Page 1 of 2

Certificate of Analysis
Vessel / Object: Cenac Island - HBC 304 (1245343), Hines Furlong Line - HFL 401 (1206173) Job No: 170-21-02876
Location: Chalmette, LA / Refinery (United States) Date Sampled: 09 May
DEC 2021
Job Type: Load Date Tested: 09 DEC
May 2021
Product Grade: Distillate / ULSD Version: 1 / 09 DEC
May 2021 09:32
Client Reference: Holding Company LLC / 19450
Client Reference: N.A. LTD / 3014

Sample Sample ID, Type & Description

170-21-02876-001 ST 404 Upper Pre-Sample

Method Test Min Max Result Units

ASTM D4052 API Gravity @60°F 39.9 °

Sample Sample ID, Type & Description

170-21-02876-002 ST 404 Middle Pre-Sample

Method Test Min Max Result Units

ASTM D4052 API Gravity @60°F 39.9 °

Sample Sample ID, Type & Description

170-21-02876-003 ST 404 Lower Pre-Sample

Method Test Min Max Result Units

ASTM D4052 API Gravity @60°F 39.9 °

Sample Sample ID, Type & Description

170-21-02876-004 ST 404 Running Pre-Sample

Method Test Min Max Result Units

ASTM D4052 Gravity by Digital Density Meter
API Gravity @60°F 39.9 °
Specific Gravity @ 20/4° C 0.8217
ASTM D86 Distillation
IBP 170.0 °C
5% 192.0 °C
10% 275 200.0 °C
20% 211.6 °C
30% 222.9 °C
40% 233.8 °C
50% 245.9 °C
60% 258.9 °C
70% 273.8 °C
80% 291.9 °C
90% 345 315.6 °C
95% 333.7 °C
FBP 350.1 °C
Recovery 98.5 %vol
Residue 1.3 %vol
Loss 0.2 %vol
ASTM D93A Flash Point 45 62.0 °C
ASTM D97 Pour Point 0 -27 °C
ASTM D2500 Cloud Point -16 °C

AmSpec LLC - 14682 Airline Highway - Destrehan - Louisiana - 70047 - EPA ID# 3960
RESULTS ARE VALID "AS AT" DATE AND LOCATION LISTED
 Page 2 of 2

Certificate of Analysis
Vessel / Object: Cenac Island - HBC 304 (1245343), Hines Furlong Line - HFL 401 (1206173) Job No: 170-21-02876
Location: Chalmette, LA / Refinery (United States) Date Sampled: 09 DEC
May 2021
Job Type: Load Date Tested: 09 DEC
May 2021
Product Grade: Distillate / ULSD Version: 1 / 09 May
DEC 2021 09:32
Client Reference: Holding Company LLC / 19450
Client Reference: N.A. LTD / 3014

Sample Sample ID, Type & Description

170-21-02876-004 ST 404 Running Pre-Sample

Method Test Min Max Result Units

ASTM D4737 Cetane Index Method A 45 51.3
ASTM D613 Cetane Number of Diesel Fuel Oil
Ignition Quality Cetane Number 45 50.3
Reference Fuel Used 46.8 / 52.2
T Batch Designation 32
U Batch Designation 32
ASTM D2622 Total Sulfur Content 15 6.8 ppmw
ASTM D130 Copper Strip Corrosion Rating 1 1A
ASTM D524 Ramsbottom Carbon Residue on 10% Distillation Residue 0.35 0.07 %wt
ASTM D2709 Water and Sediment 0.05 < 0.01 %vol
ASTM D445 Kinematic Viscosity @104°F/40°C 1.9 4.1 2.173 mm²/s
ASTM D482* Ash Content
Ash Content 0.01 < 0.010 %wt
Test Specimen Mass 100.21 g
ASTM D1500 ASTM Color 2.5 0.5
ASTM D1319 Aromatics 35 21.1 %vol
ASTM D6079 Lubricity of Diesel Fuels by HFRR
Wear Scar Appearance Normal μm
Lubricity Major Axis 650 μm
Lubricity Minor Axis 630 μm
Lubricity Average Wear Scar Diameter 520 640 μm
ASTM D2624 Electrical Conductivity of Aviation and Distillate Fuels
Electrical Conductivity 25 <1 pS/m
Temperature of Sample 21 °C

Notes: *Method Modification: Result is reported outside (lower/higher) the scope of the method

Reported by: Craig Duthu

Title: Laboratory Supervisor

Reported by: Craig Duthu

Title: Laboratory Supervisor

AmSpec LLC - 14682 Airline Highway - Destrehan - Louisiana - 70047 - EPA ID# 3960
RESULTS ARE VALID "AS AT" DATE AND LOCATION LISTED