse, not a
research project.
Need flexibility?
The Profile’s “any element, any wavelength” capability makes
it the system of choice. All internal optical components are
stationary, resulting in extremely stable spectral output. With
this patented design, the Profile’s detector is moved at very high
speed from the center of one wavelength to the next (on-peak
High Performance Optics
With ICP emission, elemental concentrations are determined by
measuring light intensities at discrete wavelengths. Because the
ICP is a very high temperature source, it emits many thousands
of wavelengths — a “complex spectrum.” The job of the
spectrometer’s optics is to make sense of this information and the
best way to do this is to use an Echelle optical system with a large
output format. In fact, Leeman Labs was the first ICP spectrometer
manufacturer to employ this design.
integration). As a result, low concentrations and complex samples
are easy because the location of the analyte peak is known before
the analysis is carried out. Time is spent measuring the peaks, not
searching to find them. When compared to CCD based sequential
ICPs, the Profile Plus provides up to four times the analysis speed
and has fewer interferences.
Versatile Design
Profile Plus is the most versatile family of ICPs in the industry and
can be configured for almost any application.
Profile’s Echelle optics disperse the spectrum, widely separating
the wavelengths thereby minimizing interferences and the need
for interelement corrections. This design improves resolution —
the ability of a spectrometer to distinguish between two closely
spaced wavelengths — without reducing the amount of light
that gets to the detector. The result is an instrument that can give
high resolution and low detection limits at the same time — a feat
impossible for conventional and small format echelle designs!
Axial, Radial, or Dual View
Profile’s Echelle design is ideally suited to allow observation of the plasma in
the radial, axial, or dual view modes. Its elegant entrance optics provide this
flexibility without the need for complex lens/aperture systems, as required
by other ICP systems. With Profile Plus, fewer optical surfaces mean more
light throughput and therefore lower detection limits.

The traditional radially viewed plasma has a well-deserved reputation

for robustness and is the configuration of choice for many applications.
Providing detection limits that are approximately ten times better than a
radial system, the axial plasma has taken ICP into application areas that were
previously difficult, if not impossible.

Combining the best features

of axial and radial viewing is
the dual view system. Capable
of running in both radial and
axial mode (on an element-
by-element basis in a single
method), the dual view is able
to analyze virtually any sample
for ultra-trace, trace and major
elements without the need for
multiple sample dilutions.

The Profile Plus combines

superb analytical capability,
versatility, and performance
into an easy-to-use benchtop
design.

The Profile’s design uses fewer optical surfaces, maximizing

light throughput for superior detection limits.

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Easy To Use Sample
Introduction System
Traditionally, most operating errors occur in the sample introduction The Profile Auto-Align Torch System eliminates the guesswork usually
encountered when installing torches and spray chambers.
area. The Profile Plus family has a new Auto-Align Torch System that
eliminates the guesswork usually encountered when installing torches
and spray chambers. Designed with the users’ needs in mind, the Auto-Align Torch
precisely repositions the torch, whenever removal and replacement is needed. Every
operator will be able to perfectly position the torch every time; consistently generating
high quality results.

The Auto-Align Torch System makes it easy to configure your Profile Plus to handle even
the most difficult analytical applications. A wide selection of sample introduction hardware
is available, including systems for use with aqueous, organic and HF samples. Each is easily
integrated with the Auto-Aligh Torch system.

High Efficiency ICP Power Supply

Incorporated into the Profile Plus is a state-of-the-art power supply. Its fast switching
design compensates for fluctuations of incoming power, resulting in outstanding stability
without requiring expensive line conditioners. This means faster warm-ups, and superior
analytical reliability.

The power supply is built into the body of the instrument, resulting in a compact,
benchtop spectrometer. This reduces laboratory space, to an absolute minimum.

The Profile Plus uses the Teledyne Leeman Labs 40.68 MHz free running oscillator for
superior tolerance to a wide variety of sample types, including high solids and organics.
Software Element Selection

Teledyne Leeman Labs’ WinICP software is designed to fully control

the analytical process — from Method Development to Final Report
Generation — providing the right amount of flexibility, without the
complexity. In the routine analytical or research environment, WinICP
has the features along with the ease-of-use necessary to get the job
done quickly and efficiently.

Element Selection
Select an element from the periodic chart. Choose the best wavelength
from the list or any other wavelength. Use as many (or as few) defaults Scan Page
as you wish to streamline data entry for each element — all standard
and check standard concentrations, as well as integration times can be
entered with a single button.

Scan Page
Simply scan a standard and sample to quickly estimate a concentration,
set a background point or identify possible interferences.

Calibration
Automatically run a calibration using up to 10 standards and 7 check
standards by placing the standards into the autosampler and initiating
the cycle. Calibration plots can be viewed quickly and easily.
Calibration
Select the autosampler rack and specify the number of samples to be
analyzed and the Profile Plus goes to work. WinICP also lets you turn
elements on or off without having to open the method.

Generate reports with as much or as little data as you wish. Take

advantage of WinICP’s ability to output data in a variety of formats,
making compatibility with other software applications straightforward.

Sample Analysis Report Generation

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 Specifications
Wavelength Range 177 – 800 nm
Resolution <0.008 nm @ 200 nm
Detector Type High Speed PMT
RF Generator Type 40.68 MHz, Free-Running
RF Generator Output 2 kW
Peristaltic Pump 4 Channel, 12 Roller

Spectrometer/ICP Source Electrical Requirements

Mounted on a single base chassis on 1” (25 mm) rubber feet Grounded Single-Phase Power Supply 190 – 230 V, 30A, 50/60Hz
Length Base 52.2” (1326 mm) Outlet Type Hubbell Twist (NEMA L6-30R)
Additional Outlets:
Depth Base 21.7” (550 mm) 115V, 15A, 60 Hz or 220 V, 10A, 50Hz
(for computer, monitor and printer)
Height (to top of chimney) 29” (735 mm)
Diameter of Chimney 6” (152 mm)
Weight 230 lb (104 kg)

Environmental Conditions Exhaust

Temperature 59 – 86 F(15 – 30 C)
o o
Exhaust Draw 100 ft3/min (2.83 m3/min)
Maximum Temperature Variation 3.6 oF/h (2 oC/h) Vent Diameter 6 – 8 “ (152 – 203 mm)
20 – 80% 3 – 4” (76 – 102 mm)
Relative Humidity Vent Height
(non-condensing) above chimney

Water Recirculator Gases

Length 16.5” (420 mm) Argon (required)
Height 12.5” (317 mm) Purity 99.995% minimum
Depth 18” (475 mm) Delivery Pressure 80 – 95 psi (560 – 630 kPa)
Weight 50 lb (12 kg) Nitrogen (optional for purge)
Purity 99.995% minimum
Delivery Pressure 80 – 95 psi (560 - 630 kPa)
Site Planning Information
More than Just an ICP
As you know, beyond the initial purchase price lies the true cost of
ownership, and that’s where the Profile Plus shines. Why? Because
Teledyne Leeman Labs builds these instruments to last.
After Sales Support
Telephone Support:  Our technicians and support chemists
can resolve most application, operation, maintenance, and
troubleshooting questions over the phone. A toll free hot line
staffed with specialists trained in emergency repair is available to
assist you.
Remote Diagnostics:  Remote diagnostics software provides our
technicians and scientists with the ability to access an instrument
via the internet. Specialist support is always at hand.
Service Agreements
A variety of optional service agreements are available including:
Full Maintenance: A set rate comprehensive package that allows
the user to budget for each instrument under the agreement.
Limited Maintenance:  Allows the user to budget for costs
associated with replacement parts and technical support. This
agreement is designed for the user who performs their own
maintenance.
Preventative Maintenance:  Designed to keep your equipment
in peak working condition and to note any items that may lead to
future problems.
Standards
Teledyne Leeman Labs prepares and validates a line of standards
and reagents for both sample digestion and analysis (Plasma-
Pure). Plasma-Pure standards provide analysts with accurate,
stable standards, made from high purity materials (traceable
to NIST standards). With Teledyne Leeman Labs you have an
analytical partner, ready to provide support for the chemistry, as
well as the mechanics, of your application.
You’re in Good Company
Are you getting the impression that we stand solidly behind
our instrumentation? You’re right. Our confidence comes from
knowing that we haven’t cut corners in the design, maintenance
or testing of our products. We build our instruments to the most
exacting specifications. We build them to do the job, and to do it
right. It’s a reputation that we worked hard to earn, and that we
work harder to maintain.
So what kind of companies and organizations rely on analytical
instruments from Teledyne Leeman Labs? Our customers come
from both the public and private sector. They are leaders in
industry, government, and academia. Add to the list hundreds
of cities, municipalities, and institutions of higher learning and
you start to get a sense of the family of Teledyne Leeman Labs
customers, and the impact that they have on our society.
We continue to invest heavily in research and development and
look forward to providing our customers with additional products
and technology advances in the years ahead.
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 ICP Spectrometers Mercury Analyzers DC Arc Spectrometers Inorganic Standards

6 Wentworth Drive
Hudson, NH 03051 U.S.A.

Tel: 603.886.8400
Fax: 603.886.9141
Email: LeemanLabsinfo@teledyne.com

www.leemanlabs.com

MADE IN THE USA Copyright © 2012