Professional Documents
Culture Documents
Vista II Series
Gas Chromatograph
ABB Analytical
Analytical
ABB Process Analytics
NOTICE
A1 January 1998
B1 March 1998
C1 July 1999
All pages C1
The revision status is noted at the bottom of each page of this manual.
2000-SVC, C1 i
For further information or assistance contact:
ii 2000-SVC, C1
TABLE OF CONTENTS
SECTION 1. INTRODUCTION
SECTION 2. TROUBLESHOOTING
2000-SVC, C1 iii
TABLE OF CONTENTS (continued)
iv 2000-SVC, C1
TABLE OF CONTENTS (continued)
SECTION 4. REPAIR
2000-SVC, C1 v
TABLE OF CONTENTS (continued)
vi 2000-SVC, C1
TABLE OF CONTENTS (continued)
2000-SVC, C1 vii
TABLE OF CONTENTS (continued)
SECTION 6. DRAWINGS
viii 2000-SVC, C1
LIST OF ILLUSTRATIONS
2000-SVC, C1 ix
LIST OF ILLUSTRATIONS (continued)
x 2000-SVC, C1
LIST OF ILLUSTRATIONS (continued)
2000-SVC, C1 xi
For further information or assistance contact:
xii 2000-SVC, C1
GLOSSARY
Auto Zero procedure bringing the detector signal as close to electrical zero as
possible
baseline analog reference point from which peak height or peak area is
measured on a chromatogram; the detector signal level at which no
components are detected
calibration run analysis that involves injecting a standard sample consisting of specific
components whose concentrations and elution sequences are known
CE Mark certification process and marking which denote that analyzer complies
with applicable new approach directives within the European Union
Chroma I/O Chromatographic Input/Output PCB; provides the interface between the
analog domain of the gas chromatographic analyzer and the digital
domain of the controller
components peaks, parameters or ratios that are being measured or calculated from
a chromatographic analysis
cursor keys front panel control keys marked with directional arrows
default values assigned parameters the controller will assume unless the operator
redefines the values
2000-SVC, C1 G-1
Digital I/O Digital Input/Output PCB; enables the use of additional stream valves
and/or alarm sensors
DIP switch PCB switch that is used to set values through hardware instead of
software
drift variances from the baseline or the norm; generally associated with
uncontrolled or unwanted changes in pressure or temperature
elution time amount of time from the start of analysis that it takes to fully detect a
peak
E2PROM Electrically Erasable Programmable Read Only Memory; used for the
safe storage of tables (sometimes written E2PROM or EEPROM)
field highlighted area on CRT screen where data entry and modification are
allowed; data entry is ended (terminated) by filling the field with
characters or by pressing ENTER or any soft key or cursor key
Gate On/Off time-coded function command which turns on and off the collection of
data from the detector
GC Gas Chromatagraph
Help key front panel control key used to access information pertaining to the
current screen display content
highway address numbers from one to 32 that uniquely identify remote GCC’s
host link serial communications link which allows the transmitting of analysis
results to the host computer
G-2 2000-SVC, C1
integer whole number that does not contain decimal points
I/O Input/Output
LO COMM Local Communication Module PCB; optional PCB in the GCC that
makes the analyzer communications network possible (sometimes
written LOCOM)
method table operator-entered data specifying the name, retention time, key
designation, response factor, low and high limits, and calibration
concentrations of the various elements of an analysis; also specifies
when, how, and under what conditions the method of data collection is
to proceed
noise any unwanted signal superimposed upon a useful signal which tends to
obscure the desired information
“Panic” key nickname for the F1 soft key; pressing this key will return the screen
display to the Background screen without changing any current values in
memory; may need to be pressed several times consecutively,
depending on where the current screen is in relation to the Background
screen
peak area method of measurement in which total peak area beneath the peak
envelope is used to calculate the concentration
Post Analysis portion of the controller program that calculates the value for the
routine components from the collected data, after completion of the analysis
2000-SVC, C1 G-3
psig pounds per square inch gauge
redundant means by which a remote GCC can be connected to one or two central
highways devices by two separate, but equivalent, data highways
retention time time, from start of analysis, that a peak maximum elutes from the
column
selection field horizontal screen display; Right and Left cursor keys move through
options displayed on screen; select a field by exiting it with Up or Down
cursor key
Soft Keys four front panel control keys directly under the screen, (F1, F2, F3, F4)
stream purging procedure allowing the next stream sample to be analyzed to flow
continuously through the sample loop of the injection valve in
preparation for the next sample injection and analysis cycle
stream step TCF command that permits the next stream sample to purge the sample
loop during the remainder of the present cycle
TCF Time-Coded Function; entry in method table that defines what action is
to be performed (e.g. Valve ON) at what time in the analysis
text field field that accepts data entered with all non-terminating keys
G-4 2000-SVC, C1
VNSA VistaNET Name Service Administrator; PC software that serves as the
address book for the VistaNET
watchdog timer hardware circuit alarm that indicates when the software fails to cycle
through its entire task structure within a set period of time
2000-SVC, C1 G-5
CAUTION
Beginning in January 1996, all analyzers bearing the CE Mark imprint on their nameplates have
EMC shielding that meets the requirements for CE Mark. When working with one of these analyz-
ers, you must handle it carefully to avoid damaging the shielding. If any shielding becomes dam-
aged or is removed from the analyzer, new shielding must be installed to maintain the CE mark
certification.
ABB Process Analytics has designed “Total Envelope Protection” into its analyzers. The basic
enclosure itself (which is fabricated from sheet steel with all seams welded), when properly
“grounded” or “earthed”, becomes the first barrier of protection from emissions that could radiate
from the unit. In addition, the enclosure also provides a high level of immunity from electromag-
netic interference (EMI) which could affect the performance of the analyzer.
In order for the analyzers produced by ABB Process Analytics to maintain their tested integrity, the
installation methods employed are of equal importance. The grounded enclosure produces a
Faraday Shield around the electronic components, detection systems, and other sensitive compo-
nents which could generate EMI or be affected by EMI. An extension of this Faraday shield must
be carried throughout the installation scheme.
G-6 2000-SVC, C1
SECTION 1. INTRODUCTION
This manual, which provides troubleshooting and repair information, applies to all
versions of the Vista II Series Gas Chromatograph. For complete information on the
analyzer, use this manual together with “Operator's Manual for the Vista II Series
Gas Chromatograph,” manual number 2000-OPS (referred to in this manual as the
Operator's Manual).
The Vista II Series Gas Chromatograph separates and measures the individual
components of gas or liquid samples. It automatically samples and analyzes
process streams, using the analyzer's Gas Chromatographic Controller (GCC) to
control analytical functions.
The analyzer (see Figure 1-1) may be mounted on a wall, a rack, or a floor stand. It
includes an insulated, air-heated Oven Compartment, a Gas Chromatographic
Controller (GCC), a Purge Air Panel, and a Pressure Control Panel.
Gas
Chromatographic
Controller
(GCC)
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1 2 3 4 5 6 7 8 9 0
F F F F FLAME
EN
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OUT HE 10 V
1 2 3 4 R LP
Pressure
Purge Air Control
Panel Panel
Oven
Compartment
Nameplate
(on side
or front)
2000-SVC, C1 1-1
The Oven Compartment houses an isothermal oven which contains the analytical
columns, the detectors, and the sample valves.
The GCC contains the card cage with PCBs, the Digital Temperature Controller
(DTC), and one or more of the following detector amplifiers: flame ionization (FID),
thermal conductivity (TCD), and flame photometric (FPD). The front panel has a
liquid crystal display (LCD), keyboard, and controller board. The FPD assembly
itself is located in a special cabinet mounted on the left side of the analyzer (see
Subsection 1.5).
Below the GCC are the Purge Air Panel and the Pressure Control Panel. The Purge
Air Panel contains the heater air and purge air gauges and regulators. The
Pressure Control Panel contains the Electronic Pressure Controller (EPC) or a
group of mechanical regulators and gauges. When the EPC is installed the
Pressure Control Panel has a blank front panel.
Each analyzer has a temperature code (T-Rating) listed on the nameplate. This T-
Rating indicates the temperature classification of the area in which the analyzer
has been designed to operate. T-Ratings and area classifications for analyzer
locations are determined and supplied by the customer.
When you communicate with ABB Process Analytics about this analyzer, please
identify the hardware and software configurations, as shown in the following
paragraphs.
The nameplate, located on the right side of the Oven Compartment, lists the
hardware configuration information (see Figures 1-1 and 1-2).
TEMPERATURE CODE:
T-Rating
The hardware configuration consists of the model number, sales order number, and
T-Rating.
The software configuration appears at the top of the Background screen just below
“Process Analytics GCC.” In Figure 1-3 the software configuration is 2020-9A.
1-2 2000-SVC, C1
** B A C K G R O U N D **
Process Analytics GCC Remote 01
2020-9A (C) 1997
**************
*** Alarm *** 16-Jan-1997 THU 08:16:01
**************
Analysis Time :00114 Peaks Found : 00
Cycle Time :00000 State : Idle
F1 F2 F3 F4
If the analyzer will be in a Class I hazardous location, an air purging system must be
installed to reduce the risk of explosion. Class I locations are those in which
flammable gases or vapors are or may be present in the air in quantities sufficient to
produce explosive or ignitable mixtures.
1.4.1 Introduction
The EMC directive (one of the new approach directives required by CE Mark) refers
to both electromagnetic “emissions” and electromagnetic “immunity.”
Electromagnetic emissions from electronic devices cause electromagnetic
interference (EMI) to the radio frequency spectrum which can disrupt emergency
communications, radio and television broadcasts, and interfere with the operation of
other electronically-controlled devices. Electromagnetic immunity refers to an
electronic device’s ability to handle interference from a wide variety of sources, such
as radiated, conducted, surges, etc.
It is the intent of Process Analytics to design into its analyzers the concept of “Total
Envelope Protection.” The basic enclosure itself, which is fabricated from sheet
2000-SVC, C1 1-3
steel with all seams welded, when properly “grounded” or “earthed,” becomes the
protection for emissions that could radiate from the unit. In addition, the enclosure
also provides a high level of immunity from electromagnetic interference (EMI)
which could affect the performance of the analyzer.
In order for the analyzers produced by Process Analytics to maintain their tested
integrity, the installation methods employed are of equal importance. The grounded
enclosure produces a “Faraday Shield” around the electronic components, detection
systems and other sensitive components which could generate EMI or be affected
by EMI. An extension of this Faraday shield must be maintained throughout the
installation scheme.
When wiring from an Analyzer changes from one zone to another, the concept of
the “Total Envelope” or Faraday Shield must be maintained. Provisions must be
made for terminating the cable in the “zero-length shielding” fashion as shown in
Details A-A and C-C of Figure 1-4.
In order to extend the Faraday shield beyond the analyzer, it is necessary to install
all power wiring, signal/control wiring and communication wiring in rigid metal
conduit or by using braided armored cable/braided armored shielded cable (see
Detail C-C of Figure 1-4). The wiring system employed must be grounded (earthed)
to the case at the point of entry of the analyzer (zero-length shielding) and to the
case at the point of entry of the equipment on the other end (zero-length shielding).
All entry connectors, Myers Scru-tite® hubs, conduit bushings, cable glands, etc.,
must make metal to metal contact with the analyzer’s enclosure. In addition, the
grounding at the point of entry, proper routing and termination of the shield and/or
drain wire are also important.
Where wiring must be terminated in a junction box or similar type of enclosure, the
enclosure must be metallic and properly grounded (earthed) as shown in Details A-
A and B-B of Figure 1-4. The conduits/cables must be grounded at the point of
entry, and wiring practices continued in the same manner as noted above in
paragraph 1.4.3.
All utility services connected to the analyzer (instrument air, carrier gas, etc.) as well
as sample inlets/vents shall be grounded at the point of entry into the envelope of
the analyzer. For the most part these connections will be provided in this manner at
the factory; however, if additional connections are made at time of installation, this
practice must be followed.
In normal operation the analyzer has its doors and access covers closed. Any
openings could present a safety hazard, as well as provide an avenue for EMI into
or out of the analyzer.
1-4 2000-SVC, C1
2000-SVC, C1
DETAIL "A-A"
APPROVED INCREASED
SAFETY JUNCTION BOX BRAIDED INSULAT
OR OTHER TYPE ARMORED CONDUC
"METAL" ENCLOSURE CABLE WASHER,
THRUST INSULATOR
SEAL,
"E1FX" (TYPE Ex d) GLAND FOIL SHIEL
OUTER SHEATH
SEAL, INNER
FERRULE SHEATH
RIGID CONDUIT, PIPE OR OTHER
APPROVED BARRIER FEED-THRU STEEL WIRE BRAID IS SCREW-TITE HUB
APPROVED FITTING GROUNDED (EARTHED)
TO THE "E1FX" (Ex d) BRAIDED SHIELD OR OPTIONAL D
METAL-TO-METAL
GLAND AT POINT-OF-ENTRY SHALL BE PROPERLY TERMINATE
CONTACT BETWEEN HUB
ZONE 1 AREA GENERAL PURPOSE OR FORMING A "ZERO-LENGTH" ANALYZER AT THE PROPER TERM
AND STEEL ENCLOSURE
NON-HAZARDOUS AREA EMI SHIELD OR IN A METAL ELECTRICAL JUNC
OR ENCLOSURE. LENGTH OF EXP
PHYSICAL BARRIER SHIELD OR DRAIN WIRE SHALL BE
DETAIL "C-C" AS SHORT AS POSSIBLE.
DETAIL "B-B"
E1FX (Ex d) GLAND ASSEMBLY/CABLE ENTRY
1-5
1.5 VISTA II WITH FLAME PHOTOMETRIC DETECTOR
Transformer
0 0
FPD Electrometer
Detector
This manual supports the 2000 basic analyzer. An appendix to the Operator's
Manual presents service material for special applications such as 2002 (simulated
distillation), 2003 (PNA), 2005 (temperature programmed GC), 2007 (fuel sulfur),
2008 (olefins), and 2030 (sparging sample conditioning system).
1-6 2000-SVC, C1
SECTION 2. TROUBLESHOOTING
baseline problems
analysis problems
temperature control problems
output problems
AMOUNT OF
OFFSET
BASELINE BASELINE
TIME TIME
NORMAL OFFSET
Causes:
3. Large difference in reference and column carrier flow rate (example: reference
1 cc/min, column 20 cc/min). Perform Test Procedure 2 (Carrier and Makeup
Gas Flow Adjustments).
2000-SVC, C1 2-1
4. Column broken or connection in column train disconnected, restricted or
leaking. Perform Test Procedure 1 (Carrier, Makeup, and Utility Gas Supplies)
and Test Procedure 2 (Carrier and Makeup Gas Flow Adjustments). If there is
no carrier gas flow or the carrier gas flow is restricted, perform Test Procedure
8 (Column Train Problems).
6. Column flooded with liquid sample. Perform Test Procedure 3 (Sample Valve
Leaking/Column Flooding).
Symptom: Baseline (detector signal) is experienceing a cyclic short term drift (see
Figure 2-2) indicated by detector signal, graphics display, or strip chart recorder (if
used). If cyclic behavior is only present on strip chart recorder, verify recorder is
functioning properly and that the recorder connecting wires are properly shielded.
Ensure shield is connected to ground at only one end.
BASELINE BASELINE
TIME TIME
At the extreme, the signal may indicate a cyclic behavior with the period of each
cycle ranging from a few seconds to several minutes.
Causes:
1. Short term drift, especially cyclic operation, could be due to temperature out of
control at the TC detector or isothermal oven, “dirty” carrier, or defective flow
controller. Perform Test Procedure 31 (Checking Temperature Table Values),
2-2 2000-SVC, C1
steps 1 to 3, 8 and 9; Test Procedure 9 (Baseline Cyclic Temperature
Controller); Test Procedure 10 (Baseline Cyclic Carrier Regulator); or Test
Procedure 11 (Baseline Cyclic Flow Controller), as applicable.
2. Another possible cause is cell vent back pressure changing. Disconnect vents
to check. Perform Test Procedure 35 (Vent Back Pressure).
BASELINE BASELINE
TIME TIME
NORMAL NOISE
2000-SVC, C1 2-3
Cause: Baseline or detector noise can result from contaminated carrier, makeup
gas, tubing or regulators. This type of contamination is much less pronounced with
a TCD than for an FID. Other causes include defective filaments (TCD), detector
wiring, or electrical noise in the detector electronics or power supplies.
AMOUNT OF
OFFSET
BASELINE BASELINE
TIME TIME
NORMAL OFFSET
2. Column flooded with liquid sample. Perform Test Procedure 3 (Sample Valve
Leaking/Column Flooding).
Symptom: Baseline characterized by random noise and or spikes (see Figure 2-6).
NORMAL NOISE
2-4 2000-SVC, C1
Cause: FID noise is generally the result of electrical noise or contamination.
a. Electrical noise from the FID amplifier could result from a noisy power
supply or defective component of the PCB.
c. Since the FID amplifier input impedances are extremely high, low noise
coaxial cable connects the detector and the FID amplifier. Defective
coaxial cables or poor electrical connections are often sources of noise.
2. Contamination can enter through the burner air, burner fuel, or carrier.
Secondary sources are contaminated air, fuel, carrier lines, or regulators.
d. If water accumulates in the FID vent, the detector effluent flow can
bubble through the accumulated water. This in effect back-pressures the
FID, causing the flame intensity to fluctuate. This can appear as a noisy
baseline as well.
2.3.1 No Peaks
Missing Peaks
BASELINE BASELINE
TIME TIME
NORMAL OFFSET
2000-SVC, C1 2-5
Cause: This generally indicates that either no sample was injected, or the injected
sample is not being detected or processed.
1. Chroma not selected on manual control screen (affects recorder output only).
2. No sample flowing to the sample valve. Verify sample is flowing to the sample
valve.
4. No air to the sample valve actuator. Perform Test Procedure 19 (Sample Valve
Actuation Air).
5. Baseline offset extreme. See Baseline Offset: Subsection 2.2.1 for TCD or
Subsection 2.2.5 for FID.
7. TCD Failure. Perform Test Procedure 5 (Detector Balance) and Test Procedure
6 (Filament Test), as applicable.
9. Low Zone Temperatures. See Subsections 2.2.3 through 2.4.22 and Test
Procedures 22 through 28.
10. Active stream is stream 9 (no inject occurs on stream 9). Change to correct
active stream.
11. Check Method Table for correct entries. Perform Test Procedure 34 (Checking
Method Table Configuration).
12. Sample Valve Failure. Perform Test Procedure 1 (Carrier, Makeup, and Utility
Gas Supplies) and Test Procedure 2 (Carrier and Makeup Gas Glow
Adjustments), as applicable. Also see Subsections 2.2.1 and 2.2.5. Repair
sample valve (see Sample Valve Repair in Section 4). Check for correct stem
volume and length.
13. Actuation solenoid valve vent is plugged or obstructed. Check and remove any
obstruction.
14. Solenoid not moving. Replace solenoid valve, driver card, or Chroma I/O
board.
2-6 2000-SVC, C1
2.3.2 Double Sampling
Symptom: The chromatogram peaks appear to have double apexes (see Figure
2-8). The trailing peak apex is generally smaller than the leading due to the first
having the greater sample size.
TIME TIME
Cause: Double sampling problems are isolated to the sample valve. Generally the
first injection occurs when the valve is turned on (valve stem inserted into the
injection chamber). The second injection is made when the valve is turned off (the
valve stem is withdrawn from the injection chamber). Perform Test Procedure 20
(Double Sampling).
Unknown
TIME TIME
Cause: If only present on calibration sample and not on process, verify that the
correct calibration and proto fuel sample is being analyzed. Possibly a new
calibration blend has been installed that contains a blending error. Perhaps the
wrong calibration sample has been selected or incorrect analysis is attached to it.
If mystery peaks are present on all process or calibration samples, the analyzer is
experiencing a sampling problem. The sample valve seals may be leaking. The
sample valve may be double sampling (see Subsection 2.3.2). The sample stem
may be scratched or deformed. Peaks may also be originating from a previous
analysis cycle.
2000-SVC, C1 2-7
2.3.4 Variable Sample Size
Variable sample size can cause a nonrepeatibility of peak concentrations if the peak
area is varying (see Figure 2-10).
TIME TIME
ANALYSIS #1 ANALYSIS #2
Figure 2-10. VARIABLE SAMPLE SIZE
Failure: The liquid sample volume is not consistent between consecutive injections.
This can be related to sample flow, defective sample valve hardware, leaks in
column train, or sample bubbling.
Cause: Leaking sample valve seal can result in random bubbling of carrier into the
sample chamber causing the sample size to vary. If the sample chamber pressure
is such that the temperature is above the bubble point of the sample, the sample will
bubble in the sample chamber, causing an inconsistent liquid fill of the sample loop.
This results in a continuously variable sample size. A defective sample valve stem
or leaking seal(s) can also cause nonrepeatability.
t0 t 30 t0 t 27 t0 t 34
1. Varying Carrier flow rate. Perform Test Procedure 2 (Carrier and Makeup Gas
Flow Adjustments).
2-8 2000-SVC, C1
2. Varying Isothermal Oven Temperature. Perform Test Procedure 31 (Checking
Temperature Table Values).
5. Variable back pressure on FID vent or TCD measurement vent. Perform Test
Procedure 35 (Vent Back Pressure).
Symptom: Chromatogram indicates all peaks are present; however, the data report
shows the peak to be nonexistent or unknown.
Cause: The gating in the method needs to be modified to ensure gating of the
missing peak in the report. This can be done by modifying the gate ON/OFF time in
the method table. Refer to the Operator’s Manual for detailed instructions.
Symptom: The peaks on the strip chart recorder are reversed or negative (see
Figure
2-12).
Baseline offset
adjusted up scale
NORMAL OFFSET
Cause: Negative peaks on the strip chart recorder could be due to reversed
recorder wiring at the analyzer or at the recorder. Some recorders are equipped
with polarity reversal. Ensure correct polarity setting on recorder. Other possible
causes include reversal of sense and reference tubing connections or filament
wiring if a TCD is used, or a grounded jet or missing jet voltage if a FID is used.
2000-SVC, C1 2-9
2. Check for reversed sense and reference tubing connections to the detector.
Symptom: The chromatogram or peak areas are excessively large. The condition
may be severe enough that all peaks are off scale on the highest attenuation (see
Figure
2-13). Chromatogram may go off scale at approximately the time of distillation on
and not return to scale until time of distillation off.
Cause: The attenuation could be set too low, making the chromatogram or peaks
appear large (loss of polarizing voltage on FID). Another possible cause is the
wrong carrier gas is being used (e.g. nitrogen used instead of helium).
The peaks may in fact be too large and saturating the detector or column. The
splitter may be out of adjustment, or the liquid sample size may be too large.
Possibly the detector gain jumper at the detector electronics is not setup correctly.
The sample valve may be injecting an excessively large sample volume due to
deformation or a scratch in sample stem or worn seals.
WARNING
Sample will spill or leak out during this procedure. Consult MSDS
sheets on file at your location for safety requirements.
4. Repair sample valve (see Sample Valve Repair in Section 4). Check sample
loop size.
Symptom: The chromatogram or peaks have reduced in size from that of a previous
analysis. This is also characterized as a reduction in detector sensitivity.
2-10 2000-SVC, C1
Cause: The attenuation could be set too high, making the chromatogram or peaks
appear small. Another possible cause is the wrong carrier gas is being used (e.g.
helium used instead of nitrogen).
The peaks may in fact be too small as a result of excessive sample splitting due to
the splitter being out of adjustment, or a small liquid sample volume injection. The
sample groove in the sample valve stem may be plugged or restricted. A
programming error in sample valve on/off timing may not allow adequate time for a
proper sample injection. Sample valve actuation malfunction can cause inadequate
sample injection. Possibly the detector gain jumper configuration at the detector
amplifier is not setup correctly. The sample valve may have a defective or wrong
stem installed. Low polarizing voltage, defective Detector Amplifier, or “dirty” FID
can also reduce sensitivity.
4. Perform Test Procedure 29 (“Flame Out” LED Remains On After FID Flame
Ignition) to check polarizing voltage.
7. Repair sample valve (see Replacing the Valve Stem in Section 4).
8. Inspect sample valve stem to check for scratches, deformation and plugging.
Check loop size and stem length.
Vista II analyzers that are utilizing only one Vista Workstation (VWS) highway must
have the second highway jumpered on the backplane. If the input to highway 2 is
left unconnected, the communications controller may perceive electrical noise-
induced line changes as information. This extraneous “information” may cause the
analysis to stop occasionally at the end of an analysis method or exhibit other
unpredictable behavior.
2000-SVC, C1 2-11
To prevent this problem from occurring it is recommended that the positive input of
the unused highway be connected to the +5 volt supply. The recommended
connection locations are as follows:
2. Connect one end of the jumper wire to J102 pin 5 (see Figure 2-14). If there is
not a connector already installed, ABB P/N 3617698-6 may be used at J102.
3. Connect the other end of the jumper wire to J110 pin 1. If there is not a
connector already installed, ABB P/N 3617698-12 may be used at J110.
TB1
J110
1
1 2 3 4 5 6 J110
J1A 1
1 2 3 4 5 6
J1B
12
6
HIGHWAY #2
5
HIGHWAY #2
1 2 3 4 5 6
4
3
2
J102
1
J102
2-12 2000-SVC, C1
Other zones’ actual temperature indicate low or ambient. At the temperature board
in electronics enclosure, all LED’s are off as the temperature control board shuts
down.
Failure: The failure is most likely isolated to the zone indicating a temperature > 500
deg. The temperature sensor(s) is a 400 ohm platinum thermocouple probe. As the
temperature of the probe increases, its resistance value increases. As the
temperature of the probe decreases, the resistance decreases. The maximum
temperature range measurable by the temperature controller is 500 degrees. An
indication greater than 500 degrees corresponds to a high resistance value at the
sensor input. The greatest resistance possible is an open circuit to the sensor input
or open probe or connection. The least resistance would be a shorted probe or
connection to the sensor input.
Cause: The sensor to the zone input has possibly opened, or is no longer connected
to the sensor input. Perform Test Procedure 22 (Open Temperature Sensor).
2000-SVC, C1 2-13
Failure: The failure is most likely isolated to the zone indicating a temperature less
than -200 deg. The temperature sensor(s) is a 400 ohm platinum thermocouple
probe. As the temperature of the probe increases, its resistance value increases.
As the temperature of the probe decreases, the resistance value decreases. The
maximum scaled temperature range measurable by the temperature controller is -
200 degrees. This corresponds to an extremely low resistance at the sensor input.
The least resistance possible is a short circuit to the sensor input or shorted probe
or connection.
Cause: The sensor to the zone input has possibly shorted. Perform Test Procedure
23 (Shorted Temperature Sensor).
Symptom: At the temperature board in electronics enclosure, all LED’s are off as
the temperature control board shuts down.
Failure: The isothermal oven heater temperature is greater than 500 degrees C.
Cause: The sensor input from the isothermal oven heater temperature monitor has
opened, or is no longer connected.
Symptom: Micro chip #2 monitors for over temperature conditions at the various
temperature zones. No heat being applied to a specific temperature zone. Actual
temperature as indicated in Manual Temperature Control Mode indicates > 500 deg
for a specific zone. At the temperature board in electronics enclosure, all LED’s are
off as the temperature control board shuts down.
2-14 2000-SVC, C1
*Reasonableness Test
*Probe Open/Shorted or TC Faulty
Failure: The failure is most likely isolated to the zone indicating a temperature > 500
deg.
Cause: The sensor to the zone input for temperature monitoring has possibly
opened, or is no longer connected. Perform Test Procedure 26 (Zone Input Sensor
Open).
Symptom: The isothermal oven (zone # 1) and programmed temperature oven (zone
#2) are not being heated. The actual temperature reduces and eventually
approaches ambient. These are the only temperature controllers that use air baths.
Failure: Malfunction is related to application of oven air to air bath ovens. The air
bath heater(s) will overheat and burn out if air is not applied to the heaters while
power is applied. The air provides the heat to ovens by displacing heat from the
heaters. The presence or lack of oven air is sensed by a pressure switch. If air is
removed, the switch opens and power is removed from the air bath heaters. When
air is applied the switch closes allowing the temperature controller to apply heat to
the air bath heaters.
Cause: The oven air has been shut off or reduced below air pressure switch setting.
The oven loss of air pressure switch has failed, or connection problem exists.
Perform Test Procedure 24 (Loss of Oven Air).
Symptom: The Actual temperature is indicating below set point for zone and alarm
indicating triac failure.
2000-SVC, C1 2-15
Cause: The output of the triac is connected to the zone heater(s). An optical
isolator connected parallel to the output senses the firing of the triac(s) as heat is
applied to the heater(s). This output is monitored by the temperature control board.
If the triac does not conduct when the gate signal is applied, the triac is diagnosed
as failed. Problem could be associated with triac monitoring optical isolators on
output board, or an open heater element.
CAUTION
Perform Test Procedure 27 (Open or Shorted Heater) to check for shorted heater.
Symptom: The temperature board has shut down and all the LED’s are off. The
zone temperatures are reducing and will approach ambient. The T-Rating display is
alternating between the two jumper settings.
Remedy: The T-rating jumpers for Micro #1 and Micro #2 must be set up identically.
Determine the correct setting and configure the jumpers for both identically.
Symptom: The temperature board has shut down and all the LED’s are off. The
zone temperatures are reducing and will approach ambient.
2-16 2000-SVC, C1
Any one of the following alarm messages or conditions could be present:
Failure: Zones not used for temperature control are excluded to prevent operation.
They are also set INACTive in the software.
Symptom: The temperature board has been shut down. If the trouble is in Micro #1
then all LED’s are Off on the Temperature Control board and the TC zone
temperature is greater than the T-Rating. If trouble is in Micro #2, then the top LED
is ON and the actual temperature is greater than the T-Rating.
Cause: The T-rating defines the maximum surface temperature allowed to prevent
the ignition of the flammable liquids and gases. The over-temperature limit prevents
the temperatures from reaching the T-rating limit. The over-temp must be less than
the T-rating limit to prevent the temperature from reaching the T-rating ignition
temperature.
2.4.10 Reasonableness
2000-SVC, C1 2-17
Any one of the following alarm messages or conditions could be present:
The heater output board monitors the AC input with a comparator circuit. This
determines the zero crossover point. This occurs when the magnitude of the AC
signal is zero. This point occurs in both the positive and negative directions. The
crossover point is used to coordinate application of power from the triac to the
heating element. Power is applied as the zero crossover point occurs preventing
unnecessary loading and surging on the temperature output circuitry.
CAUTION
2-18 2000-SVC, C1
Remedy: Replace Heater Output Control board.
Cause: Temperature control did not detect the over-temp condition when tested.
CAUTION
Remedy: The over-temp micro has possibly failed, may require replacement of
temperature control board or output board.
Symptom: The temperature board has shut down and all LED’s on temperature
controller board are off. Actual temperatures are reducing; approaching ambient.
Alarm condition present.
2000-SVC, C1 2-19
temperatures could cause electronics failure and run away zone temperature
control.
CAUTION
Install a temperature monitor and verify ambient temperature. Ensure air flow into
heater box.
2-20 2000-SVC, C1
Remedy: Perform the temperature board reconfiguration procedure. Be certain to
hold down the switch and respond by pressing “Y”.
CAUTION
The temperature controllers must be stable with respect to tracking the set point.
Symptom: The actual temperature is not stabilizing at the set point temperature.
This alarm occurs when the zone temperature has remained outside the operational
band of the set point for more than 90 seconds.
2000-SVC, C1 2-21
2.4.17 Open or Shorted Heater
Failure: The temperature controller and sensor input and heater output control
board are functioning normally. An open heater will not supply heat to the
temperature zone.
Cause: The heater to the temperature zone is possibly open. Perform Test
Procedure 27 (Open or Shorted Heater).
Cause: Open fuse causes power to be removed from zone heaters. The analyzer
may indicate an out of control or low temperature alarm. Perform Test Procedure
28 (Open Fuse to Output Board Heaters).
CAUTION
2-22 2000-SVC, C1
4. Heater orifice restricted by foreign matter. Check the heater orifice to ensure it
is not restricted or plugged.
Symptom: Programmed temperature oven ramps to final set point, but will not cool
to initial set point or is slow to cool to initial set point.
Cause: Cool down is initiated by the selection of temperature control table entry #2
in the method tables. If this instruction is missing or incorrect values are placed in
the temperature parameters, cool down will be effected and may not occur. Cool
down causes a cool down solenoid to increase the cool air flow from the vortex
cooler into the programmed temperature oven. If the cool down solenoid or vortex
cooler fails, cool down will not perform as expected. If the air flow to the vortex
cooler is inadequate, cool down will also be affected. A rate of 0.1 is needed to
activate the cool down solenoid in the temperature control table entry #2.
The following can cause problems with programmed temperature oven cool down.
1. An error has been made in programming the method table. Perform Test
Procedure 31 (Checking Temperature Table Values) to verify all control
parameters.
2. Air supply pressure is low. Verify correct air pressures. If necessary make
adjustment.
4. Listen for cool down solenoid to operate and introduce increased vortex cooler
air flow. If this does not happen, Perform Test Procedure 43 (Programmed
Temperature Oven Cool Down).
Cause: The printer may be turned off or malfunctioning. The printer may have a
blown fuse or be unplugged from power. The printer may be in alarm condition such
as being out of paper. Wiring to printer may be disconnected or in error. Printer and
analyzer output driver may be not be compatible or mismatched (RS-232).
2000-SVC, C1 2-23
If no reports are generated the report option may be set to NONE. The post
analysis calculations may still be in progress. If no report is generated before next
analysis cycle begins, there is a problem. Perform Test Procedure 36 (Printer Test)
to verify correct printer setup.
Symptom: There is no trend output at recorder or input device, or the trend output
value is not correct.
Symptom: Valves do not switch and alarm digital output not functioning.
Verify digital assignment (see Digitial I/O Option in Section 4 of the Operator’s
Manual).
Cause: The strip chart recorder may not be powered, or may be malfunctioning. A
fuse may be blown at the recorder. Other causes include defective recorder cable,
wiring error or loose connection. Possibly the wrong attenuation is selected at the
recorder or the shunt resistor is not correct. The Manual Control Screen may not
have the Chroma selection or the Chroma I/O board could be malfunctioning.
Symptom: Pressing key pad on analyzer front panel produces no response on CRT
or other analyzer output.
2-24 2000-SVC, C1
Cause: No response by key pad could indicate defective key pad or malfunction or
defect in key pad cabling from keypad to keypad assembly PCB. The CRT Control
PCB or associated wiring or connections may be defective. The controller software
may be locked up.
Cause: The remote analyzer switch address is incorrect. A remote analyzer cannot
be contacted if it is not powered or connected to the network. It is also imperative
that the network wiring be installed and wired correctly. Improper wiring may affect
several analyzers simultaneously.
Cause: The remote analyzer front panel address switch is not set correctly or
the “LOCK OUT REMOTE” switch is set to On.
Symptom: Only local chromatograms are accessible at the local panel recorder
output jacks. Remote chromatograms cannot be accessed.
Cause: This feature can only be accessed when using the network. The
jumper at JP5 located on the CRT controller may not be configured correctly.
2000-SVC, C1 2-25
Check settings and correct. Then cycle power to the device in which the switch
was modified.
7. Search for analyzer that is accessing another remote, or that is itself being
accessed, then terminate the access.
Cause: The FID flame can be extinguished by insufficient burner fuel, air or column
pressure surges, or plugged vent line (possibly moisture).
The FID flame may in fact be burning and the thermocouple or the associated flame
detection electronics may have failed to detect the flame on condition. The flameout
sensitivity for detection needs adjustment.
Perform Test Procedure 1 (Carrier, Makeup, and Utility Gas Supplies), Test
Procedure 2 (Carrier and Makeup Gas Flow Adjustments), Test Procedure 30
(“Flame Out” LED Remains On After FID Flame Ignition), and Test Procedure 35
(Vent Back Pressure), as applicable.
If, after repeated attempts to ignite the FID, it will not light, see Subsection 2.5.9.
Symptom: FID Flame out LED on, and continued attempts to light FID have failed.
Symptom: Low carrier gas alarm. If carrier is in short supply and not corrected,
carrier flow rates will reduce as the gas is depleted. Analyzer data will become
erroneous as carrier pressure drops below the analyzer requirement.
Causes: The following can be causes for low carrier pressure alarm.
2-26 2000-SVC, C1
1. Low carrier gas supply. Perform Test Procedure 1 (Carrier, Makeup, and Utility
Gas Supplies).
CAUTION
Symptom: Rotometer and pressure gauge indications are below normal. Bubbles
may be seen in analyzer effluent rotometer. Individual components, RVP and V/L
calculation values are not repeating.
Causes: The following can be causes for low sample flow alarm.
1. The sample booster pump is not operating or has failed. Check pump inlet and
discharge pressure and power.
CAUTION
2000-SVC, C1 2-27
Symptom: If X purge system installed analyzer power will be removed and cannot
be restored until purge air is restored.
1. Air supply to analyzer has been shut off. Perform Test Procedure 1 (Carrier,
Makeup, and Utility Gas Supplies).
2. The purged sections in the analyzer have developed leak(s). Leak check with
leak detector
4. Stream step instruction missing from method table. Perform Test Procedure 34
(Checking Method Table Configuration).
2-28 2000-SVC, C1
2.5.14 Analyzer Will Not Power Up (X-Purge)
CAUTION
6. Air leak in purged analyzer housing preventing X-purge time from completing.
See Subsection 2.5.12, Loss of Purge Air.
7. X-purge is locked out. Cycle power (10 seconds) to reset X-purge, and allow X-
purge sequence to initiate.
2000-SVC, C1 2-29
2.6 ELECTRONIC PRESSURE CONTROL TROUBLESHOOTING
The Pressure Control Assembly (see Figure 2-15) requires special tools and
equipment for repair. If you suspect a problem with this assembly please contact
your ABB Processs Analytics service representative.
J1A
1234 5 6
J1A
J1B 1234 5 6
J1B
2-30 2000-SVC, C1
TB1, which is called VAC #1
J1A, which is called VAC #2
J1B, which is called VAC #3
Input power to the Vista II Series Gas Chromatograph is 115VAC. This may be
supplied directly as 115VAC or stepped down from a higher voltage. The input
voltage may be conditioned or supplied from an uninterruptible power supply (UPS).
Each of these choices, made at the time of sale, affects how the power is brought
into the analyzer.
The analyzer uses three power distribution circuits to route the power (see Figure
2-17):
TB1
Hot
1
115 to 230 VAC
(Not Filtered Neut RFI VAC #1
2
or Conditioned) Filter (to heaters)
Gnd
3
3
Hot
4
115 to 230 VAC Neut
(Conditioned VAC #2
5
or UPS) (to electronics)
Gnd
6
4
Gnd
3
115VAC Neut VAC #3
(Autoformer) 2 (to solenoids
Hot and detectors)
1
2000-SVC, C1 2-31
If all power supplied to the analyzer comes from a single source it will be connected
to TB1. Instead of input cables there will be jumper plugs installed at J1A and J1B
to connect their distribution circuits to the input power source.
If unconditioned power is routed to TB1 and conditioned power to J1A, then J1B will
have a jumper plug to connect its distribution circuits to J1A.
If unconditioned power is routed to TB1 and an autoformer output is routed to J1B
(with J1A not being connected to source power), then J1A will have a jumper plug to
connect its distribution circuits to TB1.
When checking input power make sure to note the connections for source power to
determine how power is routed.
The Model 2007 Fuel Sulfur Analyzer utilizes the same power distribution circuits as
the standard Model 2000 analyzer. In addition the Model 2007 has an autoformer to
provide 40 VAC power to the furnace located in the oven section of the analyzer
(see Figure 2-18).
TB1
Hot
1
115 to 230 VAC
(Not Filtered Neut RFI VAC #1
2
or Conditioned) Filter (to heaters)
Gnd
3
3
Hot
4
115 to 230 VAC Neut
(Conditioned VAC #2
5
or UPS) (to electronics)
Gnd
6
J1B
Autoformer 5
4
Gnd
3
Neut VAC #3
2 (to solenoids
Hot and detectors)
1
40 VAC to
Temp Controller
(AC Conditioning PCB #2)
2-32 2000-SVC, C1
2.7.4 Poor Display Contrast
If the analyzer is ON but it is difficult to read the LCD display, you may need to
adjust the display.
3. On the Front Panel PCB mounted on the door, locate the contrast adjustment.
It is on the front side of the board, at the bottom center (see Figure 2-19).
Front Panel
PCB
Contrast Display
Adjustment Panel
2000-SVC, C1 2-33
2.8 ALARMS
The analyzer has different types and levels of alarms to help you resolve analyzer
problems. When an alarm signal appears on the Background Screen, press the F4
(Alarms) soft key to display the ALARMS screen with the alarm message (see
Figure 2-20).
Clear
Exit Alarms
and Exit
F1 F2 F3 F4
When you finish with the alarm messages, press the F1 (Exit) soft key to return to
the Background screen without deleting the alarms, or press the F2 (Clear Alarms
and Exit) soft key to clear the alarms and return to the Background screen.
Alarm messages are of two primary types: main alarms and subordinate alarms.
Main alarms identify a major alarm category. These alarms appear on the alarm
screen at the left margin (e.g., “Post Analysis Error:” in Figure 2-20). The main
alarms are:
Sensors Active:
Sensors Held:
Component High:
Component Low:
Clock Error:
TCF Error:
Post Analysis Error:
Communications Error:
Pressure Board:
Temperature Board:
Raw Chromatogram Storage:
Start-up Hardware Problem Found
Power Failed
2-34 2000-SVC, C1
GCC is not Running an Analysis
Message From VWS:
Flame Out
Subordinate alarms appear below the main alarms, indented and preceded by an
asterisk (*) to show their subordinate status (e.g., “*Valve Manually Switched” in
Figure 2-20).
If a main alarm has subordinate alarms, the main alarm title will include a colon (:).
The following subsections list the main alarms that have subordinate alarms,
together with their associated subordinate alarms.
When “Sensors Active:” appears as the main alarm, one or more sensor alarms
appears below the main alarm. “Sensors Active” appears when an alarm is active at
the time you look at the Alarms screen. Typical Sensors Active alarms and their
descriptions are:
NOTE
* Purge Air—activates when purge air is lost. After purge air is restored the
alarm resets.
* Carrier Gas—activates when carrier gas is lost. After carrier is restored the
alarm resets.
* Low Oven Temp—activates when oven temperature goes below the lower
setpoint. When temperature comes back within the setpoints, the alarm
resets.
* Sample Flow—activates when sample flow is lost. When the sample flow is
restored, the alarm resets.
2000-SVC, C1 2-35
2.8.2 Sensors Held
When “Sensors Held” appears as the main alarm, one or more sensor alarms
appears below the main alarm. “Sensors Held” appears when an alarm was active
at some time during the analysis, but before you looked at the Alarms screen.
Typical Sensors Held alarms are the same as those for Sensors Active. Sensors
Held alarms must be manually reset by entering the Alarms screen, after the
problem is corrected, and pressing the F2 (Clear Alarms and Exit) soft key.
When “Component High:” appears as the main alarm, one or more component
alarms appears below the main alarm. Typical Component High alarms and their
descriptions are:
When “Component Low:” appears as the main alarm, one or more component
alarms appears below the main alarm. Typical Component Low alarms and their
descriptions are:
When “Clock Error:” appears as the main alarm, one or more clock alarms appears
below the main alarm. Typical clock alarms are:
2-36 2000-SVC, C1
* Memory Shortage < 20%—activates when the GCC is short of memory. This
is usually caused by chromatogram storage. To clear this alarm return
all memory that is being used for chromatogram storage back to the
operating system and reduce the number of points being saved by
Chromatogram Storage function.
* Bad Base Projection Backward—activates when the end of a peak was not
defined in the analysis.
When “TCF Error:” appears as the main alarm, one or more time-coded function
alarms appears below the main alarm. These alarms are cleared by correcting the
associated method entry designated by the alarm. Typical TCF alarms and their
descriptions are:
* Auto Zero During Noise—activates when auto zero is performed during noise
calculation.
* Auto Zero During Gate—activates when auto zero is performed during forced
gate.
* Auto Zero During Slope Detect—activates when auto zero is performed during
slope detection.
* Gate Switched Off w/o Gate On—activates when a force gate is turned off
without the force gate being turned on.
2000-SVC, C1 2-37
* Noise Off w/o Noise On—activates when noise calculation is turned off but
never turned on.
* Not Enough Noise Points—activates when Noise On and Noise Off are too
close together in time to collect sufficient noise points to perform a
calculation.
* Invalid Peak Width—activates when the peak setting in the TCF table is
greater than 64.
* Too Many Peaks in Analysis—activates when there are more than 254 peaks
in the analysis.
When “Post Analysis Error:” appears as the main alarm, one or more post analysis
alarms appears below the main alarm. Typical post analysis alarms and their
descriptions are:
* Cal Fail: RF Out of Range—activates when calibration fails because the new
response factor for a peak was out of the limits specfied for the
component.
* Vista Basic Run-Time Error—activates when an error occurs in the Vista Basic
program when it runs.
2-38 2000-SVC, C1
VistaNET Link
VWS Link
* Transmit Failure Channel 1—activates when the GCC sends a message to the
VWS but does not receive acknowledgement.
* Transmit Failure Channel 2—activates when the GCC sends a message to the
VWS but does not receive acknowledgement.
2000-SVC, C1 2-39
* Primary/Backup Switched—activates when GCC reverses its primary and
backup data links because of timing discrepancy with the VWS. This
only signifies a failure when there is also another communication alarm.
When “Pressure Board:” appears as the main alarm, one or more pressure alarms
appears below the main alarm. Pressure alarms are of two types, overall alarms
and zone-specific alarms, with the zone-specific alarms subordinate to the overall
alarms. Typical overall pressure alarms and their descriptions are:
If the “*Zone Specific” subordinate alarm appears, at least two additional lines
appear below that. The first line identifies which zone produced the alarm and the
second line identifies the specific alarm condition. Typical zone specific alarms and
their descriptions are:
* Zero Failed—activates when the Zero pressure is not present, or the switch
has not been depressed.
* Set Point Failed—activates when Zone is inactive; zone is SWITCH zone and
switch not depressed or set point is greater than the configured pressure
range.
NOTE
2-40 2000-SVC, C1
* Entry 01, DILUTER > 600 psig (example)
When “Temperature Board:” appears as the main alarm, one or more temperature
alarms appears below the main alarm. Temperature alarms are of two types, overall
alarms and zone-specific alarms, with the zone-specific alarms subordinate to the
overall alarms. Typical overall temperature alarms and their descriptions are:
NOTE
If one of the following alarms occurs, the analyzer will stop and power
will be removed from all heaters. To resume operation, you must turn
power OFF and back ON, and then restart the analysis.
If the “*Zone Specific” subordinate alarm appears, at least two additional lines
appear below that. The first line identifies which zone produced the alarm and the
second line identifies the specific alarm condition. Typical zone specific alarms and
their descriptions are:
2000-SVC, C1 2-41
* Reasonableness Test—activates when probe and thermocouple disagree by
more than 100° C.
* Zero Failed—activates when Zero resistance is not 400 ohms, or the switch is
not depressed (Zero is not required in the field).
* Span Failed—activates when Span resistance is not 1000 ohms, or the switch
is not depressed (Span is not required in the field).
* Set Point Failed—activates when Zone is inactive; zone is SWITCH zone and
switch not depressed or set point is greater than T-Rating.
NOTE
NOTE
If one of the following alarms occurs, the analyzer will stop and power
will be removed from all heaters. To resume system operation, turn
the power OFF and back ON, and then restart the analysis.
2-42 2000-SVC, C1
2.8.11 Raw Chromatogram Storage
When “Raw Chromatogram Storage:” appears as the main alarm, one or more
chromatogram alarms appears below the main alarm. Typical chromatogram alarms
and their descriptions are:
* Could Not Save Analysis—activates when the GCC is unable to save the last
chromatogram.
2000-SVC, C1 2-43
For further information or assistance contact:
2-44 2000-SVC, C1
SECTION 3. TEST PROCEDURES
If you suspect a gas supply (flame, fuel, air) problem, perform the following test.
1. Stop Analysis at end of current analysis, and make no sample injection until
procedure is completed.
2. Check gas supply pressures at the analyzer pressure gauges or EPC screens.
Pressure indications should indicate normal operational values as indicated on
the application data sheets or last valid record.
3. If values are low, check gas supply at source gauges. Verify gas cylinder
valve(s) are open and that gas cylinder regulator(s) are adjusted for the correct
outlet pressure. Verify isolation valves which supply carrier or makeup gases to
the analyzer are open. Verify the cylinder gas supply is not depleted. Make
necessary adjustments and replace empty gas cylinders with full ones.
NOTE
Gas pressures include all carrier, hydrogen FID fuel, burner air and
utility air supplies.
CAUTION
1. Stop Analysis at the end of the current analysis and make no injection until
procedure is completed.
3. Refer to the application data sheets supplied with your analyzer and verify
correct reference and column carrier flow rates, correct hydrogen fuel and
burner air flow rates (if FID), correct splitter adjustment, and correct air pressure
adjustments.
2000-SVC, C1 3-1
3.3 TP 3: SAMPLE VALVE LEAKING/COLUMN FLOODING
WARNING
Sample will spill or leak out during this procedure. Consult MSDS
sheets on file at your location for safety requirements.
CAUTION
1. Stop Analysis at the end of the current analysis, and make no sample injections
until procedure is completed.
2. Isolate sample valve from the sample system using sample system isolation
valves.
4. Using stainless steel tubing connect a source of 25 psig nitrogen directly to the
sample valve inlet fitting (bottom). Purge all sample from the sample valve into
the waste container via the short piece of tubing previously connected. When
nitrogen purging is complete, (30 seconds), shut off nitrogen purge gas.
5. Raise the oven temperature to final set-point +20% and hold. Perform Test
Procedure 31 (Checking Temperature Table Values), steps 1 to 3, 8 and 9, and
observe the oven temperature (column).
NOTE
Steps 6 and 7 are optional. The existing column can be removed and
another installed prior to performing step 5.
6. Observe baseline for two times the normal cycle time. If baseline offset is
reduced, the sample valve is most likely leaking.
3-2 2000-SVC, C1
3.4 TP 4: CARRIER OR MAKEUP GAS REGULATOR
CAUTION
1. Stop Analysis at the end of current analysis, and make no sample injection until
the procedure is completed.
4. Leak check every connection outside the analyzer on the entire carrier flow
path. Perform step 5 only after step 4 has been completed and all leaks are
repaired.
5. Loosen inlet fitting nut and check for presence of carrier or makeup gas using a
leak detector solution.
7. Adjust carrier or makeup gas pressure for pressure indicated on the analyzer
carrier pressure gauge. If pressure adjusts to the correct value, stop this test
and perform Test Procedure 2 (Carrier and Makeup Gas Flow Adjustments) and
Test Procedure 5 (Detector Balance).
1. Stop Analysis at the end of the current analysis and make no injection until
procedure is completed.
3. On the Manual Control Mode screen press the F2 (Detector and Graphics) soft
key.
4. On the Chroma Board screen press the F3 (Manually Zero Baseline) soft key.
The Detector Reading should change to a value of 2.00 mV ±0.05 mV.
2000-SVC, C1 3-3
5. On the Chroma Board screen note the Hardware Zero, Software Zero, and
Detector Reading values.
6. Open the Controller front door and locate the Detector Amplifier on the left side
wall of the Controller.
7. Adjust the TCD Adjust potentiometer (located on the Detector Amplifier) until
the Detector Reading is equal to the sum of the Hardware Zero and Software
Zero values noted in step 5.
8. Press the F3 (Manually Zero Baseline) soft key and recheck the readings. The
detector is adequately zeroed when the Hardware Zero percentage is less than
10%.
CAUTION
1. Stop Analysis at the end of the current analysis cycle, and make no sample
injection until procedure is completed.
4. Open the Controller front door and locate the Detector Amplifier on the left side
wall.
5. Remove the six thumb nuts, cover, and plastic shield from the Detector
Amplifier. Then locate TB16 .
7. Connect ohmmeter leads between TB16 terminal 7 and the white wire removed
from terminal 8, and measure the resistance of the measure filament.
8. Connect ohmmeter leads between TB16 terminal 1 and the red wire removed
from terminal 2, and measure the resistance of the reference filament. The
measured values of the two filaments should be within one ohm of each other.
3-4 2000-SVC, C1
9. If the filaments are not within one ohm of each other, replace the filaments. See
“Filament Replacement” in Section 4.
12. Check all connections, then replace the Detector Amplifier plastic shield, cover,
and thumb nuts.
2. Remove power.
3. Open the Controller front door and locate the Detector Amplifier on the left side
wall of the Controller. Remove the six thumb nuts, cover, and plastic shield
from the Detector Amplifer.
4. Note the wire colors on Detector Amplifier TB16 terminals 1 (orange), 2 (red), 7
(black), and 8 (white). Remove filament wires from TB16 terminals 1, 2, 7 and
8, and substitute a pair of filaments that are mounted in a “dummy” detector cell
body.
8. If the detector does not balance or has excessive noise, locate the respective
detector signal connector, J13A or J13B, on the mother board.
9. Remove power from analyzer. Disconnect the cable assembly from J13A or
J13B.
2000-SVC, C1 3-5
10. Short between connector pins 1 and 2. Apply power and perform Test
Procedure 5 (Detector Balance).
13. If the Chroma I/O Test fails, remove power and replace the Chroma I/O PCB.
14. If the detector does not balance or noise remains, remove power and replace
the Detector Amplifier. Take care to copy the jumper configuration of the
original Detector Amplifier.
17. Remove the substitue filaments and replace the filament wires.
19. Replace the Detector Amplifier plastic shield, cover, and thumb nuts.
CAUTION
1. Stop Analysis at the end of the analysis and make no sample injection until
procedure is completed.
3-6 2000-SVC, C1
4. Inspect for disconnected or loose tubing connections or broken column in the
column train from the carrier regulator outlet to the column vent. Reconnect or
tighten all tubing fittings. Check for leaks and make necessary repairs. If
corrections or repairs were made, proceed to step 8.
5. Loosen the fitting connecting the column to the LSV and verify carrier presence
with a leak indicator solution.
7. If carrier flow is present and not restricted, reconnect the fitting to the LSV.
Beginning at the column vent, work back toward the previously disconnected
fitting, loosing each fitting in the column train one-at-a-time, checking each
loosened fitting for the presence of carrier. When full or nonrestricted carrier
flow is detected, the trouble has been isolated between the present and last
connection checked. Make necessary repairs. Reconnect or tighten all fittings
and check for leaks.
8. Check for correct carrier flow adjustment. Perform Test Procedure 2 (Carrier
and Makeup Gas Flow Adjustments) and Test Procedure 5 (Detector Balance),
as applicable.
1. If the cyclic baseline is not a function of the isothermal oven temperature or the
carrier regulator, and a flow controller is installed, the flow controller should be
replaced.
2000-SVC, C1 3-7
2. Perform Test Procedure 31 (Checking Temperature Table Values) and Test
Procedure 10 (Baseline Cyclic Carrier Regulator), as applicable.
1. Are other analyzers serviced from the same burner air, carrier, or burner fuel
source, experiencing noise? If Yes, then the noise problem is most likely related
to a common utility gas, tubing, fitting, or regulator.
1. Verify Burner Fuel is UHP Hydrogen (FID ONLY). If not, replace hydrogen
cylinder with UHP Hydrogen. If noise is eliminated, this test is completed. If
noise is still present, continue to step 2.
2. Verify carrier purity. If purity questionable, replace carrier gas cylinder. If noise is
eliminated, this test is completed. If noise is still present, continue to step 3.
3. Replace burner fuel cylinder (FID ONLY). If noise is eliminated, this test is
completed. If noise is still present, continue to step 4.
4. Replace carrier or burner fuel cylinder regulators. If noise is eliminated, this test
is completed. If noise is still present, continue to step 5.
2. If available, connect high purity bottled air to burner air connection. If noise
disappears, see “Repairing Air Cleanup Unit” in Section 4.
3. If bottled air is not available, see “Repairing Air Cleanup Unit” in Section 4.
CAUTION
3-8 2000-SVC, C1
1. Open isothermal oven door.
CAUTION
1. Stop analysis at the end of the current cycle and make no sample injection until
the procedure is complete.
6. Verify correct sample valve ON and OFF times in method table. Perform Test
Procedure 34 (Checking Method Table Configuration).
7. Refer to the application data sheet supplied with your chromatograph and check
carrier, makeup gases particularly splitter flow, and make any necessary
adjustments. Balance detector using Test Procedure 5 (Carrier or Makeup Gas
Regulator).
2000-SVC, C1 3-9
10. Perform Test Procedure 29 (FID Polarizing Voltage Test). If sensitivity is normal,
Test Procedure 16 is complete. If sensitivity continues to be reduced, continue
to step 11.
12. Apply power and gases to analyzer. After temperature stabilizes, check
sensitivity. If satisfactory, Test Procedure 16 is complete. If not, perform steps
13 through 15.
CAUTION
1. Ensure burner air and burner fuel are adjusted to the values shown on
application data sheets.
3. Remove power and open the Controller front door. Locate the Detector
Amplifier on the left side wall of the Controller and remove the six thumb nuts,
cover, and plastic shield.
5. On the Chroma Board screen, press the F4 (Manual Ignitor On) soft key to
ignite the cell flame. The meter should indicate 1.2 to 1.5 volts AC. If voltage is
not present, the ignitor could be shorted to ground, the auto ignite board could
be defective, or wiring could be disconnected. If the voltage is present, the
defect could be an open ignitor coil.
6. Turn off the burner fuel to extinguish the FID flame and then remove power from
the analyzer.
8. The resistance of the ignitor coil should measure 0.1 to 1 ohm. If an extremely
high resistance is measured, and the ignitor coil is open, replace the ignitor.
See “Flame Ignitor” in Section 4.
9. Connect the ohmmeter leads to one of the wires and chassis ground.
3-10 2000-SVC, C1
10. Measure the resistance of the ignitor coil to ground. If maximum ohms is not
measured, the ignitor is shorted to ground. Replace the ignitor (see “Flame
Ignitor” in Section 4).
12. If the ignitor coil was replaced, apply power to the analyzer. On the Chroma
Board screen, press the F4 (Manual Ignitor On) soft key. If the FID ignites,
proceed to step 14.
13. If the ignitor is operating properly and no voltage is present between TB16
terminals 3 and 4 when step 11 is performed, replace the Detector Amplifier.
14. Remove power and replace the Detector Amplifier plastic shield, cover, and
thumb nuts. Close and tighten the Controller front door.
One of the primary products of combustion is water. Water vapor produced by the
FID flame is discharged from the FID vent. One way to verify the FID flame is
ignited is to observe the condensation of the water vapor.
1. Disconnect the FID vent and hold a reflective surface such as a mirror, wrench
or other suitable object at such an angle that you can see the reflective surface.
2. If the FID flame is ignited, you will be able to see the condensed water vapor
form on the reflective surface.
CAUTION
2. Verify actuation air is being applied to the sample valve. Gently loosen the two
1/8 inch fittings at the actuator. Apply “Leak Tech”, “Snoop” or other similar
liquid leak detector to the back of the fittings.
3. From the background screen turn on valve 1. The outside actuation tube fitting
should produce bubbles. Turn off valve 1. The bubbles should now be
produced on the inside fitting.
2000-SVC, C1 3-11
4. If no air is present, check to ensure air is being applied to solenoid valve by
loosening the solenoid air supply inlet connection and test for the presence of
air with a leak detection solution. If air is applied to the solenoid valve, test to
ensure that the solenoid actuation voltage is being applied.
8. If the voltage is being applied, yet the valve is not switching, replace the
solenoid valve.
11. If no voltage is present, check the AC voltage to the DC Solenoid Driver PCB.
Adjust the voltmeter to read 120 Vac.
12. Connect the voltmeter leads between J( terminals 1 and 2. If voltage is present,
proceed to step 15.
13. If 120 Vac is not present, check the voltage at Solenoid #1 VAC J9A terminals 1
and 2. If voltage is present at J9A terminals 1 and 2, check the connections at
both ends of the cable connecting J9A and J9.
14. Remove power and disconnect the cable between J9A and J9. Check
continuity between J9A terminals 1, 2, and 3 and J9 terminals 1, 2, and 3,
respectively. If any wires are open replace the cable, apply power and repeat
step 11.
15. Apply power to analyzer and switch DC solenoid driver using procedure in step
7.
16. If voltage does not switch, replace DC solenoid valve driver PCB.
3-12 2000-SVC, C1
2. Verify double apex peaks by analyzing calibration standard of individually
resolved peaks.
3. When the analysis begins, stop the analysis at the end of the cycle.
5. Run a second analysis. When the second analysis begins, stop analysis at the
end of the cycle. If valve is double sampling, the peak shape will now be
normal in most cases.
7. Manually switch the Sample Valve Off and observe the chromatogram. A
second set of peaks may now appear. (This is another indication of double
sampling.)
9. Replace sample valve seals and stem (see “Sample Valve Repair” in Section 4).
1. For a liquid sample valve, observe the analyzer effluent sample flow rotometer
for the presence of bubbles. The sample pressure and temperature must be
such that the sample pressure at the sample valve is 25 psig above the bubble
point of the sample.
2. Ensure that the sample pressure at the sample valve is above the bubble point
of the sample.
3. A booster pump may be necessary for process sample if the supply pressure is
below the bubble point of the sample or the sample flow rate is not adequate at
the supply pressure.
6. For a vapor sample valve, ensure the sample valve effluent is referenced at
atmospheric pressure. A sample shutoff valve may be required or is not
operating or is not functioning properly.
2000-SVC, C1 3-13
7. Perform Test Procedure 2 (Carrier and Makeup Gas Flow Adjustments).
9. Open isothermal oven door and the programmed temperature cover (if
applicable). Remove the cover to access the column.
10. Leak test column train. When complete, close ovens with reverse procedure of
step 9.
11. If leaks were found, restore air and power. After temperatures stabilize, perform
an analysis to test repeatability. If analyzer repeats, Test Procedure 21 is
complete.
12. Repair sample valve, replacing stem and seals (see “Sample Valve Repair” in
Section 4).
13. Apply air, carrier, sample, and power to the analyzer. Let temperatures stabilize
and perform an analysis and check the repeatability.
CAUTION
4. Disconnect the sensor and measure its resistance value. The resistance of the
temperature probe should be approximately 440 ohms at 75 degrees F. If open
(extremely high), replace probe. The respective probes may be tested at the
locations given below:
Temperature J48A
Zone Board Terminals Assignment
3-14 2000-SVC, C1
5. If temperature probe is open, replace the temperature probe.
CAUTION
4. Disconnect the sensor and measure its resistance value. The resistance of the
temperature probe should be approximately 440 ohms at 75 degrees F. If
shorted or considerable lower, replace probe. The respective probes may be
tested at the locations given below:
Temperature J48A
Zone Board Terminals Assignment
2000-SVC, C1 3-15
3.24 TP 24: LOSS OF OVEN AIR
CAUTION
3. Disconnect the oven air pressure switch by removing the connector from J42B
on the DTC Backplane PCB (see Figure 3-1).
J42B
3-16 2000-SVC, C1
5. Apply oven air pressure.
6. Unscrew the pressure switch slightly and check for leakage to ensure air is
present at the switch.
8. The switch should close. Remove air and the switch should open. If switch
does not function as described, replace the oven air pressure switch.
CAUTION
5. Disconnect the thermocouple sensor from J49A terminals 1 and 2 of the Zone 1
Temperature Zone PCB.
6. Connect ohmmeter leads between the two disconnected wires and measure the
resistance value. If the resistance is extremely high, the thermocouple is open.
Replace thermocouple.
2000-SVC, C1 3-17
3.26 TP 26: ZONE INPUT SENSOR OPEN
CAUTION
5. Disconnect the RTD sensor from J49A terminals 4 and 5 of the appropriate
Temperature Zone PCB.
6. Connect ohmmeter leads between the two disconnected wires and measure the
resistance value. Typical resistance will be approximately 430 to 450 ohms at
ambient temperature. If resistance is extremely high, the RTD is open.
Replace the RTD. The respective probes may be tested at the locations given
below:
Temperature J49A
Zone Board Terminals Assignment
CAUTION
3-18 2000-SVC, C1
CAUTION
Temperature
Service Zone Board J49B
5. Remove one of the two wires to the defective temperature zone heater.
Connect an ohmmeter across these heater wires and measure the resistance
of the heater.
CAUTION
2000-SVC, C1 3-19
1. Remove power from analyzer.
4. Remove the fuse(s) in question and test with an ohmmeter. The measurement
should be approximately zero ohms. If the fuse is open, the measurement will
be extremely high.
5. Replace blown fuse. Since a blown fuse may indicate other possible
malfunctions or failures, continue with this procedure to verify the analyzer’s
operational status.
CAUTION
3. Locate the Detector Amplifier on the left side wall of the Controller. Remove the
six thumb nuts, cover, and plastic shield from the Detector Amplifier.
5. Disconnect the wire to the polarizer at TB16 terminal 5 and measure the
voltage as in step 4.
3-20 2000-SVC, C1
6. If the voltage indication is below -110 VDC at the 110 volt power supply, replace
the 110 volt power supply.
7. If the voltage is -110 VDC, remove power from the analyzer and shut down
carrier and makeup gases.
9. If any repairs were made, the sensitivity should be checked by applying power
to the analyzer and allowing temperatures to equilibrate. Balance detector per
Test Procedure 5 (Detector Balance) and perform an analysis. If analysis
demonstrates correct sensitivity, Test Procedure 29 is complete.
10. Remove power from the analyzer and shut down carrier and makeup gases.
12. Reconnect the wire to TB16 terminal 3 and apply power to the analyzer.
13. Measure with a DC voltmeter between the jet and chassis ground for -110 VDC.
Once confirmed remove power for reassembling.
15. Close and tighten the Controller front door and the isothermal oven door.
3.30 TP 30: “FLAME OUT” LED REMAINS ON AFTER FID FLAME IGNITION
CAUTION
2000-SVC, C1 3-21
1. Stop Analysis at the end of analysis cycle and make no sample injections until
procedure is completed.
2. Perform Test Procedure 1 (Carrier, Makeup, and Utility Gas Supplies) and Test
Procedure 2 (Carrier and Makeup Gas Flow Adjustments), if not previously
checked.
3. Remove power from the analyzer and open the Controller front door.
4. Locate the Detector Amplifier on the left side wall of the Controller and remove
the six thumb nuts, cover, and plastic shield from the Detector Amplifier.
7. Connect the ohmmeter between one of the thermocouple leads and chassis
ground. The resistance should be high. If it is not high, the thermocouple may
be shorted to chassis ground. Replace the thermocouple (see “FID Repair/
Replacing the Thermocouple” in Section 4).
C6
11. Extinguish the FID flame. The “Flame Out” LED should illuminate. The DVM
should indicate 2.5 mV or less.
12. Ignite flame and the LED should go out. The DVM should indicate 3.0 mV or
greater.
3-22 2000-SVC, C1
13. If the electronics does not perform as described in steps 9 through 11, remove
power and replace the Detector Amplifier.
14. Perform FID cell maintenance for cleaning jet and flame out thermocouple (see
“FID Jet Inspection and Cleaning” in Section 4).
15. Replace the plastic shield, cover, and thumb nuts on the Detector Amplifier.
Verify that the software and hardware temperature parameter values are correct and
have not been inadvertently changed. To perform this operation, it is necessary to
access the temperature configuration table and the manual temperature control
mode.
1. Press the F1 soft key until the Background screen is displayed (see Figure 3-3).
** B A C K G R O U N D **
Process Analytics GCC Remote 01
2020-9A (C) 1997
*** Alarm ***
*** Alarm *** 11-Mar-1997 TUE 08:16:01
*** Alarm ***
Analysis Time :00114 Peaks Found : 00
Cycle Time :00000 State : Idle
F1 F2 F3 F4
2000-SVC, C1 3-23
3. On the Manual Control Mode screen (see Figure 3-4), press the F4 (Press. &
Temp. Control) soft key.
F1 F2 F3 F4
4. On the Pres & Temp Control screen (see Figure 3-5), cursor up or down to
highlight TEMP CONFIGURATION.
TEMP CONTROL
PRES CONTROL
TEMP CONFIGURATION
Temp
Bd View
Escape Config Alarms
F1 F2 F3 F4
3-24 2000-SVC, C1
5. Press the F2 (Temp Bd Config) soft key to view the Temp Config Table screen
(see Figure 3-6). The temperature configuration table is factory set, and is NOT
intended to be field modified. However, in the unlikely event that one of the
parameters was changed, the values should be compared to those in the table
listing provided with chromatograph.
Exit
F1 F2 F3 F4
6. If the values shown in the temperature table agree with those of the listing,
there is no need for table modification. Exit this screen by pressing the F1 (Exit)
soft key and go to step 8.
7. If the values do not agree, the values have been changed since the analyzer
was shipped from the factory. The correct value(s) should be entered. To
modify the temperature configuration table, refer to the “Digital Temperature
Controller” in Section 4 of the Operator’s Manual.
2000-SVC, C1 3-25
9. On the Pressure and Temperature Control screen (Figure 3-5), cursor up or
down until TEMP CONTROL is highlighted. Press the F2 (Manual Temp
Control) soft key to access the Manual Temperature Control Mode screen (see
Figure 3-7).
F1 F2 F3 F4
10. Compare the set point values of temperature zones 1 through 5 with those of
the factory table listing that was provided with the chromatograph. If the values
agree, there is no need to modify the table. Exit this screen by pressing the F1
(Escape) soft key and proceed to step 12.
11. If the values do not agree, the values have been changed since the analyzer
was shipped from the factory. The correct values should be entered.
12. Return to the background screen by repeatedly pressing the F1 soft key until
the Background screen is displayed.
13. From the Background screen press the F1 (Exit to Commands) soft key.
3-26 2000-SVC, C1
****** COMMANDS ******
ANALYSIS CONTROL
REPORTS
TABLE EDIT
PRINTER
STORAGE & CONFIG.
NAMES
MISC.
TESTING/SETUP
SIM DISTILLATION
Go to Other
Background Methods Tables
F1 F2 F3 F4
15. When the Method Table #?? screen appears, enter “1” for the method and then
press the F2 (Edit the Table) soft key.
16. The Cal Define & Cycle Time screen appears. Press the F1 (Continue) soft key
to display the first eight lines of Method Table # 01 (see Figure 3-9).
F1 F2 F3 F4
2000-SVC, C1 3-27
17. Move the cursor up or down to highlight the time associated with Temperature
Control Function Two. Then move the cursor to the right to highlight the value
“Two”. The Temperature Control screen appears (see Figure 3-10).
Exit
F1 F2 F3 F4
18. Compare the set point and ramp rate values with those in the factory table
listings provided with your chromatograph. If they agree, press the F1 (Exit)
soft key. If they do not agree, modify the Temperature Control screen as
explained in “Digital Temperature Controller” (Section 4 in the Operator’s
Manual).
19. Return to background screen by repeatedly pressing the F1 soft key until the
Background screen is displayed.
CAUTION
3-28 2000-SVC, C1
2. If the jet is totally plugged, flame will be extinguished. If restricted, the flame
could possibly still be burning at low intensity.
3. Extinguish flame by reducing burner air, fuel and carrier to zero by rotating
regulator adjustment counterclockwise until burner air fuel and carrier gauges
indicate zero. When flame is out, the “Flame Out” LED will illuminate.
6. Reduce the temperature programmed (if applicable) and isothermal oven air
pressures to zero psig as indicated by their respective gauges.
9. Disconnect the column fitting at the bottom of the FID. Connect the loose
column end to a flow meter.
10. Measure the carrier flow. If flow is restored to the expected measurement, the
jet or breather is plugged. Proceed to step 12. If flow is deficient, reconnect the
column to the FID and perform step 11.
11. Perform Test Procedure 1 (Carrier, Makeup and Utility Gas Supplies), Test
Procedure 2 (Carrier and Makeup Gas Flow Adjustments), and Test Procedure
8 (Column Train Problems), as applicable. If flow is restored, Test Procedure 32
is complete.
12. Remove the breather and replace with a female connector. Attach the flow
meter to the open end of connector. Measure the carrier flow. If flow is restored
to normal, the flame arrester is plugged. Replace the flame arrester.
13. Repeat steps 4 and 5 above. If flow remains restricted, the jet is plugged.
14. Inspect jet by removing FID cap (see “FID Repair” in Section 4). If jet plugging
can not be corrected by removing accumulated matter on jet tip, the FID must
be replaced. The FID must be returned to the factor for jet replacement. See
“FID Repair” in Section 4 for instruction on removing and reinstalling the FID.
15. Disconnect flow meter, reconnect and tighten all fittings, check for leaks,
reattach programmed temperature oven cover and close isothermal oven door
using reverse procedure of steps 7 and 8.
2000-SVC, C1 3-29
2. Observe the peak areas and new response factors. If a greater percentage
change has occurred in the peak height, peak area, and response factors in the
heavier components than in the lighter, the presence of peak discrimination is
apparent.
1. Press the F1 soft key until the Background screen is displayed (see Figure
3-11).
** B A C K G R O U N D **
Process Analytics GCC Remote 01
2020-9A (C) 1997
*** Alarm ***
*** Alarm *** 11-Mar-1997 TUE 08:16:01
*** Alarm ***
Analysis Time :00114 Peaks Found : 00
Cycle Time :00300 State : Idle
F1 F2 F3 F4
3. On the Commands screen (see Figure 3-12) cursor to highlight TABLE EDIT.
Then press the F2 (Methods) soft key.
3-30 2000-SVC, C1
****** COMMANDS ******
ANALYSIS CONTROL
REPORTS
TABLE EDIT
PRINTER
STORAGE & CONFIG.
NAMES
MISC.
TESTING/SETUP
SIM DISTILLATION
Go to Other
Background Methods Tables
F1 F2 F3 F4
4. When the Method Table #?? screen appears, enter “1” for the method number
and then press the F2 (Edit the Table) soft key.
5. The Cal Define & Cycle Time screen appears. Press the F1 (Continue) soft key
to display the first eight lines of Method Table # 01 (see Figure 3-13).
F1 F2 F3 F4
2000-SVC, C1 3-31
6. Refer to the table listings provided with your chromatograph. The function
scheduling should be similar to the following:
3-32 2000-SVC, C1
CALIBRATION STREAM METHOD TABLE
2000-SVC, C1 3-33
The various time coded functions are defined as follows. Section 4 of the Operator's
Manual contains more complete descriptions of these functions.
3-34 2000-SVC, C1
NOTE
3. Replace flame arrester. Check for water in the detector. If necessary clean FID
(see “Cleaning FID/Collector” in Section 4).
2. Cursor to PRINTER and then press the F2 (Test Printer) soft key. A string of
characters should print.
4. Match baud rate, parity, parity check and data bits to printer setup.
5. Check the power. The Disconnect switch or circuit breaker to printer must be
ON.
8. Ensure printer has serial interface installed and set up correctly, using the
printer or interface operations manual.
2. Observe the chromatogram. At the end of the cycle, stop the analysis NOW.
6. Turn off power and sample to analyzer. Replace sample valve seals and O-
rings (see “Sample Valve Repair” in Section 4).
2000-SVC, C1 3-35
7. Restore power and allow temperature zones to come to temperature and
stabilize.
CAUTION
4. If current output, disconnect one wire from the output to be tested, and place
the milliammeter in series with the load. See output terminal assignment
below.
1 1 2 5
2 3 4 5
3 6 7 10
4 8 9 10
5 11 12 15
6 13 14 15
7 16 17 20
8 18 19 20
9 21 22 25
10 23 24 25
11 26 27 30
12 28 29 30
13 31 32 35
14 33 34 35
15 36 37 40
16 38 39 40
3-36 2000-SVC, C1
6. On the Background screen, press the F1 (Exit to Commands) soft key.
9. Enter the a trend test value. The output signal at the meter should respond to
equivalent percentage of output. Test for low, middle, and high.
10. If output does not respond or does not reach the expected output value, check
the following:
a. Connect meter to the output terminal strip TB7 (see connection list
below) of the analyzer and repeat step 9. If functioning normally,
problem is in loop wiring, connection, or input device and proceed to
step 11.
11. If board functions normal locally, but receiving device is not correctly reporting
signal, check the following:
a. With authorized permission, remove one wire from input device of loop
to be tested and connect the ammeter in series (voltage parallel).
Perform step 9 to determine if loop wiring to input device is functional.
CAUTION
2000-SVC, C1 3-37
1. On the Background screen, press the F1 (Exit to Commands) soft key.
4. Connect ohmmeter between output terminal of Digital PCB and output common
using proper polarity (these are transistor outputs).
6. If Digital I/O PCB does not function, it is defective. Replace the Digital I/O PCB.
CAUTION
3. If top LED is not active (flickering), there is no transmit activity. The analyzer is
off line with VWS. This must be corrected by accessing the Command Mode
parameters.
5. If the bottom LED is not active (flickering), there is no data receive activity. The
VWS is not functioning or there is a possible wiring or connection problem.
3-38 2000-SVC, C1
3.41 TP 41: LOW CARRIER PRESSURE
CAUTION
1. Check to ensure that the carrier has not been shut off. If so, restore carrier
supply.
4. Connect ohmmeter leads between the two wires previously disconnected from
J23A terminals 1 and 2.
6. The switch contacts should close. Remove carrier pressure; switch contacts
should open.
7. If switch does not function as described, remove carrier pressure and replace
pressure switch.
8. If switch functions as described in step 7, but the alarm remains after the switch
wiring has been reconnected and carrier applied, replace Chroma I/O PCB.
CAUTION
1. Check to ensure that the sample flow has not been shut off. If so, restore
sample flow.
2000-SVC, C1 3-39
2. Disconnect power to the analyzer.
5. With sample flowing, the switch should open. Stop sample flow and the switch
should close.
7. If switch functions as described in step 5, but the alarm remains after the switch
wiring has been reconnected and sample flow established, replace Chroma I/O
PCB.
CAUTION
2. Check air pressure for correct adjustment. Perform Test Procedure 1 (Carrier,
Makeup, and Utility Gas Supplies).
5. Monitor the actual zone 2 temperature. When it reaches 100 degrees, change
the set point to the normal initial set point value and rate to 0.1.
6. You should hear the coolant solenoid valve operate and hear a sudden
discharge of air into the programmed temperature oven.
7. If you do not hear the solenoid valve operate, override the X purge using the
procedure given in Section 4 of the Operator’s Manual. If you hear the solenoid
valve switch, proceed to step 23.
8. Open electronics housing door. LED DS8 should be illuminated. If not, replace
temperature control board.
3-40 2000-SVC, C1
9. Access the Manual Temperature Control Mode by performing steps 1 to 3, 8
and 9 of Test Procedure 31 (Checking Temperature Table Values). Change
zone 2 set point to 220 and rate to 50.
10. Connect voltmeter leads across J42D terminals 1 and 2 and check for the
presence of zero VAC.
11. Monitor the actual zone 2 temperature. When it reaches 100 degrees, change
the set point to the initial set point value and rate to 0.1.
12. Connect voltmeter leads across J42D terminals 1 and 2 and check for the
presence of 115 VAC. If voltage is present, replace the solenoid valve.
13. If no voltage is measured between J42D terminals 1 and 2, check for presence
of 115 VAC between J42C terminals 1 and 2.
14. If voltage is not present at J42C terminals 1 and 2, check for 115 VAC at J46A
terminals 1 and 2.
15. If voltage is present at J46A terminals 1 and 2, shut off power and replace
motherboard.
16. If voltage is present at J46D terminals 1 and 2, remove power from the
analyzer.
17. Disconnect the solenoid valve coil wires from J42D terminals 1 and 2 and
connect an ohmmeter between the solenoid valve wire leads. The solenoid coil
will have a small resistance. Check each lead to chassis ground. If shorted to
ground or questionable, replace solenoid valve or coil. Inspect leads for bare
insulation that could contact chassis or other grounded part and make
necessary repairs.
18. Disconnect the solenoid valve coil wires from J42D terminals 1 and 2 and
connect an ohmmeter between the solenoid valve wire leads. If the coil
resistance is extremely high or infinity, replace the solenoid valve or coil and
fuse. Repeat procedure in step 17.
20. Check vortex cooler efficiency in the following manner. Access the Manual
Temperature Control Mode by performing steps 1 to 3, 8 and 9 of Test
Procedure 31 (Checking Temperature Table Values). Change zone 2 set point
to 0 deg and rate to 0.1.
21. Monitor the actual zone 2 temperature until temperature measurement is stable.
WARNING
Discharge air from the vortex cooler is extremely hot and can cause
severe burns.
22. Protecting your hands with insulated gloves, adjust the vortex cooler at the
discharge end for maximum cooling (minimum temperature) as indicated on
actual zone temperature.
2000-SVC, C1 3-41
23. Enter set point at initial temperature.
CAUTION
4. If air operated valves are used for stream switching, verify actuation air is being
applied to the stream select valve actuator. Gently loosen the two fittings at the
actuator. Apply “Leak Tech”, “Snoop” or other similar liquid leak detector to the
back of the fittings.
5. Request an analysis for the steam in question. At stream step, the stream will
begin to purge as indicated on the background screen. Actuation air will be
applied to the respective actuator, producing bubbles at the loose fitting. When
the next different stream is selected, bubbles should cease at the present
actuation line. If the actuation is double acting, air will be present at the other
actuation line and bubbles will be produced by the leak detector. All streams
can be tested in this manner. Reconnect or tighten each fitting that was
loosened.
7. If air is applied to the solenoid valve, test to ensure that the solenoid actuation
voltage is being applied.
9. Loosen the four screws that retain the front cover of the heater box.
10. Request an analysis for the stream in question. At stream step the stream will
begin to purge as indicated on the background screen. Connect voltmeter
3-42 2000-SVC, C1
leads across the stream switch soleniod valve (process) or the calibration
solenoid valve (calibration). The voltage to the solenoid valve should measure
110 VDC when the valve is on and zero volts when the valve is off. If the
voltage is being applied, yet the valve is not switching, replace the solenoid
valve.
11. If no voltage is present, remove power and disconnect both solenoid valve
leads.
12. Connect an ohmmeter between the two solenoid valve coil leads. If open,
(extremely high resistance), replace the solenoid valve or coil.
14. Apply power to analyzer and switch D.C. solenoid driver using procedure in step
8.
15. If voltage does not switch, replace D.C solenoid valve driver PCB.
17. Reconnect and tighten all loose or disconnected fittings, and check for and
repair any leaks.
2000-SVC, C1 3-43
For further information or assistance contact:
3-44 2000-SVC, C1
SECTION 4. REPAIR
Temperature
Sensor
Detector
Thermocouple
Oven
Heater
CAUTION
1. Open the Controller front and side doors and the isothermal oven door.
2. On the Zone 1 PCB in the Digital Temperature Controller, disconnect J49B and
remove the isothermal oven heater wires from pins 1 and 2.
3. On the Zone 1 PCB, disconnect J49A and remove the thermocouple wires from
pins 1 and 2.
4. On the DTC Backplane PCB disconnect J42A and remove the thermocouple
wires from pins 1 and 2.
5. Connect a small feeder wire (at least 36 inches long) to one of the heater wires.
2000-SVC, C1 4-1
6. In the isothermal oven disconnect the 1/4-inch fitting from the heater.
8. Withdraw the heater and wires from the feedthrough grommet and into the
oven.
9. Connect the wires from the new heater assembly to the feeder wire pulled
through the tubing.
10. Install the new heater assembly using the reverse procedure, pulling the wires
through the tubing.
WARNING
Sample will spill or leak out during this procedure. Consult MSDS
sheets on file at your location for safety requirements.
CAUTION
1. Remove power, sample flow, and air from analyzer and allow to cool.
2. Open the Controller front and side doors, and the isothermal oven door.
3. Locate the Zone Sense Board and disconnect the LSV heater and sensor
wires.
4. Withdraw the free end of the vaporizer cable from beneath the Card Cage into
the Controller housing.
4-2 2000-SVC, C1
5. Inside the isothermal oven, loosen any cable clamps securing the vaporizer
cable assembly and free the cable.
9. Support the valve with your hand and remove the four Allen screws securing
the valve to the analyzer.
11. Remove the vaporizer assembly collar from the valve, separate the vaporizer
halves, and remove the vaporizer.
12. Reassemble and connect the vaporizer using the reverse procedure.
You must take extreme care to avoid having the sample lines exert force on the
sample connections of the Model 791 Liquid Sample Valve. For example, if stiff 1/4-
inch tubing or heat-traced lines are bent into position and attached to the valve, the
force will cause premature failure of the valve and possibly bend the stem. A loop of
1/8-inch tubing or a flex hose is recommended between the valve and the sample
line (this may be insulated if necessary).
It is also important to use two wrenches when tightening the sample line
conncections to the sample chamber. One wrench must be used to back up the
force applied to tighten the fitting (direct wrench force will bend the stem).
4 6
3 7
1 5 8
2
9
22
21
17
20
16
15 14
19 18 13 12 11 10
WARNING
Sample will spill or leak out during this procedure. Consult MSDS
sheets on file at your location for safety requirements.
2000-SVC, C1 4-3
Sample valve repair may necessitate the venting of flammable
substances into the atmosphere surrounding the analyzer. Remove
power from all sources of ignition in the immediate area. Do not open
any purged enclosures that remain powered.
CAUTION
4.2.1 Disassembly
3. Remove the two cone point set screws (1 in Figure 4-2) from the cylinder (22).
4. Slide the cylinder (22) off of piston (21) and body (2).
5. Using an Allen wrench, rotate the sleeve (20) counterclockwise until it is loose.
6. Unscrew the body (2) from the flange (13) and vaporizer chamber (10).
8. Slide the seal (3) from the stem (12) using sample chamber (4).
9. Withdraw the piston (21) and the rod assembly (18) from the sleeve (20).
10. This will free the seal (3) from the stem (12).
11. Inspect the seals for visible imperfections. If imperfections are found, replace
the seals.
12. Inspect the stem for visible imperfections. If imperfections are found, replace
the stem.
13. Remove the rear valve seat (14) from the body (2).
14. Remove the nine Belleville springs (15) from the body (2).
4-4 2000-SVC, C1
15. Remove the O-ring (19) from the body (2) and piston (21).
16. Unscrew the piston rod (18) from the piston (21). and extract the stem assembly
(12) from the piston rod (18).
17. Remove the O-ring (16) from the piston rod (18).
NOTE
2. Clean the sample chamber (10) with acetone and dry it.
3. Lightly lubricate O-Ring (17), sleeve threads (2), and internal threads and bore
of the body (2) with High Vacuum Grease.
5. Screw the sleeve (20) into the body (2) until the back of the sleeve (20) is flush
with the ears on the back of the body (2), then back the sleeve (20) out 1-1/2
turns.
6. Lightly lubricate the O-ring (16) and the threads of the piston rod (18). Install
the O-ring (16) onto the piston rod (18). Do not allow grease to enter the small
hole through the center of the piston.
7. Insert the stem assembly (12) into the rear of the piston rod (18). Screw the
piston rod (18) into the piston (21) and tighten to 27-30 in-lb. Do not overtighten
or bend the rod or stem! Do not allow grease to contact the stem.
8. Lightly lubricate the two O-rings (19). Install the O-rings (19) onto the body (2)
and the piston (21).
9. Insert the piston (21) and the rod assembly (18) into the sleeve (20). Be careful
not to cut the O-ring. Fully insert the piston (21) until it contacts the stops.
10. Stack the nine Belleville springs (15) (stack opposed) onto the 1/4-inch thin wall
plastic tubing. Using the tubing as a guide, slide the springs (15) over the stem
(12) into the bore of the body (2).
11. Install the rear valve seat (14) over the stem (12) and let it rest against the
springs (15). Do not allow the seat to scratch the stem.
12. Clean all the exposed area of the stem (12) with acetone. Ensure the stem and
groove are free of grease and contamination. Inspect the stem for visible
imperfections. If imperfections are found, replace the stem.
2000-SVC, C1 4-5
13. Slide the first cleaned seal (3) over the stem (12) using the “A” end of Seal
Insertion Tool TL-791A006B. The 30° angle (pointed end) of the seal (3) must
face the springs (15).
14. Slide the cleaned sample chamber (4) over the stem onto the seal (3).
15. Slide the second cleaned seal (3) over the stem (12) using the “B” end of Seal
Insertion Tool TL-791A006B. The 30° angled (pointed end) of the seal (3) faces
out, away from the sample chamber (4).
16. Install the vaporizer chamber (10) into the flange (13) as shown. Lightly
lubricate the threads on the body (2). Screw the body (2) into the flange (13)
against the vaporizer chamber (10) until tight. The sample chamber (4) should
be loose in the assembly at this point. If not, back out the sleeve (20) until the
sample chamber (4) is loose. Use the end of a 0.156 Allen wrench in the slot
of the sleeve (20) to adjust to the point of eliminating the longitudinal play of the
sample chamber (4).
17. Tighten the sleeve (20) in five 1/4-turn increments (1-1/4 turns total) to preload
the seals.
18. Lightly lubricate the inside bore of the cylinder (22). Align the fittings on the
cylinder (22) with the sample chamber (4) tubes, or with air lines if servicing.
Slide the cylinder (22) onto the piston (21) and the body (2). Install two cone
point set screws (1) into the cylinder #(22) and tighten into the groove on the
body (2).
NOTE
CAUTION
4-6 2000-SVC, C1
3. Reduce Isothermal Oven temperature by reducing oven air pressure to zero
psig.
4. Shut off carrier and other FID makeup gases (if applicable).
6. To remove the column, loosen the fittings on bothe ends of the column and
gently extract the column from the respective fitting connections.
7. Loosen any screw securing the column to the column mounting brackets and
remove the column.
1. Install the column, orienting it in such a way that one end can be connected to
the fitting at the LSV and the other into the bottom of the detector.
2. Fasten and secure column in place at the column mounting bracket with the
retaining screws.
3. Insert the column end into the appropriate fitting connection and finger-tighten
the nut. Then tighten it an additional 1/4 turn and test column for a secure
connection.
4. Apply carrier gas and leak check. Further tighten the two fittings as required to
ensure no leaks are present.
1. Inspect the ends of the column. The ends should be round and burr free. If
either column end is not round or burr free, the column end must be trimmed as
described in paragraph 4.3.4.
2. Insert the end of the column through the back of the tubing nut.
4. Slide the ferrule down the length of the column approximately three inches.
5. Insert the extended column length and the end of the ferrule into the
appropriate tubing connection at the sample valve.
6. Connect the tubing nut and finger-tighten; then tighten it an additional 1/4-turn
with an open-end wrench.
2000-SVC, C1 4-7
7. Test the column for a secure connection by gently pulling the column at the 1/8-
inch tubing nut. Any withdraw should be corrected. Continue to tighten the nut
until the column is securely connected at the fitting.
9. For columns connected to a Model 799 FID, insert the column end into the FID
analysis inlet connection until it stops against the jet. Then withdraw the column
approximately 1/16-inch and tighten the nut finger tight. Tighten the nut an
additional 1/4-turn with an open-end wrench, then check it for a secure fit.
NOTE
10. Apply carrier gas and check for leaks. Further tighten the two fittings as
required to stop any leaks.
12. Perform the analyzer startup procedure as described in the Operator’s Manual.
The procedure for cutting Glass or Metal Capillary Columns is the same, except that
a small sharp file may be used to score metal columns.
NOTE
1. Use a diamond or ceramic scoring tool to score the surface of the outside
tubing wall approximately one inch from the end of the column. Take care not to
cut through the tubing wall.
2. Wipe the scored area clean to prevent material from entering the column.
3. Secure the column with your fingers 1/2-inch on each side of the score and
gently bend the tubing at the score, in the direction opposite the score. When
the score point opens, bend the tubing back towards the score. The tubing
should make a clean break.
4. Inspect the end of the column for roundness and ensure it is burr free. If the
end is not round and burr free, repeat the procedure until it is.
4-8 2000-SVC, C1
CAUTION
NOTE
Breather Microdot
Adapter Connector
Thermocouple
Polarizer
Ignitor
Jet
CAUTION
2000-SVC, C1 4-9
CAUTION
Caution should be used when working with the soldering iron. The
soldering iron, melted solder and heated wiring can cause severe
burns. Safety glasses and protective gloves should be used to
protect against hot molten solder and hot surfaces. Personal
protective equipment such as goggles , face shield, lab coat and
rubber gloves should be used while cleaning with solvents such as
acetone. Cleaning with solvents should be done in a well ventilated
area.
2. Turn off oven air to the Isothermal Oven and allow all temperature zones to
cool.
4. For temperature programmed units, you must remove the insulated covers
surrounding the FID cell body to access any of the FID cell internal
components.
1. Disconnect the red coaxial cable located on the top of the detector.
2. Loosen the breather set screw using a 0.050-inch Allen wrench, then extract
the adapter fitting from the detector.
4. Remove the breather with adapter fitting from the analyzer oven.
5. Remove the adapter fitting from the breather using 3/4-inch and 1/2-inch open-
end wrenches.
6. Using a 3/4-inch open-end wrench and a 1/2-inch backup wrench, remove the
1/4-inch male connector from the existing breather.
7. Remove the existing Teflon tape from the nipple of the adapter fitting and apply
new tape.
8. Remove the existing Teflon tape from the male connector and apply new tape.
9. Install the detector outlet adapter into the breather and finger tighten. Finish
tightening using 3/4-inch and 1/2-inch open-end wrenches.
10. Install the 1/4-inch male connector into the breather using 3/4-inch and 1/2-inch
open-end wrenches.
11. Connect the 1/4-inch detector vent tubing to the breather. Finger tighten, then
tighten with a 9/16-inch open-end wrench and a 1/2-inch backup wrench.
12. Ensure the detector vent O-ring is in place in the adapter fitting.
4-10 2000-SVC, C1
13. Finish installing the breather by inserting the cylindrical end of the adapter
fitting completely into the detector outlet and tightening the set screw with a
0.050-inch Allen wrench. Note the set screw will fit into the groove of the
adapter fitting when installed correctly.
14. Reconnect the red coaxial cable to the top of the detector.
1. Disconnect the red coaxial cable located on the top the detector.
2. Locate the thermocouple assembly as identified by the two red and black
wires.
3. If applicable, remove any cable ties and free the wiring to expose the wire
splices.
4. Cut and remove the heat shrink and glass tape from the red and black wires to
expose the soldered connections.
7. Carefully insert the replacement thermocouple into the detector body and finger
tighten, taking care not to damage it. Finish tightening using a 3/8-inch open-
end wrench.
8. Roll each end of the red and black wires of the new thermocouple assembly
between your forefinger and thumb, causing the wire ends to be tightly spiral
wrapped.
9. Using the 40 watt soldering iron and approved high temperature solder, “tin” the
wire ends.
10. Spread or expand the end of approved heat shrink to allow easy installation
over the solder connection.
11. Install the heat shrink over each of the wires and slide it as far as possible from
the connection. This will prevent premature shrinking of it when the connection
is soldered.
12. Overlap the “tinned” ends of the red wire from the analyzer electronics and red
element assembly wire, then solder the wires together using approved high
temperature solder and the 40 watt soldering iron.
15. Slide the heat shrink over the soldered connection and shrink it with a heat gun.
2000-SVC, C1 4-11
16. Reconnect the red coaxial cable to the top of the detector.
The following procedure is used to access the polarizer and ignitor detector
elements.
1. Disconnect the red coaxial cable located on the top of the detector.
2. Cut cable ties securing the detector element assembly wiring and straighten the
wires to increase accessibility.
4. Visually trace the capillary tubing connections from the detector to the nearest
unions. Place temporary tape labels on each side of the union tubing
connections.
NOTE
6. Rotate the detector cover latch counterclockwise until it is freed from the
detector body.
7. Slide the detector cover from the detector heater housing and set aside.
8. Remove enough of the insulation from the detector heater housing to expose
the polarizer and ignitor; retain it for later use.
9. Position the wiring and capillary tubing such that the housing can be lifted from
the detector base up over the detector, then lift off the housing, fully exposing
the detector body and elements.
2. If applicable, remove any cable ties and free the wiring to expose the wire
splices.
3. Cut and remove the heat shrink and glass tape from the green wire to expose
the soldered connection.
4-12 2000-SVC, C1
6. Carefully insert the replacement polarizer into the detector body and finger
tighten, taking care not to damage it. Finish tightening using a 3/8-inch open-
end wrench.
7. Roll each end of the green wire of the new polarizer between your forefinger
and thumb, causing the wire ends to be tightly spiral wrapped.
8. Using the 40 watt soldering iron and approved high temperature solder, “tin” the
wire ends.
9. Spread or expand the end of approved heat shrink to allow easy installation
over the solder connection.
10. Install heat shrink over each wire and slide it as far as possible from the
connection. This will prevent premature shrinking when the connection is
soldered.
11. Overlap and solder the “tinned” ends of the green wire from the wiring harness
and the green polarizer assembly wire using approved high temperature solder
and 40 watt soldering iron.
13. Slide the heat shrink over the taped connection and shrink it with a heat gun.
2. If applicable, remove any cable ties and free the wiring to expose the wire
splices.
3. Cut and remove the heat shrink and glass tape from the two white wires to
expose the soldered connections.
6. Carefully insert the replacement ignitor into the detector body and finger
tighten, taking care not to damage it. Finish tightening using a 3/8-inch open-
end wrench.
7. Roll each end of the two white wires of the new ignitor between your forefinger
and thumb, causing the wire ends to be tightly spiral wrapped.
8. Using the 40 watt soldering iron and approved high temperature solder, “tin” the
wire ends.
9. Spread or expand the end of approved heat shrink to allow easy installation
over the solder connection.
2000-SVC, C1 4-13
10. Overlap and solder the “tinned” ends of one white wire from the wiring harness
and one white ignitor assembly wire and solder the wires together using
approved high temperature solder and 40 watt soldering iron.
13. Slide the heat shrink over the taped connection and shrink it with a heat gun.
The following procedure is used to close the detector after replacing the polarizer or
ignitor.
NOTE
3. Slide the housing down over the insulation and detector body onto the base.
The housing must slide over the circular base and rest on the mounting
bracket.
4. Bend the capillary tubing back into place, then route the wiring to the back of
the detector housing and install insulation into the housing.
5. Install the detector cover by channeling the cover slot through the machined
groove in the detector body, while sliding the cover into place. Note that the
wiring exits through the slot in the cover, and that the capillary tubing exits the
can through the sheared edge of the top cover.
6. Rotate the detector cover latch clockwise until is secured by the detector. Note
the small slot in the latch also fits into the same machined groove the cover fits.
8. Using the previously installed temporary labels, connect the capillary tubes to
their respective unions.
11. Install the red coaxial cable to the connector on top of the detector.
4-14 2000-SVC, C1
4.4.8 Cleaning the FID Jet
NOTE
1. Remove the three screws securing the detector can assembly, using a 9/64-
inch Allen wrench or ball driver.
3. CENELEC and CSA Model 799 flame ionization detectors are identified by the
presence of three packing adapter nuts (5/8-inch, 1/2-inch and 7/16-inch).
Other models contain only two packing adapter nuts (5/8-inch and 1/2-inch).
4. On CENELEC AND CSA models, loosen the 7/16-inch packing adapter nut
using a 7/16-inch open-end wrench, backed up with a 1/2-inch open-end
wrench on the
1/2-inch packing adapter nut. Continue to loosen by hand until disconnected.
5. For all models, loosen the 1/2-inch packing adapter nut using a 1/2-inch open-
end wrench with a 5/8-inch open-end back-up wrench. Continue to loosen by
hand until disconnected.
6. Withdraw the column and associated ferrules and adapters from the detector.
7. Loosen the 5/8-inch adapter fitting from the bottom of the detector.
8. Extract the jet with the adapter fitting from the jet cavity in the detector.
9. Inspect the end of the jet for damage. It should not be pitted or plugged. If
pitted, replace with a new jet.
10. Insert a 0.016-inch diameter piano wire into the jet and rod it out. If the piano
wire will not pass through, replace the jet.
11. Using a syringe and protective equipment and clothing, flush the jet with a mild
solvent such as acetone; then blow dry with 15 psig clean air, nitrogen or
helium.
12. Use a 5/8-inch adapter fitting to insert the jet into the jet cavity. Finger tighten
and finish tightening using a 5/8-inch open-end wrench.
13. Insert the column end, ferrule and adapter nut into the detector inlet and finger
tighten; then loosen 1/8 turn.
14. If the ferrule was loose and slid any length on the column, continue to push the
column into the detector analysis inlet until it stops.
15. Withdraw the column approximately one mm and tighten the 1/2-inch adapter
nut finger tight. Tighten the nut an additional 1/4 turn with a 1/2-inch open-end
wrench; then check it for a secure fit by gently attempting to pull the column
slightly away from the detector. Carefully tighten the adapter until the column is
secure.
2000-SVC, C1 4-15
16. For CENELEC and CSA models, slide the 7/16-inch packing adapter nut and
ferrule toward the detector and install finger tight. Tighten the nut an additional
1/4 turn with a 7/16-inch open-end wrench.
17. For temperature programmed units, install the detector can assembly and
secure it with the hex head screws using a 9/64-inch Allen wrench or ball driver.
Be sure to align the three holes such that the edge of the can is parallel with
edge of the temperature programmed oven.
2. Disconnect the column and remove the jet as described in paragraph 4.4.8.
6. Remove the polarizer and ignitors described in paragraphs 4.4.5 and 4.4.6.
7. Use a small stainless steel brush precleaned with acetone to remove chloride
accumulations from the collector, by inserting the brush through the detector
inlet connection and briskly scrubbing with an in-and-out motion.
10. For temperature programmed units, install and secure the temperature
programmed oven covers.
NOTE
1. Disconnect the Microdot connector located on the top of the detector (see
Figure 4-3).
2. Cut the cable just below where it passes through the Oven into the Control
Housing and remove the cable from the Oven.
3. Disconnect the other end of the cable from the FID Amplifier Assembly and
remove the cable from the Control Housing.
4-16 2000-SVC, C1
4. Remove the grommets from the grommet holes (located in the bottom of the
Control Housing and the top of the Oven) that will accommodate the routing of
the new cable.
5. The new FID Cable Assembly has a Microdot connector on one and and a BNC
connector on the other end (see Figure 4-4). Screw the Microdot connector end
of the new cable assembly into the Insertion Tool.
Microdot BNC
Connector Connector
6. Pass the Insertion Tool through the grommet holes from the Control Housing to
the Oven.
8. Make a slit in each grommet from the outer diameter to the inner hole. (This is
necessary because the cable connector will not pass through the grommet.)
9. Position the cable in the grommets in the Control Housing and the Oven.
11. Connect the cable connectors to their respective locations (BNC connector to
the FID Amplifier Assembly and Microdot connector to the top of the detector).
Refer to Figure 4-5 for Filament Thermal Conductivity Detector (TCD) component
location.
Reference Measure
Filament Filament
Reference Vent
Sample In
Sample Vent
Reference In TC Assembly
2000-SVC, C1 4-17
CAUTION
CAUTION
The filaments are fragile and can be easily damaged if not handled
with extreme care. Do not touch the end of the elements.
2. Turn off oven air to the Isothermal Oven and allow all temperature zones to
cool.
1. Use a Phillips screwdriver to loosen the two Phillips head screws located on
the front underside of the mounting bracket.
2. Remove the mounting bracket cover by sliding it out and away from the detector
assembly.
4. If they are not already labeled, label the wire pair connected to the
measurement filament “M” and the wire pair connected to the reference filament
“R”.
4-18 2000-SVC, C1
5. If the detector filament wiring connections are spliced, perform steps 6 through
8. If they are not spliced, go to step 9.
6. Position the detector wiring such that the wired splices can be accessed.
7. Cut and remove the heat shrink from each of the spliced filament wire
connections to expose the soldered connections.
8. Using a 40 watt soldering iron, de-solder and disconnect the wire splices.
9. If the detector filament wiring connections are not spliced, cut the existing
detector harness wires approximately three inches from the detector end.
10. Remove the harness retaining clamp and free the harness.
11. Clean the area around the two detector filaments to reduce the chance of
foreign particles entering the detector cavity when the filaments are removed.
12. Loosen the two detector filament retaining gland nuts with a 3/8-inch open-end
wrench. Continue to loosen by hand.
13. Carefully extract the filaments from the detector cell cavity.
Replacement filament installation kits are supplied with two cable glands, a wire
spreader, 736 RTV, high temperature solder, and heat shrink.
1. Cut the four filament wires approximately the same length as the wires on the
filaments that were removed.
2. Insert one pair of filament wires through the threaded end of the gland nut, then
carefully insert the filament into the detector cell cavity marked “M”
(measurement).
3. Slide the nut down the length of the wires to insert and align it with the
measurement cavity.
4. Tighten the cable gland finger tight, then finish tightening with a 3/8-inch open-
end wrench.
5. Insert the second pair of filament wires through the threaded end of the gland
nut, then carefully insert the filament into the detector cell cavity marked “R”
(reference).
6. Slide the nut down the length of the wires to insert and align it with the
reference cavity.
7. Tighten the cable gland finger tight, then finish tightening with a 3/8-inch open-
end wrench.
8. Using wire strippers, remove approximately 1/4 inch of insulation from the end
of each detector filament wire.
2000-SVC, C1 4-19
4.5.4 Filament Checkout
1. Obtain a multimeter and select the ohms function and a range capable of
measuring 40 ohms.
3. Connect one multimeter lead to each wire of the reference filament (installed in
the detector cavity labeled “R”). The resistance measurement should be within
one ohm of the measurement filament resistance.
4. If the resistance measurements are not within one ohm of each other, ensure
the multimeter is connected and functioning correctly, and that the correct meter
function is selected.
5. If the detector filaments are not in tolerance, the detector filaments are
defective. The filaments must be replaced and the checkout repeated.
6. Neither filament should contact the detector cell body. Connect the multimeter
leads to one of the filament wires and the detector cell body. The meter reading
should range from several hundred megohms to infinity.
7. Repeat this measurement for each of the other three filament wires. If all
resistance measurements are correct, go to subsection 4.5.5. If any resistance
is too low, go to step 8.
9. Inspect the filament for damage or bending. If it is damaged, the filament pair
will have to be replaced.
10. If the filament is slightly bent, use small needle nose pliers to gently and
carefully bend it straight.
11. If the filament orientation now appears to be correct, reinstall the detector
filament and repeat the complete checkout. If it fails again, replace the detector
filament pair and repeat the harness checkout.
12. If the filament is damaged during this attempted correction process, the
filament pair will have to be replaced.
1. Roll the ends of each stripped harness wire between your thumb and index
finger to tightly spiral wrap the wire ends.
2. Using a 40 watt soldering iron and approved high temperature solder, “tin” each
of the harness wire ends.
4-20 2000-SVC, C1
3. Roll the ends of each stripped filament wire between your thumb and index
finger to tightly spiral wrap the wire ends.
4. Using a 40 watt soldering iron and approved high temperature solder, “tin” each
of the filament wire ends.
5. Slide the insulating sheath of each filament back to reveal the stranded wire,
install approved heat shrink over each of the four filament wires, and slide it as
far from the free wire end as possible.
6. Select a harness assembly wire with the “R” label designation and overlap the
“tinned” ends of this harness wire with one of the reference filament wires.
7. Solder the wires using a 40 watt soldering iron and approved high temperature
solder. Apply solder sparingly, allowing it to flow evenly. Do not overheat the
solder or a high resistance connection could result.
8. Repeat steps 6 and 7 for the remaining harness wire labeled “R” and reference
filament wire.
9. Repeat steps 6 through 8 for the harness wires labeled “M” and the
measurement wires.
10. Slide heat shrink over each connection and shrink with a heat source.
1. Restore carrier to the analyzer and establish carrier flow to both the
measurement and reference ports of the detector.
2. Verify carrier and reference flow using a flow meter. Typically the flows should
be 30 to 40cc per minute if packed columns are used; 10 to 15 cc per minute if
0.53 mm ID capillary columns are used, and 3 to 5 cc per minute if 0.32 mm ID
capillary columns are used.
3. Test for leaks around the detector filament gland nut with a nonconductive liquid
leak detection solution. Correct all leaks before proceeding.
5. Gently remove any excess leak detection solution with a soft cloth or tissue and
blow dry with 15 psig clean dry air, helium or nitrogen.
Perform this procedure if you know that your analyzer is constructed to CENELEC
or CSA specifications or the if existing detector filament is potted.
1. Gently slide the insulation sheath out of and away from the gland nut.
2. Using a syringe filled with Silastic compound “Dow 736 RTV,” completely fill the
gland cavity with the Silastic compound.
3. With the insulation still pulled away from the gland nut, use needle nosed pliers
to install the wire spreader.
2000-SVC, C1 4-21
4. Separate and insert filament wires into the slots on either side of the spreader.
The spreader should be positioned between the end of the sheath insulation
and the back of the gland nut.
5. Press the spreader into the recess in the gland nut. The retainer must be
installed such that it is not in anyway tilted. It is normal for the retainer to
protrude slightly from the gland recess.
6. Slide the sheath insulation toward the wire spreader until it contacts the face of
the spreader.
8. Install the mounting bracket cover and secure it with two Phillips head screws.
Refer to Figure 4-6 for Thermistor Thermal Conductivity Detector (TCD) component
location.
Measure Reference
Thermistor Thermistor
CAUTION
4-22 2000-SVC, C1
4.6.1 T/C Detector Access
CAUTION
The filaments are fragile and can be easily damaged if not handled
with extreme care. Do not touch the end of the elements.
2. Turn off oven air to the Isothermal Oven and allow all temperature zones to
cool.
1. Use a Phillips screwdriver to loosen the two Phillips head screws located on
the top cover.
2. Remove the top cover by sliding it out and away from the detector assembly.
4. If they are not already labeled, label the wire pair connected to the
measurement thermistor “M” and the wire pair connected to the reference
thermistor “R”.
5. Position the detector wiring such that the wired splices can be accessed.
6. Cut and remove the heat shrink from each of the spliced thermistor wire
connections to expose the soldered connections.
7. Using a 40 watt soldering iron, de-solder and disconnect the wire splices.
2000-SVC, C1 4-23
8. Clean the area around the two detector thermistors to reduce the chance of
foreign particles entering the detector cavity when the thermistors are removed.
9. If necessary, remove the two standoffs that hold the top cover in place and
retain them for re-installation.
10. Loosen the two detector thermistor retaining gland nuts with a 5/16-inch open-
end wrench. Continue to loosen by hand.
11. Carefully extract the thermistors from the detector cell cavity.
1. Cut the four thermistor wires approximately the same length as the wires on the
thermistors that were removed.
2. Insert one thermistor assembly into the detector cell cavity marked "M"
(measurement) and screw the cable gland finger tight.
4. Insert the second thermistor assembly into the detector cell cavity marked “R”
(reference) and screw the cable gland finger tight.
6. Using wire strippers, remove approximately 1/4 inch of insulation from the end
of each detector thermistor wire.
1. Obtain a multimeter and select the ohms function and a range capable of
measuring 40 ohms.
3. Connect one multimeter lead to each wire of the reference thermistor (installed
in the detector cavity labeled “R”). The resistance measurement should be
within one ohm of the measurement thermistor resistance.
4. If the resistance measurements are not within one ohm of each other, ensure
the multimeter is connected and functioning correctly, and that the correct meter
function is selected.
5. If the detector thermistors are not in tolerance, the detector thermistors are
defective. The matched set of thermistor assemblies must be replaced and the
checkout repeated.
4-24 2000-SVC, C1
6. Neither thermistor should contact the detector cell body. Connect the
multimeter leads to one of the thermistor wires and the detector cell body. The
meter reading should range from several hundred megohms to infinity.
7. Repeat this measurement for each of the other three thermistor wires. If all
resistance measurements are correct, go to subsection 4.6.5. If any resistance
is too low, go to step 8.
9. Inspect the thermistor for damage or bending. If it is damaged, the matched set
of thermistor assemblies will have to be replaced.
10. If the thermistor is slightly bent, use small needle nose pliers to gently and
carefully bend it straight.
11. If the thermistor orientation now appears to be correct, reinstall the detector
thermistor and repeat the complete checkout. If it fails again, replace the
matched set of thermistor assemblies and repeat the harness checkout.
12. If the thermistor is damaged during this attempted correction process, the
matched set of thermistor assemblies will have to be replaced.
1. Roll the ends of each stripped harness wire between your thumb and index
finger to tightly spiral wrap the wire ends.
2. Using a 40 watt soldering iron and approved high temperature solder, “tin” each
of the harness wire ends.
3. Roll the ends of each stripped thermistor wire between your thumb and index
finger to tightly spiral wrap the wire ends.
4. Using a 40 watt soldering iron and approved high temperature solder, “tin” each
of the thermistor wire ends.
5. Install approved heat shrink over each of the four thermistor wires and slide it
as far from the free wire end as possible.
6. Select a harness assembly wire with the “R” label designation and overlap the
“tinned” ends of this harness wire with one of the reference thermistor wires.
7. Solder the wires using a 40 watt soldering iron and approved high temperature
solder. Apply solder sparingly, allowing it to flow evenly. Do not overheat the
solder or a high resistance connection could result.
8. Repeat steps 6 and 7 for the remaining harness wire labeled “R” and reference
thermistor wire.
2000-SVC, C1 4-25
9. Repeat steps 6 through 8 for the harness wires labeled “M” and the
measurement wires.
10. Slide heat shrink over each connection and shrink with a heat source.
1. Restore carrier to the analyzer and establish carrier flow to both the
measurement and reference ports of the detector.
2. Verify carrier and reference flow using a flow meter. Typically the flows should
be 30 to 40cc per minute if packed columns are used; 10 to 15 cc per minute if
0.53 mm ID capillary columns are used, and 3 to 5 cc per minute if 0.32 mm ID
capillary columns are used.
3. Test for leaks around the detector thermistor gland nut with a nonconductive
liquid leak detection solution. Correct all leaks before proceeding.
5. Gently remove any excess leak detection solution with a soft cloth or tissue and
blow dry with 15 psig clean dry air, helium or nitrogen.
CAUTION
4-26 2000-SVC, C1
FPD
Electrometer
Cables
Cables
Nuts Nuts
Photomultiplier Photomultiplier
Version 1 Version 2
FPD Electrometer in Controller Housing FPD Electrometer in FPD Enclosure Box
2. Turn off oven air to the isothermal oven and allow all temperature zones to cool.
5. Disconnect the cables to the Photomultiplier Assembly and set them aside.
6. Remove the four nuts securing the Photomultiplier Assembly to the analyzer,
being careful to retain the nuts to reinstall the Photomultiplier Assembly.
2000-SVC, C1 4-27
4.7.2 Replacing the Photomultiplier Assembly O-Ring
Vent Line
Mounting
Screws
Thermocouples
H2 and/or Sample
Carrier
Heaters
Sulfur Addition
Wafer
2. Turn off oven air to the isothermal oven and allow all temperature zones to cool.
4-28 2000-SVC, C1
4. Open the isothermal oven door.
9. Disconnect the hydrogen (H2) and carrier lines from the Burner Block.
10. Remove the bracket screws that fasten the Burner Block to the oven.
11. Slide the Burner Block off the end of the Photomultiplier Assembly and remove
the Burner Block from the oven.
12. Install the new Burner Block in reverse order of removing it.
O-Ring O-Ring
45051-4-13 45051-4-106
Figure 4-10. BURNER BLOCK, SHOWING O-RINGS
The Vista II Series Gas Chromatographs use two different models of Methanizer/Air
Cleaner Assembly, Model 781 and Model 805. These are essentially the same
except for appearance.
2000-SVC, C1 4-29
The Methanizer/Air Cleanup Assembly comes from the factory supplied with both air
cleanup and methanizer tubes. Your application may require the use of both the air
cleanup and methanizer tubes or only the air cleanup tube. The larger tube is used
for air cleanup and the smaller tube for the methanizer. If a tube is not being used,
its inlet and outlet connections will be plugged. It is necessary to replace only the
tube that is in use.
CAUTION
2. Turn off oven air to the isothermal oven and allow all temperature zones to cool.
5. Label the tubing on both sides of the associated unions with temporary
numbered tape labels. The labels are later used to ensure correct tubing
connections when the air cleanup/methanizer is reinstalled.
4-30 2000-SVC, C1
Harness Assy
3 1 2 4
4 2 1 3
Air
Cleanup
Tube
Methanizer
Tube
8. Remove the four Phillips head screws attaching the support brackets to the
isothermal oven wall. Secure the unit with your hand while removing the final
top screws.
9. Lay the Methanizer/Air Cleanup Assembly on a suitable work surface within the
constrained length of the heater harness. If only the catalytic tubes are to be
replaced, the harness will not require further disconnection.
10. Model 781 only: Remove the four Phillips head screws attaching the support
bracket to the top unit end caps and lay them aside.
CAUTION
11. Mark the top and bottom caps and housing with a grease pencil or permanent
marker. When the caps are replaced with the marks aligned, the support
bracket holes will be correctly aligned.
12. Using a 9/64-inch Allen wrench, remove the four Allen head screws attaching
the air cleanup/methanizer top cap to the outer housing.
2000-SVC, C1 4-31
13. Grasp the housing and top cap. Withdraw the internal body assembly from the
housing.
14. Using tweezers or a small screw driver, remove the insulation from around the
body assembly. Retain it for later use.
2. To remove a catalytic tube, remove the Phillips head screw and flat washer
located in the center of the body at the opposite end from the harness.
3. Grasp the long coiled or “pig tail” end of the tubing and pull the short nutted end
through the body assembly.
5. Carefully rotate the body assembly and remove the Phillips head retaining
screw and flat washer.
7. Inspect the probe end of the wiring harness for damage. If any harness wiring
or devices are damaged, replace the harness as described in Paragraphs 4.8.4
and 4.8.5.
1. To install the air cleanup tube, insert the short end of the catalytic air tube
through the larger tube passage of the body and align it with the inside air inlet
port connection of the top cap.
2. To install the methanizer tube, insert the short end of the catalytic methanizer
tube through the smaller tube passage of the body and align it with the inside
methanizer inlet port connection.
3. Insert the tube fitting into the cap and tighten the inlet fitting nut finger tight.
6. Insert the flat washer retaining screw assembly into the center hole located in
the end of the body assembly opposite the harness and tighten it with the
Phillips screwdriver.
7. If a new tube is being installed, a small loop or “pig tail” should be coiled in the
tubing to compensate for the excess tubing length. If installing an existing tube,
the pig tail will already be present.
4-32 2000-SVC, C1
8. Bend and position the coiled tubing such that the end fitting can be inserted into
the corresponding air or methanizer outlet connection port located on the
bottom of the top cap.
9. Tighten all inside catalytic tube inlet and outlet fittings, using a 1/4-inch open-
end wrench.
2. Using a 9/64-inch Allen wrench, loosen and remove the four Allen head screws
attaching the air cleaner/methanizer bottom cap to the outer housing. Separate
and set the bottom cap aside.
3. Carefully insert and press the body assembly into the outer housing.
4. Align the top cap with the marks on the outer housing. This will align the
mounting bracket holes in the top cap.
5. Install the four Allen head screws that secure the top cap to the outer housing
and tighten with a 9/64-inch Allen wrench.
6. Place a small quantity of insulation into the housing cavity and gently pack it
down using an object such as a screwdriver. Continue adding and packing in
insulation until the cavity is filled, taking care not the damage any wiring.
7. Install the bottom cap, aligning the mark on the cap with the mark on the
housing. This will align the bottom mounting bracket holes.
8. Install the four Allen head screws to secure the bottom cap to the housing, and
tighten with a 9/64-inch Allen wrench.
9. Model 781 only: Install the two mounting brackets with four Phillips head
screws. The mounting brackets should be aligned parallel to one another.
5. Using a liquid leak detection solution, test for leaks and make necessary repairs
before proceeding.
6. Route the heater harness in the oven interior, following the same path as the
original harness installation.
2000-SVC, C1 4-33
7. Connect heater one wires to J48E terminals 1 and 2, and connect heater two
wires to J48E terminals 5 and 6.
9. Close and secure the isothermal oven door, and the Controller front and side
doors.
1. Restore burner air to the cleanup unit by adjusting the burner air regulator for
the correct burner air pressure as indicated at the burner air pressure indicator.
2. If a methanizer is used, restore carrier gas by adjusting the carrier regulator for
the correct carrier pressure indication at the carrier pressure indicator.
3. Using a suitable liquid leak detection solution, test and repair any leaks that
may be present in the connections loosened or disconnected during the
maintenance procedure.
5. Restore carrier gas, oven air and fuel gas, if necessary, by adjusting the
regulators for the correct indications at the pressure indicators.
6. After ensuring the area is safe, and the proper permits are in effect, apply AC
power.
8. Access the Manual Control Mode screen by pressing the F2 (Manual Control)
soft key.
9. Access the Pressure and Temperature Control Mode by pressing the F4 (Press.
and Temp. Control) soft key.
10. From the Pres and Temp Control screen, position the cursor up or down to
highlight TEMP CONTROL and press the F2 (Manual Temperature Control) soft
key to access the Manual Temperature Control Screen.
11. On the Manual Temperature Control screen observe the setpoint value. If
necessary, change the setpoint of the air cleanup/methanizer temperature
controller to 450° C.
4-34 2000-SVC, C1
13. Press the F1 soft key as necessary to return to the Background screen.
1. Restore all utility gases and verify that the pressures and flow rates are correct.
These include oven air, purge air, carrier, burner fuel, and burner air. If the
faces of the pressure gauges were previously marked and the marked location
is known to be correct, simply adjust the pressure regulators until the gauge
pointers are aligned with the pressure indicating marks. Refer to the
engineering data package supplied with your analyzer for the correct values.
2. After sufficient air purge time and when authorized by your safety administrator,
apply power to the analyzer.
3. Verify that all Digital Temperature Control setpoint values are correct. Refer to
the engineering data package supplied with your analyzer for the correct values.
5. Verify that sample is being introduced to and is sufficiently flowing through the
analyzer sample valve.
7. Once analyzer operation and performance have been verified, place the
analyzer back in service.
2000-SVC, C1 4-35
2. Remove the screw from the Carrier Gas Panel (see Figure 4-12).
(5) Unscrew
feedthroughs
5. In the isothermal oven, unscrew the feedthroughs (see Figure 4-13) and pull
them downward approximately 0.5 inches; it is not necessary to completely
remove them.
6. Open the Controller front door to gain access the mother board.
7. In the Control Housing access area, unplug the alarm switches from the mother
board and unscrew them from the manifold (see Figure 4-14).
4-36 2000-SVC, C1
8. In the Control Housing access area, remove the plugs from the manifold (see
Figure 4-14).
9. In the Control Housing access area, remove the five socket head screws from
the manifold (see Figure 4-14).
3. Loosen the screws on the plate that secures the gauge to the panel and then
remove the plate.
7. Tighten the screws holding the gauge and plate to the panel.
2000-SVC, C1 4-37
4.9.4 Installing the Carrier Gas Panel
1. Insert the Carrier Gas Panel into the Control Housing access area of the
analyzer controller.
2. In the Control Housing access area, install the five socket head screws into the
manifold (see Figure 4-14), making sure the sealing gasket is in place.
3. In the Control Housing access area, install the plugs into the unused ports of
the manifold (see Figure 4-14).
4. In the Control Housing access area, screw the alarm switches into the manifold
(see Figure 4-14) and plug the ware harness into their original locations on the
mother board.
8. Install the screw in the Carrier Gas Panel (see Figure 4-12).
This procedure is similar to that for removing the analog Carrier Gas Panel
(paragraph 4.9.1).
2. Remove the two screws holding the EPC cover and remove the cover panel.
5. In the isothermal oven, unscrew the feedthroughs and pull them downward
approximately 0.5 inches; it is not necessary to remove them completely.
6. Open the Controller front door to gain access to the mother board.
7. At the left side of the mother board, disconnect the EPC Panel cable from J44.
8. On the EPC Multibus PCB in the card cage, disconnect the EPC Panel cable
from J43 (near the bottom of the PCB).
9. In the Control Housing access area, unplug the alarm switches from the mother
board and unscrew them from the manifold.
10. In the Control Housing access area, remove the plugs from the manifold.
4-38 2000-SVC, C1
11. In the Control Housing access area, remove the five socket head screws from
the manifold.
12. Remove the four screws holding the Purge Air Panel in place and carefully pull
the panel forward and down.
13. On the side wall behind the Purge Air Panel remove the lock nut on the pipe
nipple which retains the EPC Panel cables (see Figure 4-15).
Lock Nut
Install the new EPC Panel in the reverse order of removal, following the steps of
paragraph 4.10.1.
The EPC should only require calibration if a component has been replaced. You
should only need to calibrate the particular zone affected by the servicing. To
calibrate a zone:
2000-SVC, C1 4-39
3. Eliminate any back pressure to the zone by loosening the feedthrough fitting
associated with the zone to be calibrated (see Figure 4-16).
1 2 3 4 5
ZONE FITTINGS
4. On the Controller, verify the Background screen is displayed and then press the
F2 (Manual Control) soft key.
5. On the Manual Control Mode screen press the F4 (Press. & Temp. Control) soft
key.
6. On the Pres and Temp Control screen (see Figure 4-17), cursor to PRES
CONTROL and press the F2 (Manual Pressure Control ) soft key.
TEMP CONTROL
PRES CONTROL
TEMP CONFIGURATION
F1 F2 F3 F4
4-40 2000-SVC, C1
7. On the Manual Pressure control Mode screen (see Figure 4-18), enter the zone
number of the zone you want to calibrate.
Accept Calibrate
Escape Control Zone
Point
F1 F2 F3 F4
8. Press the F3 (Calibrate Zone) soft key. The GCC displays “Calibrate zone, hold
switch on board.”
9. Hold down the switch on the EPC Multibus PCB. The GCC displays “Are You
Sure?”
10. Continue holding down the switch and press “Y” on the keyboard to save the
new calibration.
11. When the GCC displays “This zone has been calibrated,” release the switch.
12. If the Set Point shows an unexpected value, enter the desired set point value.
(The unexpected value is an offset corrected by the calibration; this is a
software reporting function only, which is not used by the system.)
2000-SVC, C1 4-41
4.12 REPAIRING PURGE AIR PANEL COMPONENTS
1. Remove the four screws holding the panel in place (see Figure 4-19).
Mounting
Screws
2. Disconnect the lines from the back of the regulator, using 1/2-inch and
9/16-inch open-end wrenches.
4. Remove the nut and sealing gasket securing the regulator to the panel.
8. Install the sealing gasket and fasten the nut securing the regulator to the panel.
2. Disconnect the line from the back of the gauge, using a 9/16-inch open-end
wrench.
4-42 2000-SVC, C1
3. Loosen the screws on the plate that secures the gauge to the panel and then
remove the plate.
5. Insert the new gauge and sealing gasket through the hole in the panel.
7. Tighten the screws holding the gauge and plate to the panel.
1. Carefully put the panel back in place, aligning the mounting holes.
The following paragraphs describe how to set the various PCB jumpers.
The Controller Backplane PCB has six jumpers to set up (see Figure 4-20).
JP5 JP1
JP3
JP2
JP6
JP4
2000-SVC, C1 4-43
Jumpers JP1 and JP5 are used to bypass pressure switch connection points for
certain analyzer configurations. Since the purge switches are daisy chained in
series, it is necessary to jumper across switches that are not connected. Jumper
JP1 has its shunt installed between pins 1 and 2 for standard or Sparger oven
usage; the shunt is installed between pins 2 and 3 for temperature programmed
applications. Jumper JP5 has its shunt installed between pins 1 and 2 for single
purge area; the shunt is installed between pins 2 and 3 for dual purge location
applications.
Jumpers JP2, JP3 and JP6 are associated with the purge alarm switch closures
applied to the Chroma I/O PCB. Jumper JP2 has its shunt installed between pins 1
and 2 for X Purge applications only; the shunt is installed between pins 2 and 3 for Y
or Z purge applications. Jumper JP3 has its shunt installed between pins 1 and 2 for
standard analyzers; the shunt is installed between pins 2 and 3 for temperature
programmed and Sparger applications. Jumper JP6 has its shunt installed between
pins 1 and 2 for single purge configurations; the shunt is installed between pins 2
and 3 for dual purge applications.
Jumper JP4 is used to connect two detectors to a single Chroma I/O PCB. The
location of the jumper shunt depends on the revision of the Backplane PCB.
Backplane PCBs that do not have JP5 and JP6 are artwork revision D or earlier,
while those having JP5 and JP6 are artwork revision E or later.
• For revision D or earlier, the shunt is installed between pins 1 and 2 when the
outputs of two detector amplifiers are applied to a single Chroma I/O PCB; the
shunt is installed between pins 2 and 3 for normal operation (a Chroma I/O
PCB dedicated to a single detector amplifier).
• Revision E or later: the shunt goes between pins 1 and 2 for normal operation
(a Chroma I/O PCB dedicated to a single detector amplifier); the shunt is
installed between pins 2 and 3 when the outputs of two detector amplifiers are
applied to a single Chroma I/O PCB.
The Digital Temperature Controller (DTC) PCB has eight jumpers and one switch to
set up (see Figure 4-21 for location).
Switch SW1 is used to save configuration information to protected memory. Its use
is described in “Digital Temperature Controller” in Section 4 of the Operator’s
Manual, by the statement “Hold down the switch on the DTC Backplane PCB.”
4-44 2000-SVC, C1
JP4
JP1
JP5
JP6
J2
JP
3
JP3
SW
JP2
1
SW1
J3
Jumpers J2 and J3 are T-Rating jumpers. The jumper shunts must be installed
exactly as shown below to ensure the temperature control operates properly. If they
are set incorrectly, T-Rating disagreement alarms will result (0 = no jumper; 1 =
jumper installed).
JP1 is the service diagnostics jumper. For normal operation the shunt is installed
between pins 1 and 2. For service diagnostic screen use (only) the shunt is
installed between pins 2 and 3. After servicing, the shunt must be reinstalled
between pins 1 and 2.
JP4 is the VAC Conditioning Board jumper. If the analyzer has one VAC
Conditioning PCB installed, the shunt should be between pins 2 and 3. If the
2000-SVC, C1 4-45
analyzer has two VAC Conditioning PCBs installed, the shunt should be between
pins 1 and 2.
JP2, JP3, JP5, and JP6 are the jumpers for the temperature zone boards. These
jumpers are required for the software to recognize unused zones. Jumpers are
installed from the even pins of unused zones to the even pins of used zones, for
both Micro #1 (JP2 and JP3) and Micro #2 (JP5 and JP6). If all zones are in use, no
jumpers are installed. Zone jumpers are identified as follows:
Example: if Zone 5 is not used, one jumper must be run between JP2-4 and JP2-2
or one of the other pins listed under Micro #1 Pins, and a second jumper must be
run between JP6-4 and JP6-2 or one of the other pins listed under Micro #2 Pins.
There can be up to five zone boards, one for each designated temperature zone.
The only jumper on a zone board is JP1 (see Figure 4-22). How this jumper is set
depends on the type of temperature sensor used for the zone. The jumper shunt
should be between pins 1 and 2 for a 400 ohm platinum probe sensor; it should be
between pins 2 and 3 for a thermocouple sensor.
JP1
There can be either one or two VAC Conditioning PCBs, depending on the
application. Each board has two jumpers to be set, JP4 and JP5 (see Figure 4-23).
These jumpers are set according to the voltage supplied to the board, as follows
(JP4 is the hot side and JP5 is the neutral side):
4-46 2000-SVC, C1
JP4
JP5
There is one adjustment and three jumpers on this board (see Figure 4-24). The
adjustment is potentiometer R56, which is used to set the display contrast for
optimum viewing.
The jumpers relate to the LOCOM option. JP5 has its shunt is between pins 1 and 2
for normal operation, between pins 2 and 3 for LOCOM installations. JP6 and JP7
have the shunts in place for normal operation and the shunts removed for LOCOM
installations.
JP7 JP6 JP5
R56
The jumper on this PCB relates to intercolumn detector usage. For normal operation
shunts should be installed in the first two positions at the right side of J18. These
2000-SVC, C1 4-47
shunts are removed for an application using intercolumn detectors (see Figure
4-25).
J18
The jumpers on this PCB relate to amplifier gain, single or dual carrier, temperature
ranges, intercolumn detectors, and special testing (see Figure 4-26 for location).
TEMPERATURE JUMPERS
WT1 - WT6
The gain jumper is normally connected between WT11 and WT12. For high gain
applications this jumper is connected between WT12 and WT13.
4-48 2000-SVC, C1
The carrier jumper is normally connected between WT9 and WT10 (single carrier).
For dual carrier applications this jumper is connected between WT7 and WT8.
The temperature jumpers are normally connected between WT1 and WT2 and
between WT4 and WT5 (low temperature). For high temperature applications these
jumpers are connected between WT1 and WT3 and between WT4 and WT6.
For normal operation shunts should be installed in the first two positions at the right
side of J18. These shunts are removed for an application using intercolumn
detectors.
The jumper between WT14 and WT15 must be in place for normal operation. It is
only removed when when hi-pot testing is to be performed.
The Thermistor Amplifier Interface PCB currently supports one or two Thermistor
Amplifier PCBs (see Figure 4-27).
1 2 3 1 2 3 1 2 3 1 2 3
JP2 JP1 JP1A JP2A
For single detector applications, one Thermistor Amplifier PCB is used, mounted in
the Amplifier #1 position. Jumpers JP-1, JP-2, JP-1A and JP-2A all have their
shunts between terminals 1 and 2. The output signal is routed through J13A.
For dual detector applications, two Thermistor Amplifier PCBs are used, mounted in
the Amplifier #1 and Amplifier #2 positions. Jumpers JP-1, JP-2 and JP-2A all have
their shunts between terminals 1 and 2. Jumper JP-1A has its shunt between
terminals 2 and 3. The output signal of Amplifier #1 is routed through J13A and the
output signal of Amplifier #2 is routed through J13B.
2000-SVC, C1 4-49
4.13.9 EPC Multibus PCB
This board has one jumper and one switch to set up (see Figure 4-28).
JP1 is the service diagnostics jumper. For normal operation the shunt is installed
between pins 1 and 2. For installation and service the shunt is installed between
pins 2 and 3. After installation or service, the shunt must be reinstalled between
pins 1 and 2.
Switch SW1 is used to save configuration information to protected memory. Its use
is described in “Electronic Pressure Control Option” in Section 4 of the Operator’s
Manual, by the statement “Hold down the switch on the Electronic Pressure Control
PCB.”
SW1 JP1
4-50 2000-SVC, C1
4.13.10 EPC Control PCB
This board has a single jumper, JP2 (see Figure 4-29). For normal operation JP2
has a shunt between pins 2 and 3. For servicing of the block, the shunt is placed
between pins 1 and 2 to turn off the heater.
JP2
This board has two jumpers which are mutually exclusive. When there is only one
Chroma I/O PCB in the system, or the board is used as Chroma I/O PCB #1 in a
simultaneous dual detector system, the jumper will be located between the
terminals of JP1 (see Figure 4-30). This jumper is part of the printed circuit trace on
all Chroma I/O PCBs.
JP2 JP2
JP1 JP1
When a second Chroma I/O PCB is used, Chroma I/O PCB must have the JP1
jumper trace cut and a jumper installed between the JP2 terminals.
2000-SVC, C1 4-51
4.13.12 Power Supply PCB
This board has two jumpers to verify (see Figure 4-31). JP4 should always have a
shunt between pins 1 and 2. JP2 has its shunt between pins 1 and 2 for normal
operation, between pins 2 and 3 for factory test mode.
1 2 3
JP2
1 2 3
JP4
JP2 JP4
OPERATING MODE: 1 TO 2 ALWAYS SET
DIAGNOSTIC MODE: 2 TO 3 1 TO 2
The Valco DV22-2110 ten-port diaphragm valve is used in some Vista II GCs (see
Figure 4-32). This procedure and the accompanying illustrations were reprinted with
permission of VICI, Houston, TX, USA.
2. Using a 1/4-inch wrench, remove the connections from the valve cap.
4-52 2000-SVC, C1
3. Using a 7/64-inch hex key wrench, loosen the clamp ring screw.
4. Remove the valve from the clamp ring and take it out of the analyzer.
2. Note the location of port 1 on the valve, opposite the air inlet (see Figure 4-33).
3. Using a 9/64-inch hex key wrench, remove the screw from the valve cap (see
Figure 4-34).
2000-SVC, C1 4-53
4. Carefully remove the valve cap from the two alignment pins.
5. Set the cap aside, with the polished side up so that it does not get scratched.
8. Install new plungers, ensuring that the counterbored end is up toward the valve
cap (see Figure 4-34).
9. Install new diaphragm, ensuring that the marking “TOP” is toward the valve cap.
If there is no marking, ensure the indentation in the diaphragm is toward the valve
body (see Figure 4-34).
10. Reinstall the valve cap, verifying that port 1 is correctly located.
11. Install the valve cap screw and tighten with a 9/64-inch hex key wrench.
1. Place the valve in the clamp ring and rotate it to the orientation of the valve that
was removed.
2. Using a 7/64-inch hex key wrench, tighten the clamp ring screw.
3. Install the connections to the valve cap, matching the numbering on the valve to
the tags on the connections.
4.15.1 Purpose
The VistaNET Communications Board in the Card Cage has an on-board debug
monitor that allows examination of the token bus communications. Several
parameters accessible from the debug connector allow the technician to easily
troubleshoot common problems.
CAUTION
You must work carefully with the Debug Monitor. Inserting erroneous
information can cause networking problems. If such problems occur
you must reset the network to reinstate proper operation.
The VistaNET Communications Board has a connector that allows a serial cable to
be connected to the board. ABB Process Analytics Aftermarket Spares can provide
this cable (P/N 3617695-1). The RS-232 communications protocol allows the use of
a laptop PC for access. Included in Windows 95 is the Hillgraeve HyperTerminal
Application, which emulates several popular devices. This cable should be
connected to the Communications Board (see Figure 4-35) and to the appropriate
COM port (Domain 1 or 2) on the laptop PC.
4-54 2000-SVC, C1
J4
COMMUNICATIONS
PCB
COMMUNICATIONS
PCB
D E B U G J3
DOMAIN 1 J2
DOMAIN 2 J1
On the laptop PC, set the terminal emulation to VT100, and the associated serial
parameters to 9600 baud, 8 data bits, no parity, 1 stop bit, no handshaking.
4.15.3 Startup
When you have set up the terminal application and connected to the
communications board, press <CTRL> A to invoke the Main Menu (see Figure
4-36).
When you exit the application, press <CTRL> Z to end the session.
2000-SVC, C1 4-55
CAUTION
Always end the session before exiting the monitor. While the monitor
is intended to be non-invasive, it can affect operation over time.
Some performance parameters are degraded by the monitor program.
The Main Menu is divided into three sections: the Information Display at the top of
the screen, Menu Items just below this information, and Statistical Data between the
two horizontal lines.
4-56 2000-SVC, C1
Fill Memory Entered as FM XXXX YYYY ZZ where XXXX is the
starting address, YYYY ending, ZZ pattern to be used to
fill the memory block (all in hex).
Ignore Token Entered as IT, used for software loading tests. In this
mode, the communications board remains part of the
token bus, however tokens are merely passed, and no
UDP packets are transmitted or received at this node.
THIS COMMAND IS NOT TO BE USED IN THE FIELD.
2000-SVC, C1 4-57
Main Menu From the SFR display, this command returns to the main
menu.
WARNING
Reset stats Globally Entered as RG, this command resets all cumulative
statistics collected at all nodes by sending a reset
statistics command to all nodes by transmitting a special
token.
CAUTION
The Dump History command is rather invasive, and may cause this
station to drop tokens.
Dump History Entered as DH, the history buffer maintained at this node
is displayed (see Figure 4-39).
4-58 2000-SVC, C1
address of the station displaying this buffer is not seen.
The location of the asterisks (***) shows the starting point
of the display. The escape key will return to the main
menu. Pressing Enter will display the content of the next
buffer captured.
4.15.6 Statistical Display
On the screen, several items of interest to the technician are displayed. The
Statistical Display is divided, roughly, into three columns: Transmit, Receive and
General Statistics. Following is an explanation of each screen element.
Transmit Statistics
Transmit Requests Number of requests for UDP transmission from the host.
Tokens Issued Number of times this station has detected a dead line
and the slot assignment time has expired, resulting in an
issuance of a token.
Tokens Dropped Number of times the token destination did not accept
the token, or the token was lost. This indicates the
number of times this station has seen a station go off-line,
or line noise caused the packet to be corrupted.
Receive Statistics
2000-SVC, C1 4-59
1. Overrun - indicates a new character received
before the last was processed.
Backups Number of times this station has run out of receive buffers
due to host interrupt latency.
General Statistics
4-60 2000-SVC, C1
4. Transmit Requested - A UDP packet is in dual port
memory and needs to be transmitted.
Next Recvd Address of the source address of the token seen on the
wire subsequent to this station sending a token.
2000-SVC, C1 4-61
For further information or assistance contact:
4-62 2000-SVC, C1
SECTION 5. REPLACEMENT PARTS
This section provides a listing of replacement parts, with part number and
description.
NOTE
Since the component parts specific to any given system are defined by
the particular application, you should refer to the “Recommended Spare
Parts Lists” in the Data Package supplied with the analyzer, to obtain the
full and correct part number for the desired part or assembly.
The following information, found in the Data Package and on the analyzer
nameplate, should be included in any communication concerning replacement parts
or components:
• Applicable references from the “Recommended Spare Parts List” of the Data
Package, included with each analyzer
• Description of part
Contact the Service Manager for specific ordering instructions. Include a complete
description of the component, analyzer, symptoms and problems with your request.
The remainder of this section lists the replaceable parts and components by their
location in the equipment. Part numbers and drawing numbers listed here are for
identification purposes only. When you order parts for replacement, use the list of
parts included in the Engineering Data Package provided with your equipment to
ensure you have the correct version of each part.
2000-SVC, C1 5-1
5.2 GC CONTROLLER
Lo Comm
Front Panel
PCB
PCB
Lo Comm
Cable Display
Panel
5-2 2000-SVC, C1
RFI Filter
FID Amplifier
and/or
TCD Amplifier
or
FPD Amplifier
Electronic Pressure
Control PCB
2000-SVC, C1 5-3
5.2.4 Components on Right Side Door (see Figure 5-4)
AC Conditioning PCB
(has both fuses)
Panel
Assembly
DTC Zone
PCB
Pressure
Gauge Heater Air
Pressure Switch
1/4-inch
0 0 Tubing
5-4 2000-SVC, C1
5.4 ELECTRONIC PRESSURE CONTROL PANEL (DIGITAL) (see Figure 5-6)
Proportional
Valve
Sensor PCB
Heater
Control PCB
Gauges
0 0 0 0 Filter/Restrictor
Regulators
2000-SVC, C1 5-5
5.6 ISOTHERMAL OVEN COMPONENTS (see Figure 5-8)
NOTE
Part Numbers are incomplete without dash numbers. See the Recommended
Spare Parts List (in the Engineering Data Package) for application-specific
information.
Temperature
Sensor
Detector
Thermocouple
Oven
Heater
5-6 2000-SVC, C1
5.6.1 Liquid Sample Valve (see Figure 5-9)
Seals Stem
Thermocouple
Polarizer
Ignitor
Jet
2000-SVC, C1 5-7
5.6.3 Filament Type Thermal Conductivity Detector (see Figure 5-11)
Reference Measure
Filament Filament
Reference Vent
Sample In
Sample Vent
Reference In TC Assembly
Cable
Measure Reference
Thermistor Thermistor
Measurement Reference
Vent Vent
Measurement Reference
In In
5-8 2000-SVC, C1
5.6.5 M2CP Valve (see Figure 5-13)
Slider
Carrier
Harness Assy
4 2 1 3
Methanizer Tube
2000-SVC, C1 5-9
5.6.7 Model 805 Methanizer/Air Clean Up System (see Figure 5-15)
HEX HEAD
SCREW
PLUNGER ENLARGED
CAP
TO SHOW
COUNTERBORED END
DIAPHRAGM
PLUNGERS
ALIGNMENT
PINS
BODY
5-10 2000-SVC, C1
5.7 FLAME PHOTOMETRIC DETECTOR (FPD)
Transformer 3617648-1
Capillary Tubing, Burner Fuel (not shown) 5514584-39
Coaxial Cable Assy 3528546-1
Photomultiplier Assy 804A003-1
Solenoid, 3 Way (for X Purge) 3616261-3
Pressure Sensor 3615565-6
FPD Electrometer* 804A010-1
*see paragraph 5.2.2 for alternate location
Burner Block (see paragraph 5.7.2)
Pressure Sensor
Solenoid
Transformer
0 0
FPD Electrometer
Coaxial Cable
Photomultiplier
Burner Block
2000-SVC, C1 5-11
5.7.2 Burner Block Components (see Figure 5-18)
Sulfur
Addition
Wafer
5-12 2000-SVC, C1
Detector
(FID shown)
Heater
5.8.1 Flame Ionization Detector with Heater Block (see Figure 5-20)
Detector
Heater
Block
Insulation
2000-SVC, C1 5-13
5.8.2 Filament Type TC Detector with Heater Block (see Figure 5-21)
Detector
Heater
Block
Insulation
5-14 2000-SVC, C1
SECTION 6. DRAWINGS AND DIAGRAMS
The drawings and diagrams contained in this manual are of a general nature. Since analyzer
configuration depends on the particular application, you should refer to the drawings provided
in the engineering drawings supplied with your analyzer as the final authority. In addition there
is an Application Data Package which contains information on application-dependent
components or subassemblies, outline and mounting diagrams, and flow diagrams.
The following drawings and diagrams, which make up this section of the manual, provide
general information about the analyzer that is not covered elsewhere.
2000-SVC, C1 6-1
Air In PURGE AIR
PANEL
Heater Air
Purge Air
Digital Out
Analog Out
Sample In Recorder
OVEN GCC
Printer
VistaNET
Burner Fuel
Burner Air
Carrier
Air In
H2 In CARRIER
GAS
PANEL
Carrier In
6-2 2000-SVC, C1
PURGE AIR PANEL
Regulator
& Gauge
Air In Regulator
& Gauge
Solenoid Solenoid
Valve Valve
Heater Air
Purge Air
Purge Air
OVEN
Heater
Burner Air
Carrier
Air In Adj
Valve
H2 In Adj
Valve
Carrier Adj
In Valve
CARRIER GAS PANEL (Analog)
2000-SVC, C1 6-3
To LOCOM
Circuit
Display LOCOM
PCB
Keypad
SBC Trend
PCB #1
Analog
EPC
Outputs
Sensors Power
Trend
Supply
#2
PCB
EPC
Control EPC
Digital
PCB Multibus
I/O #1
PCB Digital
Zone Inputs &
PCB Outputs
Digital
(5) DTC
I/O #2
Backplane
AC PCB
Cond VistaNET
PCB Multibus VistaNET
PCB Domains
GCC
6-4 2000-SVC, C1
For further information or assistance contact:
Process Analytics Division Bomem Division Extrel Division Hartman & Braun Division Pastech Division
843 N. Jefferson Street 450 St.-Jean Baptiste 575 Epsilon Drive Heerstrasse 136 - Hortonwood 37
Lewisburg, WV 24901 Avenue Pittsburgh, PA 15238 D-60488 Frankfurt am Main Telford, Shropshire
USA Quebec, Quebec USA Germany TF1 4GT
Canada G2E 5S5 United Kingdom
Office: (304) 647-4358 Office: (412) 963-7530 Office: 49-6196-800-0
FAX: (304) 645-4236 Office: (418) 877-2944 FAX: (412) 963-6578 FAX: 49-6196-800-1119 Office: 44-1952-670-477
FAX: (418) 877-2834 FAX: 44-1952-670-455
U.S.A. Office Office: (281) 556-8102 Office: 973-725377 Office: 31-294-417291 Office: 33-3-8774-0611
6100 West By Northwest FAX: (281) 556-8157 FAX: 973-725332 FAX: 31-294-413656 FAX: 33-3-8774-7939
Blvd.
Suite 160
Houston, TX 77040 United Kingdom
Germany Italy Singapore
USA
Office: 49-6196-800-0 Office: 39-2-26232936 Office: 65-776-5711 Office: 44-1952-670-477
Office: (713) 460-9541 FAX: 44-1952-670-455
FAX: 49-6196-800-1119 FAX: 39-2-26232685 FAX: 65-779-7351
FAX: (713) 460-5918
9907