NAMA : AAN TRI SURYA RAHMAN

NIM : G30119068

KELAS : B (GENAP)

TUGAS : STATISTIK DAN KEMOMETRI

WORKSHEET 1

Box-Behnken Design
Design Summary
Factors: 3 Replicates: 1
Base runs: 15 Total runs: 15
Base blocks: 1 Total blocks: 1
Center points: 3
Design Table
Run Blk A B C
1 1 -1 -1 0
2 1 1 -1 0
3 1 -1 1 0
4 1 1 1 0
5 1 -1 0 -1
6 1 1 0 -1
7 1 -1 0 1
8 1 1 0 1
9 1 0 -1 -1
10 1 0 1 -1
11 1 0 -1 1
12 1 0 1 1
13 1 0 0 0
14 1 0 0 0
15 1 0 0 0

WORKSHEET 1

Response Surface Regression: DD (%) versus [NaOH], Suhu, waktu

Coded Coefficients
Term Coef SE Coef T-Value P-Value VIF
Constant 89.09 2.52 35.37 0.000
[NaOH] 2.82 1.54 1.83 0.127 1.00
Suhu 0.92 1.54 0.60 0.576 1.00
waktu -2.97 1.54 -1.93 0.112 1.00
 [NaOH]*[NaOH] -17.60 2.27 -7.75 0.001 1.01
Suhu*Suhu -7.07 2.27 -3.12 0.026 1.01
waktu*waktu 3.69 2.27 1.63 0.165 1.01
[NaOH]*Suhu -0.08 2.18 -0.04 0.973 1.00
[NaOH]*waktu 1.71 2.18 0.78 0.469 1.00
Suhu*waktu 1.16 2.18 0.53 0.618 1.00
Model Summary
S R-sq R-sq(adj) R-sq(pred)
4.36235 94.16% 83.65% 39.15%
Analysis of Variance
Source DF Adj SS Adj MS F-Value P-Value
Model 9 1534.60 170.51 8.96 0.013
Linear 3 141.26 47.09 2.47 0.176
[NaOH] 1 63.79 63.79 3.35 0.127
Suhu 1 6.79 6.79 0.36 0.576
waktu 1 70.69 70.69 3.71 0.112
Square 3 1376.23 458.74 24.11 0.002
[NaOH]*[NaOH] 1 1143.57 1143.57 60.09 0.001
Suhu*Suhu 1 184.76 184.76 9.71 0.026
waktu*waktu 1 50.38 50.38 2.65 0.165
2-Way Interaction 3 17.10 5.70 0.30 0.825
[NaOH]*Suhu 1 0.02 0.02 0.00 0.973
[NaOH]*waktu 1 11.70 11.70 0.61 0.469
Suhu*waktu 1 5.38 5.38 0.28 0.618
Error 5 95.15 19.03
Lack-of-Fit 3 56.55 18.85 0.98 0.542
Pure Error 2 38.60 19.30
Total 14 1629.75
Regression Equation in Uncoded Units
DD (%) = -1218 + 21.14 [NaOH] + 14.05 Suhu - 39.6 waktu - 0.1760 [NaOH]*[NaOH]
- 0.0707 Suhu*Suhu + 3.69 waktu*waktu - 0.0008 [NaOH]*Suhu + 0.171 [NaOH]*waktu
+ 0.116 Suhu*waktu
WORKSHEET 1

Response Surface Regression: Yield (%) versus [NaOH], Suhu,

waktu
Coded Coefficients
Term Coef SE Coef T-Value P-Value VIF
Constant 86.84 3.48 24.93 0.000
[NaOH] 2.98 2.13 1.40 0.221 1.00
Suhu 2.39 2.13 1.12 0.313 1.00
waktu -4.13 2.13 -1.94 0.110 1.00
[NaOH]*[NaOH] -20.59 3.14 -6.56 0.001 1.01
Suhu*Suhu -3.13 3.14 -1.00 0.365 1.01
waktu*waktu 1.29 3.14 0.41 0.697 1.01
[NaOH]*Suhu -7.75 3.02 -2.57 0.050 1.00
[NaOH]*waktu -0.68 3.02 -0.22 0.832 1.00
Suhu*waktu -0.58 3.02 -0.19 0.855 1.00
Model Summary
S R-sq R-sq(adj) R-sq(pred)
6.03367 92.04% 77.71% 0.00%
Analysis of Variance
Source DF Adj SS Adj MS F-Value P-Value
Model 9 2104.82 233.87 6.42 0.027
 Linear 3 253.76 84.59 2.32 0.192
[NaOH] 1 71.28 71.28 1.96 0.221
Suhu 1 45.70 45.70 1.26 0.313
waktu 1 136.79 136.79 3.76 0.110
Square 3 1607.64 535.88 14.72 0.006
[NaOH]*[NaOH] 1 1565.47 1565.47 43.00 0.001
Suhu*Suhu 1 36.08 36.08 0.99 0.365
waktu*waktu 1 6.18 6.18 0.17 0.697
2-Way Interaction 3 243.42 81.14 2.23 0.203
[NaOH]*Suhu 1 240.25 240.25 6.60 0.050
[NaOH]*waktu 1 1.82 1.82 0.05 0.832
Suhu*waktu 1 1.35 1.35 0.04 0.855
Error 5 182.03 36.41
Lack-of-Fit 3 170.91 56.97 10.25 0.090
Pure Error 2 11.12 5.56
Total 14 2286.85
Regression Equation in Uncoded Units
Yield (%) = -1480 + 32.89 [NaOH] + 11.26 Suhu + 0.5 waktu - 0.2059 [NaOH]*[NaOH]
- 0.0313 Suhu*Suhu + 1.29 waktu*waktu - 0.0775 [NaOH]*Suhu - 0.068 [NaOH]*waktu
- 0.058 Suhu*waktu
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Response Surface Regression: Derajat Putih versus [NaOH], Suhu,

waktu
Coded Coefficients
Term Coef SE Coef T-Value P-Value VIF
Constant 75.55 4.21 17.95 0.000
[NaOH] 0.22 2.58 0.09 0.935 1.00
Suhu 6.32 2.58 2.45 0.058 1.00
waktu -12.91 2.58 -5.01 0.004 1.00
[NaOH]*[NaOH] -14.14 3.79 -3.73 0.014 1.01
Suhu*Suhu -11.12 3.79 -2.93 0.033 1.01
waktu*waktu 8.12 3.79 2.14 0.085 1.01
[NaOH]*Suhu 9.92 3.64 2.72 0.042 1.00
[NaOH]*waktu -10.53 3.64 -2.89 0.034 1.00
Suhu*waktu 3.51 3.64 0.96 0.380 1.00
Model Summary
S R-sq R-sq(adj) R-sq(pred)
7.28890 93.80% 82.64% 16.34%
Analysis of Variance
Source DF Adj SS Adj MS F-Value P-Value
Model 9 4019.31 446.59 8.41 0.015
Linear 3 1653.66 551.22 10.38 0.014
[NaOH] 1 0.40 0.40 0.01 0.935
Suhu 1 319.67 319.67 6.02 0.058
waktu 1 1333.60 1333.60 25.10 0.004
Square 3 1479.28 493.09 9.28 0.017
[NaOH]*[NaOH] 1 737.76 737.76 13.89 0.014
Suhu*Suhu 1 456.40 456.40 8.59 0.033
waktu*waktu 1 243.58 243.58 4.58 0.085
2-Way Interaction 3 886.36 295.45 5.56 0.048
[NaOH]*Suhu 1 393.63 393.63 7.41 0.042
[NaOH]*waktu 1 443.52 443.52 8.35 0.034
Suhu*waktu 1 49.21 49.21 0.93 0.380
Error 5 265.64 53.13
Lack-of-Fit 3 217.25 72.42 2.99 0.260
Pure Error 2 48.39 24.20
Total 14 4284.95
Regression Equation in Uncoded Units
Derajat Putih = -1012 + 9.17 [NaOH] + 16.21 Suhu - 17.3 waktu -
0.1414 [NaOH]*[NaOH]
- 0.1112 Suhu*Suhu + 8.12 waktu*waktu + 0.0992 [NaOH]*Suhu
- 1.053 [NaOH]*waktu + 0.351 Suhu*waktu
Fits and Diagnostics for Unusual Observations
Derajat
Obs Putih Fit Resid Std Resid
9 90.01 82.65 7.36 2.02 R
 12 62.12 69.47 -7.35 -2.02 R

R Large residual
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Contour Plot of DD (%) vs Suhu, [NaOH]

WORKSHEET 1

Contour Plot of Yield (%) vs Suhu, [NaOH]

WORKSHEET 1

Contour Plot of Derajat Putih vs Suhu, [NaOH]

WORKSHEET 1

Surface Plot of DD (%) vs Suhu, [NaOH]

WORKSHEET 1

Surface Plot of Yield (%) vs Suhu, [NaOH]

WORKSHEET 1

Surface Plot of Derajat Putih vs Suhu, [NaOH]