Sample Code: SRPL121-001

compound is partially soluble

SANTO RIGHELLO PVT LTD

Solvent: cdcl3
SA-Varian 400MHz NMR
Date: Dec 14 2021

9 8 7 6 5 4 3 2 1 0 ppm
4.00

4.02
Plotname: SRPL121-001_PROTON_20211214_01_plot01
Sample Code: SRPL121-001

3.764
3.757
3.754
3.747
3.741
3.731

1.870
1.862
1.854
1.845
1.838

1.528
compound is partially soluble
SANTO RIGHELLO PVT LTD

Solvent: cdcl3
SA-Varian 400MHz NMR
Date: Dec 14 2021

4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 ppm

4.00

4.02
Plotname: SRPL121-001_PROTON_20211214_01_plot02
 INDEX FREQUENCY PPM HEIGHT
compound is partially soluble 1 2901.8 7.260 115.1
SANTO RIGHELLO PVT LTD 2 1504.4 3.764 9.0
3 1501.8 3.757 7.0
exp1 PROTON 4 1500.2 3.754 9.4
5 1497.8 3.747 22.8
6 1495.4 3.741 10.3
SAMPLE PRESATURATION 7 1491.2 3.731 9.5
date Dec 14 2021 satmode n 8 747.6 1.870 9.5
solvent cdcl3 wet n 9 744.3 1.862 10.8
file /home/spark-a~ SPECIAL 10 741.0 1.854 26.7
uto/data/2021/Dec/~ temp 25.0 11 737.5 1.845 11.1
12 734.4 1.838 9.3
SRPL121-001_202112~ gain 22 13 610.8 1.528 40.0
14_01/SRPL121-001_~ spin 20 14 3.1 0.008 3.8
PROTON_20211214_01~ hst 0.008 15 0.0 0.000 98.1
.fid pw90 8.900
ACQUISITION alfa 10.000
sw 7183.9 FLAGS
at 4.000 il n
np 57472 in n
fb 4000 dp y
bs 2 hs nn
d1 1.000 PROCESSING
nt 512 lb 0.50
ct 20 fn not used
TRANSMITTER DISPLAY
tn H1 sp -793.9
sfrq 399.689 wp 7183.7
tof 799.4 rfl 794.1
tpwr 60 rfp 0
pw 4.450 rp 115.1
DECOUPLER lp 0
dn C13 PLOT
dof 0 wc 268
dm nnn sc 0
decwave W40_one-NM~ vs 1805
R-9 th 3
dpwr 34 ai ph
dmf 29412

Plotname: SRPL121-001_PROTON_20211214_01_plot03