Client: M/s.Malladi Drugs,Chennai Design factor: 1.

2
Date: 15.03.12
Design of water + IPA Column Designed by : K.Santhosh
Feed (KL/day) 7.2 5868.7200 Kg/day Chd&Appd by : N.S.W
design factor feed 7042.4640

Calculation of diameter for Methanol-IPA system(Continuous)- Top Boil up properties

Feed B.P M.W Feed Feed Distillate Distillate Bottoms Bottoms Density l Viscosity
(°C) (kg/kg mol) (w/w%) (mol%) (w/w%) (mol%) (w/w%) (mol%) (gr/cc) (kcal/kg) cp
Water 100 18 15 37.072 0.5 1.6499 99.5 99.8497 0.98 540.0 0.600
IPA 82.22 60.09 85 62.928 99.5 98.3501 0.5000 0.1503 0.786 159.0 2
0.8151 160.91 1.993
Feed 282 6.3322 42.2548 Intercept = 0.12770 0.09100
kg/HR kgmole/hr 1267.64352 Rmin = -0.87 10
TIME parameter 30.000
Calculation of vapor . Column Dia calculation
0
Composition of the boilup w/w% 1.250 Max distillate rate 240.44 kg/hr
Water 0.5 1.200
IPA 99.5 1.472 Boilup rate 528.97 kg/hr
Refluxratio 1.2 (G=G' * A) 0.15 kg/sec
(L/G) 0.55 8.91 kgmol/hr
Aveg. temp of gas 82.31 °c Latent heat of vaporization 160.91 kcal/kg Structured packings (MELLAPAK 500Y)
Density of liquid 786.97 kg/m3 Heat load 85113.48 kcal/hr Ass. Dia. Of Col. 264 mm T 355.31 °K
Moles of distillate / 100 g distillate 1.6836 moles Area of the column 0.0747 m² Area of column 0.05466 m² P 1013.3 m bar
Operating pressure 760 m.m Hg Diameter of the column 308.38 mm L/G 0.55 M 59.396 kg/kgmol
Aveg M.W 59.396 kg/mol Condenser Density of gas 2.039 kg/m3 F factor 1.8834
Density of gas 2.039 kg/m3 Heat load 85113.48 kcal/hr Density of liquid 786.97 kg/m3 NTSM 4.1
X-axis 0.0278 Temp. at the top 82.31 °C Flow parameter 0.028 Height 0.00 m
Ordinate1 0.26 (pg:195 Treybal) CTW entering at 32 °C Cg,max 0.12 Pr.drop 5.0 mbar/m
1" Ceramic intallox saddles 98 CTW leaving at 37 °C Qty Evaporated 7213.19 kg Cg 0.096 Total pr.drop 0.00 mbar
Viscosity of liquid 1.993 cp LMTD 47.77 °C Correction factor, C 0.70 0.000 mm of Hg
0.001993 kg/m-sec U 500 kcal/hr-m²-°c Qty.remaining 1237.77 kg g 2.6881 kg/m2.s
Gas flow rate at flooding-G' 2.81 kg/m²-sec Main condenser area 3.5638 m² G 0.1469 kg/s
at 70% flooding 1.968 kg/m²-sec Vent condenser area 0.4928 m² Reboiler 528.9673 kg/hr
CTW Req. for Main condenser 17.0227 m3/hr Reboiler Load 85113.48 kcal/hr 8.9058 kgmol/hr
Pressure drop calculation CTW Req. for vent condenser 1.7023 m3/hr Temperature of the still at 760 m.m Hg at the end 99.9 °c T (hr) 0.0000 0.0000 0.0000 0.0000
Ordinate value 0.1274 CTW Req for sub cooler 1.5230 m3/hr Temperature of steam at 3 kg/cm2 -g 142.97 °c Distillation time 0.00 hrs
Pressure drop/m 6.746 mm Hg/m Total CTW Water Req 20.25 m3/hr l of steam at 3kg/cm²-g 508.16 kcal/kg
Total pressure drop 80.950 mm hg U 488.00 kcal/hr-m²-°c
Size of the reboiler is 4.051 m²
Steam Required is 167.493 kg/hr
(20% extra) 200.99 kg/hr

F 6.33
L 4.86
L' 11.19
L'/G 1.60

Calculation of diameter for Methanol-IPA system(Continuus)- Bottom boil up properties

Feed B.P M.W Bottoms Bottoms Density l Viscosity
(°C) (kg/kg mol) (w/w%) (mol%) (gr/cc) (kcal/kg) cp
Methanol 64.72 32 99.5 99.7331 0.98 540.0 0.600
IPA 82.22 60.09 0.5000 0.2669 0.786 159.0 2
0.9790 538.10 0.607 4

Calculation of vapor . Column Dia calculation

Composition of the boilup w/w% Max distillate rate kg/hr

Methanol 99.5 1122.62
IPA 0.5 Boilup rate 224.52 kg/hr
Refluxratio 1.60 (G=G' * A) 0.06 kg/sec
(L/G) 1.60 7.00 kgmol/hr
Aveg. temp of gas 64.81 °c Latent heat of vaporization 538.10 kcal/kg Structured packings (MELLAPAK 500Y)
Density of liquid 979.03 kg/m3 Heat load 120815.67 kcal/hr Ass. Dia. Of Col. 227 mm T 337.81 °K
Moles of distillate / 100 g distillate 3.1177 moles Area of the column 0.0387 m² Area of column 0.04058 m² P 1053.2987 m bar
Operating pressure 790 m.m Hg Diameter of the column 222.15 mm L/G 1.60 M 32.075 kg/kgmol
Aveg M.W 32.075 kg/mol Condenser Density of gas 1.204 kg/m3 F factor 1.4014
Density of gas 1.204 kg/m3 Heat load 120815.67 kcal/hr Density of liquid 979.03 kg/m3 NTSM 4.2
X-axis 0.0561 Temp. at the top 64.81 °C Flow parameter 0.056 Height 0.00 m
Ordinate1 0.21 (pg:195 Treybal) CTW entering at 32 °C Cg,max 0.08 Pr.drop 5.0 mbar/m
1" Ceramic intallox saddles 98 CTW leaving at 37 °C Cg 0.064 Total pr.drop 0.00 mbar
Viscosity of liquid 0.607 cp LMTD 30.24 °C Correction factor, C 0.70 0.000 mm of Hg
0.000607 kg/m-sec U 500 kcal/hr-m²-°c g 1.5369 kg/m2.s
Gas flow rate at flooding-G' 2.30 kg/m²-sec Main condenser area 7.9908 m² G 0.0624 kg/s
at 70% flooding 1.610 kg/m²-sec Vent condenser area 0.6990 m² Reboiler 224.5248 kg/hr
CTW Req. for Main condenser 24.1631 m3/hr Reboiler Load 120815.67 kcal/hr 7.0000 kgmol/hr
Pressure drop calculation CTW Req. for vent condenser 2.4163 m3/hr Temperature of the still at 760 m.m Hg at the end 64.8 °c T (hr) 0.0000 0.0000 0.0000 0.0000
Ordinate value 0.1029 CTW Req for sub cooler 1.5230 m3/hr Temperature of steam at 3 kg/cm2 -g 142.97 °c Distillation time 0.00 hrs
Pressure drop/m 6.746 mm Hg/m Total CTW Water Req 28.10 m3/hr l of steam at 3kg/cm²-g 508.16 kcal/kg
Total pressure drop 80.950 mm hg U 488.00 kcal/hr-m²-°c
Size of the reboiler is 3.167 m²
Steam Required is 237.751 kg/hr
(20% extra) 285.30 kg/hr
 4..3 11000 3
3 12000 4.5

FEED TIME HEAT LOAD DIAMETER

MEOH-IPA 8KL/DAY 8 159123 420
ACETONE-WATER 4KL/DAY 20 178763 441
 600 13 10000
710 20 6000

MAX. hold up in kettle

3 15
1 15